#------------------------------------------------------------------------------ #$Date: 2016-04-02 21:45:19 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180802 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/33/2013377.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2013377_Fobs loop_ _publ_author_name 'Cario, Laurent' 'Kabbour, Houria' 'Guillot-Deudon, Catherine' 'Meerschaut, Alain' _publ_section_title ; A mixed-valent niobium oxysulfide, La~2~Nb~3~S~2~O~8~ ; _journal_issue 6 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first i55 _journal_page_last i56 _journal_volume 59 _journal_year 2003 _space_group_IT_number 58 _symmetry_space_group_name_Hall '-P 2 2n' _symmetry_space_group_name_H-M 'P n n m' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 9.8698 _cell_length_b 11.7941 _cell_length_c 7.6686 _exptl_crystal_F_000 1332.00 _reflns_d_resolution_high 0.6203 _cod_data_source_file sq1017Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' La2Nb3S2O8 in Pnnm' _shelx_refln_list_code 4 _shelx_f_calc_maximum 476.00 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, z' '-x+1/2, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z+1/2' '-x, -y, -z' 'x, y, -z' 'x-1/2, -y-1/2, z-1/2' '-x-1/2, y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 50076.53 52645.42 1352.79 o 4 0 0 39588.01 39816.75 876.11 o 6 0 0 24913.27 24056.05 564.66 o 8 0 0 36884.53 36802.68 1029.63 o 10 0 0 7399.62 7483.51 249.59 o 12 0 0 21391.76 22526.52 908.63 o 14 0 0 54875.19 51354.81 2595.98 o 2 1 0 41.80 85.70 17.98 o 3 1 0 226577.62 229649.67 3455.55 o 4 1 0 6085.81 5628.97 95.29 o 5 1 0 14880.81 14585.61 223.96 o 6 1 0 109555.29 107470.54 1810.69 o 7 1 0 6389.47 6112.57 119.37 o 8 1 0 26787.84 26527.44 509.93 o 9 1 0 199.88 287.60 54.41 o 10 1 0 7233.68 7678.24 207.58 o 11 1 0 69429.62 73029.00 1926.57 o 12 1 0 193.76 453.23 149.98 o 13 1 0 18.47 -22.92 77.71 o 14 1 0 3500.76 3246.26 220.84 o 15 1 0 925.81 1005.67 256.41 o 0 2 0 25599.67 24470.36 739.58 o 1 2 0 26282.90 27050.16 514.62 o 2 2 0 54711.17 53183.34 875.64 o 3 2 0 148305.45 150900.50 2450.12 o 4 2 0 18624.42 18849.42 305.30 o 5 2 0 94326.20 93868.99 1480.88 o 6 2 0 30069.32 29136.98 504.95 o 7 2 0 5.63 8.01 35.84 o 8 2 0 21388.00 21281.79 409.65 o 9 2 0 55511.68 55041.66 1075.02 o 10 2 0 733.08 705.70 71.44 o 11 2 0 1902.81 1969.79 91.70 o 12 