#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/33/2013325.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2013325_Fobs loop_ _publ_author_name 'Lo Presti, Leonardo' 'Soave, Raffaella' 'Destro, Riccardo' _publ_section_title ; The fungal metabolite austdiol ; _journal_issue 4 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first o199 _journal_page_last o201 _journal_volume 59 _journal_year 2003 _space_group_IT_number 18 _symmetry_space_group_name_Hall 'P 2 2ab' _symmetry_space_group_name_H-M 'P 21 21 2' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 8.4480 _cell_length_b 19.9380 _cell_length_c 6.4280 _exptl_crystal_F_000 496.00 _reflns_d_resolution_high .7686 _[local]_cod_data_source_file na1600Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' Austdiol T=298 K, data 1999 from P4, Group P21 21 2' _shelx_refln_list_code 4 _shelx_f_calc_maximum 242.89 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, z' '-x+1/2, y+1/2, -z' 'x+1/2, -y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 9.19 8.99 .75 o 4 0 0 47.18 50.45 1.84 o 6 0 0 24.97 23.15 1.32 o 8 0 0 1.73 1.77 .99 o 10 0 0 180.16 205.51 7.27 o 1 1 0 336.29 342.85 1.48 o 2 1 0 3159.46 3062.55 13.92 o 3 1 0 818.68 883.42 6.07 o 4 1 0 92.92 91.17 1.35 o 5 1 0 2.89 1.97 .72 o 6 1 0 202.97 199.99 2.44 o 7 1 0 382.09 361.98 3.85 o 8 1 0 143.23 147.16 3.06 o 9 1 0 9.59 9.23 1.23 o 10 1 0 79.74 92.65 3.59 o 0 2 0 6023.75 5589.91 16.28 o 1 2 0 729.93 739.35 1.91 o 2 2 0 1642.17 1530.30 5.22 o 3 2 0 99.67 75.16 1.10 o 4 2 0 1121.86 1178.17 4.51 o 5 2 0 65.20 70.40 2.74 o 6 2 0 36.53 32.58 1.22 o 7 2 0 966.81 941.29 7.53 o 8 2 0 4.50 7.39 1.14 o 9 2 0 .00 .58 .98 o 10 2 0 1.73 2.59 1.59 o 1 3 0 530.59 504.16 1.77 o 2 3 0 104.01 108.67 1.10 o 3 3 0 10.71 11.54 .74 o 4 3 0 3653.18 3831.26 42.65 o 5 3 0 188.59 198.69 2.22 o 6 3 0 436.72 388.78 3.41 o 7 3 0 217.99 206.99 4.78 o 8 3 0 381.88 372.94 3.97 o 9 3 0 .62 1.36 1.36 o 10 3 0 15.30 14.86 3.57 o 0 4 0 110.83 91.13 1.20 o 1 4 0 1508.83 1463.54 3.58 o 2 4 0 476.97 500.79 2.30 o 3 4 0 606.56 668.81 3.11 o 4 4 0 108.25 127.72 1.65 o 5 4 0 305.08 300.37 3.57 o 6 4 0 256.48 219.70 2.70 o 7 4 0 80.63 76.74 2.11 o 8 4 0 54.86 55.22 1.89 o 9 4 0 8.00 6.86 2.21 o 10 4 0 2.75 4.84 5.32 o 1 5 0 862.03 839.01 3.34 o 2 5 0 425.20 444.69 2.32 o 3 5 0 1216.50 1360.88 5.74 o 4 5 0 13.09 20.64 1.28 o 5 5 0 66.11 59.82 1.43 o 6 5 0 16.04 14.56 1.01 o 7 5 0 518.35 472.16 4.26 o 8 5 0 1.50 1.35 1.04 o 9 5 0 37.03 35.86 2.54 o 10 5 0 11.48 12.31 2.18 o 0 6 0 4444.73 4457.93 9.17 o 1 6 0 120.62 148.38 1.34 o 2 6 0 9.85 7.26 .54 o 3 6 0 314.47 277.16 3.22 o 4 6 0 166.24 193.90 2.81 o 5 6 0 .41 .73 .78 o 6 6 0 101.45 100.45 2.26 o 7 6 0 46.00 47.79 1.67 o 8 6 0 181.24 155.23 2.82 o 9 6 0 29.34 30.09 2.43 o 10 6 0 1.97 1.86 1.74 o 1 7 0 997.81 1029.27 3.60 o 2 7 0 31.77 29.74 .90 o 3 7 0 988.08 1022.67 4.26 o 4 7 0 224.33 191.90 2.15 o 5 7 0 21.87 16.87 1.10 o 6 7 0 189.58 198.37 2.69 o 7 7 0 27.03 18.37 1.31 o 8 7 0 8.28 4.78 1.04 o 9 7 0 7.40 7.24 2.05 o 10 7 0 .90 1.06 1.84 o 0 8 0 404.30 470.22 3.67 o 1 8 0 160.90 168.30 