#------------------------------------------------------------------------------ #$Date: 2016-04-02 21:52:13 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180807 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/38/2013801.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2013801_Fobs loop_ _publ_author_name 'Garden, Simon J.' 'da Cunha, Fernando R.' 'Glidewell, Christopher' 'Low, John N.' 'Skakle, Janet M. S.' 'Wardell, James L.' _publ_section_title ; Three-dimensional aggregation in 2-hydroxy-3-iodo-5-nitrobenzaldehyde involving C---H···O, iodo--nitro and aromatic \p--\p stacking interactions, and isolated dimers in disordered 2,4-diiodo-6-nitroanisole ; _journal_issue 1 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first o12 _journal_page_last o14 _journal_volume 60 _journal_year 2004 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 95.225 _cell_angle_gamma 90.000 _cell_length_a 32.9985 _cell_length_b 4.2305 _cell_length_c 14.8328 _exptl_crystal_F_000 1472.00 _reflns_d_resolution_high 0.6600 _cod_data_source_file gg1198IIsup3.hkl _cod_data_source_block II #BEGIN Tags that were not found in dictionaries: _shelx_title ' js334' _shelx_refln_list_code 4 _shelx_f_calc_maximum 630.27 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 571.39 758.92 86.73 o 6 0 0 1728.99 1741.31 83.29 o 8 0 0 3974.81 4867.19 328.87 o 10 0 0 107291.78 120677.46 2634.54 o 12 0 0 73495.25 87571.38 870.95 o 14 0 0 32546.76 30041.74 416.44 o 16 0 0 85977.05 86631.20 794.18 o 18 0 0 44175.44 47089.26 961.30 o 20 0 0 1198.96 880.11 134.79 o 22 0 0 42826.10 45747.54 2489.98 o 24 0 0 3186.53 2710.23 201.32 o 26 0 0 1444.97 1290.88 195.15 o 28 0 0 4120.01 3905.32 318.02 o 30 0 0 4015.11 4670.35 275.70 o 32 0 0 60.42 43.37 238.52 o 34 0 0 4800.09 4698.07 462.58 o 36 0 0 10.36 115.64 238.52 o 38 0 0 2863.79 2356.27 397.53 o 40 0 0 1259.98 1525.07 354.16 o 42 0 0 21.55 122.87 289.11 o 44 0 0 63.54 325.25 318.02 o 46 0 0 245.17 585.45 318.02 o 48 0 0 6.18 274.66 310.80 o 1 1 0 581.96 585.01 97.58 o 3 1 0 5137.53 4093.07 133.11 o 5 1 0 80597.55 79438.83 548.17 o 7 1 0 148351.80 145475.23 593.85 o 9 1 0 59906.04 61961.70 948.78 o 11 1 0 40315.87 41381.38 319.75 o 13 1 0 561.40 706.41 72.27 o 15 1 0 29203.47 30117.77 381.97 o 17 1 0 11956.71 11207.14 200.72 o 19 1 0 337.83 562.23 84.67 o 21 1 0 4355.62 4784.29 171.98 o 23 1 0 33021.99 34051.54 913.88 o 25 1 0 2189.09 2573.35 192.45 o 27 1 0 1252.25 1064.17 160.00 o 29 1 0 3409.80 3290.04 247.35 o 31 1 0 2381.72 