#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/37/2013729.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2013729_Fobs loop_ _publ_author_name 'Fridman, Natalya' 'Kapon, Moshe' 'Kaftory, Menahem' _publ_section_title ; Two dimorphs of 5-methylsulfanyl-1H-tetrazole ; _journal_issue 1 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first o47 _journal_page_last o49 _journal_volume 60 _journal_year 2004 _space_group_IT_number 11 _symmetry_space_group_name_Hall '-P 2yb' _symmetry_space_group_name_H-M 'P 1 21/m 1' _cell_angle_alpha 90.000 _cell_angle_beta 96.983 _cell_angle_gamma 90.000 _cell_length_a 5.0410 _cell_length_b 6.5470 _cell_length_c 7.2475 _exptl_crystal_F_000 120.00 _reflns_d_resolution_high 0.8256 _[local]_cod_data_source_file av1152Iasup2.hkl _[local]_cod_data_source_block Ia #BEGIN Tags that were not found in dictionaries: _shelx_title ' Thiomethoxy Tetrazol P21/m' _shelx_refln_list_code 4 _shelx_f_calc_maximum 79.92 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z' '-x, -y, -z' 'x, -y-1/2, z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 1321.05 1197.00 39.97 o 2 0 0 9.52 8.81 0.44 o 3 0 0 53.59 56.92 1.56 o 4 0 0 128.84 131.28 4.07 o 5 0 0 147.60 151.82 5.08 o 6 0 0 40.09 40.77 2.61 o 1 1 0 691.83 759.48 15.60 o 2 1 0 173.73 168.94 3.65 o 3 1 0 430.66 450.52 7.98 o 4 1 0 79.46 74.37 1.64 o 5 1 0 28.98 30.58 1.61 o 6 1 0 12.23 13.17 1.54 o 0 2 0 6386.75 4414.82 174.80 o 1 2 0 757.49 811.20 12.99 o 2 2 0 12.65 13.70 0.30 o 3 2 0 25.52 25.40 0.59 o 4 2 0 95.06 96.15 2.10 o 5 2 0 110.94 117.47 3.06 o 1 3 0 289.75 305.90 4.82 o 2 3 0 63.33 58.31 0.97 o 3 3 0 212.94 220.19 4.29 o 4 3 0 44.07 46.42 1.08 o 5 3 0 19.64 19.99 0.77 o 0 4 0 1288.33 1375.01 43.47 o 1 4 0 221.82 229.33 4.51 o 2 4 0 7.90 8.60 0.31 o 3 4 0 5.28 6.00 0.42 o 4 4 0 42.63 41.37 1.23 o 5 4 0 49.18 44.98 1.52 o 1 5 0 66.88 68.60 1.56 o 2 5 0 21.46 21.25 0.49 o 3 5 0 64.28 65.63 2.20 o 4 5 0 12.41 13.01 0.91 o 0 6 0 257.05 266.76 13.39 o 1 6 0 50.56 50.62 1.33 o 2 6 0 2.16 2.04 0.47 o 3 6 0 1.09 1.24 0.35 o 1 7 0 12.09 12.66 1.02 o 2 7 0 4.87 4.83 0.73 o -6 0 1 59.32 61.08 3.43 o -5 0 1 58.77 58.95 1.94 o -4 0 1 0.10 0.00 0.63 o -3 0 1 16.79 15.64 