2.32 o 2 8 0 164.87 181.81 2.35 o 3 8 0 159.72 177.51 1.94 o 4 8 0 374.44 382.03 3.01 o 5 8 0 161.60 174.49 2.28 o 6 8 0 31.66 27.53 1.41 o 7 8 0 69.60 65.73 1.96 o 8 8 0 25.84 24.19 1.55 o 9 8 0 43.10 44.09 2.79 o 10 8 0 .23 -.81 1.54 o 1 9 0 2537.74 2765.23 11.58 o 2 9 0 23.59 23.88 .94 o 3 9 0 48.66 52.23 1.21 o 4 9 0 14.43 15.08 1.13 o 5 9 0 111.96 104.91 1.93 o 6 9 0 50.29 50.14 1.57 o 7 9 0 8.44 7.08 1.19 o 8 9 0 2.27 2.11 1.02 o 9 9 0 17.88 18.51 3.65 o 10 9 0 6.46 7.23 1.89 o 0 10 0 2869.69 3019.53 10.30 o 1 10 0 1001.18 1047.61 4.46 o 2 10 0 45.51 46.78 1.19 o 3 10 0 .54 .80 .58 o 4 10 0 .50 .26 .67 o 5 10 0 190.74 180.62 2.53 o 6 10 0 197.42 173.12 2.66 o 7 10 0 4.32 3.31 1.01 o 8 10 0 99.21 93.75 3.85 o 9 10 0 .92 .43 1.66 o 10 10 0 2.78 3.25 2.34 o 1 11 0 1121.16 1177.78 4.93 o 2 11 0 182.81 182.54 2.14 o 3 11 0 78.19 80.91 1.55 o 4 11 0 56.77 62.31 1.52 o 5 11 0 228.90 217.73 2.77 o 6 11 0 25.34 16.17 1.31 o 7 11 0 108.20 97.50 2.32 o 8 11 0 19.48 19.69 2.21 o 9 11 0 13.95 19.96 4.85 o 0 12 0 361.67 391.41 4.39 o 1 12 0 4.20 4.45 .78 o 2 12 0 246.27 254.50 2.78 o 3 12 0 106.71 106.08 1.87 o 4 12 0 383.34 362.23 3.34 o 5 12 0 118.36 122.07 2.26 o 6 12 0 224.86 205.94 3.02 o 7 12 0 161.94 153.22 2.88 o 8 12 0 5.82 7.98 3.00 o 9 12 0 28.75 25.60 3.52 o 1 13 0 1.45 .73 .76 o 2 13 0 43.56 41.98 2.98 o 3 13 0 36.75 39.13 1.30 o 4 13 0 1151.93 1085.76 5.84 o 5 13 0 94.03 90.67 2.05 o 6 13 0 380.47 330.65 4.25 o 7 13 0 1.75 1.38 1.19 o 8 13 0 17.26 16.82 2.29 o 9 13 0 27.07 31.38 2.69 o 0 14 0 83.19 75.17 2.20 o 1 14 0 286.85 284.12 2.86 o 2 14 0 387.09 376.13 3.34 o 3 14 0 199.39 198.66 2.66 o 4 14 0 81.08 79.33 2.00 o 5 14 0 316.28 320.85 5.09 o 6 14 0 9.18 7.45 1.21 o 7 14 0 15.31 14.47 1.81 o 8 14 0 2.44 1.73 1.95 o 9 14 0 .80 2.88 1.90 o 1 15 0 114.83 116.61 2.08 o 2 15 0 183.30 173.12 3.05 o 3 15 0 888.89 863.57 5.33 o 4 15 0 10.54 10.51 1.20 o 5 15 0 3.03 3.57 1.03 o 6 15 0 67.01 71.15 2.18 o 7 15 0 34.03 35.72 2.52 o 8 15 0 111.95 112.89 6.65 o 0 16 0 275.13 284.94 4.34 o 1 16 0 24.22 23.48 1.24 o 2 16 0 1061.82 1040.24 7.79 o 3 16 0 129.63 121.96 2.29 o 4 16 0 2.59 2.87 1.03 o 5 16 0 31.87 31.21 1.54 o 6 16 0 2.20 1.08 1.00 o 7 16 0 4.80 5.57 2.13 o 8 16 0 67.54 82.25 3.74 o 1 17 0 .53 1.45 1.05 o 2 17 0 332.56 306.58 4.59 o 3 17 0 59.54 59.48 1.90 o 4 17 0 12.63 10.81 1.61 o 5 17 0 83.82 82.55 2.27 o 6 17 0 31.99 33.62 3.93 o 7 17 0 35.07 38.87 2.70 o 8 17 0 5.41 10.47 2.42 o 0 18 0 244.73 241.12 4.39 o 1 18 0 402.43 320.74 3.56 o 2 18 0 15.73 14.56 1.37 o 3 18 0 2.75 2.30 .94 o 4 18 0 32.40 33.03 1.53 o 5 18 0 .12 -1.36 1.36 o 6 18 0 13.05 11.90 2.03 o 7 18 0 .00 -1.35 2.36 o 1 19 0 .67 -.16 1.13 o 2 19 0 161.31 131.76 2.55 o 3 19 0 166.62 163.91 2.99 o 4 19 0 42.46 42.50 2.34 o 5 19 0 4.59 6.75 2.04 o 6 19 0 2.43 .32 1.75 o 7 19 0 .16 -1.54 1.54 o 0 20 0 7.36 10.10 2.21 o 1 20 0 38.46 31.60 1.58 o 2 20 0 25.96 23.84 1.57 o 3 20 0 2.67 1.85 1.13 o 4 20 0 37.10 34.35 2.45 o 5 20 0 .88 .92 1.48 o 6 20 0 26.53 31.09 2.81 o 1 21 0 .91 .80 1.59 o 2 21 0 .65 1.23 1.61 o 3 21 0 .00 1.12 1.75 o 4 21 0 .16 1.94 3.00 o 5 21 