#------------------------------------------------------------------------------
#$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $
#$Revision: 26025 $
#$URL: file:///home/coder/svn-repositories/cod/hkl/2/2013467.hkl $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2013467_Fobs
loop_
_publ_author_name
'Glidewell, Christopher'
'Low, John N.'
'Marchal, Antonio'
'Quesada, Antonio'
_publ_section_title
;
Benzylation and nitrosation of
4-amino-2-(methylsulfanyl)pyrimidin-6(1H)-one: two
P2~1~/c polymorphs of
4-amino-1-benzyl-2-(methylsulfanyl)pyrimidin-6(1H)-one with
Z'=1 and 2, 4-amino-6-benzyloxy-2-(methylsulfanyl)pyrimidine
and
4-amino-1-benzyl-2-(methylsulfanyl)-5-nitrosopyrimidin-6(1H)-one
all give different hydrogen-bonded supramolecular structures
;
_journal_issue 8
_journal_name_full 'Acta Crystallographica Section C'
_journal_page_first o454
_journal_page_last o460
_journal_volume 59
_journal_year 2003
_space_group_IT_number 14
_symmetry_space_group_name_Hall '-P 2ybc'
_symmetry_space_group_name_H-M 'P 1 21/c 1'
_cell_angle_alpha 90.000
_cell_angle_beta 105.286
_cell_angle_gamma 90.000
_cell_length_a 15.7470
_cell_length_b 5.1044
_cell_length_c 15.5010
_exptl_crystal_F_000 520.00
_reflns_d_resolution_high 1.0143
_[local]_cod_data_source_file gg1172IVsup5.hkl
_[local]_cod_data_source_block IV
#BEGIN Tags that were not found in dictionaries:
_shelx_title ' 021 - EXOR'
_shelx_refln_list_code 4
_shelx_f_calc_maximum 139.56
_shelx_f_squared_multiplier 1.000
#END Tags that were not found in dictionaries
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y-1/2, z-1/2'
loop_
_refln_index_h
_refln_index_k
_refln_index_l
_refln_F_squared_calc
_refln_F_squared_meas
_refln_F_squared_sigma
_refln_observed_status
2 0 0 1191.45 390.78 354.87 o
3 0 0 189.25 215.40 22.04 o
4 0 0 36.40 54.25 17.43 o
5 0 0 79.11 109.05 19.98 o
6 0 0 99.52 124.26 28.87 o
7 0 0 434.31 495.07 53.60 o
8 0 0 90.40 126.16 21.04 o
9 0 0 207.15 264.14 26.14 o
10 0 0 57.52 82.84 21.00 o
11 0 0 1565.60 1582.59 91.98 o
12 0 0 2100.77 2210.10 139.56 o
13 0 0 2198.95 1995.60 127.38 o
14 0 0 3.99 23.73 32.87 o
1 1 0 1459.13 1635.89 75.77 o
2 1 0 858.53 876.34 34.91 o
3 1 0 2221.40 2010.62 85.82 o
4 1 0 298.07 316.33 23.43 o
5 1 0 1514.03 1507.00 57.20 o
6 1 0 6042.47 6052.59 184.36 o
7 1 0 1499.85 1518.38 51.21 o
8 1 0 909.99 960.52 33.91 o
