#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/38/2013880.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2013880_Fobs loop_ _publ_author_name 'Nygren, Cara L.' 'Bragg, M. E. T.' 'Turner, John F. C.' _publ_section_title ; Tetrakis(tetrahydrofuran-\kO)lithium mer-tris(carbazolyl-\kN)-trans-dichloro(tetrahydrofuran-\kO)zirconate ; _journal_issue 2 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first m94 _journal_page_last m96 _journal_volume 60 _journal_year 2004 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 113.220 _cell_angle_gamma 90.000 _cell_length_a 14.9840 _cell_length_b 27.4349 _cell_length_c 13.5736 _exptl_crystal_F_000 2152.00 _reflns_d_resolution_high 0.8076 _[local]_cod_data_source_file sq1141Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' sep1m in C2/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 504.56 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 40836.00 43728.04 684.04 o 4 0 0 8614.62 9073.37 158.38 o 6 0 0 38745.15 37379.56 601.56 o 8 0 0 16168.19 16378.05 288.08 o 10 0 0 17916.48 18501.57 420.00 o 12 0 0 4384.33 4621.23 170.38 o 14 0 0 3207.08 3410.08 228.35 o 16 0 0 2141.82 2451.77 212.66 o 1 1 0 41564.33 44184.80 521.73 o 3 1 0 177613.34 183367.45 2004.24 o 5 1 0 95907.27 100395.91 1106.44 o 7 1 0 12934.30 12434.43 157.71 o 9 1 0 6847.78 7402.94 111.67 o 11 1 0 2993.49 3204.24 92.22 o 13 1 0 9984.88 9755.98 204.47 o 15 1 0 3525.51 3737.16 341.71 o 17 1 0 1290.33 1171.21 119.47 o 0 2 0 21655.73 22162.31 500.75 o 2 2 0 13030.76 13444.01 153.76 o 4 2 0 29021.78 30215.96 341.52 o 6 2 0 21648.31 23799.86 296.61 o 8 2 0 8872.94 9230.63 125.74 o 10 2 0 4772.90 4750.44 87.28 o 12 2 0 3200.96 3185.09 95.15 o 14 2 0 1145.30 997.54 96.08 o 16 2 0 1333.57 1139.73 112.20 o 1 3 0 8440.33 8587.07 106.67 o 3 3 0 470.12 556.23 19.65 o 5 3 0 62.88 90.07 14.78 o 7 3 0 106.40 127.29 24.25 o 9 3 0 3209.10 3617.54 66.34 o 11 3 0 1228.31 1351.13 50.05 o 13 3 0 155.20 117.12 51.32 o 15 3 0 47.95 67.01 74.87 o 0 4 0 4088.49 4109.44 106.06 o 2 4 0 2541.63 2715.48 45.80 o 4 4 0 521.81 548.09 19.37 o 6 4 0 433.79 630.63 24.03 o 8 4 0 6518.25 6949.54 100.68 o 10 4 0 3540.19 3545.94 72.81 o 12 4 0 24.37 -30.43 32.22 o 14 4 0 1680.07 1483.16 110.00 o 16 4 0 1.44 58.26 101.73 o 1 5 0 1633.50 1516.84 27.97 o 3 5 0 40297.07 41674.13 558.48 o 5 5 0 9286.71 9774.45 123.94 o 7 5 0 9704.20 9865.34 130.72 o 9 5 0 5933.52 6156.94 101.92 o 11 5 0 1119.90 1126.28 47.30 o 13 5 0 4329.54 