0 .46 .25 2.26 o 6 21 0 13.65 11.00 2.26 o 0 22 0 107.94 106.07 5.39 o 1 22 0 .21 2.28 1.32 o 2 22 0 29.64 31.76 2.48 o 3 22 0 .07 1.93 1.90 o 4 22 0 3.16 4.52 2.29 o 5 22 0 55.64 64.81 3.63 o 1 23 0 1.32 .81 2.31 o 2 23 0 26.68 26.81 2.65 o 3 23 0 28.73 33.81 2.63 o 4 23 0 .25 1.90 1.56 o 5 23 0 12.06 13.16 3.96 o 0 24 0 5.75 9.66 2.62 o 1 24 0 4.84 7.42 3.03 o 2 24 0 50.26 55.55 3.56 o 3 24 0 .83 2.35 1.79 o 4 24 0 14.26 17.97 2.67 o 1 25 0 36.03 43.35 3.08 o 2 25 0 92.70 108.01 4.30 o 0 0 1 23.57 31.11 .94 o 1 0 1 500.06 475.39 1.67 o 2 0 1 986.99 968.30 3.60 o 3 0 1 190.20 175.12 1.28 o 4 0 1 73.16 83.69 1.09 o 5 0 1 669.30 667.52 3.13 o 6 0 1 7.02 7.15 .83 o 7 0 1 .60 2.05 1.18 o 8 0 1 16.35 14.60 1.07 o 9 0 1 20.32 21.63 1.22 o 10 0 1 2.03 .63 1.29 o 0 1 1 8545.89 8332.60 40.05 o 1 1 1 5971.07 5817.97 11.02 o 2 1 1 517.13 529.62 2.30 o 3 1 1 204.81 205.05 1.40 o 4 1 1 137.80 125.55 1.64 o 5 1 1 88.94 88.61 1.38 o 6 1 1 363.84 358.69 2.61 o 7 1 1 89.37 97.65 1.75 o 8 1 1 34.81 31.45 1.26 o 9 1 1 23.72 23.18 1.47 o 10 1 1 16.98 18.38 1.73 o 0 2 1 34.37 31.83 .62 o 1 2 1 14.21 15.59 .46 o 2 2 1 1090.61 1096.90 5.60 o 3 2 1 5460.22 5502.33 31.90 o 4 2 1 432.98 474.83 2.40 o 5 2 1 51.64 46.51 1.71 o 6 2 1 215.38 238.38 2.19 o 7 2 1 739.17 723.90 4.08 o 8 2 1 107.83 106.31 1.95 o 9 2 1 .42 1.04 1.02 o 10 2 1 17.81 17.85 2.19 o 0 3 1 4.89 4.86 .44 o 1 3 1 1421.41 1398.03 4.00 o 2 3 1 1362.78 1366.67 5.63 o 3 3 1 17.56 16.67 .69 o 4 3 1 1535.28 1669.12 7.47 o 5 3 1 520.64 525.55 3.69 o 6 3 1 791.88 754.60 3.98 o 7 3 1 399.27 390.08 3.05 o 8 3 1 18.09 18.47 1.13 o 9 3 1 .45 .61 1.09 o 10 3 1 1.21 2.64 1.20 o 0 4 1 119.26 123.10 1.28 o 1 4 1 876.67 902.33 2.33 o 2 4 1 732.32 704.79 4.17 o 3 4 1 1059.85 1048.06 6.19 o 4 4 1 89.08 96.33 1.24 o 5 4 1 51.36 40.22 1.05 o 6 4 1 283.90 266.32 2.38 o 7 4 1 61.04 55.20 1.47 o 8 4 1 7.20 5.73 .98 o 9 4 1 62.90 67.76 3.67 o 10 4 1 9.14 10.72 1.61 o 0 5 1 495.08 518.19 3.17 o 1 5 1 39.17 38.57 .90 o 2 5 1 2131.76 2071.10 10.00 o 3 5 1 1610.33 1640.65 8.32 o 4 5 1 288.03 316.99 2.10 o 5 5 1 460.88 472.04 3.09 o 6 5 1 30.78 29.28 1.30 o 7 5 1 55.99 66.07 1.81 o 8 5 1 13.79 10.30 1.00 o 9 5 1 9.97 10.77 1.38 o 10 5 1 6.75 10.16 1.63 o 0 6 1 370.19 361.60 2.36 o 1 6 1 157.82 160.83 1.18 o 2 6 1 1290.07 1298.82 6.20 o 3 6 1 329.24 360.96 2.07 o 4 6 1 45.39 55.85 1.08 o 5 6 1 118.85 123.59 1.96 o 6 6 1 22.76 22.44 1.11 o 7 6 1 161.00 149.91 2.12 o 8 6 1 14.20 16.28 1.08 o 9 6 1 16.91 18.94 1.61 o 10 6 1 12.54 15.25 3.54 o 0 7 1 11.88 12.08 .68 o 1 7 1 919.86 949.53 3.03 o 2 7 1 315.02 311.79 2.45 o 3 7 1 404.54 455.77 3.40 o 4 7 1 203.79 208.65 2.03 o 5 7 1 78.28 89.53 1.42 o 6 7 1 20.48 19.75 1.11 o 7 7 1 225.51 194.78 2.39 o 8 7 1 43.58 43.17 1.46 o 9 7 1 30.03 37.46 2.38 o 10 7 1 .44 .98 1.25 o 0 8 1 328.21 334.38 2.59 o 1 8 1 667.68 734.13 3.35 o 2 8 1 253.13 249.88 2.68 o 3 8 1 773.50 777.32 3.21 o 4 8 1 6.75 5.26 .66 o 5 8 1 36.45 36.35 1.19 o 6 8 1 28.04 27.00 1.06 o 7 8 1 183.77 157.97 2.76 o 8 8 1 2.43 .84 .82 o 9 8 1 4.84 4.45 1.24 o 10 8 1 14.23 19.54 1.89 o 0 9 1 2286.90 2462.87 7.44 o 1 