2 0 3356.73 3266.03 148.31 o 13 2 0 1702.09 1707.44 149.27 o 14 2 0 2405.84 1937.81 232.01 o 15 2 0 178.46 307.79 286.37 o 1 3 0 20075.33 18536.17 348.61 o 2 3 0 49635.17 47951.23 839.02 o 3 3 0 30322.41 31848.53 512.81 o 4 3 0 5586.84 5784.78 110.48 o 5 3 0 116239.20 117057.72 1632.51 o 6 3 0 79915.23 77721.72 1260.30 o 7 3 0 51556.00 49981.22 882.11 o 8 3 0 14195.14 14063.87 282.83 o 9 3 0 50566.77 49427.14 978.76 o 10 3 0 2815.11 2943.34 103.86 o 11 3 0 2230.33 2422.22 99.50 o 12 3 0 4719.90 4649.86 166.66 o 13 3 0 5637.43 6669.76 323.24 o 14 3 0 4873.27 4742.10 412.65 o 15 3 0 3503.25 2844.30 321.97 o 0 4 0 84692.98 86211.77 2364.04 o 1 4 0 146579.22 148058.56 2576.43 o 2 4 0 37045.80 33664.53 707.64 o 3 4 0 3569.02 3581.11 64.28 o 4 4 0 239.43 215.93 28.54 o 5 4 0 16079.48 15574.13 270.01 o 6 4 0 8221.45 7921.62 134.29 o 7 4 0 6955.86 6884.15 127.50 o 8 4 0 23.96 63.70 30.47 o 9 4 0 6207.65 6283.70 157.64 o 10 4 0 4709.68 4932.82 146.99 o 11 4 0 2178.25 2247.25 92.75 o 12 4 0 20474.43 20793.86 586.93 o 13 4 0 27440.55 27736.21 1154.62 o 14 4 0 1713.33 1557.94 221.96 o 15 4 0 4361.94 3161.96 423.50 o 1 5 0 64676.86 62661.11 1309.24 o 2 5 0 107031.89 106979.72 2635.65 o 3 5 0 14.95 83.18 23.14 o 4 5 0 65079.05 66759.33 1086.42 o 5 5 0 1918.73 2087.69 63.95 o 6 5 0 39344.72 37729.31 751.34 o 7 5 0 59053.45 58996.12 1077.03 o 8 5 0 13608.66 13524.50 293.59 o 9 5 0 805.88 835.40 63.99 o 10 5 0 50826.52 52046.07 1174.30 o 11 5 0 1035.16 1151.60 128.71 o 12 5 0 6433.72 6337.50 274.28 o 13 5 0 2811.92 2479.26 189.84 o 14 5 0 96.88 16.83 145.51 o 15 5 0 11871.77 11344.19 1049.27 o 0 6 0 38254.81 36809.80 1097.04 o 1 6 0 19824.26 20431.63 381.31 o 2 6 0 9412.75 10221.42 209.67 o 3 6 0 6437.43 6180.87 103.20 o 4 6 0 224541.03 218883.44 6016.76 o 5 6 0 1330.32 1482.17 115.88 o 6 6 0 44.73 169.52 36.99 o 7 6 0 2421.90 2262.18 89.65 o 8 6 0 3303.55 3139.09 158.26 o 9 6 0 210.95 166.98 60.54 o 10 6 0 59414.30 59201.37 1611.67 o 11 6 0 239.24 288.41 71.22 o 12 6 0 1718.28 2243.94 201.88 o 13 6 0 4350.10 4316.31 253.92 o 14 6 0 1778.19 1456.41 172.07 o 15 6 0 278.41 -164.52 217.57 o 1 7 0 61382.62 58933.14 1329.24 o 2 7 0 13520.05 12916.71 238.15 o 3 7 0 9382.82 8793.10 169.71 o 4 7 0 20043.56 19534.29 466.98 o 5 7 0 5858.18 6398.72 144.48 o 6 7 0 1565.49 1614.99 58.61 o 7 7 0 138401.91 138942.78 3666.14 o 8 7 0 5874.61 