4443.31 203.36 o 15 5 0 222.65 237.13 81.17 o 0 6 0 108479.72 108296.84 2407.42 o 2 6 0 42245.96 45017.70 631.17 o 4 6 0 36562.44 36827.09 416.55 o 6 6 0 27007.26 26605.58 310.28 o 8 6 0 7363.42 6653.13 98.17 o 10 6 0 2877.59 2955.59 67.29 o 12 6 0 7457.61 7758.08 169.71 o 14 6 0 562.24 768.32 89.43 o 16 6 0 15.10 4.89 70.38 o 1 7 0 70995.20 74518.45 1075.57 o 3 7 0 36906.31 36770.21 473.14 o 5 7 0 14567.98 14279.27 174.11 o 7 7 0 18307.29 17970.38 220.72 o 9 7 0 14087.04 12969.68 183.69 o 11 7 0 2023.89 2264.24 64.30 o 13 7 0 2997.53 3177.72 119.72 o 15 7 0 2232.65 2390.97 139.89 o 0 8 0 7674.77 7538.68 196.87 o 2 8 0 29943.03 30920.41 399.37 o 4 8 0 27117.56 26294.02 346.25 o 6 8 0 16351.25 16035.85 225.46 o 8 8 0 2811.02 2615.38 61.32 o 10 8 0 1334.19 1449.67 46.96 o 12 8 0 10376.08 10185.18 208.91 o 14 8 0 2403.82 2379.29 136.45 o 16 8 0 1369.14 1353.22 112.60 o 1 9 0 28651.69 27953.09 402.02 o 3 9 0 5890.65 5903.89 90.25 o 5 9 0 2221.59 2607.26 49.83 o 7 9 0 7389.21 7613.03 101.98 o 9 9 0 2896.07 2846.29 63.79 o 11 9 0 88.56 46.97 44.10 o 13 9 0 1798.14 1859.01 92.70 o 15 9 0 484.71 410.29 92.97 o 0 10 0 1326.32 1071.22 59.50 o 2 10 0 700.67 779.69 26.22 o 4 10 0 15.22 8.17 15.77 o 6 10 0 2823.88 2974.98 54.59 o 8 10 0 323.40 273.66 29.39 o 10 10 0 505.76 551.26 38.43 o 12 10 0 2.08 -24.59 30.36 o 14 10 0 62.92 35.65 63.99 o 16 10 0 91.34 166.20 85.30 o 1 11 0 19211.93 19707.93 292.23 o 3 11 0 875.04 611.10 27.19 o 5 11 0 748.06 766.58 28.74 o 7 11 0 567.49 535.68 29.61 o 9 11 0 542.41 584.13 33.50 o 11 11 0 1571.52 1491.48 53.91 o 13 11 0 957.80 830.52 118.19 o 15 11 0 378.20 235.28 116.34 o 0 12 0 21336.78 21814.78 525.88 o 2 12 0 22474.02 23233.89 307.68 o 4 12 0 6685.41 5603.15 99.68 o 6 12 0 28215.24 27469.17 347.15 o 8 12 0 15098.96 15031.99 222.38 o 10 12 0 3124.73 3211.53 77.36 o 12 12 0 2490.76 2351.24 76.46 o 14 12 0 1261.60 1395.18 110.17 o 1 13 0 14908.78 14978.50 268.57 o 3 13 0 31906.32 32100.11 438.83 o 5 13 0 44736.14 44365.31 578.40 o 7 13 0 37838.59 37497.03 467.41 o 9 13 0 8596.87 8559.30 135.97 o 11 13 0 7001.71 7124.68 133.22 o 13 13 0 4284.58 4711.26 156.45 o 15 13 0 1725.90 1891.17 129.14 o 0 14 0 51735.36 51876.03 975.90 o 2 14 0 33100.00 34488.25 526.38 o 4 14 0 13796.83 13363.19 208.16 o 6 14 0 16941.10 17189.36 230.29 o 8 14 0 7560.33 7337.81 167.71 o 10 14 0 20707.06 20304.28 277.97 o 12 14 0 6276.98 6581.27 141.24 o 14 14 0 665.83 704.50 98.28 o 1 15 0 10526.34 10079.60 225.54 o 