#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/36/2013667.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2013667_Fobs loop_ _publ_author_name 'Thu\'ery, Pierre' 'Takemura, Hiroyuki' _publ_section_title ; A uranyl ion complex of N-methyl-p-tert-butyldihomoammoniocalix[4]arene with diaquadipyridinelithium as counter-ion ; _journal_issue 10 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first m384 _journal_page_last m386 _journal_volume 59 _journal_year 2003 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 96.321 _cell_angle_gamma 90.000 _cell_length_a 20.8644 _cell_length_b 16.6147 _cell_length_c 19.7150 _exptl_crystal_F_000 2896.00 _reflns_d_resolution_high 0.8200 _[local]_cod_data_source_file ob1134Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title 'I in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 701.76 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 3 0 0 106745.12 100976.81 9838.19 o 4 0 0 12784.40 12332.46 1007.57 o 5 0 0 27916.66 27396.75 1834.97 o 6 0 0 41153.32 41657.79 2732.83 o 7 0 0 19511.94 21777.08 1566.22 o 8 0 0 526.26 228.49 460.00 o 9 0 0 39883.12 41686.98 2018.17 o 10 0 0 96303.09 101699.52 4867.76 o 11 0 0 10410.57 12436.14 959.26 o 12 0 0 9895.62 10709.88 971.34 o 13 0 0 63803.70 67218.56 4223.56 o 14 0 0 14121.06 13583.63 1124.34 o 15 0 0 6162.88 6084.70 986.44 o 16 0 0 14324.01 14848.88 1391.08 o 17 0 0 13930.02 17961.19 1387.05 o 18 0 0 174.46 1389.06 1284.38 o 19 0 0 7826.03 8223.65 1051.86 o 20 0 0 6924.44 6537.65 1696.07 o 22 0 0 2317.31 3237.12 992.48 o 23 0 0 7967.98 11504.06 2463.07 o 24 0 0 2884.25 4112.83 977.38 o 25 0 0 326.10 -931.07 931.07 o 3 1 0 1217.71 2019.17 561.66 o 4 1 0 93459.50 96373.79 4108.81 o 5 1 0 9313.83 9720.42 477.11 o 6 1 0 21491.18 23919.06 1222.98 o 7 1 0 23302.16 28573.42 2170.16 o 8 1 0 28871.35 28765.68 1408.19 o 9 1 0 47833.77 51120.53 2418.78 o 10 1 0 5083.79 5001.63 619.04 o 11 1 0 28722.44 29627.30 1222.98 o 12 1 0 41526.73 44119.85 1839.00 o 13 1 0 2925.36 1907.45 582.80 o 14 1 0 12999.69 12752.20 1026.70 o 15 1 0 15131.38 15117.63 824.38 o 16 1 0 1228.85 1055.89 499.26 o 17 1 0 2492.33 3575.33 478.12 o 18 1 0 6313.49 6637.30 789.15 o 19 1 0 2388.38 3099.22 1061.93 o 20 1 0 118.51 -284.86 928.06 o 21 1 0 8718.10 8445.10 1173.66 o 22 1 0 5155.46 5895.46 783.11 o 23 1 0 5.00 -704.60 1010.59 o 24 1 0 3258.43 2953.27 1209.89 o 25 1 0 2746.06 -131.86 1599.44 o 2 2 