9 1 748.56 891.51 3.20 o 2 9 1 169.46 186.65 1.60 o 3 9 1 51.26 51.48 1.07 o 4 9 1 28.94 28.29 .92 o 5 9 1 53.79 50.71 1.22 o 6 9 1 105.09 105.86 2.70 o 7 9 1 24.22 23.65 1.15 o 8 9 1 34.35 33.52 1.40 o 9 9 1 49.75 58.26 2.29 o 10 9 1 8.22 6.49 1.49 o 0 10 1 15.23 14.11 .92 o 1 10 1 317.61 309.89 3.02 o 2 10 1 97.69 106.03 1.31 o 3 10 1 25.83 27.31 .88 o 4 10 1 18.29 17.89 .83 o 5 10 1 44.62 43.64 1.24 o 6 10 1 29.05 30.82 1.18 o 7 10 1 66.36 68.03 1.67 o 8 10 1 3.95 3.25 1.09 o 9 10 1 7.93 8.13 1.34 o 10 10 1 21.58 27.93 2.13 o 0 11 1 41.28 40.02 1.41 o 1 11 1 495.71 532.27 2.76 o 2 11 1 80.61 89.75 1.31 o 3 11 1 15.29 16.15 1.06 o 4 11 1 98.74 87.14 1.79 o 5 11 1 284.83 292.49 2.61 o 6 11 1 114.20 97.83 1.96 o 7 11 1 59.79 58.36 1.66 o 8 11 1 16.80 17.59 1.46 o 9 11 1 13.68 16.93 1.58 o 0 12 1 178.09 183.05 2.51 o 1 12 1 50.79 49.09 1.06 o 2 12 1 68.99 66.67 1.35 o 3 12 1 116.02 106.69 2.12 o 4 12 1 847.72 803.04 4.06 o 5 12 1 429.98 392.01 3.11 o 6 12 1 14.38 14.48 1.03 o 7 12 1 108.96 97.61 1.98 o 8 12 1 40.73 37.93 1.91 o 9 12 1 1.69 .68 1.39 o 0 13 1 55.39 54.48 1.59 o 1 13 1 120.38 119.28 1.52 o 2 13 1 34.18 35.21 1.01 o 3 13 1 42.47 45.46 1.15 o 4 13 1 1323.52 1254.13 5.21 o 5 13 1 112.93 109.09 1.83 o 6 13 1 116.48 101.23 1.89 o 7 13 1 4.30 1.44 .88 o 8 13 1 8.22 7.04 1.42 o 9 13 1 34.61 37.08 2.34 o 0 14 1 1.38 2.16 1.04 o 1 14 1 207.10 191.99 1.97 o 2 14 1 410.44 394.07 2.82 o 3 14 1 432.48 429.60 3.06 o 4 14 1 161.56 157.21 2.57 o 5 14 1 477.69 466.57 4.42 o 6 14 1 147.45 137.65 2.22 o 7 14 1 4.00 3.78 1.10 o 8 14 1 4.36 3.75 1.32 o 9 14 1 5.92 4.25 1.88 o 0 15 1 75.58 58.11 2.32 o 1 15 1 420.78 419.14 3.94 o 2 15 1 5.78 5.56 1.05 o 3 15 1 470.08 463.00 3.27 o 4 15 1 243.40 236.08 2.60 o 5 15 1 28.15 25.35 1.49 o 6 15 1 2.58 3.53 .84 o 7 15 1 23.08 24.49 1.62 o 8 15 1 36.76 43.57 2.25 o 0 16 1 53.73 52.52 1.79 o 1 16 1 5.89 6.19 .77 o 2 16 1 1090.02 1029.54 4.84 o 3 16 1 118.42 111.69 1.87 o 4 16 1 9.93 10.51 .97 o 5 16 1 1.49 .34 1.18 o 6 16 1 19.81 22.77 1.50 o 7 16 1 1.92 .80 1.10 o 8 16 1 79.36 83.10 2.71 o 0 17 1 88.18 78.70 2.33 o 1 17 1 18.40 17.55 1.24 o 2 17 1 52.93 58.25 1.76 o 3 17 1 25.25 22.28 1.14 o 4 17 1 23.39 23.02 1.14 o 5 17 1 145.91 150.43 2.35 o 6 17 1 8.16 7.05 1.40 o 7 17 1 5.15 4.86 2.15 o 8 17 1 41.35 41.83 2.39 o 0 18 1 18.20 21.87 1.51 o 1 18 1 40.40 28.72 1.21 o 2 18 1 65.56 67.85 1.60 o 3 18 1 5.06 5.83 .89 o 4 18 1 43.55 47.19 1.50 o 5 18 1 36.02 36.77 1.85 o 6 18 1 4.10 2.53 1.17 o 7 18 1 3.00 2.64 1.26 o 0 19 1 7.55 1.74 1.33 o 1 19 1 14.90 13.74 1.03 o 2 19 1 86.93 68.67 1.86 o 3 19 1 1.07 .06 .84 o 4 19 1 59.29 58.70 1.66 o 5 19 1 7.97 8.83 1.76 o 6 19 1 2.25 3.64 1.25 o 7 19 1 19.84 24.13 1.83 o 0 20 1 4.36 4.75 1.31 o 1 20 1 27.41 19.79 1.15 o 2 20 1 10.25 9.92 1.14 o 3 20 1 81.28 82.07 1.94 o 4 20 1 17.22 15.78 1.48 o 5 20 1 16.80 19.32 1.66 o 6 20 1 .33 2.06 1.21 o 0 21 1 153.28 138.28 3.49 o 1 21 1 10.19 8.05 1.06 o 2 21 1 14.66 12.48 1.32 o 3 21 1 21.29 21.47 1.54 o 4 21 1 15.93 17.49 1.59 o 5 21 1 58.93 68.59 2.49 o 6 21 1 6.75 8.03 1.52 o 0 22 1 19.95 20.60 2.40 o 1 22 1 4.93 