9 1 0 5.90 24.20 13.42 o
10 1 0 317.13 330.76 19.04 o
11 1 0 182.61 207.40 19.83 o
12 1 0 5.50 31.38 22.29 o
13 1 0 201.08 196.27 37.26 o
14 1 0 350.24 341.62 28.52 o
0 2 0 9.01 -2.16 13.23 o
1 2 0 1254.60 1418.67 47.68 o
2 2 0 238.30 242.78 17.46 o
3 2 0 220.53 230.56 12.32 o
4 2 0 129.69 142.25 10.65 o
5 2 0 1227.30 1520.72 52.19 o
6 2 0 487.45 518.48 21.87 o
7 2 0 96.73 133.57 13.17 o
8 2 0 0.42 63.13 26.06 o
9 2 0 284.39 328.90 19.62 o
10 2 0 10.93 39.66 14.55 o
11 2 0 0.24 7.16 14.87 o
12 2 0 32.58 12.07 42.46 o
13 2 0 61.36 71.72 21.07 o
1 3 0 528.59 628.58 21.88 o
2 3 0 124.06 136.33 12.90 o
3 3 0 396.57 421.50 18.75 o
4 3 0 556.20 603.44 28.97 o
5 3 0 3.11 46.38 19.61 o
6 3 0 3.20 21.64 14.03 o
7 3 0 154.91 175.00 15.25 o
8 3 0 10.32 23.37 13.43 o
9 3 0 236.15 221.31 22.67 o
10 3 0 187.72 157.03 22.44 o
11 3 0 146.63 113.92 20.17 o
12 3 0 67.90 49.00 27.82 o
0 4 0 981.04 1251.49 86.88 o
1 4 0 4.83 20.27 21.42 o
2 4 0 789.76 809.92 67.72 o
3 4 0 324.33 376.72 17.62 o
4 4 0 76.17 101.09 13.49 o
5 4 0 12.17 33.13 12.15 o
6 4 0 32.90 51.64 13.30 o
7 4 0 47.53 69.93 11.91 o
8 4 0 0.01 32.19 13.64 o
9 4 0 119.76 143.39 33.84 o
1 5 0 54.70 53.92 32.28 o
-14 1 1 21.81 72.74 22.14 o
-13 1 1 840.26 766.05 58.33 o
-12 1 1 28.49 62.62 26.73 o
-11 1 1 467.51 479.53 36.60 o
-10 1 1 13.49 91.81 19.94 o
-9 1 1 678.64 705.05 26.80 o
-8 1 1 525.71 590.20 22.31 o
-7 1 1 556.88 655.70 22.61 o
-6 1 1 186.70 236.16 15.29 o
-5 1 1 573.37 651.94 27.06 o
-4 1 1 1345.42 1401.60 52.80 o
-3 1 1 145.85 121.43 10.84 o
-2 1 1 1177.73 1189.94 41.48 o
-1 1 1 2418.59 2621.38 100.60 o
0 1 1 3474.40 3753.81 225.18 o
1 1 1 796.14 829.30 38.91 o
2 1 1 5902.95 5570.81 221.71 o
3 1 1 2945.20 2807.75 100.87 o
4 1 1 263.77 253.53 15.96 o
5 1 1 17.91 -7.99 12.60 o
6 1 1 475.02 503.95 22.23 o
7 1 1 741.09 780.52 30.68 o
8 1 1 473.28 515.60 23.57 o
9 1 1 259.74 232.62 16.12 o
10 1 1 13.30 38.73 14.52 o
11 1 1 155.60 170.04 20.43 o
12 1 1 29.55 56.99 16.37 o
13 1 1 65.69 63.52 28.66 o
14 1 1 42.48 16.98 36.14 o
-13 2 1 463.37 425.26 28.30 o
-12 2 1 354.28 320.37 20.96 o
-11 2 1 22.47 61.54 14.86 o
-10 2 1 912.12 857.80 30.96 o
-9 2 1 310.13 296.20 22.10 o
-8 2 1 1288.70 1315.15 42.96 o
-7 2 1 220.47 902.37 112.29 o
-6 2 1 1050.00 931.19 77.37 o
-5 2 1 1771.83 1780.58 59.26 o
-4 2 1 9.59 14.36 9.77 o
-3 2 1 274.03 305.01 12.81 o
-2 2 1 599.51 598.66 21.42 o