0 4213.68 4062.51 324.11 o 3 2 0 63104.27 60168.56 2644.25 o 4 2 0 17547.09 19279.79 1189.76 o 5 2 0 7830.86 6599.05 529.45 o 6 2 0 7763.64 9240.29 510.33 o 7 2 0 356.53 975.36 344.25 o 8 2 0 1125.83 474.09 336.19 o 9 2 0 4451.35 5395.20 467.05 o 10 2 0 17781.12 19431.78 1417.25 o 11 2 0 225.12 879.74 685.47 o 12 2 0 2220.79 1261.23 462.01 o 13 2 0 5198.47 5678.05 626.08 o 14 2 0 2631.55 2240.62 539.52 o 15 2 0 2298.76 1798.74 590.85 o 16 2 0 14131.05 13593.69 1019.65 o 17 2 0 2092.44 1945.69 533.48 o 18 2 0 255.70 1038.78 598.91 o 19 2 0 340.56 -562.67 657.29 o 20 2 0 2263.86 2047.36 888.80 o 21 2 0 1223.19 1781.62 725.73 o 22 2 0 336.21 655.28 696.54 o 23 2 0 1918.03 716.68 903.90 o 24 2 0 521.57 1429.33 696.54 o 25 2 0 80.83 2625.13 1979.92 o 1 3 0 25925.64 21774.06 774.05 o 2 3 0 4723.22 5376.08 262.71 o 3 3 0 8522.36 8960.46 381.49 o 4 3 0 38782.21 36814.19 1387.05 o 5 3 0 23496.24 23863.70 908.93 o 6 3 0 11193.24 10805.50 530.46 o 7 3 0 477.09 231.51 328.14 o 8 3 0 598.69 913.96 348.27 o 9 3 0 3947.54 4074.58 494.22 o 10 3 0 2764.67 2716.73 366.39 o 11 3 0 1869.30 2650.29 434.84 o 12 3 0 526.42 72.47 548.58 o 13 3 0 987.70 2042.33 591.86 o 14 3 0 738.19 460.00 660.31 o 15 3 0 213.54 296.94 632.12 o 16 3 0 617.32 1576.28 524.42 o 17 3 0 44.31 -433.83 623.07 o 18 3 0 461.79 -576.76 576.76 o 19 3 0 199.17 846.52 603.94 o 20 3 0 17.85 -617.03 617.03 o 21 3 0 99.20 -534.49 630.11 o 22 3 0 3.38 -101.66 863.63 o 23 3 0 305.56 -220.44 642.19 o 24 3 0 25.90 1038.78 838.47 o 25 3 0 172.73 -1318.60 1601.45 o 0 4 0 26927.39 25375.56 979.39 o 1 4 0 4794.41 4795.29 246.61 o 2 4 0 21259.45 20088.06 650.24 o 3 4 0 32399.65 29830.63 1187.75 o 4 4 0 3313.03 2437.91 239.56 o 5 4 0 4854.35 5085.18 313.04 o 6 4 0 167.33 -3.02 282.85 o 7 4 0 376.43 350.29 353.31 o 8 4 0 534.68 376.46 322.10 o 9 4 0 5668.97 5553.23 461.01 o 10 4 0 7733.94 9431.54 814.31 o 11 4 0 7619.70 7240.24 490.20 o 12 4 0 937.78 1496.77 585.82 o 13 4 0 2695.95 2707.67 483.15 o 14 4 0 2754.32 3596.46 665.34 o 15 4 0 86.03 559.65 697.55 o 16 4 0 3756.43 4835.55 875.71 o 17 4 0 445.82 1205.87 581.80 o 18 4 0 548.12 633.13 745.87 o 19 4 0 608.65 614.01 524.42 o 20 4 0 112.68 -363.37 738.82 o 21 4 0 1435.80 436.85 668.36 o 22 4 0 108.92 -485.17 680.44 o 23 4 0 1981.83 1335.71 910.94 o 24 4 0 433.69 -338.21 625.08 o 1 5 0 41395.33 36694.41 1153.53 o 2 5 0 98928.99 87370.04 2740.88 o 3 5 0 2155.26 2012.13 220.44 o 4 5 