2422.47 198.54 o 33 1 0 2663.97 2725.98 235.36 o 35 1 0 59.26 -55.20 132.85 o 37 1 0 62.19 147.24 178.66 o 39 1 0 225.87 53.43 188.27 o 41 1 0 107.47 146.36 201.38 o 43 1 0 76.74 -32.14 216.80 o 45 1 0 291.46 484.26 332.48 o 47 1 0 19.41 7.23 303.57 o 49 1 0 47.06 -267.43 318.02 o 0 2 0 13717.55 13660.56 411.99 o 2 2 0 18845.98 18740.63 349.84 o 4 2 0 270.44 326.25 77.30 o 6 2 0 23.06 60.61 63.17 o 8 2 0 8288.85 7139.51 171.09 o 10 2 0 2042.65 2037.09 76.36 o 12 2 0 14.91 58.62 56.39 o 14 2 0 23709.51 25026.80 254.28 o 16 2 0 2985.53 2805.69 155.07 o 18 2 0 160.81 131.36 80.69 o 20 2 0 3218.03 3104.11 185.50 o 22 2 0 9.69 -28.39 125.17 o 24 2 0 3486.57 3481.50 210.70 o 26 2 0 998.98 781.79 145.58 o 28 2 0 33.54 163.99 135.78 o 30 2 0 17.03 73.12 132.10 o 32 2 0 462.32 512.68 175.36 o 34 2 0 0.06 -5.84 141.50 o 36 2 0 249.59 350.55 194.21 o 38 2 0 165.60 149.75 202.38 o 40 2 0 26.93 127.63 191.00 o 42 2 0 68.65 216.83 310.80 o 44 2 0 0.04 -346.93 346.93 o 46 2 0 4.79 -187.92 289.11 o 1 3 0 3922.27 3772.76 217.17 o 3 3 0 311.97 348.66 116.22 o 5 3 0 661.28 626.49 109.53 o 7 3 0 2503.10 2323.59 146.30 o 9 3 0 596.49 601.61 108.04 o 11 3 0 2641.63 2742.33 120.91 o 13 3 0 14.56 23.26 70.51 o 15 3 0 68.51 128.13 111.44 o 17 3 0 195.46 172.86 123.29 o 19 3 0 1056.78 918.36 130.57 o 21 3 0 25.54 -115.39 142.83 o 23 3 0 661.93 493.69 171.87 o 25 3 0 11.98 149.70 167.73 o 27 3 0 303.51 321.38 180.09 o 29 3 0 38.41 -170.70 170.70 o 31 3 0 59.95 338.09 299.95 o 33 3 0 1.49 230.92 196.07 o 35 3 0 229.68 388.32 214.47 o 37 3 0 8.15 146.45 220.55 o 39 3 0 56.76 98.60 205.81 o 41 3 0 67.44 143.33 238.74 o 43 3 0 2.25 121.99 256.59 o 0 4 0 5258.44 5308.73 422.83 o 2 4 0 2025.86 1870.13 242.35 o 4 4 0 883.53 1042.85 135.07 o 6 4 0 123.63 90.35 143.10 o 8 4 0 137.29 101.44 142.39 o 10 4 0 1.85 818.19 607.14 o 12 4 0 1423.17 1660.28 234.39 o 14 4 0 1096.70 1357.84 343.32 o 16 4 0 2364.01 2877.52 552.93 o 18 4 0 858.54 1049.75 216.93 o 20 4 0 119.98 179.94 274.66 o 22 4 0 474.40 274.66 178.88 o 24 4 0 29.85 109.70 186.49 o 26 4 0 1.24 166.05 368.62 o 28 4 0 127.09 190.60 206.56 o 30 4 0 171.94 220.10 249.36 o 32 4 0 90.69 147.58 218.17 o 34 4 0 159.57 489.91 451.74 o 36 4 0 72.53 220.33 236.62 o 38 4 0 40.40 538.50 419.21 o 1 5 0 5.40 -51.40 177.08 o 3 5 0 102.36 94.61 128.61 o 5 5 0 773.49 1120.70 256.59 o 7 5 0 1624.07 1488.93 339.71 o 9 5 0 998.11 1590.12 361.39 o 11 5 0 374.40 358.79 191.20 o 13 5 0 215.39 97.35 201.83 o 15 5 0 147.61 179.40 223.96 o 17 5 0 108.91 171.26 