#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2013833.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2013833_Fobs loop_ _publ_author_name 'Vembu, Nagarajan' 'Nallu, Maruthai' 'Durmus, Semih' 'Pazner, Mathew' 'Garrison, Jered' 'Youngs, Wiley J.' _publ_section_title ; 2-Chlorophenyl 3-nitrobenzenesulfonate and 2,4-dichlorophenyl 3-nitrobenzenesulfonate: supramolecular aggregation through C--H···O, \p--\p and van der Waals interactions ; _journal_issue 1 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first o65 _journal_page_last o68 _journal_volume 60 _journal_year 2004 _space_group_IT_number 19 _symmetry_space_group_name_Hall 'P 2ac 2ab' _symmetry_space_group_name_H-M 'P 21 21 21' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 6.8776 _cell_length_b 13.3298 _cell_length_c 14.9905 _exptl_crystal_F_000 704.00 _reflns_d_resolution_high 0.7475 _[local]_cod_data_source_file ob1154IIsup3.hkl _[local]_cod_data_source_block II #BEGIN Tags that were not found in dictionaries: _shelx_title ' mvp in P2(1)2(1)2(1)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 162.87 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 812.61 1082.08 62.27 o 4 0 0 1990.47 2383.46 57.72 o 6 0 0 222.82 221.41 13.53 o 8 0 0 427.68 415.13 22.50 o 1 1 0 1781.28 1767.61 26.40 o 2 1 0 7098.36 7576.64 121.95 o 3 1 0 284.45 229.15 5.53 o 4 1 0 645.89 702.81 13.81 o 5 1 0 550.23 532.65 17.21 o 6 1 0 193.38 188.85 8.77 o 7 1 0 17.47 28.89 4.47 o 8 1 0 207.23 196.03 10.30 o 9 1 0 374.37 367.64 18.99 o 0 2 0 15783.47 15686.78 568.09 o 1 2 0 2696.11 2810.26 51.52 o 2 2 0 1191.60 1228.45 26.89 o 3 2 0 3026.92 3596.87 66.33 o 4 2 0 9.93 16.42 1.79 o 5 2 0 1078.45 998.55 29.11 o 6 2 0 10.87 11.76 3.06 o 7 2 0 449.08 458.72 16.04 o 8 2 0 1.70 5.69 2.98 o 9 2 0 15.80 11.30 7.98 o 1 3 0 6766.04 6563.43 137.08 o 2 3 0 1.57 9.65 1.37 o 3 3 0 1688.60 1993.53 34.17 o 4 3 0 19.68 17.94 1.90 o 5 3 0 4.37 4.30 2.23 o 6 3 0 85.13 90.11 6.05 o 7 3 0 408.42 373.16 14.23 o 8 3 0 163.29 187.66 11.44 o 9 3 0 69.97 65.00 9.93 o 0 4 0 2410.59 2318.23 87.67 o 1 4 0 1446.25 1415.36 34.94 o 2 4 0 14.31 8.41 1.14 o 3 4 0 1323.32 1649.99 27.68 o 4 4 0 3121.28 3140.80 53.21 o 5 4 0 3.35 9.34 2.19 o 6 4 0 12.86 22.82 3.85 o 7 4 0 238.08 226.85 10.56 o 8 4 0 602.61 565.72 19.61 o 1 5 0 72.47 83.42 3.26 o 2 5 0 2882.42 2988.95 49.70 o 3 5 0 5060.01 5928.48 111.17 o 4 5 0 2051.60 2236.11 39.19 o 5 5 0 377.64 383.12 12.92 o 6 5 