#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/38/2013881.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2013881_Fobs loop_ _publ_author_name 'Korendovych, Ivan V.' 'Rybak-Akimova, Elena V.' _publ_section_title ; Chloro{2,2'-[(1S,2S)-1,2-diphenyl-1,2-ethanediylbis(nitrilomethylidyne)]diphenolato-\k^4^O,N,N',O'}(ethanol-\kO)manganese(III) ; _journal_issue 2 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first m82 _journal_page_last m84 _journal_volume 60 _journal_year 2004 _space_group_IT_number 19 _symmetry_space_group_name_Hall 'P 2ac 2ab' _symmetry_space_group_name_H-M 'P 21 21 21' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 13.3857 _cell_length_b 19.4666 _cell_length_c 20.8229 _exptl_crystal_F_000 2304.00 _reflns_d_resolution_high 0.7505 _[local]_cod_data_source_file sq1142Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' sad in P2(1)2(1)2(1)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 302.60 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 83964.34 73377.37 4289.86 o 4 0 0 2661.37 2749.40 57.00 o 6 0 0 2829.00 2849.43 56.83 o 8 0 0 4328.92 4610.14 90.50 o 10 0 0 180.67 200.88 11.98 o 12 0 0 18030.22 17657.35 477.92 o 14 0 0 4864.05 4734.29 144.65 o 16 0 0 7.15 28.46 27.48 o 1 1 0 0.74 16.85 3.05 o 2 1 0 206.25 235.38 5.19 o 3 1 0 4363.59 4197.75 57.08 o 4 1 0 63.14 72.98 3.16 o 5 1 0 806.59 801.65 13.28 o 6 1 0 901.56 887.35 14.20 o 7 1 0 219.17 252.65 6.89 o 8 1 0 387.62 374.90 9.75 o 9 1 0 299.11 328.55 11.10 o 10 1 0 150.41 153.15 8.81 o 11 1 0 199.67 225.30 11.21 o 12 1 0 77.57 82.77 9.62 o 13 1 0 1735.14 1727.23 44.23 o 14 1 0 221.21 235.05 16.91 o 15 1 0 762.02 716.01 27.38 o 16 1 0 14.15 3.35 14.40 o 17 1 0 90.06 71.64 39.25 o 1 2 0 19.06 36.63 2.93 o 2 2 0 16235.54 16866.77 298.78 o 3 2 0 13897.55 15762.80 251.47 o 4 2 0 12400.42 12671.80 200.04 o 5 2 0 28573.47 30329.49 471.73 o 6 2 0 891.71 911.42 19.95 o 7 2 0 10483.02 11224.49 160.38 o 8 2 0 285.76 274.83 9.62 o 9 2 0 2367.06 2206.54 39.69 o 10 2 0 994.62 1025.98 22.71 o 11 2 0 291.98 324.12 12.73 o 12 2 0 10192.14 10063.72 159.44 o 13 2 0 326.03 326.20 13.44 o 14 2 0 2791.96 2670.91 64.59 o 15 2 0 400.66 334.46 22.76 o 16 2 0 7.47 4.69 13.50 o 17 2 0 388.06 389.59 52.99 o 1 3 0 28.41 50.00 2.87 o 2 3 0 311.64 322.86 7.36 o 3 3 0 38.67 30.54 5.41 o 4 3 0 5223.22 5360.36 86.81 o 5 3 0 4507.84 4484.51 73.42 o 6 3 0 2593.40 2645.32 41.48 o 7 3 0 0.91 -3.66 3.66 o 8 3 0 8.58 3.89 4.30 o 9 3 0 81.30 104.64 7.20 o 10 3 0 21.45 17.81 5.22 o 11 3 0 11.42 15.62 5.99 o 12 3 0 46.61 34.06 8.78 o 13 3 0 1065.93 1035.06 28.16 o 14 3 0 7.84 -8.99 9.03 o 15 3 0 547.91 505.49 30.28 o 16 3 0 0.02 -4.26 12.44 o 17 3 0 51.07 34.35 24.53 o 0 4 0 28154.36 29122.71 809.44 o 1 4 0 8112.47 7969.60 156.03 o 2 4 0 33422.85 