#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2013404.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2013404_Fobs loop_ _publ_author_name 'Baker, Robert J.' 'Bettentrup, Helga' 'Jones, Cameron' _publ_section_title ; The synthesis of phosphorus heterocycles from tetra-tert-butyltetraphosphacubane ; _journal_issue 9 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first m339 _journal_page_last m341 _journal_volume 59 _journal_year 2003 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 101.470 _cell_angle_gamma 90.000 _cell_length_a 12.0820 _cell_length_b 17.5220 _cell_length_c 14.6150 _exptl_crystal_F_000 1664.00 _reflns_d_resolution_high 0.7702 _[local]_cod_data_source_file bm1533IIsup3.hkl _[local]_cod_data_source_block II #BEGIN Tags that were not found in dictionaries: _shelx_title ' s92 in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 429.77 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 18604.22 16487.24 863.44 o 3 0 0 29656.03 27649.18 1444.99 o 4 0 0 112232.78 113190.56 5768.66 o 5 0 0 57606.38 56004.03 3273.95 o 6 0 0 21.16 152.85 45.78 o 7 0 0 40228.98 42793.32 2948.36 o 8 0 0 21030.72 21242.45 1271.64 o 9 0 0 12564.00 12760.97 635.72 o 10 0 0 41010.84 44584.73 2515.01 o 11 0 0 3999.95 4194.69 194.82 o 12 0 0 2212.67 2225.15 108.67 o 13 0 0 254.14 258.45 46.66 o 14 0 0 889.98 857.80 111.88 o 15 0 0 8736.88 8947.29 840.14 o 2 1 0 29758.39 26565.73 1141.08 o 3 1 0 47515.39 45148.70 1691.09 o 4 1 0 40515.12 38659.01 1248.66 o 5 1 0 321.32 353.67 18.52 o 6 1 0 50100.73 49826.72 1659.84 o 7 1 0 245.80 405.66 22.54 o 8 1 0 1573.08 1611.54 83.41 o 9 1 0 48515.93 50638.77 2498.81 o 10 1 0 13268.85 13416.63 591.23 o 11 1 0 1978.88 2039.84 90.55 o 12 1 0 452.74 585.43 44.66 o 13 1 0 2400.11 2133.07 112.13 o 14 1 0 3405.30 3466.46 150.57 o 15 1 0 40.96 74.25 68.37 o 2 2 0 2609.46 2931.86 93.23 o 3 2 0 702.33 657.17 29.43 o 4 2 0 1005.99 1151.06 31.74 o 5 2 0 13337.20 12792.07 461.99 o 6 2 0 32498.60 32097.69 1197.99 o 7 2 0 10046.75 9801.90 346.82 o 8 2 0 13309.45 12967.08 524.67 o 9 2 0 11521.98 12057.53 507.63 o 10 2 0 13422.32 13590.74 577.53 o 11 2 0 388.69 436.92 35.67 o 12 2 0 1102.87 924.05 146.22 o 13 2 0 257.90 332.89 60.79 o 14 2 0 933.46 831.60 80.74 o 15 2 0 2828.78 2752.96 228.06 o 1 3 0 39760.02 38180.30 1798.24 o 2 3 0 15058.14 15759.10 520.89 o 3 3 0 35306.04 34619.52 1220.17 o 4 3 0 12554.88 13020.99 421.67 o 5 3 0 10134.89 9793.05 329.44 o 6 3 0 7074.79 6942.44 226.49 o 7 3 