0 2234.26 2258.62 52.78 o 7 5 0 20.28 19.73 3.84 o 8 5 0 15.18 17.54 4.06 o 0 6 0 3863.47 4164.93 109.28 o 1 6 0 6238.66 6243.99 107.14 o 2 6 0 402.80 479.34 9.91 o 3 6 0 729.60 627.37 12.79 o 4 6 0 451.48 459.24 10.86 o 5 6 0 441.52 456.51 18.37 o 6 6 0 0.65 1.73 2.40 o 7 6 0 8.97 4.59 3.14 o 8 6 0 157.57 175.16 11.14 o 1 7 0 3713.84 3948.96 69.31 o 2 7 0 539.17 517.55 10.75 o 3 7 0 224.89 192.76 5.63 o 4 7 0 467.69 475.01 10.99 o 5 7 0 127.17 122.81 6.51 o 6 7 0 131.51 135.80 8.71 o 7 7 0 0.41 5.58 3.64 o 8 7 0 29.27 40.11 6.50 o 0 8 0 1536.54 1344.05 39.26 o 1 8 0 110.03 107.26 4.00 o 2 8 0 452.36 414.73 10.16 o 3 8 0 1375.11 1423.07 31.24 o 4 8 0 627.09 572.68 19.16 o 5 8 0 0.49 3.77 2.49 o 6 8 0 8.71 14.65 4.39 o 7 8 0 0.91 0.13 3.24 o 8 8 0 53.20 61.70 7.97 o 1 9 0 84.25 96.87 10.73 o 2 9 0 5927.51 5767.53 107.89 o 3 9 0 317.82 299.16 8.76 o 4 9 0 28.12 26.26 3.12 o 5 9 0 39.31 56.25 5.72 o 6 9 0 90.77 77.55 7.97 o 7 9 0 142.24 137.99 10.10 o 0 10 0 3078.83 2851.99 79.07 o 1 10 0 683.27 688.57 16.87 o 2 10 0 828.79 801.64 19.20 o 3 10 0 131.34 140.57 6.45 o 4 10 0 646.77 656.34 25.60 o 5 10 0 204.79 228.16 9.60 o 6 10 0 69.47 62.45 7.55 o 7 10 0 402.83 437.22 19.07 o 1 11 0 229.89 225.88 8.22 o 2 11 0 1591.70 1487.08 32.23 o 3 11 0 233.87 232.60 11.82 o 4 11 0 31.47 41.52 5.00 o 5 11 0 306.97 300.54 20.09 o 6 11 0 68.67 74.66 10.15 o 7 11 0 579.01 583.72 36.14 o 0 12 0 3977.62 3630.39 100.60 o 1 12 0 0.90 5.67 2.31 o 2 12 0 38.49 43.93 5.66 o 3 12 0 98.04 109.86 6.45 o 4 12 0 100.35 110.45 7.43 o 5 12 0 508.48 490.30 17.73 o 6 12 0 8.17 11.48 6.11 o 1 13 0 156.90 154.84 7.12 o 2 13 0 226.85 217.48 8.76 o 3 13 0 5.11 8.07 2.65 o 4 13 0 326.59 305.21 16.31 o 5 13 0 221.98 243.67 11.94 o 6 13 0 0.54 -6.10 16.84 o 0 14 0 180.63 167.10 10.74 o 1 14 0 148.31 116.38 6.44 o 2 14 0 618.66 589.85 17.03 o 3 14 0 334.28 311.72 13.56 o 4 14 0 147.76 147.27 23.51 o 5 14 0 32.18 36.00 5.47 o 1 15 0 1315.99 1161.13 33.98 o 2 15 0 158.07 171.19 10.45 o 3 15 0 50.65 65.84 6.15 o 4 15 0 287.40 264.05 12.65 o 0 16 0 98.44 105.96 9.82 o 1 16 0 377.31 369.50 13.24 o 2 16 0 221.81 223.30 10.22 o 3 16 0 353.42 329.54 12.58 o 1 17 0 230.29 232.16 12.17 o 2 17 0 100.77 119.02 18.00 o 1 0 1 221.04 248.55 7.54 o 2 0 1 3031.28 3461.62 62.62 o 3 0 1 5683.83 6218.26 112.16 o 4 0 1 89.88 78.00 4.06 o 5 0 1 82.39 84.80 5.31 o 6 0 1 1111.94 1130.71 29.62 o 7 0 1 230.09 236.17 10.67 o 8 0 1 34.55 34.41 5.23 o 9 0 