#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2013403.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2013403_Fobs loop_ _publ_author_name 'Baker, Robert J.' 'Bettentrup, Helga' 'Jones, Cameron' _publ_section_title ; The synthesis of phosphorus heterocycles from tetra-tert-butyltetraphosphacubane ; _journal_issue 9 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first m339 _journal_page_last m341 _journal_volume 59 _journal_year 2003 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 82.906 _cell_angle_beta 81.279 _cell_angle_gamma 83.655 _cell_length_a 9.6290 _cell_length_b 12.4590 _cell_length_c 13.8670 _exptl_crystal_F_000 920.00 _reflns_d_resolution_high 0.7702 _[local]_cod_data_source_file bm1533Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' s92 in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 305.52 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l 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