#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/35/2013531.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2013531_Fobs loop_ _publ_author_name 'Ge\&smann, Renate' 'Schiemann, Norbert' 'Br\"uckner, Hans' 'Petratos, Kyriacos' _publ_section_title ; The tetrapeptide Z-Leu-Aib-Pro-Val-OBg monohydrate ; _journal_issue 8 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first o413 _journal_page_last o415 _journal_volume 59 _journal_year 2003 _space_group_IT_number 19 _symmetry_space_group_name_Hall 'P 2ac 2ab' _symmetry_space_group_name_H-M 'P 21 21 21' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 9.8820 _cell_length_b 10.7050 _cell_length_c 41.5530 _exptl_crystal_F_000 1688.00 _reflns_d_resolution_high 0.8907 _[local]_cod_data_source_file tr1055Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' alles wird gut' _shelx_refln_list_code 4 _shelx_f_calc_maximum 308.79 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' 'x+1/2, -y+1/2, -z' '-x, y+1/2, -z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 2123.67 1650.41 23.07 o 4 0 0 1720.13 1657.57 29.49 o 6 0 0 847.64 765.68 49.96 o 8 0 0 69.91 25.42 30.36 o 10 0 0 79.21 61.28 15.08 o 1 1 0 5845.18 6533.38 36.08 o 2 1 0 31939.82 38268.25 392.01 o 3 1 0 1647.53 1907.86 33.33 o 4 1 0 763.18 871.46 21.48 o 5 1 0 1271.13 1536.40 35.60 o 6 1 0 1540.82 1795.40 35.87 o 7 1 0 13.79 8.61 16.28 o 8 1 0 11.06 6.87 32.99 o 9 1 0 231.38 256.06 42.48 o 10 1 0 2.41 7.11 20.75 o 11 1 0 0.06 -19.91 19.91 o 0 2 0 9824.02 10987.35 308.71 o 1 2 0 15537.21 16641.61 343.34 o 2 2 0 34460.70 42776.92 819.00 o 3 2 0 5.68 -0.53 14.41 o 4 2 0 502.01 517.42 12.25 o 5 2 0 1380.34 1677.55 131.74 o 6 2 0 2811.41 3293.85 147.07 o 7 2 0 63.47 60.15 14.31 o 8 2 0 196.60 226.12 36.97 o 9 2 0 107.27 107.36 15.08 o 10 2 0 21.48 -3.50 25.42 o 1 3 0 7442.09 7877.80 271.08 o 2 3 0 1489.15 1752.39 32.57 o 3 3 0 26.32 0.63 12.61 o 4 3 0 24.19 23.35 7.44 o 5 3 0 1896.14 2424.62 140.59 o 6 3 0 2.98 -8.97 24.08 o 7 3 0 309.82 295.63 25.19 o 8 3 0 31.85 14.41 14.24 o 9 3 0 0.85 3.30 20.38 o 10 3 0 1.02 10.04 22.42 o 0 4 0 2153.99 1987.48 213.03 o 1 4 0 14.40 14.71 6.87 o 2 4 0 737.04 802.68 52.31 o 3 4 0 14.16 27.02 11.51 o 4 4 0 1782.49 1740.06 75.89 o 5 4 0 8.87 18.38 9.04 o 6 