0.70 o -2 0 1 146.12 144.10 3.72 o -1 0 1 1.07 1.55 0.20 o 0 0 1 227.43 216.68 5.96 o 1 0 1 17.14 16.26 0.45 o 2 0 1 556.30 595.95 15.12 o 3 0 1 412.47 423.87 10.66 o 4 0 1 1.39 2.35 0.79 o 5 0 1 2.08 2.57 1.06 o -6 1 1 10.21 10.49 1.30 o -5 1 1 74.41 77.48 1.94 o -4 1 1 133.30 127.13 2.53 o -3 1 1 451.64 483.63 8.44 o -2 1 1 452.67 492.60 9.08 o -1 1 1 774.15 843.33 16.68 o 0 1 1 279.82 275.16 5.32 o 1 1 1 1.88 1.89 0.09 o 2 1 1 539.20 540.10 8.99 o 3 1 1 6.74 6.03 0.38 o 4 1 1 20.09 24.56 0.81 o 5 1 1 5.57 7.61 0.56 o -5 2 1 44.88 45.41 4.87 o -4 2 1 0.41 0.23 0.46 o -3 2 1 10.03 9.04 0.63 o -2 2 1 89.68 88.50 1.71 o -1 2 1 10.41 9.80 0.19 o 0 2 1 157.46 172.24 2.98 o 1 2 1 4.33 3.93 0.17 o 2 2 1 300.95 319.62 5.29 o 3 2 1 299.60 320.95 6.14 o 4 2 1 0.95 1.53 0.40 o 5 2 1 1.03 1.96 0.50 o -5 3 1 44.35 45.89 1.27 o -4 3 1 80.17 82.41 1.97 o -3 3 1 235.02 246.04 4.45 o -2 3 1 147.35 143.08 2.53 o -1 3 1 219.38 233.17 4.64 o 0 3 1 64.98 63.10 1.90 o 1 3 1 5.96 5.59 0.28 o 2 3 1 219.93 218.07 5.24 o 3 3 1 2.28 2.06 0.37 o 4 3 1 9.39 9.76 0.51 o 5 3 1 2.68 2.77 0.65 o -5 4 1 19.96 18.39 0.81 o -4 4 1 0.59 0.63 0.46 o -3 4 1 4.32 4.55 0.35 o -2 4 1 32.88 35.19 0.72 o -1 4 1 11.22 10.59 0.41 o 0 4 1 37.15 40.02 0.89 o 1 4 1 0.01 0.16 0.15 o 2 4 1 90.24 90.09 1.97 o 3 4 1 118.09 125.60 2.94 o 4 4 1 0.82 0.69 0.57 o 5 4 1 0.06 0.40 0.96 o -4 5 1 29.71 28.36 0.84 o -3 5 1 70.17 70.42 3.59 o -2 5 1 36.17 33.83 0.84 o -1 5 1 47.87 49.70 1.58 o 0 5 1 21.26 21.07 0.60 o 1 5 1 4.18 4.55 0.23 o 2 5 1 55.09 56.15 1.21 o 3 5 1 0.53 0.67 0.40 o 4 5 1 3.12 2.79 0.61 o -3 6 1 1.47 1.51 0.37 o -2 6 1 8.21 8.88 0.63 o -1 6 1 1.92 2.51 0.36 o 0 6 1 7.03 6.67 0.28 o 1 6 1 0.35 0.12 0.13 o 2 6 1 24.60 22.85 0.64 o 3 6 1 27.90 28.68 0.73 o -2 7 1 6.99 6.64 0.83 o -1 7 1 10.26 8.00 0.52 o 0 7 1 5.75 6.56 1.09 o 1 7 1 0.55 1.00 0.91 o 2 7 1 9.03 9.80 1.56 o -6 0 2 4.99 2.67 1.72 o -5 0 2 14.77 14.08 1.04 o -4 0 2 126.99 124.47 3.53 o -3 0 2 414.23 440.61 11.32 o -2 0 2 269.66 263.96 6.44 o -1 0 2 64.34 59.21 1.49 o 0 0 2 235.46 224.03 5.69 o 1 0 2 150.61 148.77 3.58 o 2 0 2 216.98 221.70 5.28 o 3 0 2 133.70 120.98 3.51 o 4 0 2 136.37 124.61 3.85 o 5 0 2 0.87 1.14 1.36 o -6 1 