1 114.38 135.85 15.68 o -9 1 1 216.95 192.17 18.29 o -8 1 1 89.79 95.55 7.96 o -7 1 1 218.68 214.82 9.99 o -6 1 1 1173.29 1180.50 30.62 o -5 1 1 1985.29 1969.29 74.20 o -4 1 1 776.14 824.18 17.84 o -3 1 1 921.23 1072.83 20.83 o -2 1 1 1789.14 1990.72 36.89 o -1 1 1 3553.71 3647.50 66.46 o 0 1 1 393.48 366.43 9.37 o 2 1 1 1804.24 1985.98 36.87 o 3 1 1 900.27 1015.96 18.54 o 4 1 1 787.49 807.02 15.67 o 5 1 1 1995.47 1949.45 63.55 o 6 1 1 1174.69 1174.21 44.12 o 7 1 1 213.34 192.98 9.55 o 8 1 1 92.53 98.18 8.05 o 9 1 1 214.60 187.82 18.58 o -9 2 1 122.76 126.27 15.09 o -8 2 1 80.02 80.72 7.48 o -7 2 1 1106.85 1098.64 30.08 o -6 2 1 1434.28 1492.13 37.25 o -5 2 1 1061.04 1108.11 28.01 o -4 2 1 1999.86 2396.42 41.03 o -3 2 1 638.69 653.20 14.95 o -2 2 1 5943.95 6416.21 103.74 o -1 2 1 3713.43 3558.04 126.27 o 0 2 1 914.51 919.57 30.67 o 1 2 1 3654.74 3434.06 102.33 o 2 2 1 5892.74 6465.05 103.78 o 3 2 1 640.17 649.78 18.33 o 4 2 1 1992.02 2403.26 40.97 o 5 2 1 1077.17 1106.54 27.26 o 6 2 1 1485.21 1521.79 37.27 o 7 2 1 1097.79 1092.71 29.98 o 8 2 1 73.11 77.88 7.29 o 9 2 1 120.49 112.05 15.68 o -9 3 1 143.38 148.79 13.21 o -8 3 1 483.42 473.04 17.34 o -7 3 1 196.65 198.33 9.70 o -6 3 1 568.09 556.80 17.69 o -5 3 1 147.13 140.43 7.02 o -4 3 1 323.90 284.21 8.13 o -3 3 1 5118.97 5857.85 95.71 o -2 3 1 887.60 882.07 14.54 o -1 3 1 4859.88 5020.02 126.84 o 1 3 1 4871.91 4864.64 111.83 o 2 3 1 899.81 929.20 20.56 o 3 3 1 5033.93 5895.84 106.48 o 4 3 1 334.59 297.35 7.25 o 5 3 1 148.95 156.34 6.20 o 6 3 1 600.95 578.80 18.98 o 7 3 1 192.14 183.49 9.46 o 8 3 1 485.19 462.78 17.15 o 9 3 1 143.66 154.62 13.10 o -8 4 1 22.14 28.62 4.86 o -7 4 1 146.05 140.13 8.16 o -6 4 1 374.62 401.01 14.14 o -5 4 1 643.99 656.47 18.85 o -4 4 1 504.17 506.67 11.76 o -3 4 1 1702.96 1795.91 26.41 o -2 4 1 12.90 22.43 1.42 o -1 4 1 1337.33 1312.82 22.89 o 1 4 1 1327.56 1323.40 36.30 o 2 4 1 10.44 21.59 1.80 o 3 4 1 1676.53 1809.16 40.26 o 4 4 1 484.28 488.99 13.51 o 5 4 1 646.58 664.28 18.02 o 6 4 1 384.47 406.80 14.25 o 7 4 1 141.07 145.61 8.33 o 8 4 1 21.23 27.07 4.94 o -8 5 1 157.16 143.12 8.84 o -7 5 1 605.14 566.06 18.73 o -6 5 1 954.86 905.74 25.42 o -5 5 1 185.93 195.80 8.46 o -4 5 1 409.81 376.22 9.64 o -3 5 1 646.27 635.28 11.67 o -2 5 1 3401.16 3576.68 53.28 o -1 5 1 761.78 794.86 12.57 o 0 5 1 165.40 149.35 5.66 o 1 5 1 761.06 803.31 17.45 o 2 5 1 3321.93 3463.28 64.70 o 3 5 1 671.53 662.53 14.59 o 4 5 1 