#------------------------------------------------------------------------------
#$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $
#$Revision: 26848 $
#$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/36/2013668.hkl $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2013668_Fobs
loop_
_publ_author_name
'Koshiyama, Tamami'
'Kato, Masako'
_publ_section_title
;
[(1R,2R)-1,2-Diaminocyclohexane-\k^2^N,N'](\a-diimine-\k^2^N,N')platinum(II)
bis(hexafluorophosphate), where \a-diimine is 2,2'-bipyridine and
1,10-phenanthroline
;
_journal_issue 11
_journal_name_full 'Acta Crystallographica Section C'
_journal_page_first m446
_journal_page_last m449
_journal_volume 59
_journal_year 2003
_space_group_IT_number 5
_symmetry_space_group_name_Hall 'C 2y'
_symmetry_space_group_name_H-M 'C 1 2 1'
_[local]_cod_data_source_file ob1141Isup2.hkl
_[local]_cod_data_source_block I
loop_
_refln_index_h
_refln_index_k
_refln_index_l
_refln_F_squared_meas
_refln_F_squared_sigma
_refln_F_squared_calc
_refln_observed_status
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2 0 -1 31.85 12.72 54.86 o
2 2 0 259.49 47.31 546.23 o
2 0 1 62.91 25.08 119.69 o
1 3 0 13552.93 1109.10 12035.89 o
3 1 0 7573.47 645.79 9433.26 o
2 -2 -1 30932.84 2216.68 31735.08 o
2 2 1 32992.64 2269.84 32599.21 o
1 3 -1 12411.24 1060.03 13318.48 o
1 3 1 31879.47 2197.68 31320.69 o
0 4 0 5058.59 368.25 5114.87 o
1 1 -2 1180.19 135.41 1382.93 o
4 0 0 16710.64 1137.74 15453.56 o
1 1 2 32428.43 2595.38 25658.88 o
2 4 0 31341.79 2098.31 28190.52 o
2 0 -2 23694.97 1753.60 25885.23 o
0 2 2 81534.74 5806.90 74443.21 o
4 0 -1 165.53 64.07 16.28 o
3 3 -1 13287.89 1155.73 14967.82 o
4 2 0 3337.65 281.05 2806.58 o
2 4 -1 32086.41 2353.67 33076.76 o
3 3 1 7802.49 717.22 7138.37 o
4 0 1 140.66 39.43 138.68 o
2 2 -2 3961.04 341.56 3890.75 o
2 4 1 35987.58 2814.68 31700.62 o
1 5 0 3858.62 384.68 4929.73 o
4 -2 -1 37502.43 2587.92 37232.02 o
-1 3 2 88767.91 6366.91 69995.85 o
2 2 2 4767.02 375.36 3502.56 o
3 1 -2 27122.11 2066.58 24610.17 o
1 3 2 12978.75 1248.23 15104.02 o
4 2 1 44320.54 3673.31 41922.74 o
1 5 -1 49368.00 4037.12 49547.51 o
1 5 1 57602.30 4854.19 58569.44 o
3 1 2 61105.55 4177.47 49603.73 o
5 1 0 20938.24 1331.38 15372.46 o
0 4 2 6872.70 530.67 5950.48 o
5 1 -1 17918.44 1396.47 21103.65 o
0 6 0 37780.78 3097.71 38243.47 o
4 0 -2 34345.89 2712.54 34751.93 o
4 4 0 33953.37 2580.28 37790.73 o
3 5 0 24805.09 1920.21 29174.99 o
-3 3 2 80857.77 6140.67 77376.02 o
