#------------------------------------------------------------------------------ #$Date: 2016-04-02 21:51:04 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180806 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/37/2013746.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2013746_Fobs loop_ _publ_author_name 'Wang, Jin-Ping' 'Niu, Chun-Ji' 'Hu, Ning-Hai' _publ_section_title ; Heptaaquatetra-\m~3~-hydroxy-hexa-\m~2~-L-leucine-(L-leucine)tetraytterbium(III) tetrachlorozinc(II) trichlorohydroxyzinc(II) tetrachloride octahydrate ; _journal_issue 3 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first m143 _journal_page_last m146 _journal_volume 60 _journal_year 2004 _space_group_IT_number 19 _symmetry_space_group_name_Hall 'P 2ac 2ab' _symmetry_space_group_name_H-M 'P 21 21 21' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 18.1707 _cell_length_b 22.1299 _cell_length_c 23.2506 _exptl_crystal_F_000 4904.00 _reflns_d_resolution_high 0.8413 _cod_data_source_file bm1556Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' n030 in P2(1)2(1)2(1)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 887.30 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 82849.59 90078.53 1550.67 o 4 0 0 45017.26 44200.08 1702.69 o 6 0 0 240978.55 263427.84 4509.10 o 8 0 0 3857.12 2286.47 851.35 o 10 0 0 86453.35 87855.91 3475.32 o 12 0 0 18936.41 17109.02 1654.04 o 14 0 0 468.51 36.49 1638.84 o 16 0 0 9213.83 6138.82 2213.50 o 18 0 0 5569.98 5117.20 2031.07 o 20 0 0 189.09 681.08 1845.60 o 3 1 0 116038.37 122646.20 1631.54 o 4 1 0 2116.98 213.91 375.99 o 5 1 0 135432.48 131596.28 2589.00 o 6 1 0 82464.45 84322.75 1996.00 o 7 1 0 160541.52 150103.56 2656.97 o 8 1 0 2308.29 825.00 659.48 o 9 1 0 13689.54 13091.99 2038.67 o 10 1 0 3088.28 1990.88 883.47 o 11 1 0 69123.83 57401.22 9235.59 o 12 1 0 368.53 947.96 907.36 o 13 1 0 281.45 1202.06 972.91 o 14 1 0 1672.59 1146.92 1207.79 o 15 1 0 5251.94 2439.01 1420.39 o 16 1 0 255.30 435.89 1386.01 o 17 1 0 14320.22 14482.28 1676.11 o 18 1 0 234.46 1002.74 1238.11 o 19 1 0 11.89 451.92 1260.63 o 20 1 0 161.83 578.28 1417.38 o 21 1 0 1.65 499.64 1353.57 o 1 2 0 50783.47 48974.80 831.51 o 2 2 0 231414.83 243381.69 2928.02 o 3 2 0 92984.36 83231.27 2076.68 o 4 2 0 22588.93 22718.79 1121.95 o 5 2 0 454990.13 449866.59 5749.63 o 6 2 0 71560.38 72127.28 2645.25 o 7 2 0 4758.75 4314.50 976.01 o 8 2 0 21606.61 20490.08 1386.48 o 9 2 0 8820.44 6743.88 1343.91 o 10 2 0 11819.14 8750.62 1471.61 o 11 2 0 906.36 