3 15 0 2621.46 2366.87 49.97 o 5 15 0 20272.81 19442.68 366.45 o 7 15 0 9630.40 8983.06 137.84 o 9 15 0 781.64 818.02 41.06 o 11 15 0 6542.38 6605.87 128.02 o 13 15 0 3698.62 3705.77 133.54 o 15 15 0 691.25 781.28 101.23 o 0 16 0 365.81 291.22 67.77 o 2 16 0 2939.13 2678.31 60.66 o 4 16 0 2.99 -15.37 19.58 o 6 16 0 8278.12 8342.77 148.11 o 8 16 0 1298.39 1324.79 49.64 o 10 16 0 659.77 610.64 39.20 o 12 16 0 506.64 592.08 49.61 o 14 16 0 163.49 67.36 69.60 o 1 17 0 653.78 653.26 44.32 o 3 17 0 1240.62 1330.19 58.66 o 5 17 0 91.01 82.69 27.01 o 7 17 0 371.96 307.47 35.54 o 9 17 0 18.07 -30.30 30.30 o 11 17 0 8.26 -32.34 32.34 o 13 17 0 144.54 241.07 77.23 o 0 18 0 12167.22 12377.28 341.59 o 2 18 0 4.48 32.66 29.27 o 4 18 0 2553.45 2586.77 85.69 o 6 18 0 3.16 -32.70 32.70 o 8 18 0 1025.06 1113.14 63.59 o 10 18 0 1483.32 1535.76 74.85 o 12 18 0 487.18 446.15 119.31 o 1 19 0 5760.25 5374.23 194.20 o 3 19 0 10879.88 10539.02 217.48 o 5 19 0 3901.96 3888.89 111.76 o 7 19 0 1901.67 1922.56 80.50 o 9 19 0 4386.56 4352.48 129.51 o 11 19 0 2.13 29.34 47.30 o 13 19 0 1557.90 1529.72 164.50 o 0 20 0 16041.96 16214.69 434.83 o 2 20 0 10498.03 10498.38 217.89 o 4 20 0 13552.09 13098.35 297.82 o 6 20 0 6787.73 6264.27 313.67 o 8 20 0 3518.05 3624.15 115.74 o 10 20 0 2263.76 2153.93 134.81 o 12 20 0 1479.94 1615.19 123.46 o 1 21 0 8972.25 9732.45 260.75 o 3 21 0 3258.70 3444.31 106.45 o 5 21 0 3601.49 3443.41 199.04 o 7 21 0 7908.83 7655.64 186.16 o 9 21 0 6321.80 6656.20 206.43 o 11 21 0 2852.04 2991.51 123.34 o 13 21 0 1974.19 1891.45 183.71 o 0 22 0 186.70 253.89 61.15 o 2 22 0 354.65 444.00 50.48 o 4 22 0 1671.44 1601.19 120.43 o 6 22 0 10089.38 10564.18 254.89 o 8 22 0 1604.57 1707.13 96.81 o 10 22 0 1805.05 1703.88 109.23 o 12 22 0 2517.59 2511.45 150.82 o 1 23 0 945.78 885.47 68.60 o 3 23 0 3763.35 3368.98 109.71 o 5 23 0 228.88 209.01 50.34 o 7 23 0 1806.77 1845.24 106.67 o 9 23 0 682.52 788.42 67.59 o 11 23 0 522.34 674.32 73.37 o 0 24 0 165.82 327.38 112.28 o 2 24 0 474.44 418.27 53.96 o 4 24 0 43.12 -7.01 41.43 o 6 24 0 202.93 202.97 53.36 o 8 24 0 464.32 384.73 61.49 o 10 24 0 356.33 340.41 66.27 o 1 25 0 2856.26 2803.45 102.50 o 3 25 0 3262.01 3236.61 111.57 o 5 25 0 2325.30 2450.01 111.45 o 7 25 0 121.49 85.47 49.07 o 9 25 0 1113.81 1229.22 80.08 o 11 25 0 611.08 742.98 80.85 o 0 26 0 8804.45 9012.85 512.03 o 2 26 0 7257.80 6760.66 175.71 o 4 26 0 6157.00 6076.66 187.32 o 6 26 0 3137.98 3099.06 115.95 o 8 26 0 1314.38 