2 4 -2 23419.86 1705.39 24410.46 o
5 1 1 49565.55 3553.78 47616.04 o
4 4 -1 18897.34 1706.49 16183.31 o
3 3 2 40534.48 2778.95 36092.29 o
4 2 -2 9141.31 652.29 9127.70 o
3 5 -1 32520.50 2617.12 30611.90 o
2 4 2 22043.67 1690.77 20480.13 o
4 0 2 111113.17 8370.68 106951.16 o
0 0 3 182.04 41.84 345.67 o
0 6 1 3892.00 360.23 5612.92 o
5 3 0 38881.50 2760.15 34420.82 o
2 6 0 52698.83 3440.21 44094.90 o
3 5 1 38172.59 2570.53 34880.52 o
4 4 1 44653.86 3099.33 41516.86 o
1 1 -3 44303.86 3585.36 48793.36 o
1 1 3 62071.45 4811.53 58625.77 o
1 5 -2 9357.16 854.38 8483.20 o
5 3 -1 3494.84 270.49 3938.40 o
2 0 -3 362.02 50.43 365.26 o
4 2 2 10259.96 780.91 8263.44 o
0 2 3 35748.92 2638.18 31576.39 o
1 5 2 1994.60 177.31 2640.64 o
2 6 -1 2957.16 225.43 2562.73 o
6 0 0 26302.55 2031.38 24126.02 o
2 6 1 8876.77 660.08 9225.63 o
5 3 1 258.90 46.46 365.36 o
2 0 3 125.04 41.68 84.97 o
2 2 -3 53691.50 3956.49 54018.88 o
5 1 -2 23454.24 1729.95 23506.05 o
6 0 -1 251.76 57.62 260.34 o
6 2 0 5174.28 483.74 4510.00 o
1 3 -3 891.81 93.56 992.62 o
1 7 0 3120.16 284.48 4365.17 o
3 1 -3 13583.84 1188.29 17444.96 o
2 -2 3 94364.57 7217.96 87942.12 o
1 3 3 95.16 64.41 334.91 o
6 0 1 532.63 89.35 549.99 o
4 4 -2 9055.57 619.77 6352.00 o
6 -2 -1 65599.12 4530.25 64721.98 o
3 5 -2 27789.22 2202.49 31326.99 o
5 1 2 8297.21 656.57 7701.53 o
0 6 2 63382.40 4449.09 53710.38 o
1 7 -1 31766.96 2564.23 31853.45 o
1 7 1 41855.77 3218.56 39495.93 o
6 2 1 58624.57 4672.84 56008.95 o
3 5 2 10252.37 769.15 10376.48 o
4 4 2 18632.36 1373.34 18566.12 o
0 4 3 33185.73 2583.20 32645.58 o
5 5 0 3489.27 297.21 3095.64 o
4 0 -3 989.50 111.51 736.69 o
3 3 -3 2203.07 178.93 1892.06 o
4 6 -1 6061.48 501.90 6214.28 o
5 -5 -1 83496.84 6410.71 78663.20 o
2 4 -3 35774.29 2921.90 37435.74 o
2 6 2 43415.95 2974.12 42095.15 o
6 0 -2 11422.58 933.45 15679.68 o
3 7 0 28928.23 1998.55 23047.36 o
5 3 2 77062.08 5674.96 67783.79 o
4 2 -3 24214.56 1586.20 20038.12 o
6 4 0 16955.43 1223.92 11755.38 o
4 6 1 1663.75 176.60 2208.37 o
5 5 1 26081.52 2402.14 24923.78 o
7 1 0 18945.78 1379.88 17879.75 o
2 -4 3 103303.79 7269.14 90444.27 o
3 3 3 2999.09 249.40 2458.39 o
0 8 0 9543.38 821.44 12065.39 o
4 0 3 125.53 77.50 214.21 o
3 7 -1 80405.84 5764.78 60389.87 o
6 2 -2 31706.12 2135.06 28607.88 o
6 -4 -1 64404.68 5151.15 66781.23 o
7 1 -1 25713.43 1817.88 22058.36 o
3 7 1 39852.10 3686.53 39208.75 o
1 5 -3 48253.41 3839.07 49193.18 o
6 0 2 14392.80 1127.04 16936.10 o
1 5 3 20723.62 1483.20 20139.79 o
1 7 -2 27110.83 2327.38 29614.37 o