2 46.75 44.39 1.97 o -5 1 2 18.49 17.47 0.81 o -4 1 2 5.92 5.51 0.50 o -3 1 2 32.93 38.38 0.76 o -2 1 2 179.23 188.25 3.50 o -1 1 2 586.26 576.77 10.87 o 0 1 2 1208.43 1115.51 21.75 o 1 1 2 69.54 61.42 1.01 o 2 1 2 96.83 107.75 1.79 o 3 1 2 5.75 5.60 0.29 o 4 1 2 43.16 45.97 0.92 o 5 1 2 156.26 166.07 4.44 o -5 2 2 11.16 10.15 0.81 o -4 2 2 96.78 95.90 1.97 o -3 2 2 291.17 301.78 5.72 o -2 2 2 154.25 144.20 2.55 o -1 2 2 60.01 55.60 1.16 o 0 2 2 126.76 129.66 2.14 o 1 2 2 114.74 112.59 3.87 o 2 2 2 127.09 128.09 2.37 o 3 2 2 94.16 89.14 1.58 o 4 2 2 104.65 99.57 3.77 o 5 2 2 0.75 0.66 0.52 o -5 3 2 8.40 8.75 0.90 o -4 3 2 4.82 4.50 0.51 o -3 3 2 12.79 13.64 0.53 o -2 3 2 91.59 93.86 1.90 o -1 3 2 239.18 237.84 4.10 o 0 3 2 346.46 361.72 7.28 o 1 3 2 40.02 37.63 0.63 o 2 3 2 33.84 36.66 0.58 o 3 3 2 1.19 1.12 0.38 o 4 3 2 21.74 22.98 0.64 o 5 3 2 89.45 90.68 3.18 o -5 4 2 5.65 4.47 0.79 o -4 4 2 41.27 40.11 1.53 o -3 4 2 112.51 114.08 2.17 o -2 4 2 49.37 47.52 0.88 o -1 4 2 22.89 21.98 0.64 o 0 4 2 31.07 31.99 0.71 o 1 4 2 35.99 34.24 0.64 o 2 4 2 39.47 38.57 0.66 o 3 4 2 35.13 34.74 0.75 o 4 4 2 46.63 46.74 3.26 o -4 5 2 3.32 2.31 0.66 o -3 5 2 5.40 5.58 0.48 o -2 5 2 27.34 24.38 0.89 o -1 5 2 53.51 50.73 1.65 o 0 5 2 74.52 78.07 2.00 o 1 5 2 10.09 10.96 0.43 o 2 5 2 9.69 10.23 0.39 o 3 5 2 0.38 0.82 0.45 o 4 5 2 5.85 5.56 0.55 o -3 6 2 26.72 26.98 1.25 o -2 6 2 11.18 11.73 0.92 o -1 6 2 3.27 3.39 0.51 o 0 6 2 6.72 7.08 0.42 o 1 6 2 4.13 3.66 0.17 o 2 6 2 7.41 7.12 0.45 o 3 6 2 6.82 7.16 0.52 o -2 7 2 6.15 6.01 0.95 o -1 7 2 7.36 8.06 0.63 o 0 7 2 10.74 11.98 0.57 o 1 7 2 0.94 1.17 0.51 o 2 7 2 2.84 1.88 1.44 o -5 0 3 0.25 1.08 0.96 o -4 0 3 98.84 91.13 2.81 o -3 0 3 168.61 162.90 4.49 o -2 0 3 5.71 4.47 0.51 o -1 0 3 11.03 10.64 0.48 o 0 0 3 124.26 129.20 3.60 o 1 0 3 81.40 79.55 1.97 o 2 0 3 231.12 222.79 5.55 o 3 0 3 82.81 78.94 2.53 o 4 0 3 25.10 26.48 1.15 o 5 0 3 37.28 37.09 2.15 o -5 1 3 66.18 63.93 1.88 o -4 1 3 40.61 38.33 0.92 o -3 1 3 6.01 5.83 0.47 o -2 1 3 0.11 0.13 0.31 o -1 1 3 86.45 84.16 1.72 o 0 1 3 622.06 635.78 12.03 o 1 1 3 128.65 135.63 2.21 o 2 1 3 0.32 0.45 0.38 o 3 1 3 46.77 45.62 1.03 o 4 1 3 11.99 11.79 0.66 o 5 1 3 6.76 