4.62 1.48 o 2 22 1 7.98 7.72 1.44 o 3 22 1 6.90 6.77 1.39 o 4 22 1 38.28 42.09 2.11 o 5 22 1 1.35 1.22 1.32 o 0 23 1 33.81 41.20 2.69 o 1 23 1 .49 -.93 .93 o 2 23 1 15.66 21.05 1.70 o 3 23 1 8.88 8.75 1.91 o 4 23 1 2.37 1.45 1.26 o 0 24 1 9.94 10.95 2.15 o 1 24 1 6.31 9.10 1.41 o 2 24 1 11.31 10.25 1.75 o 3 24 1 16.01 22.32 2.62 o 0 25 1 8.37 10.18 2.73 o 1 25 1 15.96 17.33 1.79 o 2 25 1 33.24 35.56 2.21 o 0 0 2 58993.49 51087.37 226.49 o 1 0 2 122.25 127.86 1.05 o 2 0 2 442.71 429.64 2.98 o 3 0 2 147.52 149.88 1.35 o 4 0 2 4.22 4.73 .57 o 5 0 2 93.65 96.99 1.37 o 6 0 2 14.55 15.63 1.00 o 7 0 2 14.95 11.34 1.00 o 8 0 2 .40 .51 .81 o 9 0 2 .81 .22 1.07 o 10 0 2 65.23 76.48 2.58 o 0 1 2 3577.98 3675.92 23.07 o 1 1 2 302.72 329.45 2.13 o 2 1 2 561.70 581.71 2.35 o 3 1 2 43.66 46.75 .91 o 4 1 2 3.95 3.79 .55 o 5 1 2 13.66 15.23 .99 o 6 1 2 211.28 210.94 2.15 o 7 1 2 102.32 109.32 1.85 o 8 1 2 187.65 199.49 2.69 o 9 1 2 .16 1.68 1.04 o 10 1 2 63.88 71.92 2.60 o 0 2 2 7281.00 7706.73 27.43 o 1 2 2 262.22 217.26 1.34 o 2 2 2 426.17 433.97 2.03 o 3 2 2 22.03 24.68 .69 o 4 2 2 374.67 384.41 2.33 o 5 2 2 89.29 90.56 1.37 o 6 2 2 42.84 43.91 1.19 o 7 2 2 620.87 623.38 6.26 o 8 2 2 1.01 1.08 .83 o 9 2 2 3.43 1.26 1.01 o 10 2 2 10.43 10.21 1.62 o 0 3 2 428.51 446.64 4.58 o 1 3 2 475.16 493.72 2.88 o 2 3 2 1044.06 1001.90 6.45 o 3 3 2 92.07 77.62 1.33 o 4 3 2 1109.88 1154.63 4.01 o 5 3 2 70.34 73.41 1.74 o 6 3 2 174.59 165.73 2.01 o 7 3 2 143.84 146.84 2.11 o 8 3 2 110.80 113.87 2.06 o 9 3 2 .07 .35 .94 o 10 3 2 19.30 17.39 1.77 o 0 4 2 601.78 556.95 3.05 o 1 4 2 12.80 12.96 .49 o 2 4 2 532.89 514.08 3.22 o 3 4 2 78.01 97.08 1.23 o 4 4 2 119.19 127.88 1.45 o 5 4 2 175.15 182.15 1.89 o 6 4 2 141.34 130.45 1.84 o 7 4 2 35.13 34.18 1.21 o 8 4 2 49.11 48.37 1.90 o 9 4 2 2.60 3.26 1.37 o 10 4 2 17.52 17.89 1.69 o 0 5 2 .51 .74 .60 o 1 5 2 259.58 250.08 1.59 o 2 5 2 257.84 273.69 1.75 o 3 5 2 1402.29 1487.35 4.31 o 4 5 2 119.38 139.40 1.55 o 5 5 2 92.79 93.38 1.49 o 6 5 2 50.19 48.50 1.29 o 7 5 2 227.97 213.65 2.45 o 8 5 2 3.92 3.87 .95 o 9 5 2 47.88 50.54 2.14 o 10 5 2 9.71 11.25 1.42 o 0 6 2 137.00 147.45 1.87 o 1 6 2 145.80 148.23 1.65 o 2 6 2 188.35 164.64 1.47 o 3 6 2 105.12 106.39 1.34 o 4 6 2 7.60 12.59 .83 o 5 6 2 53.16 52.51 1.48 o 6 6 2 52.77 58.78 1.42 o 7 6 2 9.40 9.02 .90 o 8 6 2 148.94 139.04 2.32 o 9 6 2 35.57 33.64 1.99 o 10 6 2 .96 1.67 1.42 o 0 7 2 29.09 27.45 .95 o 1 7 2 274.30 286.24 1.84 o 2 7 2 288.14 308.91 1.99 o 3 7 2 289.36 312.33 2.24 o 4 7 2 64.35 54.77 1.14 o 5 7 2 52.82 53.54 1.27 o 6 7 2 214.50 222.62 2.98 o 7 7 2 99.41 88.96 1.86 o 8 7 2 .50 .26 .85 o 9 7 2 7.78 9.66 1.96 o 10 7 2 2.18 2.68 1.22 o 0 8 2 18.70 21.09 .99 o 1 8 2 378.18 430.82 2.32 o 2 8 2 145.43 154.70 1.67 o 3 8 2 50.13 52.66 1.06 o 4 8 2 56.25 60.27 1.18 o 5 8 2 174.55 172.46 2.36 o 6 8 2 13.95 11.69 .89 o 7 8 2 55.85 49.65 1.52 o 8 8 2 26.60 22.86 1.33 o 9 8 2 46.86 49.42 2.26 o 10 8 2 1.73 1.08 1.28 o 0 9 2 40.04 42.65 1.28 o 1 9 2 1169.69 1226.41 4.03 o 2 9 2 101.40 97.77 1.29 o 3 9 2 32.44 31.31 .89 o 4 9 2 155.89 160.29 1.79 o 5 9 2 54.93 56.81 