-1 2 1 2104.31 2300.41 91.60 o
0 2 1 0.09 -9.49 9.49 o
1 2 1 748.41 731.91 37.04 o
2 2 1 639.60 608.73 39.70 o
3 2 1 129.57 114.59 9.26 o
4 2 1 115.62 134.68 10.80 o
5 2 1 2736.02 2736.93 102.11 o
6 2 1 921.61 968.33 38.79 o
7 2 1 15.19 44.38 12.26 o
8 2 1 2.76 43.89 12.29 o
9 2 1 313.56 270.55 16.88 o
10 2 1 247.24 271.19 24.03 o
11 2 1 18.26 54.70 14.56 o
12 2 1 1071.20 833.45 97.68 o
13 2 1 1.78 8.52 23.11 o
-12 3 1 28.17 19.75 12.69 o
-11 3 1 20.06 30.81 22.22 o
-10 3 1 78.74 114.36 15.26 o
-9 3 1 231.27 225.25 24.93 o
-8 3 1 25.63 24.21 11.19 o
-7 3 1 232.22 272.30 14.85 o
-6 3 1 5.38 36.59 56.97 o
-5 3 1 1005.16 1055.84 66.44 o
-4 3 1 215.86 227.99 12.77 o
-3 3 1 973.78 1088.88 33.67 o
-2 3 1 264.98 316.43 14.79 o
-1 3 1 1.64 42.56 10.86 o
0 3 1 1082.62 1169.50 48.41 o
1 3 1 0.04 29.37 13.66 o
2 3 1 1366.20 1330.30 57.98 o
3 3 1 149.68 164.06 17.06 o
4 3 1 273.36 279.32 23.38 o
5 3 1 306.71 311.32 19.91 o
6 3 1 1130.68 1021.32 58.75 o
7 3 1 161.63 149.95 22.14 o
8 3 1 1099.18 977.20 64.52 o
9 3 1 973.10 762.51 81.84 o
10 3 1 32.15 44.25 16.19 o
11 3 1 84.45 121.53 24.54 o
-9 4 1 83.13 100.22 28.36 o
-8 4 1 40.20 57.94 13.30 o
-7 4 1 258.99 359.51 25.14 o
-6 4 1 138.65 184.67 14.64 o
-5 4 1 465.14 491.41 33.35 o
-4 4 1 47.34 37.97 11.36 o
-3 4 1 18.52 20.59 11.07 o
-2 4 1 19.53 56.22 11.54 o
-1 4 1 290.89 344.00 27.91 o
0 4 1 333.00 389.83 34.23 o
1 4 1 343.15 340.96 14.78 o
2 4 1 60.04 103.96 24.69 o
3 4 1 251.35 294.30 33.51 o
4 4 1 139.23 123.74 11.53 o
5 4 1 28.98 45.44 11.90 o
6 4 1 781.60 713.47 35.95 o
7 4 1 347.42 326.94 24.87 o
8 4 1 169.68 120.89 32.22 o
-1 5 1 197.73 128.84 71.11 o
0 5 1 1.62 26.14 33.42 o
1 5 1 227.71 291.84 50.90 o
-15 0 2 2.89 27.81 37.17 o
-14 0 2 97.55 242.64 52.98 o
-13 0 2 2484.49 2631.16 166.85 o
-12 0 2 2348.01 2361.59 127.24 o
-11 0 2 1249.63 1235.87 48.16 o
-10 0 2 257.17 245.11 19.55 o
-9 0 2 231.04 223.08 32.92 o
-8 0 2 0.38 6.11 16.79 o
-7 0 2 1762.42 1791.82 77.32 o
-6 0 2 552.32 496.79 31.81 o
-5 0 2 521.24 457.13 37.93 o
-4 0 2 2661.78 2371.32 132.53 o
-3 0 2 64.15 57.63 17.73 o
-2 0 2 7401.82 5932.45 529.59 o
-1 0 2 1330.25 1281.93 191.76 o
0 0 2 223.54 111.21 121.02 o
1 0 2 129.63 126.45 16.36 o
2 0 2 17048.54 13629.27 1022.80 o
3 0 2 618.00 563.58 37.24 o
4 0 2 1711.05 1605.46 90.30 o
5 0 2 2813.87 2613.97 138.36 o
6 0 2 2710.60 2677.62 128.17 o