4 0 622.00 677.87 44.63 o 7 4 0 125.20 90.25 57.35 o 8 4 0 10.59 -7.34 28.19 o 9 4 0 168.32 245.13 26.26 o 10 4 0 4.27 -10.07 33.36 o 1 5 0 133.66 121.15 7.77 o 2 5 0 845.69 1102.26 82.84 o 3 5 0 1549.58 1778.63 135.28 o 4 5 0 936.06 902.51 72.72 o 5 5 0 190.00 189.45 19.49 o 6 5 0 93.93 136.95 39.47 o 7 5 0 59.69 81.30 12.44 o 8 5 0 302.27 348.98 16.65 o 9 5 0 5.38 8.57 24.42 o 10 5 0 27.98 19.35 8.97 o 0 6 0 269.78 270.81 16.19 o 1 6 0 1575.85 1567.75 105.32 o 2 6 0 164.73 137.03 12.75 o 3 6 0 161.43 208.23 33.40 o 4 6 0 37.31 53.51 21.58 o 5 6 0 447.93 549.84 46.23 o 6 6 0 29.51 36.33 21.08 o 7 6 0 53.92 118.49 29.22 o 8 6 0 27.93 10.74 25.15 o 9 6 0 85.58 133.58 36.00 o 1 7 0 16.83 16.25 18.65 o 2 7 0 665.05 767.13 52.12 o 3 7 0 960.88 1003.39 75.08 o 4 7 0 684.43 843.66 82.06 o 5 7 0 169.57 199.12 13.58 o 6 7 0 253.89 243.42 42.11 o 7 7 0 16.54 27.99 22.12 o 8 7 0 102.07 131.21 17.82 o 9 7 0 2.59 1.30 18.71 o 0 8 0 1067.13 886.26 93.26 o 1 8 0 193.70 173.24 19.32 o 2 8 0 225.67 240.48 13.81 o 3 8 0 265.92 276.42 32.93 o 4 8 0 129.46 204.15 24.19 o 5 8 0 6.71 14.24 16.88 o 6 8 0 20.37 7.17 31.62 o 7 8 0 0.13 -20.85 20.85 o 8 8 0 66.49 86.67 16.35 o 1 9 0 12.30 30.19 10.51 o 2 9 0 99.83 92.08 12.04 o 3 9 0 191.34 254.88 21.55 o 4 9 0 58.05 91.44 22.95 o 5 9 0 222.61 265.83 61.63 o 6 9 0 0.93 6.70 15.44 o 7 9 0 17.85 28.19 14.98 o 0 10 0 8.41 -15.75 20.82 o 1 10 0 47.68 78.03 10.91 o 2 10 0 3.67 15.28 9.47 o 3 10 0 13.10 -6.74 19.05 o 4 10 0 3.07 -35.56 38.76 o 5 10 0 6.27 -17.71 23.62 o 6 10 0 15.91 -3.80 18.01 o 1 11 0 29.65 31.16 9.37 o 2 11 0 1.22 18.18 20.65 o 3 11 0 65.93 74.63 10.31 o 4 11 0 5.99 -14.31 17.78 o 0 12 0 0.00 17.15 15.11 o 1 0 1 2859.15 4446.89 94.15 o 2 0 1 4895.96 4780.52 98.65 o 3 0 1 2163.08 2648.60 18.75 o 4 0 1 428.48 444.10 10.62 o 5 0 1 17.28 -10.24 30.76 o 6 0 1 4.58 -11.14 23.38 o 7 0 1 145.52 173.83 15.51 o 8 0 1 112.17 113.00 15.21 o 9 0 1 28.04 30.36 12.71 o 10 0 1 16.96 7.14 30.76 o 11 0 1 7.54 -14.14 22.08 o 0 1 1 3631.50 3304.98 72.62 o 1 1 1 9585.00 9642.96 169.03 o 2 1 1 676.52 655.28 14.11 o 3 1 1 658.18 824.87 17.44 o 4 1 1 2562.78 3148.00 48.20 o 5 1 1 117.13 154.38 10.16 o 6 1 1 29.57 50.77 11.72 o 7 1 1 17.52 38.07 13.02 o 8 1 1 62.87 84.34 17.98 o 9 1 1 23.21 