402.18 356.48 10.18 o 5 5 1 187.19 184.99 8.76 o 6 5 1 958.58 937.76 25.64 o 7 5 1 594.46 554.00 18.57 o 8 5 1 154.12 154.00 12.83 o -8 6 1 202.58 188.66 11.55 o -7 6 1 276.11 249.33 12.56 o -6 6 1 29.51 30.77 4.52 o -5 6 1 576.81 583.40 23.75 o -4 6 1 465.01 475.96 10.14 o -3 6 1 413.83 462.03 9.20 o -2 6 1 923.37 932.91 15.86 o -1 6 1 818.03 833.30 18.66 o 0 6 1 4057.12 4235.40 83.33 o 1 6 1 864.41 862.76 16.81 o 2 6 1 916.21 945.93 21.12 o 3 6 1 415.92 457.71 11.33 o 4 6 1 484.40 512.90 13.15 o 5 6 1 584.82 570.50 15.12 o 6 6 1 28.15 31.38 4.53 o 7 6 1 273.82 246.55 12.66 o 8 6 1 202.99 201.33 22.35 o -8 7 1 170.21 186.13 11.85 o -7 7 1 136.56 137.10 9.35 o -6 7 1 15.06 16.61 4.14 o -5 7 1 226.42 208.49 8.77 o -4 7 1 2989.59 2954.85 53.41 o -3 7 1 506.81 482.08 9.27 o -2 7 1 2542.72 2599.05 41.66 o -1 7 1 1648.14 1822.13 33.20 o 0 7 1 621.81 573.90 13.32 o 1 7 1 1654.33 1796.92 33.26 o 2 7 1 2576.83 2632.98 47.21 o 3 7 1 514.88 494.21 12.05 o 4 7 1 2957.40 2998.39 56.96 o 5 7 1 223.32 240.31 10.29 o 6 7 1 17.81 20.97 4.26 o 7 7 1 139.90 139.13 9.47 o 8 7 1 171.32 167.04 13.78 o -8 8 1 15.39 15.17 4.47 o -7 8 1 470.56 473.42 30.44 o -6 8 1 465.95 431.35 17.30 o -5 8 1 235.17 205.42 12.11 o -4 8 1 111.01 109.31 5.70 o -3 8 1 4237.82 4164.61 74.47 o -2 8 1 425.36 379.88 9.67 o -1 8 1 462.00 448.18 10.55 o 0 8 1 1358.71 1180.99 24.83 o 1 8 1 482.53 463.85 12.79 o 2 8 1 427.02 405.15 11.61 o 3 8 1 4207.89 4241.25 74.74 o 4 8 1 125.15 114.75 5.16 o 5 8 1 243.10 225.54 9.46 o 6 8 1 450.51 425.79 17.29 o 7 8 1 463.82 453.11 18.90 o 8 8 1 15.70 25.08 6.44 o -7 9 1 163.39 146.38 10.42 o -6 9 1 74.57 79.03 7.94 o -5 9 1 139.37 147.55 7.86 o -4 9 1 348.56 367.89 12.15 o -3 9 1 1665.47 1594.11 31.21 o -2 9 1 819.67 790.15 18.22 o -1 9 1 1352.47 1204.62 62.60 o 0 9 1 1392.58 1267.98 26.88 o 1 9 1 1336.96 1150.27 32.85 o 2 9 1 834.64 747.54 18.07 o 3 9 1 1683.96 1622.96 35.57 o 4 9 1 341.02 335.79 10.02 o 5 9 1 142.66 138.43 7.63 o 6 9 1 72.02 73.90 7.94 o 7 9 1 163.50 147.15 12.24 o -7 10 1 180.80 218.81 20.44 o -6 10 1 137.12 147.73 10.01 o -5 10 1 32.98 44.03 4.86 o -4 10 1 844.79 840.70 23.99 o -3 10 1 735.07 706.14 17.86 o -2 10 1 1019.22 983.98 22.53 o -1 10 1 73.56 63.20 4.29 o 0 10 1 2.70 5.95 1.85 o 1 10 1 66.43 62.09 4.38 o 2 10 1 1038.06 986.72 22.67 o 3 10 1 745.00 730.87 18.12 o 4 10 1 831.26 843.13 23.63 o 5 10 1 32.77 41.63 5.08 o 6 10 1 135.68 142.26 10.02 o 7 10 1 177.54 215.31 12.76 