1.36 o 6 9 2 15.94 15.79 1.03 o 7 9 2 7.77 8.01 .95 o 8 9 2 11.35 11.51 1.32 o 9 9 2 24.18 25.80 1.75 o 0 10 2 1114.12 1215.38 5.83 o 1 10 2 876.56 870.23 3.56 o 2 10 2 21.77 19.35 .81 o 3 10 2 49.46 50.16 1.11 o 4 10 2 6.33 6.49 .74 o 5 10 2 60.62 57.38 1.38 o 6 10 2 143.83 134.31 2.13 o 7 10 2 18.39 16.11 1.65 o 8 10 2 68.51 73.51 2.31 o 9 10 2 .85 .26 1.42 o 0 11 2 40.67 37.63 1.34 o 1 11 2 705.98 755.05 3.45 o 2 11 2 106.66 106.60 1.61 o 3 11 2 25.05 24.49 .99 o 4 11 2 22.22 21.23 .99 o 5 11 2 57.68 51.84 1.41 o 6 11 2 28.86 28.58 1.59 o 7 11 2 38.49 32.25 1.40 o 8 11 2 29.83 30.77 1.83 o 9 11 2 6.93 7.54 1.35 o 0 12 2 13.65 14.97 1.11 o 1 12 2 103.83 104.71 1.52 o 2 12 2 19.28 19.38 .85 o 3 12 2 47.45 44.05 1.16 o 4 12 2 101.04 102.74 1.68 o 5 12 2 60.03 61.32 2.72 o 6 12 2 140.64 134.51 2.17 o 7 12 2 103.99 97.77 2.11 o 8 12 2 13.88 16.17 2.16 o 9 12 2 15.40 14.43 2.05 o 0 13 2 22.49 23.30 2.54 o 1 13 2 23.86 28.80 .95 o 2 13 2 17.70 17.32 .88 o 3 13 2 147.27 145.99 2.08 o 4 13 2 540.47 509.37 3.49 o 5 13 2 150.21 151.59 2.63 o 6 13 2 169.26 140.59 2.33 o 7 13 2 8.57 6.08 1.35 o 8 13 2 17.48 21.24 1.77 o 9 13 2 14.73 14.98 1.73 o 0 14 2 231.96 239.86 3.24 o 1 14 2 73.84 78.87 1.42 o 2 14 2 221.17 213.13 2.21 o 3 14 2 39.28 36.77 1.46 o 4 14 2 66.87 67.91 1.61 o 5 14 2 183.47 187.69 2.43 o 6 14 2 27.32 27.75 1.54 o 7 14 2 4.13 1.78 1.14 o 8 14 2 1.95 2.25 1.14 o 0 15 2 33.36 36.67 1.56 o 1 15 2 57.67 60.30 1.35 o 2 15 2 97.10 91.49 1.62 o 3 15 2 487.31 487.26 3.50 o 4 15 2 16.78 15.11 1.03 o 5 15 2 8.88 7.54 .97 o 6 15 2 1.62 .93 1.05 o 7 15 2 26.63 28.86 1.76 o 8 15 2 54.08 53.41 2.38 o 0 16 2 169.07 178.57 2.98 o 1 16 2 13.97 14.05 .95 o 2 16 2 503.30 498.41 3.49 o 3 16 2 70.85 71.40 2.00 o 4 16 2 1.19 1.54 .76 o 5 16 2 11.63 12.45 1.05 o 6 16 2 .72 1.90 1.04 o 7 16 2 2.22 2.01 1.35 o 8 16 2 33.30 38.53 2.15 o 0 17 2 1.98 1.82 1.04 o 1 17 2 19.60 18.94 1.04 o 2 17 2 151.24 133.09 2.11 o 3 17 2 20.13 21.31 1.15 o 4 17 2 25.20 23.34 1.24 o 5 17 2 11.58 11.89 1.32 o 6 17 2 20.38 23.13 1.55 o 7 17 2 8.19 8.86 1.75 o 0 18 2 36.62 35.56 1.73 o 1 18 2 205.25 177.98 2.45 o 2 18 2 7.23 8.80 1.11 o 3 18 2 14.26 15.18 1.07 o 4 18 2 3.73 4.95 .94 o 5 18 2 1.21 1.18 1.00 o 6 18 2 8.76 8.23 1.37 o 7 18 2 .06 1.25 1.13 o 0 19 2 13.80 15.01 1.59 o 1 19 2 26.34 27.21 1.23 o 2 19 2 102.62 85.46 1.85 o 3 19 2 36.28 37.63 1.37 o 4 19 2 46.47 43.72 1.90 o 5 19 2 15.57 13.25 1.63 o 6 19 2 .76 .56 1.13 o 7 19 2 10.40 11.10 1.72 o 0 20 2 11.54 11.14 1.44 o 1 20 2 5.62 3.25 .92 o 2 20 2 15.15 15.39 1.36 o 3 20 2 18.12 20.46 1.57 o 4 20 2 21.28 20.23 1.52 o 5 20 2 4.11 4.27 1.43 o 6 20 2 18.64 21.77 1.71 o 0 21 2 8.24 10.88 2.54 o 1 21 2 1.69 1.36 1.08 o 2 21 2 8.03 7.31 1.24 o 3 21 2 12.30 13.79 1.38 o 4 21 2 5.88 7.51 1.26 o 5 21 2 .01 .82 1.27 o 0 22 2 90.57 91.37 3.38 o 1 22 2 15.06 14.04 1.82 o 2 22 2 6.23 7.47 1.68 o 3 22 2 7.94 9.92 1.37 o 4 22 2 4.93 6.38 1.37 o 5 22 2 34.67 39.81 2.46 o 0 23 2 5.10 2.83 2.07 o 1 23 2 10.03 10.75 1.50 o 2 23 2 15.26 15.56 1.58 o 3 23 2 33.34 37.17 2.98 o 4 23 2 8.64 8.74 1.46 o 0 24 2 .78 1.55 1.69 o 1 