32.33 17.71 o 10 1 1 55.12 26.73 23.34 o 11 1 1 23.49 7.71 10.67 o 0 2 1 6143.31 5707.37 280.66 o 1 2 1 9105.12 8143.29 115.28 o 2 2 1 2686.32 2982.09 116.93 o 3 2 1 1727.27 2017.01 36.25 o 4 2 1 1916.47 2306.88 43.49 o 5 2 1 180.69 178.67 10.72 o 6 2 1 185.46 247.04 15.25 o 7 2 1 27.75 50.36 13.32 o 8 2 1 7.38 31.57 39.83 o 9 2 1 52.89 86.20 13.89 o 10 2 1 33.83 26.15 15.41 o 0 3 1 8831.08 9458.87 678.74 o 1 3 1 351.57 388.21 29.82 o 2 3 1 3002.93 3312.13 140.98 o 3 3 1 1355.63 1431.24 47.91 o 4 3 1 198.74 253.49 20.87 o 5 3 1 217.88 258.15 23.89 o 6 3 1 609.41 695.04 18.20 o 7 3 1 392.44 414.76 17.87 o 8 3 1 119.36 141.54 14.50 o 9 3 1 69.39 87.11 13.92 o 10 3 1 31.05 -3.34 22.88 o 0 4 1 413.26 634.76 55.39 o 1 4 1 2810.91 2681.47 159.16 o 2 4 1 377.82 362.39 25.52 o 3 4 1 451.45 420.53 44.43 o 4 4 1 217.42 219.31 10.31 o 5 4 1 103.17 95.75 11.16 o 6 4 1 210.07 292.63 48.15 o 7 4 1 321.89 337.90 31.90 o 8 4 1 123.76 169.46 20.05 o 9 4 1 51.65 63.00 12.89 o 10 4 1 15.36 -17.74 17.74 o 0 5 1 2164.67 2062.30 209.71 o 1 5 1 981.50 987.55 34.20 o 2 5 1 162.16 176.92 13.03 o 3 5 1 395.04 447.86 39.24 o 4 5 1 98.81 86.20 9.75 o 5 5 1 470.64 457.11 43.79 o 6 5 1 54.99 90.03 16.15 o 7 5 1 312.74 261.14 28.45 o 8 5 1 80.65 69.32 26.69 o 9 5 1 7.04 23.92 11.17 o 10 5 1 25.83 11.51 8.92 o 0 6 1 2135.29 1985.41 129.81 o 1 6 1 493.14 406.42 43.66 o 2 6 1 141.54 186.27 17.50 o 3 6 1 136.73 152.22 10.56 o 4 6 1 255.27 308.72 44.18 o 5 6 1 484.78 484.91 45.96 o 6 6 1 154.69 162.09 18.30 o 7 6 1 593.95 701.64 77.94 o 8 6 1 26.48 51.24 35.96 o 9 6 1 8.24 7.62 20.68 o 0 7 1 43.98 50.41 22.45 o 1 7 1 100.60 112.32 12.49 o 2 7 1 108.19 116.60 11.07 o 3 7 1 361.56 397.91 51.46 o 4 7 1 356.55 311.98 27.75 o 5 7 1 123.80 120.80 55.28 o 6 7 1 134.49 138.45 13.21 o 7 7 1 106.95 131.45 23.99 o 8 7 1 15.43 -2.05 22.51 o 9 7 1 24.70 17.41 15.68 o 0 8 1 867.41 991.50 130.00 o 1 8 1 105.17 131.57 11.71 o 2 8 1 662.64 654.89 56.42 o 3 8 1 21.15 17.18 10.51 o 4 8 1 20.81 -8.26 21.23 o 5 8 1 27.96 22.22 10.16 o 6 8 1 92.31 67.80 32.79 o 7 8 1 24.99 21.09 15.31 o 8 8 1 40.74 35.16 13.56 o 0 9 1 574.65 496.47 66.53 o 1 9 1 48.83 28.99 21.13 o 2 9 1 192.01 245.02 46.63 o 3 9 1 75.68 66.10 10.53 o 4 9 1 10.62 -22.72 22.72 o 5 9 1 32.45 15.15 13.04 