o -7 11 1 22.44 22.64 7.25 o -6 11 1 627.94 673.17 28.45 o -5 11 1 362.37 371.87 14.40 o -4 11 1 38.22 39.58 7.00 o -3 11 1 43.50 50.14 4.56 o -2 11 1 847.43 774.31 19.18 o -1 11 1 18.86 23.14 3.11 o 0 11 1 603.42 535.96 14.38 o 1 11 1 18.98 26.55 3.33 o 2 11 1 837.73 781.76 30.34 o 3 11 1 47.45 68.25 5.95 o 4 11 1 40.01 50.36 8.00 o 5 11 1 359.30 374.88 14.63 o 6 11 1 624.94 645.55 28.22 o -6 12 1 51.96 56.13 9.83 o -5 12 1 11.23 19.29 7.56 o -4 12 1 262.15 249.55 11.23 o -3 12 1 128.52 115.01 6.02 o -2 12 1 1361.42 1301.70 29.15 o -1 12 1 858.42 772.55 19.36 o 0 12 1 38.66 39.25 4.08 o 1 12 1 824.54 773.41 19.46 o 2 12 1 1363.27 1254.38 33.87 o 3 12 1 125.99 112.41 6.06 o 4 12 1 261.36 245.34 11.28 o 5 12 1 11.68 10.56 3.46 o 6 12 1 54.75 70.14 10.50 o -6 13 1 45.68 38.90 19.45 o -5 13 1 260.83 287.82 16.25 o -4 13 1 86.46 97.67 10.16 o -3 13 1 234.42 227.46 11.06 o -2 13 1 123.92 111.98 6.24 o -1 13 1 624.78 580.93 16.25 o 0 13 1 51.53 44.22 4.38 o 1 13 1 636.06 597.33 16.46 o 2 13 1 115.62 103.92 7.27 o 3 13 1 235.43 238.08 23.75 o 4 13 1 85.29 90.94 7.39 o 5 13 1 257.63 262.48 12.61 o 6 13 1 46.50 33.67 20.90 o -5 14 1 104.54 101.46 8.00 o -4 14 1 481.73 514.15 23.00 o -3 14 1 131.65 136.59 7.20 o -2 14 1 118.44 114.33 6.56 o -1 14 1 184.88 156.54 7.46 o 0 14 1 94.04 99.54 6.07 o 1 14 1 182.18 160.88 8.21 o 2 14 1 113.51 112.58 6.71 o 3 14 1 125.33 125.13 7.11 o 4 14 1 478.47 495.37 22.92 o 5 14 1 98.64 90.95 8.03 o -4 15 1 308.99 305.90 17.50 o -3 15 1 64.25 72.21 9.09 o -2 15 1 265.52 245.30 10.11 o -1 15 1 223.86 188.48 8.66 o 0 15 1 0.03 -0.41 2.01 o 1 15 1 220.14 184.64 8.58 o 2 15 1 265.60 239.34 10.08 o 3 15 1 66.76 73.34 9.33 o 4 15 1 312.09 355.20 31.35 o -3 16 1 13.96 18.76 3.62 o -2 16 1 64.16 69.99 6.42 o -1 16 1 201.60 177.68 8.70 o 0 16 1 253.83 226.00 9.88 o 1 16 1 205.47 186.69 8.85 o 2 16 1 66.29 69.89 6.20 o 3 16 1 15.58 17.44 3.28 o -2 17 1 40.54 39.77 11.90 o -1 17 1 34.23 44.19 7.20 o 0 17 1 41.60 48.31 5.30 o 1 17 1 33.98 37.78 5.23 o 2 17 1 43.61 45.57 11.90 o 0 0 2 1003.36 1077.04 32.11 o 1 0 2 2326.98 2437.94 41.54 o 2 0 2 1924.48 2124.31 80.41 o 3 0 2 3167.57 3623.19 65.91 o 4 0 2 233.83 248.66 7.44 o 5 0 2 431.60 429.15 11.55 o 6 0 2 757.21 749.05 30.60 o 7 0 2 22.36 26.17 4.20 o 8 0 2 112.02 115.24 9.94 o 9 0 2 298.09 286.22 23.51 o -9 1 2 25.62 27.58 8.71 o -8 1 2 276.91 266.86 15.04 o -7 1 2 293.20 265.44 11.40 o -6 1 2 76.20 81.90 6.25 o -5 1 2 968.34 