5732.78 140.27 o 9 7 0 447.55 465.43 75.03 o 10 7 0 13457.30 14237.96 422.11 o 11 7 0 1514.51 1438.22 125.70 o 12 7 0 2578.99 2940.50 182.98 o 13 7 0 352.74 17.72 117.76 o 14 7 0 89.93 145.82 142.50 o 0 8 0 513.15 454.04 144.38 o 1 8 0 163921.38 161077.75 5451.34 o 2 8 0 18504.01 18146.66 637.66 o 3 8 0 35534.24 34000.27 917.21 o 4 8 0 44033.03 43234.13 947.17 o 5 8 0 1387.99 1582.78 77.62 o 6 8 0 1138.36 1070.88 71.11 o 7 8 0 5867.72 6032.81 172.51 o 8 8 0 354.60 395.03 75.73 o 9 8 0 4.72 291.52 254.10 o 10 8 0 7389.19 7444.76 283.29 o 11 8 0 7217.31 7653.57 347.79 o 12 8 0 7799.66 8642.19 459.96 o 13 8 0 34045.91 34836.56 1601.66 o 14 8 0 46.30 158.96 169.00 o 1 9 0 9957.44 9466.67 373.28 o 2 9 0 38990.91 38629.95 1314.22 o 3 9 0 6140.83 6059.62 332.35 o 4 9 0 7530.24 7860.79 306.24 o 5 9 0 40144.34 39334.71 1192.43 o 6 9 0 734.78 614.98 67.03 o 7 9 0 3737.71 3927.97 165.18 o 8 9 0 185.33 212.28 108.97 o 9 9 0 25304.92 25504.84 742.41 o 10 9 0 33223.86 34377.94 1154.14 o 11 9 0 194.73 26.19 110.52 o 12 9 0 8268.66 8443.96 469.85 o 13 9 0 3711.19 3579.19 263.49 o 14 9 0 155.41 52.07 225.19 o 0 10 0 10134.83 9733.27 468.49 o 1 10 0 110.02 160.99 54.10 o 2 10 0 49421.96 48146.17 1867.86 o 3 10 0 19586.77 19000.58 539.81 o 4 10 0 21129.04 20513.62 484.87 o 5 10 0 22552.11 22449.31 768.15 o 6 10 0 9645.54 9361.32 414.23 o 7 10 0 1866.57 1929.63 125.47 o 8 10 0 5883.40 5930.93 229.08 o 9 10 0 13649.96 13721.14 471.46 o 10 10 0 2284.92 2207.62 174.68 o 11 10 0 3138.78 3480.59 249.75 o 12 10 0 5026.18 5075.25 488.20 o 13 10 0 1487.51 1363.30 201.56 o 1 11 0 1837.04 1962.16 77.39 o 2 11 0 234.54 219.06 105.69 o 3 11 0 9866.34 10282.51 309.63 o 4 11 0 20433.16 20304.34 904.57 o 5 11 0 11392.23 11106.42 446.93 o 6 11 0 56422.73 57455.95 2200.32 o 7 11 0 5773.81 6059.06 274.31 o 8 11 0 30280.47 30710.19 951.89 o 9 11 0 3861.53 3978.96 190.04 o 10 11 0 5088.69 5277.52 303.31 o 11 11 0 6963.15 6950.33 629.07 o 12 11 0 109.61 216.18 157.69 o 0 12 0 97898.37 100111.20 3715.86 o 1 12 0 6935.98 6570.35 287.04 o 2 12 0 5597.34 5653.07 198.92 o 3 12 0 13221.54 13588.15 362.99 o 4 12 0 285.13 206.01 80.18 o 5 12 0 1748.87 1766.62 151.15 o 6 12 0 5423.61 5878.16 293.13 o 7 12 0 3647.65 3775.93 211.31 o 8 12 0 12076.80 12729.79 456.83 o 9 12 0 630.82 668.75 199.59 o 10 12 0 1593.41 1837.23 208.36 o 11 12 0 62.04 -20.61 192.59 o 12 12 