0 2418.03 2362.45 88.22 o 8 3 0 10644.08 10405.34 396.31 o 9 3 0 17189.46 16241.72 652.00 o 10 3 0 4249.18 4261.88 205.83 o 11 3 0 1.99 35.49 29.94 o 12 3 0 59.31 60.94 30.82 o 13 3 0 1178.58 1158.25 126.56 o 14 3 0 10.66 39.90 69.63 o 15 3 0 58.16 139.76 83.76 o 0 4 0 8127.21 8472.26 709.37 o 1 4 0 7053.96 7470.37 341.32 o 2 4 0 7181.83 6959.51 258.29 o 3 4 0 15812.88 15878.73 465.09 o 4 4 0 157.02 222.69 25.23 o 5 4 0 22645.04 22044.96 680.45 o 6 4 0 5164.28 4786.32 187.23 o 7 4 0 2088.69 1893.84 73.99 o 8 4 0 165.43 304.76 37.42 o 9 4 0 327.60 408.77 37.99 o 10 4 0 3565.39 3476.92 148.45 o 11 4 0 7.37 42.27 31.66 o 12 4 0 543.63 656.55 67.69 o 13 4 0 1412.34 1599.42 98.36 o 14 4 0 1696.81 2014.35 133.52 o 15 4 0 54.05 154.85 77.56 o 1 5 0 87097.43 89409.96 4796.55 o 2 5 0 1.37 151.69 23.93 o 3 5 0 6240.43 7078.80 239.25 o 4 5 0 60559.14 61228.36 1878.61 o 5 5 0 6288.93 6171.27 236.18 o 6 5 0 28943.93 28056.99 1005.26 o 7 5 0 12818.35 12099.78 547.83 o 8 5 0 1115.82 1164.97 61.32 o 9 5 0 25863.41 25109.35 1224.29 o 10 5 0 1708.45 1686.06 92.41 o 11 5 0 6868.25 7255.28 298.76 o 12 5 0 8508.10 8322.92 250.96 o 13 5 0 4342.28 4778.01 260.75 o 14 5 0 4956.03 5163.06 272.59 o 0 6 0 73990.88 76647.01 9628.22 o 1 6 0 11324.61 11565.36 547.50 o 2 6 0 24033.88 24504.63 1051.79 o 3 6 0 13737.28 13029.65 540.80 o 4 6 0 204.99 244.24 17.21 o 5 6 0 118870.42 118359.30 4617.45 o 6 6 0 4837.94 4410.72 169.28 o 7 6 0 681.19 644.91 36.61 o 8 6 0 8901.57 8389.99 402.99 o 9 6 0 8218.72 7551.14 397.14 o 10 6 0 18350.61 19074.68 508.95 o 11 6 0 1026.52 1178.27 81.58 o 12 6 0 13.40 85.11 49.98 o 13 6 0 4567.28 4699.88 168.33 o 14 6 0 3834.13 4038.81 294.10 o 1 7 0 44334.05 41695.20 2336.31 o 2 7 0 522.37 429.75 19.86 o 3 7 0 5347.81 5212.48 232.76 o 4 7 0 50016.29 49430.39 1885.48 o 5 7 0 1198.03 1225.65 61.42 o 6 7 0 13541.98 13337.86 512.10 o 7 7 0 164.74 235.88 18.74 o 8 7 0 10342.99 10107.97 484.43 o 9 7 0 15651.38 15510.42 689.35 o 10 7 0 120.80 79.53 29.40 o 11 7 0 6510.00 6105.63 213.79 o 12 7 0 1282.02 1127.93 155.89 o 13 7 0 3315.76 3571.84 164.16 o 14 7 0 1473.74 1479.94 227.88 o 0 8 0 134725.27 141042.53 16178.38 o 1 8 0 202.06 280.63 28.45 o 2 8 0 3261.63 3199.89 114.51 o 3 8 0 9587.24 9060.57 378.13 o 4 8 0 19902.37 20386.52 682.06 o 5 8 0 17183.29 16888.06 645.75 o 6 8 0 5105.01 4752.03 185.58 o 7 8 0 3468.03 3231.86 135.75 o 8 8 0 2206.56 1916.73 106.99 o 9 8 0 4819.75 4521.83 183.38 o 10 8 0 13370.20 12945.06 654.76 o 11 8 0 