178.73 o 19 5 0 2.33 132.00 193.41 o 21 5 0 334.84 831.19 365.00 o 23 5 0 322.03 453.44 212.05 o 25 5 0 162.88 354.33 234.90 o 27 5 0 109.52 -55.19 231.29 o 29 5 0 55.60 -141.75 217.17 o 31 5 0 65.56 -252.97 361.39 o 2 6 0 297.40 383.07 303.57 o 4 6 0 46.98 448.12 346.93 o 6 6 0 2.93 534.86 339.71 o 8 6 0 12.09 -43.37 310.80 o 10 6 0 21.94 209.61 296.34 o 12 6 0 10.74 -260.20 296.34 o 14 6 0 113.37 130.10 289.11 o 16 6 0 93.20 318.02 318.02 o -49 1 1 15.49 -144.56 332.48 o -47 1 1 93.35 22.02 218.17 o -45 1 1 0.51 104.03 213.02 o -43 1 1 203.34 219.69 219.59 o -41 1 1 113.91 435.80 224.70 o -39 1 1 23.62 144.17 188.89 o -37 1 1 1810.66 1584.68 234.43 o -35 1 1 62.70 82.67 183.99 o -33 1 1 406.22 434.20 144.38 o -31 1 1 2.55 -27.51 124.79 o -29 1 1 386.78 350.93 130.02 o -27 1 1 676.17 745.12 151.47 o -25 1 1 12463.17 12643.83 444.08 o -23 1 1 551.54 386.68 125.98 o -21 1 1 15907.50 17180.85 289.08 o -19 1 1 2128.61 2165.46 107.01 o -17 1 1 179.71 173.58 66.29 o -15 1 1 22068.82 25192.05 262.58 o -13 1 1 3373.36 3608.43 98.43 o -11 1 1 78.81 39.22 53.28 o -9 1 1 64290.87 58486.81 1331.18 o -7 1 1 52356.33 56337.18 308.99 o -5 1 1 4622.54 5456.46 86.07 o -3 1 1 96431.19 101715.73 1105.36 o -1 1 1 29222.07 29067.81 670.09 o 1 1 1 43980.53 44213.14 1334.08 o 3 1 1 21889.06 20830.08 443.38 o 5 1 1 20440.78 19795.27 286.77 o 7 1 1 1478.77 1669.98 66.75 o 9 1 1 65962.09 65305.54 391.85 o 11 1 1 0.69 8.39 59.46 o 13 1 1 33836.04 36743.24 328.32 o 15 1 1 13816.97 13314.92 631.54 o 17 1 1 650.87 513.62 83.58 o 19 1 1 8464.24 8344.86 191.96 o 21 1 1 8110.19 8037.93 199.24 o 23 1 1 13.85 -45.20 84.99 o 25 1 1 382.25 505.32 113.53 o 27 1 1 470.70 406.69 134.63 o 29 1 1 1048.51 781.09 137.85 o 31 1 1 5592.23 5115.69 252.14 o 33 1 1 2.33 -3.38 131.59 o 35 1 1 519.75 362.15 146.99 o 37 1 1 18.51 0.66 167.73 o 39 1 1 129.27 186.95 188.89 o 41 1 1 44.29 -190.38 190.38 o 43 1 1 144.34 -83.12 194.01 o 45 1 1 0.23 36.14 303.57 o 47 1 1 95.00 28.91 310.80 o -46 2 1 19.15 50.59 346.93 o -44 2 1 140.84 325.25 318.02 o -42 2 1 1.17 -339.71 339.71 o -40 2 1 93.69 -166.24 303.57 o -38 2 1 0.23 -21.98 182.08 o -36 2 1 774.31 866.40 260.43 o -34 2 1 151.48 177.35 139.97 o -32 2 1 4185.91 4083.86 254.10 o -30 2 1 4790.84 4771.77 262.16 o -28 2 1 1664.61 1789.98 180.34 o -26 2 1 2192.05 2289.87 191.32 o -24 2 1 1433.71 1100.87 160.18 o -22 2 1 649.22 770.20 143.58 o -20 2 1 1755.65 1502.30 155.70 o -18 2 1 11382.35 11015.35 291.01 o -16 2 1 19383.37 17999.27 291.07 o -14 2 1 54911.05 