0 4829.82 4779.13 358.76 o 1 13 0 430.07 562.67 79.60 o 2 13 0 735.51 845.65 94.19 o 3 13 0 72907.09 73113.64 2161.07 o 4 13 0 555.10 778.63 102.68 o 5 13 0 1284.20 1878.95 224.41 o 6 13 0 5442.73 5876.10 309.83 o 7 13 0 13337.59 13840.25 596.75 o 8 13 0 3456.14 3125.29 267.49 o 9 13 0 6240.46 6652.27 367.65 o 10 13 0 956.29 974.88 174.33 o 11 13 0 30951.90 33165.19 1574.13 o 0 14 0 32296.46 32500.76 2746.07 o 1 14 0 7273.55 7370.08 270.82 o 2 14 0 55.42 202.81 68.10 o 3 14 0 25758.40 26757.00 964.31 o 4 14 0 4023.74 4494.28 323.53 o 5 14 0 17009.92 18213.22 804.15 o 6 14 0 2921.10 3068.54 199.64 o 7 14 0 675.66 597.23 178.15 o 8 14 0 14554.08 15650.83 751.23 o 9 14 0 12723.88 14047.01 772.85 o 10 14 0 354.23 362.43 153.52 o 1 15 0 7370.21 7840.04 587.46 o 2 15 0 3261.22 3450.80 215.07 o 3 15 0 66.45 184.13 92.33 o 4 15 0 1185.33 1626.95 375.68 o 5 15 0 15021.00 14834.27 856.76 o 6 15 0 27028.23 29806.85 1396.82 o 7 15 0 1221.52 1314.79 263.87 o 8 15 0 10775.47 10716.51 606.98 o 9 15 0 6954.23 7398.84 457.26 o 0 16 0 28373.90 30314.84 2753.85 o 1 16 0 3837.64 3953.73 247.69 o 2 16 0 29679.89 32165.56 1280.89 o 3 16 0 3747.52 3832.81 453.77 o 4 16 0 351.95 459.40 227.15 o 5 16 0 3371.36 3420.28 270.23 o 6 16 0 2688.07 3061.56 443.71 o 7 16 0 149.51 170.91 421.73 o 8 16 0 390.71 611.82 173.53 o 1 17 0 5516.17 5928.45 373.71 o 2 17 0 7836.39 8198.06 430.35 o 3 17 0 3169.58 3425.14 374.41 o 4 17 0 6564.87 7040.94 431.51 o 5 17 0 569.20 500.48 191.22 o 6 17 0 2763.41 2499.72 404.92 o 7 17 0 1918.34 1483.56 458.66 o 0 18 0 19.68 271.71 241.61 o 1 18 0 9436.06 9908.85 549.89 o 2 18 0 45.73 159.08 178.12 o 3 18 0 6142.22 6194.90 409.34 o 4 18 0 14477.66 14480.42 1357.52 o 5 18 0 2798.38 2282.30 526.68 o 1 0 1 8.16 82.83 10.63 o 3 0 1 4632.89 4416.53 74.24 o 5 0 1 198.23 175.51 29.63 o 7 0 1 580.92 596.14 42.80 o 9 0 1 2012.07 1948.24 105.37 o 11 0 1 3400.62 3318.20 117.33 o 13 0 1 11862.97 12385.90 476.13 o 15 0 1 6897.51 7254.63 810.42 o 0 1 1 214.99 292.65 8.02 o 1 1 1 2.28 34.23 6.38 o 2 1 1 1324.53 1348.03 20.00 o 3 1 1 631.97 680.32 15.09 o 4 1 1 438.96 449.32 19.71 o 5 1 1 4017.62 4015.98 54.86 o 6 1 1 4016.97 3960.09 76.83 o 7 1 1 7556.71 7407.50 99.24 o 8 1 1 1591.17 1541.48 46.13 o 9 1 1 7374.68 7460.08 119.51 o 10 1 1 4379.77 4527.15 97.52 o 11 1 1 3970.37 4144.08 93.93 o 12 1 1 582.26 676.53 52.46 o 13 1 1 