24 2 6.99 6.86 1.47 o 2 24 2 12.45 15.83 1.63 o 3 24 2 4.50 3.06 1.37 o 0 25 2 .11 -.52 1.30 o 1 25 2 22.50 26.85 1.83 o 0 0 3 1209.22 1312.42 5.28 o 1 0 3 97.95 98.99 1.20 o 2 0 3 39.86 42.75 .87 o 3 0 3 371.10 371.63 2.32 o 4 0 3 34.71 33.47 1.00 o 5 0 3 446.68 436.42 2.92 o 6 0 3 53.99 57.61 1.39 o 7 0 3 26.48 23.89 1.21 o 8 0 3 14.82 14.73 1.15 o 9 0 3 8.07 7.54 1.30 o 10 0 3 26.57 26.52 2.05 o 0 1 3 1326.16 1315.67 5.87 o 1 1 3 1114.77 1227.37 3.71 o 2 1 3 3.99 4.96 .84 o 3 1 3 387.42 402.29 2.46 o 4 1 3 7.61 7.80 .78 o 5 1 3 45.48 42.02 1.13 o 6 1 3 194.53 200.90 2.27 o 7 1 3 96.49 100.76 1.90 o 8 1 3 13.52 12.75 1.18 o 9 1 3 14.17 12.87 1.40 o 10 1 3 2.77 4.62 1.73 o 0 2 3 219.56 185.69 2.12 o 1 2 3 585.71 562.42 2.56 o 2 2 3 182.09 192.24 1.62 o 3 2 3 1169.46 1154.29 4.06 o 4 2 3 287.67 294.99 2.27 o 5 2 3 25.61 26.91 1.34 o 6 2 3 48.21 49.79 1.35 o 7 2 3 301.40 315.50 3.02 o 8 2 3 23.27 22.10 1.23 o 9 2 3 5.65 4.62 1.26 o 10 2 3 11.46 11.88 1.74 o 0 3 3 .61 .08 .58 o 1 3 3 283.05 263.68 1.81 o 2 3 3 186.05 188.21 1.63 o 3 3 3 28.84 26.14 1.05 o 4 3 3 276.47 286.01 3.51 o 5 3 3 166.25 171.09 1.94 o 6 3 3 255.08 260.19 2.85 o 7 3 3 207.44 211.39 4.02 o 8 3 3 13.86 11.46 1.18 o 9 3 3 1.43 1.32 1.26 o 10 3 3 .02 .86 1.25 o 0 4 3 2.88 2.79 .67 o 1 4 3 79.40 78.85 1.09 o 2 4 3 269.18 272.54 1.99 o 3 4 3 444.30 462.78 3.24 o 4 4 3 40.52 39.43 1.05 o 5 4 3 9.50 10.18 .84 o 6 4 3 165.44 166.70 2.21 o 7 4 3 48.60 43.49 1.49 o 8 4 3 5.35 7.45 1.31 o 9 4 3 32.48 40.77 1.97 o 10 4 3 7.56 7.87 1.83 o 0 5 3 168.08 180.13 2.20 o 1 5 3 9.63 13.63 .62 o 2 5 3 126.61 103.56 1.66 o 3 5 3 416.65 417.56 2.81 o 4 5 3 136.54 140.22 2.66 o 5 5 3 126.32 128.28 1.78 o 6 5 3 39.32 41.13 1.69 o 7 5 3 36.80 39.61 1.44 o 8 5 3 .66 2.97 1.04 o 9 5 3 11.05 14.04 1.46 o 10 5 3 4.24 2.32 1.59 o 0 6 3 24.23 27.84 1.08 o 1 6 3 28.44 29.96 .82 o 2 6 3 427.85 434.36 2.55 o 3 6 3 246.79 277.02 2.19 o 4 6 3 14.66 17.59 .90 o 5 6 3 21.90 21.34 1.40 o 6 6 3 34.23 34.62 1.27 o 7 6 3 95.38 92.57 1.94 o 8 6 3 5.13 5.56 1.32 o 9 6 3 5.95 6.08 1.46 o 0 7 3 86.57 98.83 3.17 o 1 7 3 264.46 251.94 1.96 o 2 7 3 5.38 5.47 .64 o 3 7 3 245.69 247.14 2.55 o 4 7 3 32.58 34.15 1.08 o 5 7 3 3.09 3.38 .80 o 6 7 3 13.99 12.77 1.23 o 7 7 3 63.05 59.01 1.72 o 8 7 3 10.25 10.03 1.29 o 9 7 3 18.40 22.48 1.82 o 0 8 3 108.84 104.65 1.90 o 1 8 3 16.33 18.47 1.05 o 2 8 3 20.88 20.88 .89 o 3 8 3 181.87 184.76 2.71 o 4 8 3 4.83 3.21 .79 o 5 8 3 27.94 28.06 1.18 o 6 8 3 6.92 7.03 .91 o 7 8 3 100.18 92.46 1.95 o 8 8 3 1.01 -.18 1.00 o 9 8 3 1.51 1.59 1.60 o 0 9 3 642.85 672.32 6.61 o 1 9 3 415.57 425.06 3.96 o 2 9 3 38.30 38.73 1.04 o 3 9 3 24.92 26.80 1.67 o 4 9 3 14.58 16.87 1.24 o 5 9 3 28.73 29.16 1.14 o 6 9 3 16.72 15.65 1.61 o 7 9 3 1.97 2.53 .89 o 8 9 3 10.67 12.25 1.32 o 9 9 3 12.99 19.94 1.96 o 0 10 3 2.90 4.02 .88 o 1 10 3 28.62 28.04 1.01 o 2 10 3 11.10 8.69 .77 o 3 10 3 7.35 9.39 1.06 o 4 10 3 24.50 21.92 1.05 o 5 10 3 6.70 4.33 .74 o 6 10 3 14.01 13.72 1.07 o 7 10 3 72.94 72.06 1.85 o 8 10 3 8.71 7.91 1.35 o 9 10 3 1.43 1.68 1.22 o 0 11 3 .11 .08 .88 o 1 11 3 109.81 123.85 1.64 