0 3549.96 4508.42 275.80 o 5 5 0 50580.77 49471.77 1826.92 o 6 5 0 3940.77 4356.42 306.00 o 7 5 0 2699.28 3273.36 333.17 o 8 5 0 9925.71 9632.85 501.27 o 9 5 0 32527.56 32387.31 1296.46 o 10 5 0 1303.78 564.68 424.77 o 11 5 0 9167.27 8569.91 584.82 o 12 5 0 25861.40 25606.07 1413.22 o 13 5 0 834.22 746.87 616.02 o 14 5 0 3208.55 3041.85 543.55 o 15 5 0 18929.63 19066.40 942.15 o 16 5 0 1603.68 1745.39 522.41 o 17 5 0 3162.39 3894.41 585.82 o 18 5 0 10177.50 10127.07 1020.66 o 19 5 0 5986.91 6776.21 703.59 o 20 5 0 81.13 465.03 595.89 o 21 5 0 3117.00 2411.74 817.33 o 22 5 0 2063.56 1932.61 927.05 o 23 5 0 356.83 775.06 870.68 o 24 5 0 1304.03 987.44 835.45 o 0 6 0 84904.73 76762.83 3088.15 o 1 6 0 17018.21 15770.89 475.10 o 2 6 0 131.34 230.50 188.23 o 3 6 0 51390.38 49368.10 1797.73 o 4 6 0 29752.46 25811.40 920.00 o 5 6 0 4497.68 5391.17 328.14 o 6 6 0 22390.11 22537.04 782.10 o 7 6 0 7543.59 7167.77 369.41 o 8 6 0 4577.64 5444.52 462.01 o 9 6 0 14392.22 15824.24 844.51 o 10 6 0 18660.12 17262.63 905.91 o 11 6 0 7062.42 6976.52 523.41 o 12 6 0 9749.63 9525.15 594.88 o 13 6 0 22272.55 22268.29 1023.68 o 14 6 0 13495.57 13152.81 871.69 o 15 6 0 421.42 -405.65 605.95 o 16 6 0 14212.03 13203.14 924.03 o 17 6 0 8394.40 9326.85 793.17 o 18 6 0 272.65 127.83 542.54 o 19 6 0 8025.01 9575.47 876.72 o 20 6 0 6977.02 7570.39 830.42 o 21 6 0 2423.11 4048.41 768.01 o 22 6 0 2745.05 2647.27 748.89 o 23 6 0 4629.83 3444.47 845.52 o 24 6 0 2529.90 2901.93 944.16 o 1 7 0 62654.36 59753.86 1583.33 o 2 7 0 48718.14 44900.95 1201.84 o 3 7 0 4915.23 4616.12 272.78 o 4 7 0 11168.51 9934.82 396.59 o 5 7 0 51140.38 48806.43 1594.40 o 6 7 0 15853.98 16492.61 634.14 o 7 7 0 24592.23 25780.20 854.58 o 8 7 0 39100.64 37830.82 1198.82 o 9 7 0 11813.17 11173.90 538.51 o 10 7 0 1898.52 1574.27 497.24 o 11 7 0 33613.07 34488.02 1514.88 o 12 7 0 11931.19 13157.85 708.62 o 13 7 0 368.43 -500.26 500.26 o 14 7 0 6539.09 7740.50 618.03 o 15 7 0 30426.65 30227.21 1480.66 o 16 7 0 2041.29 2649.28 532.47 o 17 7 0 5583.81 4752.00 739.83 o 18 7 0 15513.95 15495.10 979.39 o 19 7 0 2536.00 1749.41 560.66 o 20 7 0 304.89 437.86 597.90 o 21 7 0 6516.66 5254.28 704.60 o 22 7 0 3394.55 4644.30 992.48 o 23 7 0 154.99 -497.24 580.79 o 0 8 0 57026.39 56034.59 1796.72 o 1 8 0 14530.28 14464.37 446.92 o 2 8 0 11081.77 10968.56 376.46 o 3 8 0 52816.68 50197.51 1347.79 o 4 8 0 26135.88 24260.29 811.29 o 5 8 0 5587.92 