#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/36/2013666.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2013666_Fobs loop_ _publ_author_name 'Wang, Yan' 'Li, Yi-Zhi' 'Jin, Qiong-Hua' 'Zheng, He-Gen' 'Hu, Zheng' 'Xin, Xin-Quan' _publ_section_title ; Tris[diphenyl(2-pyridyl)phosphine]-\m~3~-iodo-tri-\m~3~-sulfido-sulfidotrisilvertungsten dichloromethane hemisolvate ; _journal_issue 10 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first m390 _journal_page_last m391 _journal_volume 59 _journal_year 2003 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 74.860 _cell_angle_beta 87.990 _cell_angle_gamma 64.230 _cell_length_a 12.0450 _cell_length_b 13.3670 _cell_length_c 19.8860 _exptl_crystal_F_000 1534.00 _reflns_d_resolution_high 0.8409 _[local]_cod_data_source_file ob1133Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 21207Am in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 354.34 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 4274.28 4515.60 80.28 o 3 0 0 3103.02 2969.26 74.05 o 4 0 0 10765.86 10837.40 171.43 o 5 0 0 2496.02 2481.93 91.60 o 6 0 0 8210.43 8372.11 190.79 o 7 0 0 57.06 82.20 58.99 o 8 0 0 30.02 73.37 57.75 o 9 0 0 1973.46 2050.77 129.42 o 10 0 0 340.33 427.32 91.15 o 11 0 0 2454.94 2523.26 149.46 o 12 0 0 0.40 9.40 87.41 o -10 1 0 365.34 332.32 84.47 o -9 1 0 1909.57 1962.45 122.06 o -8 1 0 13.84 23.44 57.18 o -7 1 0 3623.69 3734.11 148.89 o -6 1 0 13744.00 15303.41 281.03 o -5 1 0 88.73 157.05 43.82 o -4 1 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