2.69 -46.27 46.27 o 12 8 0 339.43 440.01 70.75 o 13 8 0 2.90 -26.81 81.86 o 14 8 0 1148.51 977.29 120.24 o 1 9 0 20568.21 19980.24 1340.77 o 2 9 0 3209.47 3244.11 114.28 o 3 9 0 15796.80 17146.60 614.91 o 4 9 0 4063.05 4218.35 158.88 o 5 9 0 1094.65 1247.79 60.30 o 6 9 0 13052.17 12664.97 491.43 o 7 9 0 4383.02 4276.98 166.19 o 8 9 0 557.03 533.77 57.61 o 9 9 0 2049.64 1959.76 116.92 o 10 9 0 2226.55 1918.28 115.99 o 11 9 0 746.06 505.92 49.52 o 12 9 0 508.22 565.26 77.92 o 13 9 0 9.66 33.96 81.84 o 14 9 0 572.34 632.44 85.52 o 0 10 0 408.15 462.25 62.12 o 1 10 0 809.09 790.64 54.61 o 2 10 0 11383.62 11367.38 514.85 o 3 10 0 7185.07 7193.50 335.67 o 4 10 0 406.04 375.04 24.33 o 5 10 0 4594.19 4621.01 176.98 o 6 10 0 20913.27 20647.25 904.43 o 7 10 0 7.12 16.60 21.68 o 8 10 0 673.09 627.31 38.02 o 9 10 0 112.00 76.11 34.94 o 10 10 0 474.60 413.15 51.25 o 11 10 0 1737.98 1534.78 91.71 o 12 10 0 139.97 150.77 60.31 o 13 10 0 2707.46 2983.67 176.70 o 1 11 0 6297.90 6398.88 310.51 o 2 11 0 392.21 494.80 27.68 o 3 11 0 17522.25 17970.18 852.46 o 4 11 0 46963.87 47792.83 1847.04 o 5 11 0 17406.61 17727.63 704.00 o 6 11 0 3876.56 3838.73 174.77 o 7 11 0 12262.39 11196.10 447.93 o 8 11 0 4069.43 4142.26 220.37 o 9 11 0 447.14 445.20 50.54 o 10 11 0 26.14 47.59 45.94 o 11 11 0 396.64 417.22 66.74 o 12 11 0 2003.88 1876.11 120.43 o 13 11 0 251.35 148.46 69.23 o 0 12 0 1187.42 1126.09 58.93 o 1 12 0 5543.16 5595.63 294.15 o 2 12 0 9695.99 10100.10 452.31 o 3 12 0 6785.39 6819.46 274.77 o 4 12 0 495.57 543.65 38.59 o 5 12 0 17937.46 18134.36 596.43 o 6 12 0 3127.52 3092.22 178.66 o 7 12 0 2625.00 2569.45 90.85 o 8 12 0 415.51 400.12 44.61 o 9 12 0 428.15 523.28 78.95 o 10 12 0 3922.36 3711.67 295.77 o 11 12 0 413.80 465.54 74.67 o 12 12 0 149.37 133.94 59.64 o 13 12 0 1771.30 1821.03 157.15 o 1 13 0 4599.28 4616.34 191.75 o 2 13 0 6345.51 6142.84 354.33 o 3 13 0 2341.62 2570.77 106.83 o 4 13 0 26298.76 27886.19 1262.94 o 5 13 0 2553.08 2586.94 135.80 o 6 13 0 5128.56 5187.85 210.84 o 7 13 0 896.91 856.68 69.04 o 8 13 0 3725.88 3738.55 222.88 o 9 13 0 3326.42 3041.07 216.85 o 10 13 0 194.71 187.42 72.10 o 11 13 0 5573.03 5284.06 399.36 o 12 13 0 559.15 545.83 85.42 o 0 14 0 500.92 543.08 85.79 o 1 14 0 12088.35 12755.59 676.02 o 2 14 0 10679.80 10545.37 491.82 o 3 14 0 3681.96 3760.58 195.29 o 4 14 0 16.26 17.72 22.17 o 5 14 0 44344.48 46787.07 1680.68 o 6 14 0 4907.21 5060.64 333.99 o 7 14 0 3003.93 2863.19 176.91 o 8 14 0 208.40 211.42 