1806.07 1325.67 o 12 2 0 10283.71 7877.99 1736.14 o 13 2 0 69.56 1301.34 1413.84 o 14 2 0 158.75 291.89 1660.13 o 15 2 0 6619.02 4658.08 2046.27 o 16 2 0 13719.49 9985.08 2380.73 o 17 2 0 74.03 -94.26 2064.51 o 18 2 0 5372.10 4530.38 2116.20 o 19 2 0 2472.30 3606.06 2040.19 o 20 2 0 89.07 717.56 1985.46 o 21 2 0 621.22 54.73 2286.47 o 1 3 0 111683.53 125222.09 4439.17 o 2 3 0 22079.30 16139.09 799.66 o 4 3 0 215937.70 208649.78 3721.60 o 5 3 0 109231.03 103511.55 3013.16 o 6 3 0 141543.66 136510.34 3578.70 o 7 3 0 51540.47 53355.09 2645.25 o 8 3 0 5393.38 7017.53 1012.49 o 9 3 0 351.33 383.11 1173.64 o 10 3 0 2.80 285.81 1377.36 o 11 3 0 277.35 2009.79 1325.67 o 12 3 0 10955.38 8090.83 1678.37 o 13 3 0 1756.91 1267.90 1444.25 o 14 3 0 5832.31 3955.72 1787.83 o 15 3 0 1863.95 1596.27 1848.64 o 16 3 0 4479.66 4241.53 1942.89 o 17 3 0 12411.30 11347.23 2405.05 o 18 3 0 4669.53 5025.98 2201.34 o 19 3 0 2176.56 2517.55 2335.12 o 20 3 0 1705.19 994.25 2368.57 o 21 3 0 490.19 547.29 2304.72 o 1 4 0 11342.14 13872.92 661.31 o 2 4 0 9463.24 7333.74 589.86 o 3 4 0 28636.47 26178.90 1495.94 o 4 4 0 3410.16 3888.83 805.74 o 5 4 0 57431.40 48222.69 2234.78 o 6 4 0 60237.93 59870.93 2660.46 o 7 4 0 50815.04 55571.64 2715.19 o 8 4 0 9242.57 5853.01 1076.35 o 9 4 0 10779.92 10787.77 1346.95 o 10 4 0 7524.12 7960.09 1462.49 o 11 4 0 18421.46 15448.90 1745.26 o 12 4 0 2753.46 2836.81 1587.15 o 13 4 0 1754.57 1374.32 1495.94 o 14 4 0 1067.42 814.86 1696.61 o 15 4 0 9330.17 7732.05 2094.92 o 16 4 0 5767.80 8902.65 2061.47 o 17 4 0 1354.00 1407.76 2070.60 o 18 4 0 6255.35 4153.35 2383.77 o 19 4 0 5643.29 4031.73 2365.53 o 20 4 0 1872.93 1845.60 2547.96 o 21 4 0 529.79 164.19 2365.53 o 1 5 0 79873.72 90709.42 1673.75 o 3 5 0 84841.45 72282.34 2487.15 o 4 5 0 13247.24 18516.78 1048.98 o 5 5 0 682.44 699.32 784.45 o 6 5 0 7066.54 6634.42 921.28 o 7 5 0 1348.85 1647.96 957.76 o 8 5 0 1921.28 4144.23 1112.83 o 9 5 0 25261.19 22144.13 1651.00 o 10 5 0 412.04 565.54 1252.70 o 11 5 0 28358.06 28763.34 2049.31 o 12 5 0 15926.59 15667.81 1793.91 o 13 5 0 126.72 -30.41 1502.02 o 14 5 0 45.53 790.54 1532.42 o 15 5 0 7747.24 9024.27 2186.14 o 16 5 0 514.28 1286.14 1942.89 o 17 5 0 150.88 0.00 1979.38 o 18 5 0 7970.94 8236.78 2547.96 o 19 5 0 4375.01 367.90 2444.58 o 20 5 0 1582.60 1745.26 2587.48 o 21 5 0 1973.60 3487.48 2551.00 o 0 6 0 377816.56 430477.22 5238.82 o 1 6 0 197681.31 209921.41 2686.38 o 2 6 0 1656.77 3429.71 775.33 o 3 6 0 8857.10 8981.70 869.59 o 4 6 0 308.29 -2909.78 2909.78 o 5 6 0 7235.61 6023.28 881.75 o 6 6 0 2182.75 2678.70 936.48 o 7 6 0 61832.45 64605.03 2955.39 o 8 6 0 570.46 1073.30 1112.83 o 9 6 0 8581.34 7409.75 1307.42 o 10 6 0 78611.23 76083.00 3487.48 o 11 6 0 7910.45 6613.14 1526.34 o 12 6 0 844.45 425.67 1316.55 o 13 6 0 5190.34 7713.81 1647.96 o 14 6 0 5048.53 3910.11 1909.45 o 15 6 0 193.72 1201.01 1824.31 o 16 6 0 1341.98 2076.68 2031.07 o 17 6 0 1378.55 1912.49 2024.99 o 18 6 0 140.33 453.04 1961.14 o 19 6 0 3779.90 4816.19 2246.95 o 20 6 0 2198.58 3338.49 2386.81 o 21 6 0 0.09 142.90 2450.66 o 1 7 0 98790.55 101120.79 4919.57 o 2 7 0 49173.55 50977.41 2316.88 o 3 7 0 2287.39 1359.11 830.06 o 4 7 0 64063.58 70965.80 2730.39 o 5 7 0 279.86 215.88 814.86 o 6 7 0 19726.42 18525.90 1280.06 o 7 7 0 50065.77 46641.62 2703.02 o 8 7 0 60584.63 64580.70 3077.01 o 9 7 0 11465.13 12523.91 1523.30 o 10 7 0 5171.79 3931.40 1334.79 o 11 7 0 19608.31 17595.50 1827.35 o 12 7 0 5666.79 5998.95 1620.60 o 13 7 0 8622.88 6658.74 1796.95 o 14 7 0 14.06 0.00 1796.95 o 15 7 0 3376.26 3022.28 1912.49 o 16 7 0 2066.47 1921.61 1787.83 o 17 7 0 1226.05 2177.01 1997.62 o 18 7 0 900.69 -477.36 1891.21 o 19 7 0 617.66 -179.39 2277.35 o 20 7 0 338.31 -127.70 2338.16 o 0 8 0 126904.75 124637.11 3332.41 o 1 8 0 327.18 1671.33 950.16 o 2 8 0 109.68 349.66 738.85 o 3 8 0 124764.15 129012.42 3496.60 o 4 8 0 23161.09 21654.60 1213.17 o 5 8 0 113836.66 108084.51 3599.98 o 6 8 0 187397.34 181865.83 4563.82 o 7 8 0 37710.93 38438.29 1860.80 o 8 8 0 1337.55 1061.14 1216.21 o 9 8 0 54831.27 59195.94 2827.69 o 10 8 0 577.99 1447.29 1377.36 o 11 8 0 1959.73 2590.53 1529.38 o 12 8 0 3369.78 3238.16 1568.91 o 13 8 0 531.91 2213.50 1617.56 o 14 8 0 10920.74 13022.56 2170.93 o 15 8 0 717.99 -398.31 1745.26 o 16 8 0 686.28 -395.27 1976.34 o 17 8 0 65.69 465.20 2009.79 o 18 8 0 1806.62 -450.00 2249.99 o 19 8 0 20.89 -1337.83 2104.04 o 20 8 0 598.10 1356.07 2158.77 o 1 9 0 38601.04 45187.30 2522.11 o 2 9 0 26966.84 24345.46 1505.06 o 3 9 0 91019.54 95752.15 3232.08 o 4 9 0 115089.55 121295.56 3703.36 o 5 9 0 15140.05 14062.42 1298.30 o 6 9 0 101894.98 106968.63 3919.23 o 7 9 0 150325.42 140767.08 4387.47 o 8 9 0 29125.78 29882.26 1891.21 o 9 9 0 1072.10 1474.65 1316.55 o 10 9 0 11806.12 13107.69 1733.10 o 11 9 0 2411.06 2329.04 1529.38 o 12 9 0 23126.05 18221.85 2225.66 o 13 9 0 21663.91 21520.82 2313.84 o 14 9 0 328.31 -337.50 1760.46 o 15 9 0 421.47 1553.71 1799.99 o 16 9 0 19.59 960.81 1763.50 o 17 9 0 4940.24 7342.86 2283.43 