7 0 2 2832.25 2792.79 125.94 o
8 0 2 694.18 682.68 36.52 o
9 0 2 56.16 43.19 23.38 o
10 0 2 474.57 528.11 38.41 o
11 0 2 35.72 34.23 38.40 o
12 0 2 169.67 153.19 32.81 o
13 0 2 2.35 -27.32 27.32 o
14 0 2 8.72 75.75 56.84 o
-15 1 2 228.86 194.90 38.80 o
-14 1 2 358.32 373.34 50.02 o
-13 1 2 1175.37 1120.57 72.56 o
-12 1 2 112.06 271.01 27.69 o
-11 1 2 131.89 144.35 15.25 o
-10 1 2 1103.00 1130.99 41.44 o
-9 1 2 272.75 394.09 22.40 o
-8 1 2 79.52 66.37 12.44 o
-7 1 2 406.92 478.35 19.41 o
-6 1 2 1.42 -10.41 11.04 o
-5 1 2 618.54 599.99 56.80 o
-4 1 2 3405.01 3399.25 99.44 o
-3 1 2 714.99 651.13 26.82 o
-2 1 2 1.27 28.61 17.49 o
-1 1 2 7320.64 7336.07 332.70 o
0 1 2 7327.22 7373.37 361.77 o
1 1 2 10525.70 10067.86 344.81 o
2 1 2 7644.82 7096.03 265.06 o
3 1 2 811.32 863.29 30.43 o
4 1 2 41.51 57.48 11.86 o
5 1 2 52.21 68.05 15.07 o
6 1 2 373.20 387.61 18.60 o
7 1 2 559.38 520.06 22.27 o
8 1 2 1191.93 1296.97 46.66 o
9 1 2 124.30 132.71 16.68 o
10 1 2 143.10 151.20 16.61 o
11 1 2 31.94 63.24 17.43 o
12 1 2 999.81 984.92 45.44 o
13 1 2 12.12 33.41 17.55 o
-14 2 2 155.47 192.06 22.95 o
-13 2 2 26.72 99.79 42.29 o
-12 2 2 21.83 168.92 31.43 o
-11 2 2 95.58 114.63 15.28 o
-10 2 2 2.19 37.32 14.65 o
-9 2 2 13.68 35.99 10.87 o
-8 2 2 120.90 271.76 29.61 o
-7 2 2 5325.73 5803.64 176.10 o
-6 2 2 129.02 153.70 13.62 o
-5 2 2 1051.75 1057.71 38.42 o
-4 2 2 620.11 666.69 28.92 o
-3 2 2 419.75 490.40 19.57 o
-2 2 2 117.28 108.66 8.97 o
-1 2 2 374.79 401.15 30.93 o
0 2 2 494.28 520.67 34.82 o
1 2 2 793.43 759.74 45.86 o
2 2 2 56.03 67.45 7.97 o
3 2 2 0.30 -6.49 9.53 o
4 2 2 744.12 752.00 30.94 o
5 2 2 572.78 592.16 25.16 o
6 2 2 1226.42 1305.03 66.58 o
7 2 2 181.16 197.33 22.76 o
8 2 2 13.37 44.55 17.28 o
9 2 2 26.44 22.25 14.13 o
10 2 2 96.52 103.32 17.30 o
11 2 2 53.42 61.30 18.79 o
12 2 2 27.89 70.15 22.11 o
13 2 2 29.18 71.60 21.17 o
-12 3 2 97.32 141.11 31.24 o
-11 3 2 190.39 312.39 30.61 o
-10 3 2 157.40 158.56 17.87 o
-9 3 2 152.27 251.64 20.31 o
-8 3 2 83.07 111.04 11.89 o
-7 3 2 187.89 234.22 15.02 o
-6 3 2 184.84 217.20 13.03 o
-5 3 2 21.78 89.48 13.18 o
-4 3 2 575.15 578.69 22.33 o
-3 3 2 236.28 291.43 16.01 o
-2 3 2 3.71 28.85 11.32 o
-1 3 2 1047.52 1272.24 58.00 o
0 3 2 16.63 23.59 13.70 o
1 3 2 73.43 64.01 13.53 o
2 3 2 2.25 21.76 7.65 o
3 3 2 173.26 173.87 19.44 o
4 3 2 178.25 199.97 18.46 o
5 3 2 20.77 37.79 11.28 o