990.86 1110.04 123.64 o 14 1 1 282.62 222.96 147.05 o 15 1 1 7.92 133.88 216.61 o 1 2 1 657.02 710.62 14.32 o 2 2 1 857.25 944.63 17.34 o 3 2 1 461.53 532.50 19.76 o 4 2 1 2332.73 2407.99 38.26 o 5 2 1 2151.60 2267.83 41.00 o 6 2 1 364.46 367.08 22.40 o 7 2 1 14.06 42.23 20.56 o 8 2 1 254.36 260.24 23.91 o 9 2 1 6.34 35.05 24.10 o 10 2 1 3544.37 3547.27 86.73 o 11 2 1 1227.60 1142.19 50.01 o 12 2 1 5988.56 6531.53 177.28 o 13 2 1 563.81 559.68 81.79 o 14 2 1 7003.88 7007.78 281.08 o 15 2 1 1632.85 1618.90 158.24 o 0 3 1 197.30 286.57 18.88 o 1 3 1 478.40 550.19 15.16 o 2 3 1 8.41 48.03 15.26 o 3 3 1 557.97 552.03 18.42 o 4 3 1 4174.75 4192.67 53.24 o 5 3 1 358.74 402.89 18.79 o 6 3 1 6026.52 6043.48 87.77 o 7 3 1 1023.95 1022.31 49.62 o 8 3 1 12169.91 11901.18 166.91 o 9 3 1 82.80 64.63 26.56 o 10 3 1 6102.06 6151.85 130.65 o 11 3 1 104.87 116.57 37.64 o 12 3 1 3532.02 3522.01 118.32 o 13 3 1 40.34 13.32 83.44 o 14 3 1 114.46 76.15 78.78 o 15 3 1 2.47 3.75 142.10 o 1 4 1 1457.94 1443.48 26.42 o 2 4 1 1621.00 1607.95 33.87 o 3 4 1 8.80 -7.08 10.37 o 4 4 1 1436.97 1472.47 27.62 o 5 4 1 1282.53 1250.80 30.56 o 6 4 1 1416.77 1461.90 47.82 o 7 4 1 637.41 645.33 31.74 o 8 4 1 0.09 38.94 32.79 o 9 4 1 552.52 531.92 32.59 o 10 4 1 375.58 412.11 35.12 o 11 4 1 4219.61 4074.15 105.69 o 12 4 1 3976.43 3616.12 125.63 o 13 4 1 3288.44 3262.80 189.83 o 14 4 1 4089.14 3952.32 247.98 o 15 4 1 4167.91 4526.03 302.31 o 0 5 1 6445.05 6188.31 141.15 o 1 5 1 237.99 245.30 19.79 o 2 5 1 51.70 54.56 13.77 o 3 5 1 1730.50 1843.02 37.97 o 4 5 1 1938.95 1850.72 36.68 o 5 5 1 4506.98 4535.59 70.33 o 6 5 1 1228.10 1200.76 34.11 o 7 5 1 6901.42 6715.25 103.78 o 8 5 1 26.99 -8.94 33.38 o 9 5 1 7739.65 7919.40 134.99 o 10 5 1 1688.30 1682.88 69.81 o 11 5 1 4977.41 4966.51 131.90 o 12 5 1 128.09 92.59 54.96 o 13 5 1 1215.26 1262.97 102.72 o 14 5 1 310.16 306.57 123.53 o 15 5 1 92.83 -8.35 118.38 o 1 6 1 251.35 246.92 19.27 o 2 6 1 63.38 38.81 14.73 o 3 6 1 5575.36 5477.29 80.86 o 4 6 1 33.81 75.46 28.48 o 5 6 1 320.76 369.48 26.99 o 6 6 1 864.88 839.44 39.93 o 7 6 1 1491.57 1557.99 63.93 o 8 6 1 193.23 224.03 32.71 o 9 6 1 1756.53 1871.88 78.87 o 10 6 1 1453.91 1412.90 66.66 o 11 6 1 1971.88 1929.72 87.49 o 12 6 1 916.91 882.94 84.42 o 13 6 1 7176.33 7313.05 259.65 o 14 6 1 1848.87 1841.49 201.52 o 15 6 1 4698.54 4878.08 345.35 o 0 7 1 162.24 