o 18 9 0 740.67 3298.97 2329.04 o 19 9 0 693.11 2277.35 2356.41 o 20 9 0 120.96 -130.74 2389.85 o 0 10 0 731.78 -446.96 869.59 o 1 10 0 68804.95 63160.21 1953.63 o 2 10 0 27391.04 30095.09 1720.94 o 3 10 0 55285.54 60336.13 2763.84 o 4 10 0 8898.86 8233.74 1225.33 o 5 10 0 92884.22 101614.27 3663.83 o 6 10 0 41480.16 38955.18 1945.93 o 7 10 0 68807.05 77344.82 3502.68 o 8 10 0 87184.95 83951.87 3590.86 o 9 10 0 23449.31 21864.40 1888.16 o 10 10 0 3291.12 4132.07 1587.15 o 11 10 0 37479.69 33333.25 2386.81 o 12 10 0 13101.53 15819.84 2107.08 o 13 10 0 13750.39 13667.15 2189.18 o 14 10 0 7302.11 6795.57 2034.11 o 15 10 0 163.44 754.05 1702.69 o 16 10 0 3128.21 5205.38 2204.38 o 17 10 0 2120.19 2648.30 2073.64 o 18 10 0 3624.33 2402.01 2304.72 o 19 10 0 3228.07 4116.87 2578.36 o 1 11 0 10697.07 13629.12 886.18 o 2 11 0 26829.47 27300.85 1489.86 o 3 11 0 43179.38 49770.32 2727.35 o 4 11 0 102659.63 108057.14 3721.60 o 5 11 0 17059.31 19526.24 1550.67 o 6 11 0 99629.57 98449.09 3742.88 o 7 11 0 19181.66 17969.49 1687.49 o 8 11 0 9381.57 8890.49 1587.15 o 9 11 0 32156.54 31451.17 2143.57 o 10 11 0 31081.86 25582.96 2140.53 o 11 11 0 13073.12 12067.83 1976.34 o 12 11 0 67792.53 66617.85 3320.25 o 13 11 0 4584.30 4028.69 2143.57 o 14 11 0 12121.63 14436.40 2307.76 o 15 11 0 60.48 -963.85 1739.18 o 16 11 0 1986.79 -668.92 2067.56 o 17 11 0 3264.51 4387.47 2365.53 o 18 11 0 7215.41 9684.06 2608.77 o 19 11 0 1411.22 1052.02 2423.30 o 0 12 0 17485.58 17850.91 1483.78 o 1 12 0 270.55 588.43 798.71 o 2 12 0 4654.33 4834.43 1277.02 o 3 12 0 13787.45 12499.59 1483.78 o 4 12 0 217.85 921.28 1410.80 o 5 12 0 91728.35 91693.05 3621.26 o 6 12 0 2862.79 2605.73 1301.34 o 7 12 0 19020.72 16093.49 1672.29 o 8 12 0 7021.19 5491.18 1517.22 o 9 12 0 10514.68 8267.18 1720.94 o 10 12 0 9430.74 6740.84 1669.25 o 11 12 0 65445.99 72790.11 3408.43 o 12 12 0 4996.11 4864.84 2000.66 o 13 12 0 52406.91 51840.91 3232.08 o 14 12 0 610.94 477.36 2076.68 o 15 12 0 7966.28 9060.76 2265.19 o 16 12 0 789.47 1188.84 1967.22 o 17 12 0 6587.13 9884.74 2450.66 o 18 12 0 70.25 -1173.64 2815.52 o 19 12 0 4975.44 6898.95 2547.96 o 1 13 0 8058.06 8753.44 925.34 o 2 13 0 41387.28 49484.51 2554.04 o 3 13 0 7660.76 9781.36 1635.80 o 4 13 0 17443.00 16205.98 1723.98 o 5 13 0 101.26 526.01 1401.68 o 6 13 0 27675.69 32545.76 1933.77 o 7 13 0 3451.01 1900.33 1465.53 o 8 13 0 3680.09 2684.78 1359.11 o 9 13 0 174.14 103.38 1429.05 o 10 13 0 31644.59 32810.28 2316.88 o 11 13 0 8440.12 6521.92 2110.12 o 