36408.64 625.14 o 3 4 0 4442.59 4647.94 76.42 o 4 4 0 5489.64 6483.77 116.07 o 5 4 0 4643.02 4383.00 72.01 o 6 4 0 1366.79 1487.07 27.32 o 7 4 0 3586.53 3533.78 59.67 o 8 4 0 681.21 647.06 18.64 o 9 4 0 4513.32 4309.88 83.21 o 10 4 0 620.84 553.58 15.36 o 11 4 0 133.27 122.28 8.51 o 12 4 0 1832.83 1771.66 39.80 o 13 4 0 981.48 979.63 27.64 o 14 4 0 1902.04 1803.63 42.62 o 15 4 0 46.68 34.63 14.53 o 16 4 0 123.90 103.38 17.51 o 17 4 0 571.94 579.02 32.23 o 1 5 0 247.12 161.00 6.44 o 2 5 0 256.10 262.64 7.41 o 3 5 0 10081.39 9350.77 185.60 o 4 5 0 64.40 90.20 4.86 o 5 5 0 9.22 33.57 5.15 o 6 5 0 2650.59 2849.98 48.96 o 7 5 0 131.43 145.97 6.05 o 8 5 0 0.85 -1.32 4.94 o 9 5 0 470.76 470.91 16.13 o 10 5 0 4.18 10.98 5.52 o 11 5 0 168.39 186.92 12.34 o 12 5 0 19.66 6.65 7.34 o 13 5 0 1708.54 1551.30 37.63 o 14 5 0 0.43 -4.60 8.45 o 15 5 0 27.17 38.82 11.17 o 16 5 0 162.51 197.63 21.99 o 17 5 0 104.56 52.33 21.38 o 0 6 0 4567.95 4511.41 131.84 o 1 6 0 2.78 13.85 4.15 o 2 6 0 50469.29 52389.57 905.04 o 3 6 0 110.11 112.56 6.44 o 4 6 0 1445.80 1258.34 40.73 o 5 6 0 2585.99 2106.82 37.63 o 6 6 0 2412.85 2674.81 46.69 o 7 6 0 6809.48 6899.19 112.96 o 8 6 0 199.90 216.03 10.83 o 9 6 0 2330.99 2197.05 49.95 o 10 6 0 2648.06 2552.37 57.57 o 11 6 0 162.78 177.55 12.34 o 12 6 0 1110.01 1083.25 28.97 o 13 6 0 892.17 869.02 26.34 o 14 6 0 738.77 716.20 24.42 o 15 6 0 184.25 182.47 15.83 o 16 6 0 657.39 688.90 33.94 o 17 6 0 466.56 451.09 36.00 o 1 7 0 324.77 375.32 12.94 o 2 7 0 0.31 -0.96 3.18 o 3 7 0 1146.30 1071.47 21.18 o 4 7 0 7.79 8.08 4.12 o 5 7 0 223.94 214.34 9.05 o 6 7 0 75.31 81.91 5.26 o 7 7 0 173.11 153.14 8.60 o 8 7 0 5.18 9.48 5.47 o 9 7 0 563.11 549.33 18.98 o 10 7 0 12.60 14.64 7.22 o 11 7 0 4364.55 4327.73 92.09 o 12 7 0 16.51 14.34 8.51 o 13 7 0 1547.62 1499.65 37.57 o 14 7 0 548.10 549.07 22.06 o 15 7 0 415.99 395.53 19.87 o 16 7 0 0.18 -11.43 11.43 o 17 7 0 78.95 82.08 24.17 o 0 8 0 1560.91 1451.22 49.61 o 1 8 0 3381.30 3518.07 75.44 o 2 8 0 21291.13 21056.91 367.81 o 3 8 0 234.92 349.38 10.24 o 4 8 0 11389.14 11453.67 226.55 o 5 8 0 427.00 372.25 12.55 o 6 8 0 964.65 888.14 19.74 o 7 8 0 1636.57 1653.40 35.66 o 8 8 0 1534.14 1449.34 35.93 o 9 8 0 4853.50 4707.35 98.42 o 10 8 0 4946.22 4834.32 101.79 o 11 8 0 82.53 94.95 16.60 o 12 8 0 2944.83 2949.78 68.34 o 13 8 0 169.28 196.38 14.73 o 14 8 0 703.29 659.42 23.94 o 15 8 0 89.08 89.18 13.05 o 16 8 0 1716.38 1821.26 43.12 o 1 9 0 211.03 212.30 11.11 o 2 9 0 474.10 456.29 16.45 o 3 9 0 508.55 559.50 14.27 o 4 9 0 353.62 417.94 15.21 o 5 9 0 611.95 650.81 18.05 o 6 9 0 798.84 740.00 20.10 o 7 9 0 961.80 858.85 20.43 o 8 9 0 271.97 266.79 12.17 o 9 9 0 93.70 105.97 10.09 o 10 9 0 89.64 102.38 10.69 o 11 9 0 2214.78 2090.49 61.16 o 12 9 0 52.31 48.47 10.69 o 