6 3 2 87.83 62.18 15.03 o
7 3 2 28.91 38.90 11.78 o
8 3 2 27.66 46.72 13.63 o
9 3 2 13.06 36.15 15.82 o
10 3 2 22.73 32.73 27.86 o
11 3 2 4.00 40.09 16.71 o
-9 4 2 276.05 283.26 21.57 o
-8 4 2 16.14 58.08 18.32 o
-7 4 2 984.29 981.45 69.99 o
-6 4 2 6.00 26.60 10.19 o
-5 4 2 24.09 44.50 10.45 o
-4 4 2 0.37 24.47 11.83 o
-3 4 2 241.54 266.66 28.75 o
-2 4 2 108.29 94.13 18.81 o
-1 4 2 54.33 100.31 14.84 o
0 4 2 117.68 156.39 19.45 o
1 4 2 5.04 24.94 18.65 o
2 4 2 620.83 587.62 27.89 o
3 4 2 37.60 76.78 13.23 o
4 4 2 2233.35 2085.02 88.05 o
5 4 2 2247.98 1872.17 167.37 o
6 4 2 33.11 57.37 16.51 o
7 4 2 6.20 21.33 13.25 o
8 4 2 1.14 14.06 12.64 o
-15 1 3 2.72 43.26 12.43 o
-14 1 3 645.04 624.86 42.31 o
-13 1 3 274.23 261.59 23.66 o
-12 1 3 343.75 492.38 31.48 o
-11 1 3 44.14 38.76 25.82 o
-10 1 3 13.89 48.55 11.41 o
-9 1 3 914.73 1065.44 36.94 o
-8 1 3 189.98 263.84 27.68 o
-7 1 3 0.50 16.85 14.68 o
-6 1 3 1.32 34.12 61.58 o
-5 1 3 237.90 259.66 18.09 o
-4 1 3 218.40 198.66 10.91 o
-3 1 3 270.85 294.34 15.16 o
-2 1 3 2577.17 2562.54 102.32 o
-1 1 3 4987.68 4722.05 184.60 o
0 1 3 4.60 19.03 10.28 o
1 1 3 19476.83 17492.25 639.98 o
2 1 3 928.31 867.86 33.79 o
3 1 3 438.22 448.58 20.04 o
4 1 3 797.86 760.61 28.29 o
5 1 3 174.71 188.78 13.66 o
6 1 3 1088.83 1155.03 42.48 o
7 1 3 977.51 970.35 31.74 o
8 1 3 5.62 25.84 13.89 o
9 1 3 214.87 210.68 17.37 o
10 1 3 32.58 62.99 16.23 o
11 1 3 549.09 543.06 27.75 o
12 1 3 480.52 435.25 38.63 o
13 1 3 953.21 818.99 51.74 o
-14 2 3 58.07 76.09 31.27 o
-13 2 3 24.11 77.92 23.10 o
-12 2 3 725.03 655.43 37.42 o
-11 2 3 11.57 40.36 18.75 o
-10 2 3 178.85 167.75 14.66 o
-9 2 3 48.45 55.82 14.91 o
-8 2 3 1757.49 1725.18 84.25 o
-7 2 3 357.31 391.60 26.37 o
-6 2 3 891.62 818.52 35.94 o
-5 2 3 172.31 238.19 13.90 o
-4 2 3 1837.53 1891.39 60.06 o
-3 2 3 122.36 130.04 10.79 o
-2 2 3 1125.23 1097.67 48.89 o
-1 2 3 1353.90 1407.11 49.59 o
0 2 3 2476.51 2189.81 241.88 o
1 2 3 4479.47 4677.37 167.74 o
2 2 3 1170.85 1095.08 40.70 o
3 2 3 860.74 773.78 33.10 o
4 2 3 779.50 722.76 28.27 o
5 2 3 519.18 534.13 22.28 o
6 2 3 92.54 97.11 14.67 o
7 2 3 432.21 471.21 21.13 o
8 2 3 13.63 48.32 15.01 o
9 2 3 207.70 234.50 22.96 o
10 2 3 231.00 259.00 19.07 o
11 2 3 20.24 47.15 24.09 o
12 2 3 54.72 57.42 23.17 o
-12 3 3 58.17 61.42 18.85 o
-11 3 3 729.72 553.52 67.65 o
-10 3 3 0.44 29.64 12.96 o
-9 3 3 687.87 667.04 40.10 o