o 6 9 1 72.58 55.35 11.41 o 7 9 1 8.97 4.76 10.73 o 0 10 1 40.45 42.80 10.84 o 1 10 1 145.89 139.82 11.76 o 2 10 1 15.52 42.05 9.69 o 3 10 1 49.66 63.58 27.69 o 4 10 1 86.28 88.48 16.56 o 5 10 1 11.83 -9.82 19.32 o 6 10 1 14.14 21.25 12.38 o 0 11 1 2.79 4.77 18.08 o 1 11 1 31.26 -6.51 21.94 o 2 11 1 58.70 72.49 26.14 o 3 11 1 1.10 -10.22 21.42 o 4 11 1 23.02 27.93 8.35 o 0 12 1 0.07 11.94 7.34 o 0 0 2 3858.86 2466.62 13.50 o 1 0 2 11009.91 12407.38 336.85 o 2 0 2 4053.38 4880.89 135.73 o 3 0 2 3314.39 3737.34 44.10 o 4 0 2 1315.45 1379.70 27.56 o 5 0 2 1231.52 1331.81 83.96 o 6 0 2 3.37 8.94 22.78 o 7 0 2 12.85 11.44 29.59 o 8 0 2 90.46 67.49 16.35 o 9 0 2 306.77 299.23 17.09 o 10 0 2 19.87 11.11 15.71 o 11 0 2 71.03 14.15 23.85 o 0 1 2 9868.57 7165.64 303.29 o 1 1 2 4354.75 4169.92 151.58 o 2 1 2 2974.22 4009.40 150.84 o 3 1 2 3578.68 3812.25 80.02 o 4 1 2 3257.43 3470.43 69.10 o 5 1 2 258.80 310.69 11.75 o 6 1 2 701.93 957.63 53.64 o 7 1 2 63.61 79.37 14.58 o 8 1 2 26.56 52.49 37.51 o 9 1 2 158.30 196.41 16.95 o 10 1 2 38.59 -24.09 24.09 o 11 1 2 18.14 11.88 8.54 o 0 2 2 5536.84 4199.82 291.62 o 1 2 2 14662.22 14614.46 601.49 o 2 2 2 1386.26 1250.76 25.77 o 3 2 2 5961.00 6791.01 406.98 o 4 2 2 664.39 623.68 26.23 o 5 2 2 678.10 790.46 36.65 o 6 2 2 282.83 346.36 14.33 o 7 2 2 361.69 455.34 44.44 o 8 2 2 26.08 27.02 32.39 o 9 2 2 105.71 120.03 15.53 o 10 2 2 24.44 11.31 14.48 o 0 3 2 192.90 193.14 14.99 o 1 3 2 1842.86 2182.31 96.91 o 2 3 2 1406.85 1432.53 92.66 o 3 3 2 626.77 620.04 12.65 o 4 3 2 554.91 622.28 64.06 o 5 3 2 45.77 47.47 9.40 o 6 3 2 653.28 842.47 37.53 o 7 3 2 250.36 253.25 20.64 o 8 3 2 146.11 187.73 52.53 o 9 3 2 270.45 300.34 53.07 o 10 3 2 5.32 -1.67 11.84 o 0 4 2 1071.32 996.15 61.92 o 1 4 2 716.53 847.05 45.88 o 2 4 2 192.48 216.67 13.43 o 3 4 2 960.57 840.61 52.77 o 4 4 2 858.03 880.86 64.83 o 5 4 2 96.71 120.16 20.07 o 6 4 2 316.90 332.31 15.34 o 7 4 2 152.89 185.39 28.94 o 8 4 2 69.27 63.63 13.28 o 9 4 2 40.88 35.78 16.34 o 10 4 2 26.41 20.26 8.54 o 0 5 2 2482.38 2491.59 203.76 o 1 5 2 767.38 618.25 62.73 o 2 5 2 1864.98 1887.75 154.70 o 3 5 2 17.50 30.05 16.40 o 4 5 2 141.90 194.80 17.08 o 5 5 2 297.00 309.35 14.24 o 6 5 2 293.58 308.87 15.31 o 7 5 2 549.64 702.99 87.62 o 8 5 2 