40.09 o 9 14 0 463.01 499.85 86.85 o 10 14 0 1207.85 1218.32 101.54 o 11 14 0 565.02 510.36 81.73 o 12 14 0 951.45 895.10 92.34 o 1 15 0 353.21 466.20 30.42 o 2 15 0 10107.05 10407.13 399.85 o 3 15 0 273.98 201.99 25.31 o 4 15 0 13233.20 13424.66 492.61 o 5 15 0 2604.33 2449.71 117.07 o 6 15 0 184.49 215.87 42.96 o 7 15 0 2404.17 2492.73 236.26 o 8 15 0 4752.30 4077.01 275.32 o 9 15 0 370.27 275.04 52.97 o 10 15 0 2122.87 1882.26 208.15 o 11 15 0 2513.84 2460.64 137.55 o 0 16 0 2124.34 2263.69 167.77 o 1 16 0 6141.65 6473.22 226.48 o 2 16 0 231.39 201.15 34.31 o 3 16 0 266.32 238.23 28.25 o 4 16 0 196.72 224.82 43.43 o 5 16 0 1396.18 1609.33 83.61 o 6 16 0 714.64 870.18 71.63 o 7 16 0 5111.51 4557.77 265.22 o 8 16 0 4073.85 3681.42 238.91 o 9 16 0 0.57 16.18 132.60 o 10 16 0 1352.41 1476.84 110.38 o 1 17 0 352.13 336.82 37.21 o 2 17 0 16021.01 16912.31 996.98 o 3 17 0 2212.54 2175.92 71.46 o 4 17 0 1387.30 1305.25 70.52 o 5 17 0 459.66 427.76 40.01 o 6 17 0 782.61 798.02 59.21 o 7 17 0 310.59 397.35 57.22 o 8 17 0 220.05 53.68 71.07 o 9 17 0 1195.46 1218.89 154.01 o 10 17 0 1319.42 1336.86 132.93 o 0 18 0 3834.61 4158.53 300.21 o 1 18 0 5029.60 5082.20 533.15 o 2 18 0 8.81 70.61 39.98 o 3 18 0 2061.70 2249.66 138.70 o 4 18 0 69.78 60.19 30.23 o 5 18 0 614.82 553.72 97.96 o 6 18 0 11.74 23.17 53.60 o 7 18 0 73.13 137.10 82.12 o 8 18 0 2303.88 2014.80 152.50 o 9 18 0 802.86 1196.51 110.08 o 1 19 0 3211.70 3549.03 489.05 o 2 19 0 34.01 77.84 48.51 o 3 19 0 42.59 69.56 39.30 o 4 19 0 1309.25 1440.54 150.49 o 5 19 0 91.07 190.06 55.63 o 6 19 0 4419.73 4974.10 600.52 o 7 19 0 955.26 1104.79 139.09 o 8 19 0 42.11 130.21 83.57 o 0 20 0 2401.68 2814.19 223.16 o 1 20 0 20.66 99.96 81.58 o 2 20 0 202.50 244.13 56.19 o 3 20 0 468.34 464.87 109.16 o 4 20 0 4.23 30.91 60.65 o 5 20 0 859.91 1166.69 104.14 o 6 20 0 903.57 946.39 169.91 o 7 20 0 424.54 489.60 100.98 o 1 21 0 209.49 210.21 90.42 o 2 21 0 209.24 48.68 129.25 o 3 21 0 701.96 795.53 96.80 o 4 21 0 149.49 226.36 88.57 o 5 21 0 909.12 1126.12 215.94 o 0 22 0 338.38 530.84 133.51 o 1 22 0 1515.21 1911.61 208.31 o 2 22 0 607.09 808.20 114.92 o 3 22 0 4.50 33.19 158.27 o -15 1 1 18.02 79.28 82.59 o -14 1 1 556.19 621.41 89.98 o -13 1 1 203.22 152.72 66.14 o -12 1 1 541.62 607.82 36.15 o -11 1 1 1495.34 1322.25 49.53 o -10 1 1 5.61 81.41 27.51 o -9 1 1 2813.43 2875.37 112.39 o -8 1 1 1257.79 1153.27 57.87 o -7 1 1 7848.29 7989.25 375.99 o -6 1 1 46.14 110.81 15.05 o -5 1 1 34130.39 