52330.73 780.62 o -12 2 1 2875.83 2874.10 96.59 o -10 2 1 24276.06 26265.36 570.22 o -8 2 1 12526.99 12405.91 253.27 o -6 2 1 4595.03 4518.35 128.32 o -4 2 1 196.10 144.94 96.70 o -2 2 1 91624.82 89316.16 788.12 o 0 2 1 16206.00 16195.28 324.27 o 2 2 1 58050.70 57432.89 504.90 o 4 2 1 11150.48 11249.41 281.79 o 6 2 1 10984.04 11445.45 226.25 o 8 2 1 81105.21 77580.45 740.72 o 10 2 1 2284.18 2177.13 84.83 o 12 2 1 3531.56 3134.60 95.86 o 14 2 1 19704.93 20314.59 497.00 o 16 2 1 11499.82 11478.51 195.90 o 18 2 1 1073.30 1054.56 104.92 o 20 2 1 13616.61 13365.47 322.96 o 22 2 1 2078.75 1957.78 165.83 o 24 2 1 13597.23 13767.89 357.79 o 26 2 1 2417.18 2362.15 185.38 o 28 2 1 34.09 -62.61 121.13 o 30 2 1 0.72 79.45 133.01 o 32 2 1 627.03 325.15 173.62 o 34 2 1 18.63 -39.81 159.48 o 36 2 1 1048.67 1188.62 419.21 o 38 2 1 519.95 723.24 307.18 o 40 2 1 142.66 42.73 201.44 o 42 2 1 203.12 130.10 281.88 o 44 2 1 8.28 -144.56 296.34 o 46 2 1 56.23 -209.61 361.39 o -43 3 1 51.17 15.36 239.62 o -41 3 1 232.48 400.50 318.02 o -39 3 1 303.13 508.23 237.92 o -37 3 1 258.56 336.05 215.01 o -35 3 1 44.93 34.57 343.32 o -33 3 1 12.50 -40.52 172.48 o -31 3 1 54.41 188.96 173.47 o -29 3 1 168.93 216.34 185.24 o -27 3 1 1054.95 884.17 206.56 o -25 3 1 4410.22 4810.09 336.27 o -23 3 1 7065.76 7277.77 382.90 o -21 3 1 5202.34 5488.71 250.64 o -19 3 1 860.55 970.57 140.78 o -17 3 1 526.44 468.20 120.18 o -15 3 1 933.30 1126.59 138.98 o -13 3 1 2.40 -67.54 106.05 o -11 3 1 2048.94 1774.10 124.56 o -9 3 1 23844.08 24209.69 395.39 o -7 3 1 29439.58 28556.61 524.82 o -5 3 1 10176.28 10002.66 252.99 o -3 3 1 5664.11 6041.55 262.28 o -1 3 1 6625.29 6782.47 280.96 o 1 3 1 17128.56 15740.83 465.40 o 3 3 1 3333.05 3227.28 172.03 o 5 3 1 4263.33 4019.44 199.51 o 7 3 1 16477.15 16848.78 333.90 o 9 3 1 12175.85 12144.41 286.84 o 11 3 1 2408.93 2469.32 136.66 o 13 3 1 6262.88 6251.88 153.57 o 15 3 1 12096.34 11908.31 228.81 o 17 3 1 9720.72 9729.80 403.37 o 19 3 1 411.29 349.16 164.63 o 21 3 1 477.77 870.74 192.40 o 23 3 1 108.78 97.36 172.87 o 25 3 1 375.36 231.19 175.40 o 27 3 1 299.50 412.90 178.80 o 29 3 1 1824.15 2364.32 292.73 o 31 3 1 1831.41 2150.50 273.72 o 33 3 1 355.48 620.04 211.75 o 35 3 1 89.47 477.38 224.06 o 37 3 1 0.04 -175.75 191.00 o 39 3 1 30.76 243.78 230.96 o 41 3 1 1.82 -120.01 242.13 o 43 3 1 22.97 272.61 252.95 o -38 4 1 73.54 147.60 239.51 o -36 4 1 32.55 188.73 614.36 o -34 4 1 103.52 -14.29 211.81 o -32 4 1 209.34 225.46 212.05 o -30 4 1 521.06 475.72 222.10 o -28 