166.71 27.84 o 1 7 1 1318.74 1296.86 40.97 o 2 7 1 2217.56 2228.65 51.56 o 3 7 1 504.17 533.83 32.32 o 4 7 1 1295.42 1282.46 51.92 o 5 7 1 1017.30 971.29 37.01 o 6 7 1 6642.50 6793.52 110.05 o 7 7 1 1418.49 1362.85 47.93 o 8 7 1 3640.75 3717.79 95.80 o 9 7 1 4924.84 4782.63 133.72 o 10 7 1 4525.09 4817.96 139.68 o 11 7 1 1059.45 1060.16 80.79 o 12 7 1 409.37 406.70 86.14 o 13 7 1 1418.99 1224.18 124.31 o 14 7 1 197.55 254.06 121.12 o 1 8 1 45.47 95.14 33.65 o 2 8 1 866.14 912.52 67.34 o 3 8 1 1021.75 1005.67 32.84 o 4 8 1 900.45 906.17 32.86 o 5 8 1 976.76 1033.61 56.07 o 6 8 1 695.63 695.24 42.61 o 7 8 1 1080.64 1120.42 44.23 o 8 8 1 482.37 501.62 52.80 o 9 8 1 1036.08 1042.34 71.94 o 10 8 1 1702.03 1816.39 102.11 o 11 8 1 66.06 -7.84 65.29 o 12 8 1 5823.17 5868.77 245.79 o 13 8 1 64.74 171.85 95.34 o 14 8 1 5056.46 4892.28 262.77 o 0 9 1 1483.02 1641.58 98.47 o 1 9 1 1640.97 1673.15 51.87 o 2 9 1 5.13 6.08 30.19 o 3 9 1 2331.97 2459.87 65.51 o 4 9 1 103.82 124.19 28.33 o 5 9 1 1792.67 1828.76 65.03 o 6 9 1 2513.53 2356.54 85.21 o 7 9 1 2395.83 2467.95 139.22 o 8 9 1 4144.11 4405.78 134.84 o 9 9 1 764.14 795.97 74.17 o 10 9 1 4264.18 4101.05 146.60 o 11 9 1 525.18 516.15 87.06 o 12 9 1 3089.96 3491.84 189.18 o 13 9 1 0.32 -37.70 93.69 o 1 10 1 123.51 130.80 27.85 o 2 10 1 1178.29 1226.09 75.13 o 3 10 1 80.34 123.90 42.05 o 4 10 1 1279.98 1307.13 52.22 o 5 10 1 86.06 147.92 69.54 o 6 10 1 3473.43 3652.06 126.44 o 7 10 1 209.17 232.16 58.06 o 8 10 1 153.65 157.36 63.78 o 9 10 1 715.94 692.46 76.44 o 10 10 1 290.77 381.88 89.74 o 11 10 1 3621.50 3784.68 171.33 o 12 10 1 904.07 851.75 116.27 o 13 10 1 4171.16 4001.44 223.28 o 0 11 1 6324.41 6226.48 267.91 o 1 11 1 1.59 53.63 33.44 o 2 11 1 696.56 672.46 39.30 o 3 11 1 42.60 24.96 29.00 o 4 11 1 3494.39 3725.29 112.37 o 5 11 1 2623.08 2766.40 117.78 o 6 11 1 1.80 18.41 56.32 o 7 11 1 2653.44 2785.86 103.66 o 8 11 1 366.42 330.95 98.43 o 9 11 1 6586.15 6522.17 214.33 o 10 11 1 165.05 286.88 81.98 o 11 11 1 1619.36 1580.05 144.30 o 12 11 1 0.88 10.48 112.94 o 1 12 1 402.57 387.26 32.43 o 2 12 1 7.48 94.67 34.41 o 3 12 1 5527.64 5912.18 139.51 o 4 12 1 74.64 102.06 58.02 o 5 12 1 313.89 448.54 74.50 o 6 12 1 256.03 252.62 76.79 o 7 12 1 2705.16 2837.06 179.99 o 8 12 1 1162.69 1564.31 131.50 o 9 12 1 246.51 70.58 81.87 o 10 12 1 1917.44 2022.64 151.68 o 11 12 1 170.87 