12 13 0 84665.86 90203.20 3934.44 o 13 13 0 811.89 1210.13 2198.30 o 14 13 0 27086.00 32567.04 3040.52 o 15 13 0 858.30 197.63 2021.95 o 16 13 0 5132.11 5330.04 2216.54 o 17 13 0 1015.77 2031.07 2301.68 o 18 13 0 6160.07 7458.40 2715.19 o 0 14 0 7051.34 7017.53 1362.15 o 1 14 0 29629.15 31163.80 1272.74 o 2 14 0 2412.43 1243.57 1337.83 o 3 14 0 1407.92 434.79 1322.63 o 4 14 0 8029.22 7105.70 1565.87 o 5 14 0 26936.56 30833.94 1973.30 o 6 14 0 10024.81 7963.13 1605.40 o 7 14 0 9257.79 8306.71 1617.56 o 8 14 0 5542.15 5083.75 1647.96 o 9 14 0 7658.19 6442.87 1751.34 o 10 14 0 952.26 1830.39 1681.41 o 11 14 0 53709.84 57219.60 3110.45 o 12 14 0 2367.64 4430.04 2307.76 o 13 14 0 37449.04 38854.84 3177.35 o 14 14 0 1634.11 2377.69 2222.62 o 15 14 0 6269.44 8784.07 2243.91 o 16 14 0 706.98 -516.89 2091.88 o 17 14 0 5269.80 5874.29 2344.24 o 18 14 0 1382.80 2256.07 2301.68 o 1 15 0 1410.01 2791.75 1053.69 o 2 15 0 2107.12 1903.37 1429.05 o 3 15 0 22243.61 19118.81 1766.54 o 4 15 0 8847.36 8148.60 1687.49 o 5 15 0 1130.08 2623.97 1392.56 o 6 15 0 18731.93 15631.33 1809.11 o 7 15 0 26025.65 24473.17 2143.57 o 8 15 0 2974.62 4837.47 1863.84 o 9 15 0 6256.61 6661.79 1866.88 o 10 15 0 18668.43 19909.34 2131.41 o 11 15 0 1751.02 4484.77 1936.81 o 12 15 0 19657.22 20678.60 2481.07 o 13 15 0 6225.61 5676.66 2125.33 o 14 15 0 5901.78 4512.14 2216.54 o 15 15 0 3.26 -1651.00 2034.11 o 16 15 0 3811.55 5308.75 2377.69 o 17 15 0 3617.89 5025.98 2508.43 o 0 16 0 12048.13 13727.96 1660.13 o 1 16 0 4167.61 3200.43 1051.01 o 2 16 0 5479.44 4974.30 1468.57 o 3 16 0 1967.11 3213.83 1517.22 o 4 16 0 6272.19 5092.88 1550.67 o 5 16 0 4571.18 4533.42 1526.34 o 6 16 0 24806.63 23117.09 2189.18 o 7 16 0 10454.95 8866.16 1955.06 o 8 16 0 28408.56 26227.55 2438.50 o 9 16 0 11439.83 12031.35 2015.87 o 10 16 0 2601.92 3919.23 1745.26 o 11 16 0 1589.59 191.55 1663.17 o 12 16 0 4239.75 3058.77 1997.62 o 13 16 0 3138.93 3858.42 2021.95 o 14 16 0 5671.64 6020.23 2265.19 o 15 16 0 679.51 738.85 1967.22 o 16 16 0 2475.90 2456.74 2152.69 o 17 16 0 333.22 -1806.07 2231.74 o 1 17 0 839.58 81.09 962.75 o 2 17 0 4626.02 3116.54 1538.50 o 3 17 0 8249.20 11228.65 1784.79 o 4 17 0 2456.58 4098.62 1617.56 o 5 17 0 2657.26 6676.99 1681.41 o 6 17 0 1793.70 3070.93 1790.87 o 7 17 0 32979.32 33080.89 2471.95 o 8 17 0 13940.87 14168.83 2158.77 o 9 17 0 2592.23 1602.36 1702.69 o 10 17 0 530.59 72.97 1441.21 o 11 17 0 1094.80 635.47 1687.49 o 12 17 0 1316.73 2155.73 1970.26 o 13 17 0 6733.81 7935.76 