1482.31 85.65 o 10 26 0 1400.15 1623.08 101.64 o 1 27 0 3335.31 3445.48 118.15 o 3 27 0 7308.87 7411.39 190.08 o 5 27 0 1990.25 1890.26 112.23 o 7 27 0 3922.52 3726.10 190.73 o 9 27 0 1191.20 1288.20 140.27 o 0 28 0 7531.53 7032.72 261.02 o 2 28 0 774.52 919.16 71.07 o 4 28 0 1188.03 1302.80 129.35 o 6 28 0 5590.15 5220.67 190.48 o 8 28 0 618.51 640.06 78.34 o 1 29 0 1982.03 1894.18 92.59 o 3 29 0 1571.39 1675.34 101.43 o 5 29 0 369.36 368.75 64.27 o 7 29 0 656.08 722.78 79.66 o 0 30 0 3124.10 3132.80 168.40 o 2 30 0 3.76 -45.70 45.70 o 4 30 0 28.45 -44.79 48.96 o 6 30 0 817.45 852.96 83.44 o 1 31 0 168.03 176.30 60.04 o 3 31 0 160.23 239.14 72.67 o 5 31 0 107.89 32.26 56.45 o 0 32 0 52.47 -1.87 74.38 o 2 32 0 2185.07 2128.94 105.21 o 4 32 0 441.95 389.41 72.24 o 1 33 0 1014.24 990.07 84.51 o 3 33 0 983.89 909.22 113.80 o -17 1 1 354.92 203.57 85.13 o -15 1 1 1302.53 1058.99 103.92 o -13 1 1 1359.37 1246.16 100.39 o -11 1 1 3410.40 3348.79 66.88 o -9 1 1 891.26 830.32 30.53 o -7 1 1 1515.02 1586.41 36.98 o -5 1 1 31981.42 33507.20 379.10 o -3 1 1 184.71 215.63 11.76 o -1 1 1 22777.81 23747.09 285.26 o 1 1 1 77.60 56.47 8.99 o 3 1 1 4644.22 4811.41 70.20 o 5 1 1 2845.00 3149.40 50.69 o 7 1 1 2223.63 2387.71 46.71 o 9 1 1 440.28 491.25 28.10 o 11 1 1 33.93 47.39 34.31 o 13 1 1 648.85 631.85 54.52 o 15 1 1 21.52 -59.63 59.63 o -16 2 1 2557.64 2680.61 155.57 o -14 2 1 7455.46 7110.26 248.91 o -12 2 1 1800.75 1746.30 64.77 o -10 2 1 12717.94 12759.41 169.96 o -8 2 1 8535.25 8004.94 111.25 o -6 2 1 33515.55 34913.89 398.10 o -4 2 1 382.17 428.86 27.90 o -2 2 1 12517.95 13347.27 190.87 o 0 2 1 114676.20 117160.23 1373.86 o 2 2 1 2561.27 2586.73 39.69 o 4 2 1 13029.13 12741.60 152.97 o 6 2 1 13722.39 14844.38 181.92 o 8 2 1 6034.73 6320.60 94.41 o 10 2 1 805.32 931.45 71.15 o 12 2 1 4262.29 3940.58 121.97 o 14 2 1 207.98 175.04 144.75 o 16 2 1 192.37 85.33 76.21 o -17 3 1 832.75 820.74 117.53 o -15 3 1 2854.33 3109.70 282.73 o -13 3 1 15362.77 15895.85 432.26 o -11 3 1 6286.33 6662.10 128.19 o -9 3 1 17784.85 19060.00 235.45 o -7 3 1 31689.44 31839.56 368.40 o -5 3 1 27506.95 25927.75 342.22 o -3 3 1 8374.53 7502.79 91.99 o -1 3 1 24767.71 28100.79 298.61 o 1 3 1 4737.48 4799.21 58.85 o 3 3 1 67223.60 67366.39 741.92 o 5 3 1 20862.79 20607.38 241.95 o 7 3 1 10218.55 10018.49 132.38 o 9 3 1 14910.82 15470.77 211.95 o 11 3 1 322.77 410.62 46.73 o 13 3 1 1393.97 1202.87 89.77 o 15 3 1 855.93 797.39 98.60 o -16 4 1 1246.43 