6 4 1 51467.97 3505.09 49238.20 o
4 2 3 23780.94 1565.48 19782.82 o
0 8 1 67316.45 5243.50 58170.17 o
1 7 2 11146.15 895.36 11027.73 o
2 8 0 1294.07 113.86 935.32 o
5 1 -3 26868.19 2444.08 23659.89 o
7 1 1 54781.66 4267.66 51393.00 o
6 2 2 6010.98 486.65 7846.65 o
7 3 0 75050.42 5186.86 74371.14 o
0 0 4 50567.85 4327.23 59717.69 o
5 5 -2 12701.12 937.95 10587.96 o
4 6 -2 65959.69 5042.04 57190.69 o
2 8 -1 40331.99 3193.73 44294.00 o
1 1 -4 21325.47 1609.42 18302.18 o
4 4 -3 5911.17 473.93 8045.10 o
7 3 -1 1565.35 142.75 1836.67 o
2 8 1 48980.65 3760.46 39223.34 o
3 5 -3 63378.88 4776.74 55330.36 o
2 0 -4 39372.67 3019.82 34385.15 o
1 1 4 1109.04 106.52 738.68 o
0 2 4 22803.81 1556.57 21244.56 o
6 4 -2 9869.75 855.97 12426.50 o
4 6 2 64638.86 4690.91 62521.99 o
0 6 3 952.25 118.89 907.53 o
3 7 -2 16818.06 1189.81 14964.71 o
5 3 -3 4636.16 360.79 5468.47 o
5 1 3 45246.97 3483.88 45108.85 o
7 1 -2 1497.68 162.94 2213.08 o
5 5 2 9128.95 708.07 8694.45 o
7 3 1 300.90 80.33 247.51 o
2 2 -4 7347.59 571.85 6333.42 o
2 0 4 70758.39 6087.81 78091.85 o
3 5 3 10450.76 762.02 10213.38 o
2 6 -3 3195.04 251.97 2514.33 o
3 7 2 5776.11 555.72 5797.49 o
4 4 3 13284.89 979.50 12692.07 o
5 7 0 63672.27 5027.96 58657.55 o
8 0 0 19105.65 1545.61 18777.93 o
3 1 -4 8309.75 623.71 9575.49 o
1 3 -4 64853.56 4740.07 64380.59 o
6 0 -3 91.75 49.82 113.38 o
6 6 0 77326.34 5323.96 68065.95 o
0 8 2 7205.13 573.51 6715.49 o
1 9 0 34870.18 2802.58 36721.08 o
6 4 2 11178.73 848.91 10152.22 o
2 2 4 3884.35 318.21 4233.92 o
2 6 3 812.86 121.40 597.13 o
1 3 4 22460.91 1640.06 21693.49 o
8 0 -1 218.10 68.22 235.11 o
5 7 -1 58564.67 4317.90 49909.13 o
4 8 0 20224.32 1823.17 16954.28 o
6 6 -1 2179.47 209.07 3479.48 o
7 1 2 18419.30 1450.38 17424.74 o
8 2 0 30041.88 2281.20 24773.10 o
6 2 -3 41824.06 3197.20 40924.82 o
5 3 3 2565.21 226.05 2467.47 o
7 3 -2 20737.52 1559.24 25582.71 o
2 8 -2 5213.04 458.95 6015.66 o
1 9 -1 2910.06 237.07 3640.24 o
5 7 1 33798.34 2347.57 26897.53 o
7 5 0 3515.02 275.60 2685.13 o
1 9 1 107.89 99.47 87.47 o
8 2 -1 33133.35 2306.21 33539.43 o
3 1 4 22239.38 1509.10 15823.17 o
4 8 -1 51723.54 3839.86 53058.06 o
6 6 1 2868.72 272.75 3958.40 o
8 0 1 567.30 83.60 0.12 o
4 0 -4 17111.33 1447.17 17011.85 o
0 4 4 1847.39 189.52 2019.73 o
2 8 2 3501.93 316.83 4027.68 o
3 3 -4 52088.57 4054.50 61489.83 o
7 5 -1 69944.01 5492.49 68081.03 o
4 8 1 43103.30 3143.49 46126.75 o
1 7 -3 55931.71 4528.11 56858.00 o
2 4 -4 13355.38 940.84 13466.33 o