2088.84 o 14 17 0 6.74 404.39 2070.60 o 15 17 0 0.70 -258.44 2088.84 o 16 17 0 0.78 796.62 2116.20 o 0 18 0 1549.39 2827.69 1614.52 o 1 18 0 7727.79 7702.11 1250.85 o 2 18 0 519.70 1687.49 1657.08 o 3 18 0 18451.34 17142.47 2015.87 o 4 18 0 24.01 948.64 1626.68 o 5 18 0 2669.01 1103.71 1654.04 o 6 18 0 3575.37 3177.35 1593.23 o 7 18 0 5773.79 6403.34 1763.50 o 8 18 0 5420.86 6400.30 2037.15 o 9 18 0 3173.42 2590.53 1754.38 o 10 18 0 84.55 -18.24 1605.40 o 11 18 0 2716.33 3040.52 1961.14 o 12 18 0 1772.51 2204.38 2073.64 o 13 18 0 8192.90 6783.41 2240.86 o 14 18 0 941.92 1134.11 1924.65 o 15 18 0 10.86 -66.89 2028.03 o 1 19 0 14.88 -252.89 1206.45 o 2 19 0 32441.43 39280.52 2587.48 o 3 19 0 2416.07 3317.21 1711.81 o 4 19 0 14.57 -866.55 1578.03 o 5 19 0 0.82 -796.62 1453.37 o 6 19 0 2694.09 3554.37 1784.79 o 7 19 0 31.51 1006.41 1909.45 o 8 19 0 8160.18 10045.89 1985.46 o 9 19 0 1269.38 866.55 1815.19 o 10 19 0 967.80 608.10 1827.35 o 11 19 0 33.72 203.72 1872.96 o 12 19 0 16507.88 13883.03 2560.12 o 13 19 0 3.06 948.64 2113.16 o 14 19 0 1565.92 2769.92 2009.79 o 0 20 0 3851.67 5433.41 1708.77 o 1 20 0 10033.79 10671.52 1400.16 o 2 20 0 292.38 2353.36 1781.75 o 3 20 0 5772.54 5375.64 1836.48 o 4 20 0 4083.86 4728.01 1921.61 o 5 20 0 5024.48 4819.23 1778.71 o 6 20 0 2368.05 2672.62 1775.67 o 7 20 0 49.98 -893.91 1775.67 o 8 20 0 5149.64 4676.32 2110.12 o 9 20 0 2138.39 2964.51 2076.68 o 10 20 0 3755.67 2265.19 2055.39 o 11 20 0 12604.13 13496.88 2511.47 o 12 20 0 74.88 611.15 2061.47 o 13 20 0 5456.88 7774.62 2277.35 o 14 20 0 9.41 243.24 2253.03 o 1 21 0 4213.99 4177.40 1280.92 o 2 21 0 9433.33 9197.58 2046.27 o 3 21 0 19.19 -237.16 1751.34 o 4 21 0 5179.52 5764.83 1964.18 o 5 21 0 7022.37 6950.64 1876.00 o 6 21 0 1779.45 644.59 1994.58 o 7 21 0 13221.93 11484.05 2316.88 o 8 21 0 50.43 -504.73 2207.42 o 9 21 0 6604.90 6272.60 2292.55 o 10 21 0 1586.75 1772.62 2015.87 o 11 21 0 220.97 778.37 2113.16 o 12 21 0 5702.72 5585.44 2332.08 o 0 22 0 9104.02 12618.17 2107.08 o 1 22 0 750.04 606.88 1163.13 o 2 22 0 5227.38 4135.11 2021.95 o 3 22 0 93.01 820.94 1894.25 o 4 22 0 4.70 -1419.92 1885.12 o 5 22 0 8752.71 8917.85 2268.23 o 6 22 0 19917.24 19039.75 2669.58 o 7 22 0 1055.27 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13 4 16642.54 18687.05 1644.92 o 4 13 4 9123.14 6911.11 1465.53 o 5 13 4 570.61 751.01 1201.01 o 6 13 4 1252.72 1377.36 1371.28 o 7 13 4 12690.73 16105.65 1790.87 o 8 13 4 7321.11 8759.75 1903.37 o 9 13 4 12582.41 8464.82 1851.68 