5929.69 371.42 o 6 8 0 35314.24 36025.04 1183.72 o 7 8 0 24752.63 24943.74 777.07 o 8 8 0 67.75 469.06 309.02 o 9 8 0 13047.90 13377.28 698.56 o 10 8 0 12791.52 12808.57 595.89 o 11 8 0 2753.97 1797.73 416.72 o 12 8 0 7911.01 7541.20 582.80 o 13 8 0 15309.63 14362.71 820.35 o 14 8 0 7465.09 8404.84 669.37 o 15 8 0 399.42 256.67 544.55 o 16 8 0 12093.44 12603.23 1036.76 o 17 8 0 5994.95 5643.82 833.44 o 18 8 0 176.04 -30.20 571.73 o 19 8 0 2348.87 1240.09 570.72 o 20 8 0 2488.96 2895.89 694.53 o 21 8 0 67.76 -349.28 720.70 o 22 8 0 1862.87 2257.73 723.72 o 23 8 0 2720.00 2325.17 995.50 o 1 9 0 11261.20 12313.34 455.97 o 2 9 0 2059.37 1804.78 258.69 o 3 9 0 1278.14 1046.83 273.79 o 4 9 0 3642.70 3883.34 292.91 o 5 9 0 15470.83 14709.97 559.65 o 6 9 0 665.21 714.66 299.96 o 7 9 0 1623.79 2442.94 314.05 o 8 9 0 4734.32 4505.40 390.55 o 9 9 0 608.72 842.50 346.26 o 10 9 0 3132.05 3014.67 395.58 o 11 9 0 1900.39 1488.71 568.71 o 12 9 0 197.13 -190.24 448.93 o 13 9 0 2.61 -158.03 494.22 o 14 9 0 345.44 35.23 475.10 o 15 9 0 1608.13 1431.34 526.43 o 16 9 0 286.75 722.72 492.21 o 17 9 0 14.10 -74.49 838.47 o 18 9 0 459.21 810.29 634.14 o 19 9 0 331.19 927.05 703.59 o 20 9 0 17.41 -480.13 727.75 o 21 9 0 1096.75 -125.82 735.80 o 22 9 0 465.89 183.20 722.72 o 0 10 0 2296.01 2804.30 400.61 o 1 10 0 159.55 506.30 280.83 o 2 10 0 2565.32 2711.69 265.73 o 3 10 0 2191.80 2198.34 268.75 o 4 10 0 1191.14 774.05 321.09 o 5 10 0 1016.65 1071.99 286.87 o 6 10 0 42.94 -127.83 300.96 o 7 10 0 146.17 -82.54 338.21 o 8 10 0 90.30 -99.65 348.27 o 9 10 0 509.04 965.30 386.52 o 10 10 0 1411.35 1936.64 477.11 o 11 10 0 5513.66 4988.55 537.51 o 12 10 0 71.65 761.97 522.41 o 13 10 0 2929.09 1488.71 564.68 o 14 10 0 12.03 -441.88 489.19 o 15 10 0 2346.69 2582.85 559.65 o 16 10 0 1614.42 197.29 643.20 o 17 10 0 50.46 -329.15 454.97 o 18 10 0 11.69 -231.51 574.75 o 19 10 0 68.11 -9.06 650.24 o 20 10 0 43.51 822.37 694.53 o 21 10 0 100.10 648.23 752.91 o 1 11 0 7351.84 6954.37 438.86 o 2 11 0 3165.72 3264.30 311.03 o 3 11 0 29.49 -240.57 269.76 o 4 11 0 5733.32 5867.28 358.34 o 5 11 0 14285.14 12570.01 546.57 o 6 11 0 3480.55 3450.51 375.45 o 7 11 0 864.81 359.34 331.16 o 8 11 0 9943.84 9900.60 565.69 o 9 11 0 4098.52 3005.61 511.34 o 10 11 0 1689.36 2075.54 431.82 o 11 11 0 1423.26 1668.89 419.74 o 12 11 0 2535.90 2665.39 542.54 o 13 11 0 7.39 728.75 535.49 o 14 11 0 5250.82 5107.32 667.35 o 15 11 0 