185.03 227.40 14.78 o 9 5 2 229.80 327.55 59.44 o 10 5 2 32.62 -5.65 8.77 o 0 6 2 0.00 -8.81 12.88 o 1 6 2 168.67 194.69 9.73 o 2 6 2 486.39 574.04 37.52 o 3 6 2 819.64 988.98 88.81 o 4 6 2 205.20 272.90 17.38 o 5 6 2 430.98 530.66 47.76 o 6 6 2 255.21 290.60 15.70 o 7 6 2 538.70 523.54 59.31 o 8 6 2 61.94 81.17 27.79 o 9 6 2 6.41 3.77 16.98 o 0 7 2 371.29 411.47 70.65 o 1 7 2 1039.78 885.93 114.53 o 2 7 2 269.77 275.99 53.42 o 3 7 2 934.94 1033.23 79.77 o 4 7 2 96.28 79.28 12.36 o 5 7 2 118.54 156.92 13.06 o 6 7 2 443.70 460.12 54.95 o 7 7 2 116.44 93.12 14.68 o 8 7 2 65.38 82.92 12.52 o 9 7 2 16.45 -15.93 29.96 o 0 8 2 11.85 -1.00 17.75 o 1 8 2 401.23 320.29 20.71 o 2 8 2 281.09 302.69 24.64 o 3 8 2 18.34 31.55 10.60 o 4 8 2 138.80 130.64 12.39 o 5 8 2 102.46 89.25 17.58 o 6 8 2 1.55 -3.58 13.35 o 7 8 2 4.02 27.52 9.93 o 8 8 2 11.38 8.76 12.26 o 0 9 2 38.24 33.09 11.24 o 1 9 2 122.63 93.72 12.10 o 2 9 2 114.06 93.69 11.72 o 3 9 2 129.47 169.11 31.84 o 4 9 2 58.73 29.82 11.26 o 5 9 2 59.10 68.35 10.33 o 6 9 2 15.39 -2.72 13.30 o 7 9 2 34.30 49.00 9.22 o 0 10 2 29.53 8.74 24.95 o 1 10 2 159.69 118.44 28.73 o 2 10 2 40.56 23.84 21.97 o 3 10 2 36.93 67.07 29.91 o 4 10 2 6.90 -9.71 36.28 o 5 10 2 2.11 8.99 17.27 o 6 10 2 7.98 -5.43 13.28 o 0 11 2 123.03 119.57 22.65 o 1 11 2 10.88 9.28 12.05 o 2 11 2 16.99 -16.04 19.59 o 3 11 2 30.25 -18.11 22.01 o 4 11 2 9.12 -5.04 17.18 o 0 12 2 9.32 -14.64 15.81 o 1 0 3 17.74 44.37 6.71 o 2 0 3 11220.82 11536.70 371.99 o 3 0 3 783.00 353.92 331.90 o 4 0 3 323.73 315.33 9.45 o 5 0 3 909.24 914.38 31.27 o 6 0 3 21.28 28.12 24.35 o 7 0 3 806.19 763.31 21.00 o 8 0 3 153.05 170.72 16.92 o 9 0 3 96.66 108.06 17.72 o 10 0 3 145.79 116.87 12.11 o 11 0 3 7.72 2.80 18.41 o 0 1 3 6323.93 5400.69 222.70 o 1 1 3 9564.63 7721.95 347.11 o 2 1 3 1245.45 1247.64 22.83 o 3 1 3 3094.03 3570.77 89.43 o 4 1 3 1476.54 1646.22 38.94 o 5 1 3 226.78 210.64 11.22 o 6 1 3 299.22 345.26 14.45 o 7 1 3 140.82 133.19 15.73 o 8 1 3 30.60 63.78 14.98 o 9 1 3 35.04 48.80 18.94 o 10 1 3 66.64 39.90 20.42 o 11 1 3 83.10 -2.77 25.29 o 0 2 3 13252.10 12313.98 807.05 o 1 2 3 18600.64 18034.10 692.04 o 2 2 3 2060.18 2217.40 120.19 o 3 2 3 139.95 147.04 7.46 o 4 2 3 710.71 734.76 43.54 o 5 2 3 177.96 169.82 26.68 o 