o 10 13 4 4642.45 6074.96 1733.10 o 11 13 4 1553.55 3143.90 1790.87 o 12 13 4 21716.10 19322.52 2268.23 o 13 13 4 1131.29 -781.41 1833.44 o 14 13 4 2607.25 3682.07 1830.39 o 15 13 4 31.95 1079.39 1900.33 o 16 13 4 635.37 1173.64 2116.20 o 17 13 4 516.95 629.39 2170.93 o 18 13 4 3033.89 4022.61 2490.19 o -1 14 4 12138.89 10106.70 1605.40 o 0 14 4 18926.63 13983.36 1605.40 o 1 14 4 11575.16 13420.87 1514.18 o 2 14 4 14748.81 15774.23 1611.48 o 3 14 4 28424.47 28872.80 1879.04 o 4 14 4 5482.90 4496.93 1526.34 o 5 14 4 3415.89 3487.48 1422.96 o 6 14 4 26919.31 23691.75 2043.23 o 7 14 4 22014.64 26166.74 2177.01 o 8 14 4 16890.96 15622.21 2170.93 o 9 14 4 3522.84 1663.17 1763.50 o 10 14 4 448.94 167.23 1663.17 o 11 14 4 3070.08 4211.12 1733.10 o 12 14 4 1305.08 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5205.29 6056.72 1711.81 o 5 16 4 8610.29 7041.85 1702.69 o 6 16 4 35583.55 37261.61 2587.48 o 7 16 4 23834.92 23700.87 2526.67 o 8 16 4 23919.24 21809.67 2551.00 o 9 16 4 3328.81 5661.45 1882.08 o 10 16 4 2129.40 1903.37 1815.19 o 11 16 4 2492.83 3484.44 1705.73 o 12 16 4 5689.27 7169.55 2097.96 o 13 16 4 3603.93 2478.03 2052.35 o 14 16 4 984.99 678.04 2006.74 o 15 16 4 295.84 744.93 2037.15 o 16 16 4 3120.51 1678.37 2423.30 o -1 17 4 12693.35 12374.93 1979.38 o 0 17 4 11794.95 11286.42 1955.06 o 1 17 4 12978.06 14454.65 1815.19 o 2 17 4 2845.02 2982.75 1696.61 o 3 17 4 818.70 1693.57 1596.27 o 4 17 4 1280.09 623.31 1559.79 o 5 17 4 17417.59 15950.58 2018.91 o 6 17 4 11229.47 9544.20 1973.30 o 7 17 4 34233.21 33892.71 2666.54 o 8 17 4 7132.96 10650.95 2161.81 o 9 17 4 7131.93 7002.32 1991.54 o 10 17 4 3208.59 5263.14 1803.03 o 11 17 4 4402.01 7315.50 2055.39 o 12 17 4 9588.05 8388.80 2268.23 o 13 17 4 4068.09 4810.11 2262.15 o 14 17 4 2738.26 638.51 2073.64 o 15 17 4 415.84 1006.41 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o 9 21 4 1178.88 820.94 2055.39 o 10 21 4 3120.42 1076.35 2088.84 o 11 21 4 3872.36 1705.73 2405.05 o 12 21 4 9122.45 7750.29 2727.35 o -1 22 4 2818.56 3022.28 1702.69 o 0 22 4 652.86 -349.66 1602.36 o 1 22 4 2740.49 641.55 1894.25 o 2 22 4 9989.61 9358.73 2225.66 o 3 22 4 11011.05 8705.02 2198.30 o 4 22 4 4776.66 5439.50 2128.37 o 5 22 4 8789.38 9340.49 2101.00 o 6 22 4 5307.85 2499.31 2058.43 o 7 22 4 5625.61 4648.96 2152.69 o 8 22 4 3394.43 3575.65 2012.83 o 9 22 4 995.38 991.21 2116.20 o 10 22 4 909.94 1571.95 2140.53 o 11 22 4 3333.41 5336.12 2347.28 o -1 23 4 37.17 1295.26 1556.75 o 0 23 4 478.12 1514.18 