936.92 26.86 o -4 1 2 381.85 374.56 9.69 o -3 1 2 417.91 439.26 9.04 o -2 1 2 634.15 690.06 14.65 o -1 1 2 1747.44 1711.01 39.16 o 0 1 2 1.10 3.66 0.57 o 2 1 2 605.76 675.93 13.96 o 3 1 2 425.72 443.46 10.50 o 4 1 2 376.33 350.73 9.62 o 5 1 2 929.35 957.39 21.22 o 6 1 2 69.79 76.16 6.07 o 7 1 2 278.23 264.88 11.39 o 8 1 2 276.70 271.81 17.78 o 9 1 2 26.47 40.06 10.16 o -9 2 2 62.42 53.70 12.19 o -8 2 2 181.07 163.94 11.60 o -7 2 2 105.95 109.79 7.24 o -6 2 2 273.78 263.12 10.76 o -5 2 2 1701.89 1815.67 36.68 o -4 2 2 2979.58 3279.07 55.25 o -3 2 2 1764.36 1870.49 32.03 o -2 2 2 2575.82 2725.02 50.57 o -1 2 2 2599.24 2704.14 49.23 o 0 2 2 2928.85 2897.96 73.25 o 1 2 2 2628.90 2756.48 53.23 o 2 2 2 2578.29 2726.66 101.89 o 3 2 2 1779.81 1854.64 35.97 o 4 2 2 2989.77 3310.47 62.03 o 5 2 2 1693.46 1823.86 36.86 o 6 2 2 290.95 270.65 10.84 o 7 2 2 95.66 100.69 7.12 o 8 2 2 183.54 183.64 12.25 o 9 2 2 62.12 65.60 12.48 o -9 3 2 592.61 547.77 35.41 o -8 3 2 90.31 106.37 10.73 o -7 3 2 381.73 379.55 14.39 o -6 3 2 356.26 342.48 12.60 o -5 3 2 279.76 281.95 8.91 o -4 3 2 609.36 616.86 12.93 o -3 3 2 3131.93 3375.02 52.00 o -2 3 2 3543.87 3555.61 58.62 o 0 3 2 3754.69 3694.68 72.82 o 1 3 2 2013.59 1787.29 68.80 o 2 3 2 3589.82 3575.46 130.34 o 3 3 2 3154.88 3415.43 63.23 o 4 3 2 604.87 640.68 14.90 o 5 3 2 277.25 286.58 9.10 o 6 3 2 342.30 333.18 12.95 o 7 3 2 381.25 374.77 14.26 o 8 3 2 93.33 94.62 10.14 o -8 4 2 19.38 20.53 5.51 o -7 4 2 2.13 4.72 2.83 o -6 4 2 250.90 246.04 10.37 o -5 4 2 1195.45 1150.39 29.56 o -4 4 2 12.43 18.02 2.11 o -3 4 2 78.25 64.93 2.27 o -2 4 2 2282.56 2357.73 37.69 o 0 4 2 184.56 217.32 5.61 o 2 4 2 2366.93 2345.51 91.44 o 3 4 2 73.49 64.00 3.74 o 4 4 2 10.99 16.21 2.55 o 5 4 2 1211.48 1230.73 28.16 o 6 4 2 248.77 243.52 10.25 o 7 4 2 2.91 2.73 2.70 o 8 4 2 21.44 28.44 6.09 o -8 5 2 256.92 255.14 12.13 o -7 5 2 13.04 17.91 3.89 o -6 5 2 192.69 186.55 8.94 o -5 5 2 760.23 774.29 21.12 o -4 5 2 190.14 205.00 6.23 o -3 5 2 1835.05 1924.97 30.48 o -2 5 2 310.08 332.60 6.12 o 1 5 2 3017.55 2905.76 111.18 o 2 5 2 322.93 358.45 9.35 o 3 5 2 1804.84 1942.12 37.59 o 4 5 2 204.14 224.57 9.18 o 5 5 2 756.63 735.68 20.86 o 6 5 2 197.98 188.01 8.97 o 7 5 2 14.93 14.86 3.71 o 8 5 2 257.55 250.49 14.64 o -8 6 2 180.87 174.95 10.94 o -7 6 2 203.81 193.99 11.10 o -6 6 2 507.64 496.24 16.46 o -5 6 2 363.33 369.54 12.87 o -4 6 2 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