6 2 3 527.61 657.79 43.81 o 7 2 3 446.42 616.99 29.96 o 8 2 3 104.38 112.72 22.65 o 9 2 3 26.04 -11.25 30.39 o 10 2 3 29.50 35.63 13.94 o 0 3 3 9902.79 10254.96 712.85 o 1 3 3 1480.91 1280.55 88.30 o 2 3 3 4740.01 4555.82 163.68 o 3 3 3 829.49 868.45 64.48 o 4 3 3 73.71 77.92 10.68 o 5 3 3 1261.93 1514.41 146.36 o 6 3 3 531.31 588.73 16.94 o 7 3 3 301.35 340.74 19.07 o 8 3 3 78.28 107.38 14.94 o 9 3 3 3.13 -26.98 26.98 o 10 3 3 39.58 13.28 26.59 o 0 4 3 1012.46 878.67 104.43 o 1 4 3 1879.53 1749.80 164.04 o 2 4 3 298.82 287.36 26.63 o 3 4 3 1277.75 1348.90 53.39 o 4 4 3 1169.71 1394.95 85.92 o 5 4 3 26.92 59.99 27.59 o 6 4 3 282.78 272.64 15.01 o 7 4 3 649.52 752.56 76.02 o 8 4 3 101.00 125.11 14.20 o 9 4 3 22.39 59.06 19.13 o 10 4 3 44.08 36.19 7.87 o 0 5 3 1512.51 1339.01 152.91 o 1 5 3 79.54 58.06 14.65 o 2 5 3 1433.22 1270.60 99.62 o 3 5 3 472.07 538.43 27.81 o 4 5 3 197.79 201.67 31.47 o 5 5 3 91.85 93.81 11.48 o 6 5 3 58.81 74.92 16.55 o 7 5 3 435.66 420.16 67.45 o 8 5 3 4.74 18.06 24.15 o 9 5 3 128.65 164.07 24.76 o 10 5 3 29.58 19.83 7.07 o 0 6 3 918.30 1026.19 106.02 o 1 6 3 162.97 137.04 15.98 o 2 6 3 344.49 446.40 65.23 o 3 6 3 40.25 33.47 8.83 o 4 6 3 318.68 365.34 37.11 o 5 6 3 531.46 536.75 63.82 o 6 6 3 756.76 777.63 99.26 o 7 6 3 220.93 245.47 30.45 o 8 6 3 4.29 16.26 20.22 o 9 6 3 2.41 -3.48 19.52 o 0 7 3 93.30 97.75 10.41 o 1 7 3 171.01 173.29 11.46 o 2 7 3 180.37 197.02 31.80 o 3 7 3 331.69 300.73 21.64 o 4 7 3 407.02 383.72 36.83 o 5 7 3 81.84 58.31 24.52 o 6 7 3 261.26 298.21 38.24 o 7 7 3 149.29 202.10 36.68 o 8 7 3 20.36 40.00 10.83 o 0 8 3 561.57 618.75 60.85 o 1 8 3 538.67 512.12 60.68 o 2 8 3 299.59 295.50 57.01 o 3 8 3 61.32 39.03 14.10 o 4 8 3 235.28 238.11 14.06 o 5 8 3 3.75 -12.33 23.47 o 6 8 3 112.63 94.08 11.36 o 7 8 3 30.22 14.66 22.29 o 8 8 3 47.32 55.60 13.11 o 0 9 3 395.26 460.32 79.10 o 1 9 3 78.16 66.85 11.00 o 2 9 3 145.29 183.88 13.31 o 3 9 3 57.13 92.52 53.36 o 4 9 3 92.80 90.78 11.75 o 5 9 3 14.43 23.51 41.66 o 6 9 3 36.80 47.72 13.34 o 7 9 3 8.50 -3.36 21.30 o 0 10 3 376.09 339.23 48.22 o 1 10 3 10.11 -3.69 22.89 o 2 10 3 46.65 54.07 11.83 o 3 10 3 21.51 22.07 20.53 o 4 10 3 164.25 158.33 19.70 o 5 10 3 31.28 39.96 33.76 o 6 10 3 45.67 36.65 16.68 o 0 11 3 56.29 