13 9 0 83.09 65.81 11.05 o 14 9 0 3.94 4.23 8.62 o 15 9 0 94.79 129.71 13.50 o 16 9 0 100.05 123.14 14.66 o 0 10 0 20.46 57.84 10.74 o 1 10 0 835.09 977.46 27.71 o 2 10 0 915.77 605.77 19.94 o 3 10 0 3968.52 3905.26 67.67 o 4 10 0 26776.13 27605.34 481.71 o 5 10 0 131.39 204.90 21.05 o 6 10 0 56.04 66.31 8.13 o 7 10 0 769.93 715.84 18.79 o 8 10 0 8899.47 8850.94 157.67 o 9 10 0 346.57 361.79 14.94 o 10 10 0 2516.29 2428.71 51.25 o 11 10 0 1025.28 1105.31 34.35 o 12 10 0 305.03 304.06 16.22 o 13 10 0 280.13 234.33 15.82 o 14 10 0 104.51 112.23 12.73 o 15 10 0 193.12 179.82 14.90 o 16 10 0 2685.35 2753.46 111.87 o 1 11 0 28.97 36.49 7.37 o 2 11 0 1271.30 1258.15 34.00 o 3 11 0 262.71 275.39 12.25 o 4 11 0 0.26 2.12 6.00 o 5 11 0 57.70 55.22 8.36 o 6 11 0 501.57 477.96 18.59 o 7 11 0 19.26 -0.62 6.07 o 8 11 0 102.38 114.76 9.94 o 9 11 0 438.16 493.88 17.72 o 10 11 0 4644.30 4565.00 87.82 o 11 11 0 2746.09 2657.99 63.99 o 12 11 0 2.54 3.95 8.54 o 13 11 0 499.89 472.08 20.57 o 14 11 0 522.73 554.13 21.05 o 15 11 0 285.44 298.86 17.98 o 16 11 0 29.68 10.64 35.33 o 0 12 0 120.30 229.58 24.53 o 1 12 0 5175.53 5064.11 109.29 o 2 12 0 3973.41 3977.47 88.30 o 3 12 0 403.00 461.69 23.25 o 4 12 0 7542.00 7075.25 145.58 o 5 12 0 2695.83 2854.94 65.19 o 6 12 0 12.92 6.75 7.17 o 7 12 0 476.61 457.34 16.50 o 8 12 0 98.20 110.50 10.90 o 9 12 0 2280.97 2347.68 55.91 o 10 12 0 28.56 24.10 8.45 o 11 12 0 212.29 268.06 18.49 o 12 12 0 102.22 92.95 13.39 o 13 12 0 441.39 398.22 19.29 o 14 12 0 883.35 959.63 31.32 o 15 12 0 38.68 29.82 11.61 o 1 13 0 185.99 131.06 15.30 o 2 13 0 1378.83 1284.21 41.92 o 3 13 0 15.65 8.59 8.83 o 4 13 0 182.74 206.17 17.09 o 5 13 0 659.27 685.27 23.36 o 6 13 0 12.24 17.52 7.81 o 7 13 0 197.53 182.86 12.82 o 8 13 0 38.06 48.39 9.20 o 9 13 0 4.62 4.54 8.55 o 10 13 0 1648.68 1625.81 43.49 o 11 13 0 115.73 91.69 14.67 o 12 13 0 1.94 -6.80 12.44 o 13 13 0 630.31 684.69 25.38 o 14 13 0 442.26 527.30 23.17 o 15 13 0 358.39 398.42 50.05 o 0 14 0 4630.21 4396.91 138.78 o 1 14 0 6225.06 6395.91 137.26 o 2 14 0 5107.84 5047.50 128.96 o 3 14 0 3749.76 3576.57 96.07 o 4 14 0 2294.79 2269.05 66.41 o 5 14 0 4522.77 4414.45 96.76 o 6 14 0 182.70 236.04 15.24 o 7 14 0 3586.17 3432.02 69.35 o 8 14 0 280.18 367.98 17.93 o 9 14 0 26.13 29.55 9.52 o 10 14 0 1788.73 1827.25 47.60 o 11 14 0 546.29 502.52 26.99 o 12 14 0 96.30 113.62 17.64 o 13 14 0 304.27 309.68 22.80 o 14 14 0 840.98 917.31 35.84 o 15 14 0 43.46 11.78 30.42 o 1 15 0 1440.56 1360.22 45.89 o 2 15 0 3814.81 3774.76 101.19 o 3 15 0 780.00 723.98 35.91 o 4 15 0 148.01 131.50 15.71 o 5 15 0 40.51 21.88 11.53 o 6 15 0 135.46 125.32 15.78 o 7 15 0 74.52 92.07 12.18 o 8 15 0 0.78 7.78 10.10 o 9 15 0 640.43 647.57 29.30 o 10 15 0 386.53 370.90 20.06 o 11 15 0 110.32 