1209.32 115.64 o -14 4 1 5013.80 5147.29 318.04 o -12 4 1 5243.63 5470.31 101.30 o -10 4 1 25802.05 25909.94 314.58 o -8 4 1 11960.11 11391.01 148.97 o -6 4 1 51009.73 51290.69 732.32 o -4 4 1 5071.91 4480.80 72.99 o -2 4 1 14.01 22.06 7.94 o 0 4 1 4025.47 4121.87 51.30 o 2 4 1 423.42 309.65 27.42 o 4 4 1 28154.12 27623.77 336.66 o 6 4 1 8342.21 8000.62 108.15 o 8 4 1 3070.94 2839.11 63.84 o 10 4 1 2689.04 2811.44 76.98 o 12 4 1 5071.00 5129.14 130.89 o 14 4 1 649.60 771.37 92.79 o 16 4 1 71.51 2.23 74.03 o -17 5 1 505.50 560.44 108.61 o -15 5 1 2.09 -30.64 74.67 o -13 5 1 9182.13 8302.77 268.00 o -11 5 1 4961.18 5065.86 103.43 o -9 5 1 11495.18 10935.44 147.60 o -7 5 1 7165.95 7390.60 109.92 o -5 5 1 1903.27 1706.41 49.52 o -3 5 1 8749.23 8083.68 187.50 o -1 5 1 22801.33 24881.22 263.81 o 1 5 1 226.78 171.53 11.28 o 3 5 1 4367.14 4847.52 76.36 o 5 5 1 5751.38 5450.66 78.08 o 7 5 1 7065.18 6994.84 99.85 o 9 5 1 480.90 503.59 30.90 o 11 5 1 2019.63 2025.32 75.73 o 13 5 1 268.13 193.20 44.31 o 15 5 1 71.47 -56.28 61.69 o -16 6 1 825.87 884.66 110.77 o -14 6 1 207.28 204.83 110.25 o -12 6 1 0.63 -24.65 24.65 o -10 6 1 2376.07 2345.23 57.14 o -8 6 1 198.11 335.45 24.24 o -6 6 1 1934.34 1698.46 50.17 o -4 6 1 11614.76 12946.75 165.14 o -2 6 1 1565.40 1557.72 28.96 o 0 6 1 2374.81 2428.03 34.80 o 2 6 1 7141.29 6920.49 86.93 o 4 6 1 3067.46 2800.56 48.31 o 6 6 1 12631.08 13861.40 200.60 o 8 6 1 1850.91 1649.97 45.28 o 10 6 1 228.19 357.14 48.46 o 12 6 1 264.98 212.15 46.21 o 14 6 1 56.35 -8.56 61.21 o 16 6 1 16.69 113.11 69.82 o -17 7 1 41.08 -3.66 77.99 o -15 7 1 369.91 355.49 85.19 o -13 7 1 868.42 1095.98 94.79 o -11 7 1 3776.29 3858.94 79.41 o -9 7 1 1098.17 1184.59 46.39 o -7 7 1 2646.64 2736.43 51.81 o -5 7 1 0.42 -12.90 12.90 o -3 7 1 11733.47 12083.46 157.04 o -1 7 1 929.05 1021.81 31.74 o 1 7 1 333.51 394.20 38.26 o 3 7 1 743.64 822.21 46.71 o 5 7 1 442.51 498.07 25.27 o 7 7 1 381.18 469.95 24.46 o 9 7 1 126.94 127.41 25.11 o 11 7 1 1149.62 1072.57 80.60 o 13 7 1 86.98 69.99 51.24 o 15 7 1 180.23 252.90 86.55 o -16 8 1 1270.80 1331.56 253.24 o -14 8 1 296.21 246.04 72.51 o -12 8 1 70.90 77.96 30.08 o -10 8 1 29.73 13.95 22.38 o -8 8 1 1640.87 1591.43 40.18 o -6 8 1 14571.88 16040.08 196.98 o -4 8 1 1157.93 1306.53 41.75 o -2 8 1 341.59 398.18 15.37 o 0 8 1 10944.13 10352.66 144.52 o 2 8 1 1614.51 1539.50 29.61 o 4 8 1 24987.97 26279.85 304.80 o 6 8 1 45.11 23.67 19.99 o 8 8 1 1296.27 1432.80 42.70 o 10 8 1 