7.87 1.13 o -5 2 3 0.06 0.59 0.76 o -4 2 3 71.86 67.85 1.45 o -3 2 3 125.08 119.52 2.47 o -2 2 3 1.96 1.02 0.27 o -1 2 3 6.11 5.59 0.25 o 0 2 3 67.57 69.42 1.25 o 1 2 3 74.90 70.10 2.28 o 2 2 3 161.26 162.88 2.60 o 3 2 3 59.49 60.33 1.90 o 4 2 3 17.61 18.42 0.94 o 5 2 3 28.66 28.36 3.66 o -5 3 3 39.79 38.83 1.39 o -4 3 3 22.27 20.35 0.74 o -3 3 3 1.83 1.66 0.42 o -2 3 3 0.05 0.10 0.26 o -1 3 3 61.71 60.64 1.72 o 0 3 3 234.08 244.40 4.30 o 1 3 3 51.29 55.13 2.14 o 2 3 3 0.10 0.54 0.29 o 3 3 3 26.08 26.83 0.91 o 4 3 3 7.12 8.11 0.83 o -5 4 3 0.06 0.31 0.96 o -4 4 3 27.50 29.38 1.14 o -3 4 3 48.24 48.66 1.08 o -2 4 3 0.64 0.83 0.29 o -1 4 3 1.64 1.46 0.20 o 0 4 3 22.78 22.49 0.52 o 1 4 3 35.72 33.39 0.68 o 2 4 3 64.49 68.80 1.29 o 3 4 3 27.32 28.14 0.71 o 4 4 3 7.08 6.91 0.61 o -4 5 3 9.48 9.82 0.73 o -3 5 3 0.11 0.11 0.40 o -2 5 3 0.05 0.15 0.17 o -1 5 3 18.89 19.25 1.69 o 0 5 3 65.95 65.61 1.59 o 1 5 3 16.37 17.67 0.47 o 2 5 3 0.33 0.46 0.37 o 3 5 3 6.68 6.73 0.47 o -3 6 3 9.47 9.52 1.14 o -2 6 3 0.35 1.10 0.98 o -1 6 3 0.16 0.21 0.78 o 0 6 3 5.91 6.01 0.50 o 1 6 3 7.79 7.37 0.30 o 2 6 3 17.02 18.52 0.93 o 3 6 3 9.29 9.95 0.81 o -2 7 3 0.47 0.04 1.02 o -1 7 3 2.81 3.08 0.74 o 0 7 3 14.92 16.71 0.95 o 1 7 3 4.92 4.32 0.69 o -5 0 4 72.16 70.30 3.54 o -4 0 4 8.40 8.77 0.90 o -3 0 4 27.90 25.62 1.03 o -2 0 4 1.93 2.58 0.59 o -1 0 4 651.17 648.99 19.61 o 0 0 4 411.56 391.20 10.58 o 1 0 4 24.23 24.63 0.79 o 2 0 4 4.67 4.06 0.61 o 3 0 4 20.55 22.45 1.10 o 4 0 4 69.00 67.81 2.78 o 5 0 4 71.60 71.89 4.05 o -5 1 4 13.48 15.27 1.14 o -4 1 4 158.48 158.98 2.95 o -3 1 4 134.50 140.60 2.82 o -2 1 4 328.08 328.82 5.80 o -1 1 4 56.28 55.98 1.31 o 0 1 4 164.51 176.00 3.19 o 1 1 4 222.74 229.77 4.07 o 2 1 4 562.77 563.93 9.74 o 3 1 4 288.59 278.44 5.91 o 4 1 4 20.23 20.50 1.13 o 5 1 4 0.10 0.00 1.67 o -5 2 4 54.52 45.77 2.65 o -4 2 4 6.35 7.03 0.62 o -3 2 4 24.63 23.75 0.66 o -2 2 4 0.77 1.03 0.38 o -1 2 4 455.55 478.91 10.17 o 0 2 4 254.61 257.87 5.28 o 1 2 4 20.82 21.02 0.85 o 2 2 4 4.31 3.76 0.31 o 3 2 4 17.63 17.88 0.66 o 4 2 4 52.14 51.33 1.67 o -5 3 4 7.47 6.88 1.10 o -4 3 4 92.60 93.90 2.10 o -3 3 4 78.81 83.09 1.79 o -2 3 4 160.42 164.89 3.30 o -1 3 4 34.40 36.53 