1803.03 o 1 23 4 29.21 592.90 1733.10 o 2 23 4 2614.20 1669.25 1833.44 o 3 23 4 4455.20 5095.92 1888.16 o 4 23 4 8400.62 5688.82 2055.39 o 5 23 4 2627.59 3280.72 2000.66 o 6 23 4 4230.90 3572.61 2240.86 o 7 23 4 5070.97 5360.44 2386.81 o 8 23 4 2656.90 1869.92 2173.97 o 9 23 4 1117.01 -297.97 2167.89 o -1 24 4 1018.17 1386.48 1876.00 o 0 24 4 4448.52 5126.32 2000.66 o 1 24 4 1215.84 678.04 1833.44 o 2 24 4 1493.56 -82.09 1799.99 o 3 24 4 3746.98 3122.62 1976.34 o 4 24 4 1319.75 1629.72 1812.15 o 5 24 4 2102.60 3028.36 2034.11 o 6 24 4 3469.27 4162.48 2368.57 o 7 24 4 2967.81 3423.63 2158.77 o 8 24 4 1335.58 -124.66 2237.82 o -1 25 4 4436.21 5518.55 2189.18 o 0 25 4 2021.24 3022.28 2097.96 o 1 25 4 4320.07 4390.51 2064.51 o 2 25 4 2277.39 4010.45 1888.16 o 3 25 4 1074.71 1812.15 2070.60 o 4 25 4 843.84 112.50 2055.39 o 5 25 4 540.22 36.49 1897.29 o -1 26 4 1290.54 1854.72 2140.53 o 0 26 4 3966.51 4122.95 2234.78 o 1 0 5 2024.92 1680.64 360.89 o 2 0 5 15531.90 13183.71 744.93 o 3 0 5 20877.54 21742.78 1140.20 o 4 0 5 177.43 182.43 668.92 o 5 0 5 147795.69 147434.94 3563.49 o 6 0 5 38554.61 45124.40 1936.81 o 7 0 5 246.53 1426.01 842.22 o 8 0 5 35609.50 33102.17 1821.27 o 9 0 5 20076.10 13405.67 1328.71 o 10 0 5 23208.97 23895.47 1574.99 o 11 0 5 126.77 -161.15 1191.88 o 12 0 5 29942.90 30937.32 2067.56 o 13 0 5 1894.42 3560.45 1508.10 o 14 0 5 105.44 702.36 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805.74 2097.96 o 2 7 26 10319.89 11839.79 2402.01 o 3 7 26 8159.48 8261.10 2195.26 o 4 7 26 3689.18 2012.83 2091.88 o -1 8 26 12886.54 10976.29 2514.51 o 0 8 26 187.65 571.62 2037.15 o 1 8 26 12294.95 13013.44 2313.84 o 2 8 26 6976.73 7221.24 2219.58 o 3 8 26 1696.12 2648.30 2000.66 o 1 0 27 746.41 1043.44 1201.47 o 2 0 27 15.74 -310.13 1766.54 o 3 0 27 434.12 -629.39 1775.67 o 4 0 27 12155.96 8233.74 2237.82 o -4 1 27 2767.41 598.98 2012.83 o -3 1 27 2147.17 3478.36 1842.56 o -2 1 27 541.12 1094.59 1863.84 o -1 1 27 1496.70 -169.60 1226.52 o 0 1 27 1429.45 1380.61 1241.59 o 1 1 27 1852.04 2064.46 1149.86 o 2 1 27 576.52 -72.97 1894.25 o 3 1 27 2489.58 2298.64 1961.14 o 4 1 27 2833.58 2563.16 2231.74 o -1 2 27 1441.75 1830.39 2012.83 o 0 2 27 5247.31 5059.43 1836.48 o 1 2 27 1699.49 2249.99 1632.76 o 2 2 27 1719.21 544.25 1869.92 o 3 2 27 1892.90 2578.36 1973.30 o 4 2 27 7667.26 4627.68 2231.74 o -1 3 27 6722.20 2976.67 1936.81 o 0 3 27 4596.17 5479.02 2173.97 o 1 3 27 6507.28 2876.33 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