812.31 844.77 41.74 o 12 8 1 1561.53 1503.09 69.12 o 14 8 1 143.20 116.72 53.12 o 16 8 1 69.92 52.37 81.56 o -15 9 1 3054.24 3195.85 163.07 o -13 9 1 7376.20 7489.81 209.56 o -11 9 1 3801.94 3961.32 81.42 o -9 9 1 3735.65 3899.33 76.01 o -7 9 1 2109.55 2063.72 45.00 o -5 9 1 12627.09 11639.06 147.12 o -3 9 1 67732.29 66195.06 780.97 o -1 9 1 7184.82 6376.81 95.84 o 1 9 1 17093.89 16272.02 207.04 o 3 9 1 23.83 9.92 12.57 o 5 9 1 1770.09 2016.53 47.41 o 7 9 1 5799.36 5930.09 90.62 o 9 9 1 1607.51 1609.48 51.76 o 11 9 1 4963.33 4654.63 120.35 o 13 9 1 65.77 -37.29 37.29 o 15 9 1 733.77 713.14 105.79 o -16 10 1 3039.65 2886.77 161.16 o -14 10 1 5503.49 5857.12 241.20 o -12 10 1 12030.80 12757.41 228.91 o -10 10 1 4569.13 4718.18 83.03 o -8 10 1 34265.69 34257.79 429.37 o -6 10 1 27893.35 26520.37 360.31 o -4 10 1 8850.31 7229.72 120.04 o -2 10 1 17985.39 17934.24 223.58 o 0 10 1 62468.58 63580.76 818.32 o 2 10 1 13843.35 13999.34 178.49 o 4 10 1 1390.84 1031.15 29.42 o 6 10 1 8226.07 7945.22 111.78 o 8 10 1 7518.18 7637.59 120.48 o 10 10 1 713.22 693.49 39.45 o 12 10 1 4905.23 5109.74 132.40 o 14 10 1 2475.88 2370.36 110.21 o -15 11 1 1969.17 2001.70 140.15 o -13 11 1 5253.21 5455.07 142.49 o -11 11 1 8346.86 8213.48 135.82 o -9 11 1 6756.61 6820.03 112.45 o -7 11 1 33723.63 34346.45 427.57 o -5 11 1 13701.19 12253.44 206.56 o -3 11 1 15159.45 14915.62 203.84 o -1 11 1 43017.59 46463.80 604.90 o 1 11 1 32654.14 34038.93 410.54 o 3 11 1 29309.28 29624.41 340.99 o 5 11 1 10993.62 10710.60 155.11 o 7 11 1 4310.26 4196.35 77.64 o 9 11 1 507.84 540.72 34.10 o 11 11 1 3334.14 3309.26 91.51 o 13 11 1 1809.33 1722.83 93.10 o 15 11 1 284.06 343.23 87.29 o -16 12 1 690.06 838.54 113.82 o -14 12 1 949.55 882.83 92.39 o -12 12 1 4229.72 4475.09 111.27 o -10 12 1 1388.74 1461.08 48.73 o -8 12 1 6332.09 6388.98 145.39 o -6 12 1 3187.78 3013.14 59.68 o -4 12 1 13947.43 13848.57 285.77 o -2 12 1 31415.11 33187.83 433.38 o 0 12 1 19289.94 19818.68 270.11 o 2 12 1 10329.16 10001.77 134.21 o 4 12 1 2074.00 1989.21 48.48 o 6 12 1 13812.88 14929.83 202.69 o 8 12 1 1918.36 2027.92 52.84 o 10 12 1 148.75 183.92 32.76 o 12 12 1 537.60 544.78 53.49 o 14 12 1 60.59 -45.19 60.20 o -15 13 1 783.45 839.62 103.34 o -13 13 1 17.51 -10.42 46.82 o -11 13 1 1869.66 1884.79 57.76 o -9 13 1 236.59 274.00 30.84 o -7 13 1 8326.88 8388.06 127.59 o -5 13 1 5833.92 5680.82 99.81 o -3 13 1 1196.57 1404.43 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