0.91 o 0 3 4 69.61 70.38 1.94 o 1 3 4 128.84 131.55 2.45 o 2 3 4 301.52 314.48 6.27 o 3 3 4 165.21 165.00 3.49 o 4 3 4 12.28 13.04 1.07 o -4 4 4 3.10 3.31 0.65 o -3 4 4 13.70 14.41 0.64 o -2 4 4 0.22 0.39 0.33 o -1 4 4 170.68 180.94 3.47 o 0 4 4 89.48 92.37 1.79 o 1 4 4 10.48 12.41 0.55 o 2 4 4 2.02 2.36 0.36 o 3 4 4 9.31 8.53 0.68 o 4 4 4 23.26 23.59 1.47 o -4 5 4 31.97 28.95 1.28 o -3 5 4 27.67 30.48 2.01 o -2 5 4 53.94 57.54 1.48 o -1 5 4 10.79 11.40 0.41 o 0 5 4 18.42 15.85 1.41 o 1 5 4 42.34 39.86 0.95 o 2 5 4 107.13 104.44 2.53 o 3 5 4 59.65 54.95 1.52 o -3 6 4 4.91 4.87 1.38 o -2 6 4 0.28 0.15 0.83 o -1 6 4 39.91 38.66 1.39 o 0 6 4 22.77 22.74 0.93 o 1 6 4 2.78 3.01 0.37 o 2 6 4 0.42 0.45 0.58 o -1 7 4 2.24 1.87 1.11 o 0 7 4 3.87 2.73 0.91 o -5 0 5 9.27 9.46 1.65 o -4 0 5 0.25 1.03 1.04 o -3 0 5 130.88 123.74 3.62 o -2 0 5 291.68 284.13 7.14 o -1 0 5 93.39 85.31 2.55 o 0 0 5 281.62 288.39 7.73 o 1 0 5 4.01 5.18 0.69 o 2 0 5 150.47 146.20 3.61 o 3 0 5 9.61 11.41 1.12 o 4 0 5 7.40 7.78 2.13 o -5 1 5 8.44 8.22 1.33 o -4 1 5 85.93 88.10 1.98 o -3 1 5 187.31 178.88 3.86 o -2 1 5 6.48 8.42 0.49 o -1 1 5 26.48 26.64 1.44 o 0 1 5 0.08 0.67 0.37 o 1 1 5 84.74 77.63 1.53 o 2 1 5 8.64 8.15 0.48 o 3 1 5 7.17 6.01 0.66 o 4 1 5 12.42 12.63 1.14 o -5 2 5 7.10 8.76 1.33 o -4 2 5 0.07 0.51 0.78 o -3 2 5 97.44 96.39 2.23 o -2 2 5 211.91 216.69 4.60 o -1 2 5 77.91 78.39 1.85 o 0 2 5 191.36 201.20 4.49 o 1 2 5 1.90 2.67 0.36 o 2 2 5 107.43 102.91 2.04 o 3 2 5 7.26 7.46 0.80 o 4 2 5 5.38 6.58 1.28 o -4 3 5 48.89 51.95 1.58 o -3 3 5 107.42 108.19 2.36 o -2 3 5 4.92 6.18 0.71 o -1 3 5 15.42 15.56 0.55 o 0 3 5 0.02 0.38 0.36 o 1 3 5 49.06 47.01 0.92 o 2 3 5 3.66 4.24 0.37 o 3 3 5 5.84 4.77 0.72 o 4 3 5 7.60 6.54 1.14 o -4 4 5 0.00 0.14 0.76 o -3 4 5 44.41 42.52 4.06 o -2 4 5 91.41 94.62 3.87 o -1 4 5 37.33 38.14 0.93 o 0 4 5 72.21 76.85 1.58 o 1 4 5 0.26 0.27 0.40 o 2 4 5 45.26 41.39 1.03 o 3 4 5 2.66 2.26 0.86 o -3 5 5 35.39 35.59 1.28 o -2 5 5 2.14 1.60 0.41 o -1 5 5 5.88 4.88 0.43 o 0 5 5 0.02 0.14 0.35 o 1 5 5 14.01 13.63 0.84 o 2 5 5 0.34 0.68 0.50 o -2 6 5 26.74 21.37 1.84 o -1 6 5 9.74 9.35 1.13 o 0 6 5 18.21 19.09 1.09 o 1 6 5 0.01 0.15 0.76 o -4 0 6 64.91 