61.42 24.15 o 1 11 3 16.58 14.65 9.46 o 2 11 3 74.31 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41 98.84 69.73 16.21 o 1 4 41 24.03 -11.46 20.47 o 2 4 41 17.71 13.07 17.71 o 3 4 41 15.47 26.55 16.18 o 0 5 41 79.72 102.99 10.14 o 1 5 41 19.17 8.01 18.75 o 2 5 41 25.70 33.17 8.63 o 0 0 42 42.45 42.10 10.07 o 1 0 42 73.32 89.57 11.14 o 2 0 42 34.83 41.63 11.21 o 3 0 42 8.57 9.31 14.04 o 4 0 42 0.42 10.91 8.64 o 0 1 42 45.76 40.00 17.31 o 1 1 42 45.55 47.14 14.83 o 2 1 42 77.86 84.29 10.91 o 3 1 42 39.13 45.83 9.95 o 4 1 42 4.91 12.31 8.27 o 0 2 42 5.13 -9.57 21.45 o 1 2 42 4.90 2.42 11.77 o 2 2 42 64.06 56.00 21.98 o 3 2 42 15.65 9.58 19.69 o 4 2 42 11.79 25.57 14.24 o 0 3 42 0.10 3.07 18.11 o 1 3 42 154.36 174.68 45.34 o 2 3 42 13.42 22.23 11.53 o 3 3 42 67.24 106.92 21.88 o 0 4 42 0.01 -12.81 21.32 o 1 4 42 21.34 35.31 9.14 o 2 4 42 44.00 58.57 13.59 o 3 4 42 33.63 55.10 8.87 o 0 5 42 33.94 30.39 8.71 o 1 5 42 16.12 38.63 13.28 o 1 0 43 2.97 4.64 18.71 o 2 0 43 151.60 203.92 20.19 o 3 0 43 15.33 4.20 17.68 o 4 0 43 9.25 20.88 12.51 o 0 1 43 0.74 -2.34 13.11 o 1 1 43 30.93 44.42 9.66 o 2 1 43 46.94 64.36 10.26 o 3 1 43 43.87 56.11 9.00 o 4 1 43 10.26 -26.44 32.42 o 0 2 43 0.21 0.77 15.61 o 1 2 43 40.04 61.36 13.39 o 2 2 43 100.38 113.03 27.47 o 3 2 43 62.63 65.02 12.36 o 0 3 43 24.37 -4.34 20.78 o 1 3 43 4.97 -20.12 20.12 o 2 3 43 7.46 -9.25 21.27 o 3 3 43 3.71 16.26 16.51 o 0 4 43 12.05 22.88 8.81 o 1 4 43 10.82 26.36 39.83 o 2 4 43 1.37 -6.30 10.02 o 0 0 44 8.57 20.95 19.51 o 1 0 44 86.39 86.57 10.58 o 2 0 44 67.91 87.44 22.82 o 3 0 44 28.96 11.74 17.38 o 0 1 44 54.31 62.62 11.48 o 1 1 44 62.70 58.13 9.95 o 2 1 44 32.11 36.63 9.73 o 3 1 44 21.07 32.04 31.24 o 0 2 44 20.31 32.59 9.24 o 1 2 44 3.85 14.08 17.33 o 2 2 44 41.15 47.31 18.38 o 3 2 44 41.19 14.27 19.51 o 0 3 44 12.42 21.92 14.98 o 1 3 44 4.86 16.41 8.36 o 2 3 44 4.85 7.51 10.46 o 1 0 45 89.58 67.96 37.90 o 2 0 45 11.45 14.01 12.88 o 0 1 45 30.58 27.02 15.25 o 1 1 45 54.93 74.65 23.60 o 2 1 45 25.18 22.75 11.23 o 0 2 45 0.07 13.31 18.08 o 1 2 45 0.38 5.75 16.56 o 2 2 45 7.36 5.67 16.56 o 0 3 45 2.99 6.20 16.91 o 0 0 46 30.93 49.30 9.51 o 1 0 46 115.35 148.50 24.92 o 0 1 46 27.17 14.08 17.41 o 1 1 46 18.52 30.96 8.05 o 0 2 46 27.25 6.10 18.45 o