-8 3 3 272.19 256.45 14.23 o
-7 3 3 182.07 134.12 14.44 o
-6 3 3 840.71 769.85 38.97 o
-5 3 3 1070.24 1144.76 40.40 o
-4 3 3 1999.77 2090.23 88.16 o
-3 3 3 176.53 222.74 18.15 o
-2 3 3 6.42 38.53 12.02 o
-1 3 3 692.82 783.99 47.79 o
0 3 3 249.60 251.73 25.27 o
1 3 3 0.39 32.72 15.51 o
2 3 3 1833.28 1691.23 111.53 o
3 3 3 152.02 159.99 12.55 o
4 3 3 157.69 193.62 12.76 o
5 3 3 24.58 53.11 10.45 o
6 3 3 19.20 22.83 12.35 o
7 3 3 1907.68 2022.48 74.69 o
8 3 3 121.50 132.50 18.07 o
9 3 3 2.24 75.11 14.18 o
10 3 3 165.55 134.95 23.90 o
-9 4 3 83.37 78.90 18.77 o
-8 4 3 250.08 292.23 19.59 o
-7 4 3 142.99 140.10 25.48 o
-6 4 3 10.67 40.70 10.58 o
-5 4 3 13.17 21.62 15.93 o
-4 4 3 182.11 222.96 18.03 o
-3 4 3 565.10 601.25 29.35 o
-2 4 3 3.10 14.67 12.82 o
-1 4 3 625.36 567.52 25.83 o
0 4 3 32.20 35.47 13.57 o
1 4 3 23.08 58.77 12.92 o
2 4 3 20.06 50.98 12.76 o
3 4 3 41.48 139.52 54.00 o
4 4 3 54.56 135.19 60.51 o
5 4 3 770.52 719.12 68.26 o
6 4 3 71.26 54.42 15.06 o
7 4 3 293.52 227.69 30.39 o
-15 0 4 228.59 183.99 48.41 o
-14 0 4 6294.51 4941.06 598.03 o
-13 0 4 268.35 247.56 24.18 o
-12 0 4 1180.32 1034.56 167.37 o
-11 0 4 1510.11 1589.46 72.89 o
-10 0 4 0.21 29.19 18.04 o
-9 0 4 1192.53 889.35 153.03 o
-8 0 4 438.41 434.08 78.24 o
-7 0 4 589.21 633.26 53.83 o
-6 0 4 7507.05 7426.91 314.51 o
-5 0 4 254.97 245.84 24.58 o
-4 0 4 50.03 9.49 18.98 o
-3 0 4 5332.33 4576.20 263.81 o
-2 0 4 17892.63 15786.81 963.94 o
-1 0 4 5080.51 4650.54 286.87 o
0 0 4 33.65 35.57 24.43 o
1 0 4 2563.91 2332.76 125.71 o
2 0 4 2283.94 2009.60 122.28 o
3 0 4 58.76 36.63 13.30 o
4 0 4 8.86 25.81 17.27 o
5 0 4 528.30 458.44 35.57 o
6 0 4 1.41 28.51 19.94 o
7 0 4 2139.88 2215.20 101.57 o
8 0 4 2494.20 2510.47 107.79 o
9 0 4 3130.19 3106.40 134.87 o
10 0 4 69.78 98.23 24.88 o
11 0 4 769.53 695.94 58.84 o
12 0 4 28.80 22.81 25.70 o
13 0 4 226.18 240.13 45.50 o
-13 1 4 55.56 129.02 21.37 o
-12 1 4 1041.20 1055.05 74.17 o
-11 1 4 0.14 36.82 25.00 o
-10 1 4 59.35 74.29 24.67 o
-9 1 4 249.14 236.68 24.27 o
-8 1 4 2332.45 2298.98 139.18 o
-7 1 4 905.22 977.94 50.68 o
-6 1 4 2695.35 2547.75 72.95 o
-5 1 4 1233.36 1186.86 41.48 o
-4 1 4 18.11 30.12 11.30 o
-3 1 4 274.02 300.49 17.92 o
-2 1 4 595.66 572.18 27.41 o
-1 1 4 1976.63 1873.88 76.41 o
0 1 4 494.03 518.19 25.58 o
1 1 4 12382.28 11479.72 408.75 o
2 1 4 391.99 376.31 19.81 o