o 2 11 3 39.25 38.88 1.10 o 3 11 3 10.27 12.39 .89 o 4 11 3 109.03 104.23 2.38 o 5 11 3 192.94 185.65 2.60 o 6 11 3 68.47 64.65 1.67 o 7 11 3 10.05 9.96 1.37 o 8 11 3 7.95 7.22 1.39 o 9 11 3 16.82 21.12 1.79 o 0 12 3 55.08 52.26 1.66 o 1 12 3 47.02 55.39 1.26 o 2 12 3 6.47 7.34 .77 o 3 12 3 28.51 29.54 1.13 o 4 12 3 424.27 417.77 3.28 o 5 12 3 206.08 189.30 2.42 o 6 12 3 17.49 18.45 1.22 o 7 12 3 55.07 53.21 2.59 o 8 12 3 25.14 24.12 2.37 o 0 13 3 14.81 14.57 1.32 o 1 13 3 39.72 38.04 1.18 o 2 13 3 79.62 75.42 1.48 o 3 13 3 54.23 56.66 1.47 o 4 13 3 467.96 470.42 4.25 o 5 13 3 62.35 64.68 1.73 o 6 13 3 47.09 43.82 1.61 o 7 13 3 6.32 6.66 1.63 o 8 13 3 .87 -.41 1.22 o 0 14 3 14.72 15.21 1.32 o 1 14 3 61.22 60.89 1.36 o 2 14 3 141.68 137.55 2.05 o 3 14 3 166.37 169.74 2.30 o 4 14 3 96.19 98.42 1.92 o 5 14 3 167.18 164.52 2.46 o 6 14 3 48.16 44.30 1.87 o 7 14 3 22.45 21.36 1.68 o 8 14 3 1.45 2.28 1.26 o 0 15 3 .67 3.39 2.12 o 1 15 3 148.38 143.66 2.43 o 2 15 3 6.97 6.56 1.08 o 3 15 3 186.41 184.97 2.38 o 4 15 3 139.47 146.45 2.30 o 5 15 3 56.36 58.70 1.69 o 6 15 3 13.14 11.52 1.48 o 7 15 3 5.66 6.61 2.06 o 8 15 3 11.85 13.10 1.69 o 0 16 3 58.47 60.53 2.07 o 1 16 3 22.45 22.71 1.37 o 2 16 3 490.81 497.01 3.70 o 3 16 3 82.62 87.40 2.44 o 4 16 3 25.16 24.78 1.24 o 5 16 3 8.56 10.26 1.88 o 6 16 3 9.93 11.55 1.38 o 7 16 3 7.53 5.80 1.39 o 0 17 3 12.75 10.20 2.21 o 1 17 3 2.33 2.49 .83 o 2 17 3 70.60 65.87 1.81 o 3 17 3 19.92 22.34 1.36 o 4 17 3 34.57 34.10 2.31 o 5 17 3 59.12 58.76 3.39 o 6 17 3 2.34 2.89 1.15 o 7 17 3 1.62 .43 1.00 o 0 18 3 .00 1.40 1.10 o 1 18 3 23.38 21.23 1.23 o 2 18 3 77.97 78.40 1.79 o 3 18 3 6.53 6.16 1.01 o 4 18 3 11.65 10.73 1.51 o 5 18 3 35.81 35.49 1.96 o 6 18 3 2.82 2.45 1.11 o 0 19 3 .00 .18 1.13 o 1 19 3 8.66 7.98 1.03 o 2 19 3 50.22 44.67 1.90 o 3 19 3 5.96 8.98 1.27 o 4 19 3 34.82 32.67 1.77 o 5 19 3 .61 .25 1.18 o 6 19 3 2.23 2.83 1.28 o 0 20 3 32.24 35.94 2.72 o 1 20 3 9.61 7.97 1.30 o 2 20 3 4.08 3.37 1.23 o 3 20 3 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6.19 .90 o 3 10 4 5.59 8.65 .90 o 4 10 4 3.44 4.20 .95 o 5 10 4 16.94 18.03 1.36 o 6 10 4 57.84 61.41 2.25 o 7 10 4 20.33 19.04 2.33 o 8 10 4 45.86 53.80 2.39 o 0 11 4 17.75 16.88 1.41 o 1 11 4 177.98 173.21 2.14 o 2 11 4 80.97 85.05 1.87 o 3 11 4 48.53 50.16 1.45 o 4 11 4 40.86 36.54 1.32 o 5 11 4 55.37 50.49 1.55 o 6 11 4 37.80 40.64 1.90 o 7 11 4 34.83 37.35 1.99 o 8 11 4 6.29 7.40 1.46 o 0 12 4 33.43 31.31 1.69 o 1 12 4 68.60 70.81 1.52 o 2 12 4 18.19 18.02 1.06 o 3 12 4 58.71 52.29 1.46 o 4 12 4 33.86 35.05 1.45 o 5 12 4 19.62 20.90 1.26 o 6 12 4 28.89 27.50 2.24 o 7 12 4 30.31 29.54 1.92 o 8 12 4 5.25 6.93 1.55 o 0 13 4 77.38 76.16 2.33 o 1 13 4 63.36 74.08 1.60 o 2 13 4 16.77 17.84 1.09 o 3 13 4 37.58 40.53 1.41 o 4 13 4 159.53 156.10 2.40 o 5 13 4 25.06 29.98 1.70 o 6 13 4 65.38 59.68 2.21 o 7 13 4 1.02 -.70 1.19 o 0 14 4 49.54 56.87 2.19 o 1 14 4 83.93 84.22 1.74 o 2 14 4 166.00 166.72 4.03 o 3 14 4 14.55 14.20 1.18 o 4 14 4 32.85 34.77 1.41 o 5 14 4 64.38 68.87 2.44 o 6 14 4 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