65.12 3.10 o -3 0 6 10.67 11.79 0.95 o -2 0 6 0.06 0.12 0.74 o -1 0 6 0.11 0.44 0.70 o 0 0 6 108.99 102.62 3.19 o 1 0 6 90.78 83.85 2.60 o 2 0 6 43.90 43.37 1.11 o 3 0 6 66.27 62.62 3.26 o -4 1 6 3.65 3.08 1.18 o -3 1 6 5.07 4.56 1.17 o -2 1 6 12.86 13.66 0.62 o -1 1 6 219.93 220.26 4.67 o 0 1 6 164.50 177.80 3.56 o 1 1 6 1.36 0.86 0.56 o 2 1 6 18.17 18.83 0.83 o 3 1 6 1.88 2.29 0.99 o -4 2 6 49.59 49.69 3.18 o -3 2 6 7.49 8.49 0.66 o -2 2 6 0.29 0.37 0.61 o -1 2 6 0.10 0.33 0.53 o 0 2 6 79.73 74.57 1.67 o 1 2 6 69.85 65.04 1.35 o 2 2 6 30.93 29.74 0.91 o 3 2 6 49.01 51.44 3.09 o -4 3 6 1.69 1.57 0.83 o -3 3 6 2.98 3.01 0.87 o -2 3 6 7.79 8.93 0.59 o -1 3 6 122.21 122.28 2.95 o 0 3 6 83.40 89.13 1.86 o 1 3 6 0.73 0.60 0.46 o 2 3 6 11.56 12.20 0.56 o 3 3 6 1.47 2.50 1.49 o -3 4 6 2.14 1.87 0.67 o -2 4 6 0.91 0.92 0.78 o -1 4 6 0.01 0.15 0.61 o 0 4 6 34.98 32.92 2.01 o 1 4 6 29.97 26.59 0.75 o 2 4 6 11.15 9.89 0.57 o -2 5 6 2.58 2.27 0.72 o -1 5 6 38.03 39.16 1.26 o 0 5 6 25.03 25.67 0.90 o 1 5 6 0.46 0.15 0.67 o -4 0 7 55.82 55.37 3.68 o -3 0 7 84.53 78.98 3.68 o -2 0 7 19.96 20.19 1.12 o -1 0 7 0.01 0.00 1.03 o 0 0 7 2.67 2.61 1.01 o 1 0 7 41.13 43.50 1.72 o 2 0 7 80.28 83.59 3.26 o 3 0 7 0.98 1.06 1.68 o -4 1 7 2.06 2.45 1.38 o -3 1 7 6.54 7.27 0.96 o -2 1 7 44.29 43.43 1.17 o -1 1 7 41.83 46.35 1.68 o 0 1 7 28.25 29.07 0.88 o 1 1 7 4.24 4.58 1.00 o 2 1 7 37.16 36.15 1.77 o -3 2 7 65.53 63.43 2.82 o -2 2 7 15.57 16.61 0.86 o -1 2 7 0.03 0.02 0.21 o 0 2 7 2.79 2.32 0.63 o 1 2 7 30.89 32.34 2.14 o 2 2 7 61.91 63.28 1.67 o -3 3 7 2.88 2.31 0.83 o -2 3 7 23.16 23.11 1.74 o -1 3 7 24.12 25.02 0.98 o 0 3 7 15.45 16.65 0.72 o 1 3 7 2.69 2.96 0.72 o 2 3 7 20.31 19.73 1.03 o -2 4 7 8.43 8.62 1.25 o -1 4 7 0.24 0.15 0.98 o 0 4 7 2.57 1.98 0.71 o 1 4 7 12.30 12.43 0.86 o -3 0 8 0.00 0.00 1.69 o -2 0 8 45.77 49.94 2.90 o -1 0 8 98.50 101.49 5.61 o 0 0 8 63.59 60.58 3.28 o 1 0 8 5.61 5.33 2.21 o -3 1 8 22.06 21.40 1.48 o -2 1 8 18.56 19.02 1.28 o -1 1 8 9.10 9.07 1.47 o 0 1 8 1.47 1.92 1.14 o 1 1 8 45.16 43.30 1.94 o -2 2 8 35.48 38.68 1.85 o -1 2 8 76.23 78.76 3.16 o 0 2 8 48.86 50.79 2.29 o 1 2 8 4.46 2.59 0.79 o -1 3 8 5.96 4.10 0.99 o 0 3 8 0.58 0.27 1.06 o