4777.75 3631.69 597.90 o 16 11 0 881.18 908.93 591.86 o 17 11 0 739.78 458.99 607.97 o 18 11 0 3612.22 3397.16 748.89 o 19 11 0 1427.86 1622.59 609.98 o 20 11 0 33.31 -781.10 781.10 o 21 11 0 1275.02 256.67 610.99 o 0 12 0 41351.96 39184.66 2194.32 o 1 12 0 5613.32 5726.36 382.50 o 2 12 0 1460.22 1773.57 316.06 o 3 12 0 10178.13 9558.36 463.02 o 4 12 0 17009.04 16728.14 654.27 o 5 12 0 42.08 113.74 307.00 o 6 12 0 9519.52 9061.12 484.16 o 7 12 0 5025.43 5605.57 429.80 o 8 12 0 2233.76 2227.53 451.95 o 9 12 0 5751.05 5097.26 479.13 o 10 12 0 6776.44 7201.99 535.49 o 11 12 0 810.00 308.01 523.41 o 12 12 0 148.85 425.78 409.67 o 13 12 0 12092.07 12409.97 831.42 o 14 12 0 8839.60 10059.63 767.00 o 15 12 0 361.19 1014.62 527.44 o 16 12 0 5207.90 5211.00 653.26 o 17 12 0 6513.75 6571.88 762.98 o 18 12 0 231.12 -35.23 571.73 o 19 12 0 2808.48 1925.56 591.86 o 20 12 0 4007.90 2999.57 718.69 o 1 13 0 15875.50 15930.94 658.29 o 2 13 0 31599.65 30746.60 1149.50 o 3 13 0 4758.32 4948.28 388.53 o 4 13 0 11634.38 11393.34 589.85 o 5 13 0 15579.18 15572.60 701.58 o 6 13 0 4703.78 4501.37 390.55 o 7 13 0 2489.60 1776.59 391.55 o 8 13 0 12700.78 12667.65 637.16 o 9 13 0 11443.04 11378.24 554.62 o 10 13 0 51.62 748.89 391.55 o 11 13 0 9770.15 10745.11 619.04 o 12 13 0 10935.62 11145.72 701.58 o 13 13 0 1099.15 377.46 605.95 o 14 13 0 2698.64 2750.95 685.47 o 15 13 0 9691.84 11367.16 817.33 o 16 13 0 2336.10 1874.23 798.21 o 17 13 0 825.91 1191.78 649.24 o 18 13 0 4682.82 3845.09 698.56 o 19 13 0 1775.02 1900.40 677.42 o 0 14 0 13232.08 13004.85 854.58 o 1 14 0 3045.46 2893.88 337.20 o 2 14 0 896.99 901.88 368.40 o 3 14 0 8631.13 9033.94 588.84 o 4 14 0 11264.44 12359.64 784.12 o 5 14 0 1587.85 1568.23 385.52 o 6 14 0 8343.55 8344.44 692.52 o 7 14 0 6412.91 5771.66 569.72 o 8 14 0 448.22 175.14 350.29 o 9 14 0 4473.26 4760.06 501.27 o 10 14 0 12973.92 12642.48 644.20 o 11 14 0 1215.02 1683.99 458.99 o 12 14 0 1322.28 931.07 488.19 o 13 14 0 3806.34 4620.14 663.33 o 14 14 0 3170.82 2658.34 579.78 o 15 14 0 363.11 495.23 504.29 o 16 14 0 2788.17 711.64 659.30 o 17 14 0 4610.09 3907.49 661.31 o 18 14 0 210.96 1173.66 928.06 o 1 15 0 6052.68 6854.72 426.78 o 2 15 0 2143.87 2323.16 356.32 o 3 15 0 3364.54 3403.20 401.62 o 4 15 0 427.93 666.35 432.82 o 5 15 0 8342.03 7644.88 581.80 o 6 15 0 399.99 1335.71 484.16 o 7 15 0 808.42 1520.92 527.44 o 8 15 0 2158.37 1536.02 413.70 o 9 15 0 1301.38 