34628.46 1367.92 o -4 1 1 17725.80 16772.56 624.11 o -3 1 1 19779.93 19693.33 696.93 o -2 1 1 224.71 167.98 15.92 o 2 1 1 53690.41 53978.52 1161.15 o 3 1 1 1300.55 1403.36 41.04 o 4 1 1 1772.66 2093.01 63.33 o 5 1 1 1338.65 1350.07 55.93 o 6 1 1 31.13 141.16 28.21 o 7 1 1 664.28 703.04 38.45 o 8 1 1 472.35 509.34 45.41 o 9 1 1 1425.47 1389.12 66.24 o 10 1 1 5488.43 5688.25 303.10 o 11 1 1 1278.17 1645.58 67.69 o 12 1 1 156.67 197.10 37.06 o 13 1 1 135.61 152.77 55.86 o 14 1 1 201.54 303.93 92.63 o 15 1 1 2300.74 2371.63 237.50 o -15 2 1 101.98 134.40 69.51 o -14 2 1 606.68 490.92 74.41 o -13 2 1 6769.39 6922.86 202.31 o -12 2 1 903.75 791.33 76.61 o -11 2 1 147.76 166.63 29.47 o -10 2 1 6065.85 5796.10 308.67 o -9 2 1 5543.36 6046.32 187.56 o -8 2 1 53633.73 54009.91 2074.08 o -7 2 1 17414.53 16811.04 624.69 o -6 2 1 10573.91 11061.68 485.01 o -5 2 1 23333.20 22624.53 932.20 o -4 2 1 93869.52 92478.20 3570.61 o -3 2 1 23251.01 21806.81 694.59 o -2 2 1 7018.78 7263.75 261.31 o -1 2 1 16631.21 11124.18 1869.33 o 1 2 1 53868.70 48896.15 4747.89 o 2 2 1 29610.10 30370.84 952.16 o 3 2 1 11508.81 10978.25 311.59 o 4 2 1 91568.19 87349.91 2653.33 o 5 2 1 1429.30 1468.43 58.19 o 6 2 1 26623.49 25461.10 828.85 o 7 2 1 7522.04 7432.21 259.42 o 8 2 1 16.09 86.45 18.45 o 9 2 1 8676.24 8658.64 368.68 o 10 2 1 3291.36 3005.56 139.62 o 11 2 1 32518.63 35623.45 680.72 o 12 2 1 164.58 218.34 37.96 o 13 2 1 346.54 328.72 45.10 o 14 2 1 10013.60 9804.67 458.67 o 15 2 1 1358.71 1458.06 157.05 o -15 3 1 3263.06 3210.61 145.79 o -14 3 1 8518.55 9532.92 347.75 o -13 3 1 1703.90 1828.66 200.65 o -12 3 1 2394.00 2258.59 96.06 o -11 3 1 765.75 774.02 41.22 o -10 3 1 7172.96 7270.55 328.41 o -9 3 1 25256.56 24426.34 1062.95 o -8 3 1 8001.10 8020.60 331.07 o -7 3 1 24442.96 23493.17 945.99 o -6 3 1 10582.78 9779.28 402.35 o -5 3 1 72755.00 72378.01 2862.09 o -4 3 1 24144.57 23051.12 783.90 o -3 3 1 35704.67 36538.24 1412.70 o -2 3 1 2873.04 3073.74 107.94 o -1 3 1 7953.13 7603.88 304.31 o 0 3 1 60590.47 51860.71 4712.33 o 1 3 1 121287.06 128490.16 9037.65 o 2 3 1 155630.69 153804.95 6713.32 o 3 3 1 24338.19 23500.63 775.37 o 4 3 1 4132.08 4037.27 138.90 o 5 3 1 152983.22 153400.22 5118.01 o 6 3 1 3300.07 3182.76 103.17 o 7 3 1 10517.92 10414.27 438.93 o 8 3 1 123.11 144.48 26.49 o 9 3 1 65.24 267.56 47.99 o 10 3 1 47205.06 47779.94 2185.16 o 11 3 1 451.89 577.23 41.38 o 12 3 1 9416.50 10228.99 334.59 o 13 3 1 6041.49 5805.29 248.54 o 14 3 1 3570.34 3955.39 