4 1 131.18 292.27 199.68 o -26 4 1 45.97 153.41 204.24 o -24 4 1 74.85 63.22 181.38 o -22 4 1 94.84 70.12 271.04 o -20 4 1 7.65 -31.44 151.04 o -18 4 1 1470.94 1128.97 212.05 o -16 4 1 4422.85 4577.30 324.27 o -14 4 1 1872.54 1781.44 232.50 o -12 4 1 927.70 749.92 193.41 o -10 4 1 1.77 198.76 168.66 o -8 4 1 1195.71 1179.80 161.59 o -6 4 1 1364.74 1441.29 198.54 o -4 4 1 443.87 535.30 166.04 o -2 4 1 2296.03 1847.22 135.55 o 0 4 1 5788.29 5220.89 282.23 o 2 4 1 584.38 513.49 123.27 o 4 4 1 395.11 335.02 115.30 o 6 4 1 3562.89 3205.78 188.68 o 8 4 1 3247.18 2796.87 240.05 o 10 4 1 2010.88 2049.20 167.40 o 12 4 1 58.75 387.46 152.82 o 14 4 1 504.43 604.51 196.32 o 16 4 1 412.77 432.35 202.38 o 18 4 1 87.60 175.53 176.92 o 20 4 1 57.97 140.26 183.98 o 22 4 1 1293.06 1153.10 221.92 o 24 4 1 870.25 988.68 210.95 o 26 4 1 437.30 415.60 209.54 o 28 4 1 46.99 39.21 267.43 o 30 4 1 0.15 -112.87 182.33 o 32 4 1 19.96 13.14 196.72 o 34 4 1 16.43 373.96 245.16 o 36 4 1 3.60 329.14 332.48 o 38 4 1 50.53 330.09 247.52 o -31 5 1 27.55 29.42 251.09 o -29 5 1 9.51 90.16 241.76 o -27 5 1 24.71 28.07 218.17 o -25 5 1 39.98 104.24 263.81 o -23 5 1 133.44 270.29 321.64 o -21 5 1 3.63 -199.84 227.68 o -19 5 1 75.55 331.41 206.56 o -17 5 1 8.89 80.71 182.08 o -15 5 1 4.15 -121.34 169.85 o -13 5 1 21.84 -72.28 267.43 o -11 5 1 15.75 -72.28 245.75 o -9 5 1 290.08 195.15 245.75 o -7 5 1 550.87 527.63 289.11 o -5 5 1 3.95 -59.89 138.77 o -3 5 1 153.68 116.09 128.09 o -1 5 1 81.09 104.97 238.52 o 1 5 1 147.40 260.83 175.82 o 3 5 1 110.82 -22.11 172.87 o 5 5 1 40.20 25.19 173.54 o 7 5 1 88.81 86.73 238.52 o 9 5 1 8.46 -3.77 176.27 o 11 5 1 2.48 -36.34 185.24 o 13 5 1 0.80 -47.13 181.38 o 15 5 1 323.22 574.49 221.92 o 17 5 1 266.10 43.37 204.43 o 19 5 1 11.87 251.73 218.77 o 21 5 1 2.36 -18.91 186.49 o 23 5 1 24.45 -1.31 183.78 o 25 5 1 54.54 181.23 206.56 o 27 5 1 2.05 3.61 209.54 o 29 5 1 11.72 -226.77 357.78 o -16 6 1 0.19 151.78 318.02 o -14 6 1 15.87 458.59 218.77 o -12 6 1 37.97 105.79 209.61 o -10 6 1 71.33 144.56 332.48 o -8 6 1 3.56 346.93 339.71 o -6 6 1 16.69 144.56 289.11 o -4 6 1 1.40 -101.19 289.11 o -2 6 1 1.20 57.82 339.71 o 4 6 1 56.03 289.11 354.16 o 6 6 1 3.13 520.40 339.71 o 8 6 1 0.30 -50.59 318.02 o 10 6 1 0.20 -43.37 289.11 o 12 6 1 3.38 368.62 318.02 o 14 6 1 4.06 346.93 310.80 o 16 6 1 20.91 72.28 332.48 o -48 0 2 21.80 -195.15 289.11 o -46 0 2 548.42 722.78 346.93 o -44 0 2 217.76 318.02 310.80 o -42 0 2 90.11 -86.73 281.88 o -40 0 2 820.74 383.07 303.57 o -38 0 2 57.92 346.93 281.88 o -36 0 2 373.23 411.99 310.80 o -34 0 2 2799.58 3339.25 433.67 o -32 0 2 10119.94 9453.97 607.14 o -30 0 2 10551.73 10082.79 607.14 o -28 0 2 4832.01 4640.25 433.67 o -26 0 2 0.91 -13.01 120.28 o -24 0 2 40239.01 41352.52 896.25 o -22 0 2 8776.08 8380.66 266.07 o -20 0 2 2038.86 2557.93 209.61 o -18 0 2 4790.65 3601.69 173.78 o -16 0 2 111287.56 112560.43 877.86 o -14 0 2 12602.72 11308.37 243.35 o -12 0 2 75550.08 78487.59 2190.02 o -10 0 2 47764.51 47129.55 440.48 o -8 0 2 145321.19 145153.80 3288.65 o -6 0 2 230899.41 226382.34 1236.79 o -4 0 2 36631.34 41210.95 338.46 o -2 0 2 1723.19 2677.74 58.67 o 0 0 2 12844.03 15859.96 309.55 o 2 0 2 8567.49 10458.32 213.22 o 4 0 2 20387.01 22189.37 375.85 o 6 0 2 292161.28 288411.22 2161.11 o 8 0 2 137875.86 134377.09 1955.12 o 10 0 2 160417.58 154901.14 2009.33 o 12 0 2 12669.23 14199.60 281.10 o 14 0 2 439.16 493.15 109.79 o 16 0 2 19670.53 20063.07 513.17 o 18 0 2 5691.88 6934.27 249.81 o 20 0 2 11.29 -51.65 104.68 o 22 0 2 50884.83 52314.13 739.85 o 24 0 2 11773.50 12552.06 411.98 o 26 0 2 3481.61 3563.76 234.33 o 28 0 2 4207.61 4602.10 307.18 o 30 0 2 54.20 6.65 125.03 o 32 0 2 5137.98 5555.06 312.79 o 34 0 2 186.55 -50.59 216.83 o 36 0 2 432.03 346.93 245.75 o 38 0 2 114.41 86.73 260.20 o 40 0 2 630.41 556.54 289.11 o 42 0 2 2.40 173.47 281.88 o 44 0 2 449.32 484.26 318.02 o 46 0 2 6.36 -14.46 310.80 o 48 0 2 44.59 -21.68 310.80 o -49 1 2 9.18 -114.55 252.64 o -47 1 2 10.81 188.63 260.50 o -45 1 2 24.08 326.28 397.53 o -43 1 2 28.66 56.79 213.93 o -41 1 2 274.09 258.72 208.38 o -39 1 2 2201.74 2567.65 308.41 o -37 1 2 600.94 763.45 299.95 o -35 1 2 1944.86 1790.69 249.03 o -33 1 2 168.89 130.86 132.69 o -31 1 2 249.95 419.04 135.49 o -29 1 2 2243.70 2180.69 178.84 o -27 1 2 2268.28 1619.57 163.11 o -25 1 2 4721.82 4417.86 214.59 o -23 1 2 20510.67 20224.11 639.02 o -21 1 2 12586.54 12720.08 309.59 o -19 1 2 6275.92 5912.36 135.63 o -17 1 2 30540.72 30284.37 418.51 o -15 1 2 33529.38 34211.95 462.74 o -13 1 2 31414.82 33348.16 405.87 o -11 1 2 15550.10 16253.37 264.78 o -9 1 2 43766.62 43194.56 404.48 o -7 1 2 19123.93 18560.83 248.90 o -5 1 2 3305.75 3290.16 83.46 o -3 1 2 990.93 945.33 63.08 o -1 1 2 397241.88 387675.38 1576.85 o 1 1 2 132250.94 133417.17 1740.87 o 3 1 2 7449.06 8547.02 143.49 o 5 1 2 48.58 28.19 60.64 o 7 1 2 32970.67 33637.29 425.81 o 9 1 2 25921.96 23680.43 378.27 o 11 1 2 9319.54 9608.04 250.38 o 13 1 2 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