1876.24 452.96 o 10 15 0 211.69 112.74 433.83 o 11 15 0 1930.37 1640.70 495.23 o 12 15 0 2563.25 2320.14 496.24 o 13 15 0 169.44 236.54 688.49 o 14 15 0 1299.65 1280.35 549.59 o 15 15 0 1150.71 1294.45 601.93 o 16 15 0 676.33 354.31 655.28 o 17 15 0 29.90 1311.56 593.87 o 0 16 0 554.47 828.40 474.09 o 1 16 0 23.66 248.62 361.36 o 2 16 0 125.00 -6.04 435.84 o 3 16 0 367.27 -235.54 464.03 o 4 16 0 87.85 481.14 413.70 o 5 16 0 347.98 -89.58 476.11 o 6 16 0 601.21 853.57 507.31 o 7 16 0 28.87 -398.60 398.60 o 8 16 0 31.34 -187.22 468.05 o 9 16 0 18.86 -424.77 424.77 o 10 16 0 233.96 -203.33 493.22 o 11 16 0 100.94 -189.23 484.16 o 12 16 0 301.93 -126.83 448.93 o 13 16 0 148.81 330.15 471.07 o 14 16 0 34.62 -113.74 556.63 o 15 16 0 83.88 -589.85 589.85 o 1 17 0 1302.02 1433.35 441.88 o 2 17 0 2112.90 2362.41 447.92 o 3 17 0 122.15 82.54 386.52 o 4 17 0 2398.75 3316.64 533.48 o 5 17 0 3343.58 4109.81 575.76 o 6 17 0 977.88 822.37 464.03 o 7 17 0 419.13 369.41 516.37 o 8 17 0 1831.24 1471.60 532.47 o 9 17 0 386.77 523.41 462.01 o 10 17 0 12.97 540.53 518.38 o 11 17 0 456.29 -45.30 489.19 o 12 17 0 1504.96 881.75 514.36 o 13 17 0 2.70 -315.06 588.84 o 0 18 0 8461.87 9617.75 1239.08 o 1 18 0 4446.69 4876.82 634.14 o 2 18 0 706.15 221.44 472.08 o 3 18 0 8324.04 8886.98 743.85 o 4 18 0 3120.24 3405.22 497.24 o 5 18 0 41.78 335.19 534.49 o 6 18 0 4387.67 3819.92 552.61 o 7 18 0 5406.54 5601.55 615.01 o 8 18 0 399.83 532.47 593.87 o 9 18 0 1267.47 348.27 542.54 o 10 18 0 3530.73 4496.34 563.68 o 11 18 0 1452.50 795.19 562.67 o 1 19 0 5610.53 7120.46 702.58 o 2 19 0 4579.15 5306.62 591.86 o 3 19 0 34.95 58.38 419.74 o 4 19 0 1993.29 1524.95 662.32 o 5 19 0 4265.53 4927.15 670.37 o 6 19 0 2110.80 2134.93 599.91 o 7 19 0 763.13 370.42 582.80 o 8 19 0 4363.98 3094.19 553.61 o 0 20 0 4388.55 5390.17 832.43 o 1 20 0 1829.58 1981.93 599.91 o 2 20 0 605.95 555.63 647.22 o 3 20 0 5097.37 4796.29 572.74 o 4 20 0 2265.37 2341.28 690.51 o -25 1 1 452.21 -2225.52 2225.52 o -24 1 1 595.00 1658.82 652.26 o -23 1 1 3.93 -472.08 614.01 o -22 1 1 1640.04 1171.64 671.38 o -21 1 1 1630.25 1436.37 586.83 o -20 1 1 673.63 187.22 766.00 o -19 1 1 940.82 1217.95 536.50 o -18 1 1 7062.79 6750.04 807.27 o -17 1 1 418.99 -463.02 463.02 o -16 1 1 306.54 162.06 621.05 o -15 1 1 3736.80 4264.83 563.68 o -14 1 1 124.31 253.65 516.37 o -13 1 1 507.97 1170.64 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