313.20 o 15 3 1 5324.55 5603.61 339.52 o -15 4 1 2550.48 2454.01 127.47 o -14 4 1 5125.83 5611.33 369.88 o -13 4 1 726.46 1130.32 114.58 o -12 4 1 167.77 230.74 51.04 o -11 4 1 14108.65 14283.50 349.34 o -10 4 1 724.34 712.75 66.36 o -9 4 1 108.46 122.24 27.31 o -8 4 1 18942.57 18316.33 858.88 o -7 4 1 697.41 749.20 27.28 o -6 4 1 18235.96 17885.33 774.06 o -5 4 1 12257.42 11463.71 463.11 o -4 4 1 83323.80 83683.63 2861.27 o -3 4 1 14655.25 13825.76 505.38 o -2 4 1 66641.28 68768.17 2475.46 o -1 4 1 12550.27 12368.68 619.84 o 0 4 1 36441.05 35041.41 2555.35 o 1 4 1 93280.17 88859.99 5057.67 o 2 4 1 65805.33 66638.36 2351.27 o 3 4 1 26710.98 25868.38 865.13 o 4 4 1 66003.27 64799.02 1699.12 o 5 4 1 2092.16 2108.25 73.01 o 6 4 1 62655.18 62111.63 1972.33 o 7 4 1 441.28 657.54 32.06 o 8 4 1 187.31 279.50 22.99 o 9 4 1 26794.35 26944.90 1031.96 o 10 4 1 219.38 308.27 53.72 o 11 4 1 17660.48 17294.92 789.85 o 12 4 1 108.10 220.01 37.29 o 13 4 1 2872.37 2704.37 235.55 o 14 4 1 2528.63 2897.78 184.08 o -15 5 1 1423.61 1261.49 98.40 o -14 5 1 1296.80 1384.33 111.19 o -13 5 1 576.57 732.76 64.75 o -12 5 1 533.98 473.94 54.41 o -11 5 1 2235.63 2243.81 104.64 o -10 5 1 3171.68 3122.42 188.70 o -9 5 1 12084.10 11551.43 561.77 o -8 5 1 11.46 132.79 25.23 o -7 5 1 929.27 812.47 52.43 o -6 5 1 1566.75 1452.46 53.09 o -5 5 1 96169.12 96577.73 3593.67 o -4 5 1 104.25 184.07 12.74 o -3 5 1 6307.77 6675.41 220.80 o -2 5 1 3476.34 3701.34 174.60 o -1 5 1 37153.82 39841.79 2127.81 o 0 5 1 7211.29 6370.47 471.49 o 1 5 1 88424.11 90175.99 6444.61 o 2 5 1 57196.02 56847.69 2474.66 o 3 5 1 3029.25 2807.07 93.74 o 4 5 1 350.60 434.56 28.50 o 5 5 1 74441.89 76095.38 2424.29 o 6 5 1 2185.20 2059.37 74.23 o 7 5 1 2193.74 2116.74 87.78 o 8 5 1 2423.65 2369.13 99.72 o 9 5 1 3.86 91.94 29.91 o 10 5 1 18587.62 18500.51 582.49 o 11 5 1 371.88 326.39 40.12 o 12 5 1 1405.57 1319.45 59.08 o 13 5 1 2418.63 2516.70 196.50 o 14 5 1 4163.39 4352.54 281.94 o -14 6 1 2849.44 2794.58 179.32 o -13 6 1 800.50 780.99 78.14 o -12 6 1 1629.66 1419.93 128.34 o -11 6 1 265.89 234.19 46.84 o -10 6 1 2191.30 1781.69 98.05 o -9 6 1 478.68 475.63 40.72 o -8 6 1 18660.23 18195.98 820.65 o -7 6 1 7097.30 6550.80 256.78 o -6 6 1 4401.56 3933.88 171.28 o -5 6 1 376.67 436.55 32.73 o -4 6 1 29842.73 28724.11 1186.92 o -3 6 1 18283.50 17527.24 525.63 o -2 6 1 6852.34 6964.52 300.58 o -1 6 1 4480.39 4832.67 252.66 o 0 6 1 10504.31 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