171.77 125.39 o 12 12 1 2340.42 2307.69 182.54 o 0 13 1 218.92 385.57 51.05 o 1 13 1 2484.15 2462.54 75.10 o 2 13 1 2124.38 2209.66 85.56 o 3 13 1 1759.40 1700.87 85.47 o 4 13 1 149.80 39.56 66.85 o 5 13 1 12.08 27.98 70.03 o 6 13 1 5106.21 5588.93 220.46 o 7 13 1 14.25 108.28 75.14 o 8 13 1 1667.28 1661.93 119.71 o 9 13 1 1279.83 1608.10 131.27 o 10 13 1 3382.55 3754.19 231.11 o 11 13 1 412.09 82.76 170.37 o 1 14 1 137.01 244.11 54.11 o 2 14 1 768.98 573.23 66.95 o 3 14 1 222.18 134.41 68.31 o 4 14 1 416.10 379.48 83.17 o 5 14 1 1321.81 1107.01 94.02 o 6 14 1 1428.58 1557.11 135.06 o 7 14 1 964.81 1148.30 118.41 o 8 14 1 72.84 168.74 100.35 o 9 14 1 1754.89 1873.57 142.08 o 10 14 1 16.05 49.92 125.88 o 0 15 1 2975.98 3147.52 194.68 o 1 15 1 1207.22 1156.14 87.43 o 2 15 1 520.78 572.71 98.26 o 3 15 1 1088.48 1166.06 87.51 o 4 15 1 507.77 512.82 74.19 o 5 15 1 1998.71 1774.03 130.54 o 6 15 1 430.53 528.08 98.27 o 7 15 1 923.65 769.64 248.55 o 8 15 1 999.43 872.66 132.72 o 9 15 1 1703.54 1656.27 156.50 o 1 16 1 63.00 11.16 82.94 o 2 16 1 599.14 587.31 90.12 o 3 16 1 690.47 563.90 121.17 o 4 16 1 1264.01 1197.03 98.22 o 5 16 1 29.25 231.21 107.80 o 6 16 1 2110.22 2040.55 167.22 o 7 16 1 39.91 -114.65 134.06 o 8 16 1 795.85 683.17 164.50 o 0 17 1 2045.80 1954.16 280.35 o 1 17 1 477.19 483.49 105.65 o 2 17 1 1651.15 1695.95 130.37 o 3 17 1 257.52 307.51 105.94 o 4 17 1 1377.44 1221.76 202.57 o 5 17 1 583.98 726.17 146.68 o 6 17 1 708.82 535.69 128.25 o 7 17 1 457.94 327.26 512.33 o 1 18 1 26.98 255.23 112.36 o 2 18 1 34.12 -58.25 104.07 o 3 18 1 2290.39 2663.62 232.96 o 4 18 1 49.18 154.17 130.87 o 0 0 2 173.59 440.02 22.05 o 2 0 2 84677.91 82562.95 1108.51 o 4 0 2 100544.98 96554.27 1813.84 o 6 0 2 27234.12 26374.44 438.49 o 8 0 2 20911.72 20711.80 376.69 o 10 0 2 11436.48 11643.78 263.64 o 12 0 2 2691.92 2821.48 119.11 o 14 0 2 1395.28 1253.67 140.69 o 1 1 2 1539.71 1799.15 20.40 o 2 1 2 67176.96 66872.98 642.53 o 3 1 2 1131.61 658.88 14.28 o 4 1 2 64522.09 65232.63 668.89 o 5 1 2 84962.93 82876.71 975.28 o 6 1 2 31550.52 30641.94 354.32 o 7 1 2 37582.71 36002.96 447.89 o 8 1 2 15818.54 15141.68 244.83 o 9 1 2 19889.18 19534.87 276.53 o 10 1 2 43792.25 44381.30 707.47 o 11 1 2 10382.63 10310.25 194.56 o 12 1 2 3857.88 3768.71 111.58 o 13 1 2 3047.97 2914.00 114.92 o 14 1 2 186.48 279.11 122.22 o 15 1 2 377.12 395.48 