3 1 4 2215.47 2151.79 76.83 o
4 1 4 819.62 779.71 27.98 o
5 1 4 2139.21 2082.19 64.32 o
6 1 4 25.75 14.68 11.27 o
7 1 4 304.22 338.12 18.76 o
8 1 4 592.59 584.89 25.01 o
9 1 4 277.21 278.40 23.99 o
10 1 4 41.45 35.01 15.67 o
11 1 4 110.50 193.52 27.12 o
12 1 4 17.90 48.96 20.31 o
13 1 4 36.76 83.30 26.96 o
-14 2 4 30.53 81.84 29.62 o
-13 2 4 138.15 125.42 23.90 o
-12 2 4 23.25 27.94 30.17 o
-11 2 4 32.90 54.53 15.77 o
-10 2 4 182.76 221.19 19.55 o
-9 2 4 38.40 30.81 14.04 o
-8 2 4 52.33 111.46 41.71 o
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1 1 10 216.74 244.22 16.59 o
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1 2 10 211.21 194.60 20.30 o
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1 3 10 0.20 34.75 20.09 o
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1 1 11 1.21 6.85 12.81 o
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5 1 11 210.29 198.67 23.44 o
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1 2 11 281.20 259.13 20.77 o
2 2 11 3.90 44.45 21.59 o
3 2 11 26.27 48.36 19.33 o
4 2 11 89.17 97.47 22.90 o
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1 3 11 213.51 208.38 19.84 o
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0 0 12 362.30 325.29 30.84 o
1 0 12 289.71 273.78 25.54 o
2 0 12 229.82 263.33 29.91 o
3 0 12 5.02 20.62 36.77 o
4 0 12 48.55 54.72 31.09 o
5 0 12 42.42 95.86 36.77 o
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-1 1 12 359.32 327.26 27.85 o
0 1 12 91.22 169.58 27.84 o
1 1 12 126.32 140.25 16.38 o
2 1 12 231.11 270.59 22.34 o
3 1 12 442.66 418.49 26.84 o
4 1 12 119.36 87.33 30.01 o
5 1 12 432.73 414.27 46.07 o
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-1 2 12 2.33 21.39 23.54 o
0 2 12 8.50 24.97 18.27 o
1 2 12 95.24 119.53 19.92 o
2 2 12 0.02 28.02 22.66 o
3 2 12 2.05 27.36 22.27 o
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-1 1 13 34.04 85.65 32.35 o
0 1 13 221.79 250.51 23.81 o
1 1 13 12.57 61.52 21.78 o
2 1 13 110.09 73.39 21.73 o
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0 2 13 377.66 374.85 30.70 o
1 2 13 362.02 351.28 28.75 o
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0 0 14 41.99 4.91 41.61 o
1 0 14 98.41 49.32 34.53 o
2 0 14 411.78 345.51 51.13 o
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-1 1 14 2.25 30.72 34.54 o
0 1 14 121.89 127.31 33.79 o
1 1 14 298.00 308.52 29.92 o