6 0 3 84.16 56.48 244.38 o
1 7 3 16468.30 1404.26 18522.23 o
8 2 1 30577.91 2386.85 28584.10 o
4 2 -4 23726.91 1897.75 22442.74 o
3 9 0 32004.67 2443.75 31702.45 o
7 3 2 47295.74 3731.74 46451.41 o
7 5 1 84026.77 6619.28 76314.01 o
4 6 -3 14800.37 996.25 13019.73 o
8 0 -2 15778.69 1371.46 19792.52 o
6 2 3 32870.03 2527.87 33452.91 o
2 4 4 51933.30 3582.02 43165.54 o
3 3 4 23418.16 1690.73 21721.23 o
5 7 -2 24552.57 1916.71 23228.68 o
3 9 -1 5232.42 402.92 4222.15 o
6 6 -2 34264.38 2427.01 33177.44 o
4 0 4 114104.11 9183.27 93497.16 o
8 4 0 12751.98 1023.76 13231.57 o
1 5 -4 21550.69 1822.41 21853.40 o
6 4 -3 52075.42 4767.92 48175.15 o
3 9 1 834.61 119.33 694.65 o
7 1 -3 22105.23 1729.55 23846.95 o
3 7 -3 44867.14 3403.82 42419.15 o
8 2 -2 5564.35 405.19 5034.09 o
5 1 -4 9853.61 871.49 11192.03 o
1 5 4 121.44 61.40 260.75 o
8 4 -1 27364.05 2073.93 25637.60 o
1 9 -2 30255.63 2495.20 32678.98 o
0 10 0 33856.60 2331.15 26098.23 o
4 6 3 13225.90 1086.87 10917.14 o
4 8 -2 3429.51 280.11 4073.30 o
4 2 4 1112.12 125.69 959.12 o
1 9 2 56079.94 4443.93 57191.48 o
5 5 3 65122.98 4598.45 56231.03 o
7 5 -2 352.79 51.96 256.59 o
5 7 2 33835.46 2673.81 30495.52 o
6 6 2 69171.43 5403.56 60294.50 o
3 7 3 10906.42 858.62 9835.43 o
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3 9 2 35793.55 2437.78 33275.20 o
0 0 5 464.91 77.21 23.60 o
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6 2 -4 9613.05 660.74 8001.91 o
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2 6 4 102766.82 7531.85 84921.77 o
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1 1 5 14864.21 1390.60 14737.04 o
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5 7 -3 60883.57 4414.30 60408.77 o
6 6 -3 5532.40 404.87 4617.35 o
7 3 3 1807.27 226.64 3058.72 o
7 7 1 69069.25 5527.84 62828.89 o
0 10 2 16259.59 1272.27 13352.05 o
5 3 4 53978.31 3810.47 48879.00 o
9 3 1 1832.36 171.40 1908.95 o
5 9 1 14251.93 1063.74 12059.99 o
2 2 -5 27966.33 1932.43 27117.02 o
8 2 -3 40660.61 3145.83 36596.29 o
8 4 2 8278.39 697.85 7308.70 o
8 6 -1 1016.96 116.82 1093.66 o
2 0 5 37.56 37.89 72.94 o
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14 2 -8 240.37 170.64 190.74 o
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15 15 -1 1195.11 220.68 1499.19 o
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1 17 7 6196.01 579.35 5997.73 o
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1 -21 -4 6424.17 546.08 5096.26 o
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