152.26 o 0 2 2 152437.11 155112.97 1721.18 o 1 2 2 204410.69 206483.77 1627.18 o 2 2 2 142.92 174.96 13.11 o 3 2 2 47403.91 49422.27 570.21 o 4 2 2 10742.10 10626.41 116.62 o 5 2 2 5001.09 4826.53 58.74 o 6 2 2 11625.54 11068.75 152.53 o 7 2 2 14926.70 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5053.21 4867.38 258.85 o 4 9 10 224.15 171.32 122.11 o 5 9 10 9114.99 7714.35 473.09 o 0 10 10 33337.91 35469.61 3290.27 o 1 10 10 11020.77 9755.67 536.38 o 2 10 10 9451.88 9599.35 525.49 o 3 10 10 70.71 -86.89 154.71 o 4 10 10 1195.96 1143.58 232.44 o 1 11 10 2431.62 2087.47 205.72 o 1 0 11 1636.58 800.91 202.16 o 3 0 11 1.27 72.80 161.33 o 5 0 11 2086.56 1879.92 569.10 o 7 0 11 125.04 209.18 171.37 o 0 1 11 1081.14 1120.14 280.26 o 1 1 11 0.13 132.72 131.22 o 2 1 11 140.16 277.13 186.86 o 3 1 11 138.94 93.04 113.06 o 4 1 11 1821.03 1686.40 150.32 o 5 1 11 594.12 591.42 139.43 o 6 1 11 23.61 13.32 139.36 o 7 1 11 1752.79 1202.37 228.02 o 1 2 11 737.75 673.03 143.09 o 2 2 11 217.60 216.18 106.22 o 3 2 11 1091.60 781.92 131.13 o 4 2 11 336.74 259.52 114.39 o 5 2 11 337.89 472.93 114.90 o 6 2 11 233.09 349.77 130.80 o 7 2 11 610.36 503.99 233.95 o 0 3 11 1358.07 1409.84 277.44 o 1 3 11 160.46 19.01 120.23 o 2 3 11 707.87 676.22 116.55 o 3 3 11 210.72 479.71 136.12 o 4 3 11 33.65 -3.35 122.25 o 5 3 11 20.36 237.51 138.22 o 6 3 11 4473.78 4011.11 262.99 o 1 4 11 293.94 381.84 177.95 o 2 4 11 169.04 198.91 107.05 o 3 4 11 639.62 876.59 163.09 o 4 4 11 251.69 312.47 133.64 o 5 4 11 430.71 449.73 152.64 o 6 4 11 142.00 -134.55 161.35 o 0 5 11 133.91 353.66 161.96 o 1 5 11 0.21 91.66 115.59 o 2 5 11 816.77 700.05 150.23 o 3 5 11 219.28 486.35 142.19 o 4 5 11 173.55 162.96 138.00 o 5 5 11 1025.37 932.45 161.16 o 1 6 11 592.61 464.17 143.92 o 2 6 11 31.62 162.01 115.14 o 3 6 11 42.87 -22.54 130.89 o 4 6 11 134.82 30.55 162.15 o 5 6 11 1892.57 1792.45 318.29 o 0 7 11 1494.30 1268.78 292.27 o 1 7 11 95.19 193.31 123.11 o 2 7 11 31.64 109.82 167.90 o 3 7 11 65.37 8.38 121.19 o 4 7 11 2000.17 1325.47 205.03 o 1 8 11 597.30 550.45 186.23 o 2 8 11 289.85 347.21 153.73 o 2 0 12 17977.17 14926.07 2123.37 o 1 1 12 6143.55 5343.45 691.31 o 2 1 12 19.96 43.27 239.16 o 3 1 12 9448.71 7671.18 637.22 o 0 2 12 625.94 373.64 367.98 o 1 2 12 3320.13 3109.42 555.05 o 2 2 12 387.48 113.65 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