102.54 16.42 o 12 15 0 87.24 94.65 16.76 o 13 15 0 421.91 428.83 24.15 o 0 16 0 615.78 507.35 45.14 o 1 16 0 5611.00 5509.54 149.28 o 2 16 0 3133.07 3366.24 93.08 o 3 16 0 44.21 18.72 12.44 o 4 16 0 6.24 -10.35 10.35 o 5 16 0 0.18 0.84 11.30 o 6 16 0 150.10 123.35 17.01 o 7 16 0 50.28 33.41 11.59 o 8 16 0 742.20 713.38 30.71 o 9 16 0 4.57 4.32 11.62 o 10 16 0 343.79 348.03 43.87 o 11 16 0 568.21 544.50 49.56 o 12 16 0 316.81 335.89 33.39 o 13 16 0 724.75 736.62 67.23 o 1 17 0 9.58 -8.13 13.52 o 2 17 0 561.94 533.61 29.32 o 3 17 0 958.59 1035.93 40.74 o 4 17 0 42.02 37.00 13.40 o 5 17 0 153.66 142.30 18.11 o 6 17 0 126.49 127.96 17.84 o 7 17 0 1179.61 1250.90 39.01 o 8 17 0 149.98 175.61 18.29 o 9 17 0 123.15 137.43 17.71 o 10 17 0 118.33 129.34 17.34 o 11 17 0 0.75 -14.86 14.86 o 12 17 0 7.20 -11.52 16.69 o 0 18 0 5264.51 4907.61 225.70 o 1 18 0 1679.23 1568.81 66.24 o 2 18 0 1491.69 1604.20 66.96 o 3 18 0 302.45 305.61 28.64 o 4 18 0 814.73 849.52 37.39 o 5 18 0 252.81 245.23 23.46 o 6 18 0 251.99 234.13 23.23 o 7 18 0 13.09 13.47 11.68 o 8 18 0 860.85 879.39 36.53 o 9 18 0 272.91 310.62 24.43 o 10 18 0 812.44 812.70 35.78 o 11 18 0 534.57 538.70 45.14 o 12 18 0 348.03 273.90 35.82 o 1 19 0 18.59 1.66 16.99 o 2 19 0 1.14 -6.38 15.27 o 3 19 0 74.75 57.17 18.70 o 4 19 0 485.13 426.75 28.97 o 5 19 0 186.71 224.09 23.30 o 6 19 0 1.66 -2.78 14.38 o 7 19 0 1053.36 1076.18 53.81 o 8 19 0 158.84 192.97 20.68 o 9 19 0 260.77 284.71 23.70 o 10 19 0 49.66 34.80 16.20 o 11 19 0 77.02 26.78 21.20 o 0 20 0 4501.51 4106.85 199.21 o 1 20 0 1218.89 1160.72 57.22 o 2 20 0 1784.78 1806.19 75.92 o 3 20 0 1005.23 952.25 50.53 o 4 20 0 663.21 605.94 40.78 o 5 20 0 0.81 -6.67 14.30 o 6 20 0 0.53 -16.12 17.45 o 7 20 0 9.20 11.88 14.00 o 8 20 0 170.05 238.31 23.14 o 9 20 0 15.25 1.75 12.97 o 10 20 0 17.17 -10.65 15.17 o 11 20 0 419.63 535.32 45.63 o 1 21 0 102.30 111.06 23.24 o 2 21 0 2.34 -2.87 17.31 o 3 21 0 167.38 212.81 27.52 o 4 21 0 138.43 159.94 31.89 o 5 21 0 76.71 78.94 23.93 o 6 21 0 303.41 344.66 29.88 o 7 21 0 235.22 268.02 32.53 o 8 21 0 0.17 -14.00 14.00 o 9 21 0 81.27 76.30 18.68 o 10 21 0 159.60 166.57 23.14 o 0 22 0 1173.86 1214.88 87.34 o 1 22 0 601.42 671.80 44.06 o 2 22 0 1775.08 1809.05 78.74 o 3 22 0 91.68 101.14 23.18 o 4 22 0 721.36 658.83 44.26 o 5 22 0 22.90 -8.43 18.70 o 6 22 0 13.43 6.11 19.55 o 7 22 0 10.58 -18.86 18.86 o 8 22 0 5.21 -6.63 23.04 o 9 22 0 554.93 541.05 43.37 o 1 23 0 28.96 1.96 18.58 o 2 23 0 104.99 76.71 24.26 o 3 23 0 0.70 -5.55 18.30 o 4 23 0 10.21 19.01 22.54 o 5 23 0 3.86 -0.23 20.25 o 6 23 0 498.39 527.24 41.36 o 7 23 0 7.86 -0.98 28.46 o 8 23 0 33.26 21.13 24.53 o 0 24 0 856.03 748.75 70.66 o 1 24 0 330.45 336.78 37.47 o 2 24 0 489.39 589.11 55.94 o 3 24 0 172.24 190.02 31.52 o 4 24 0 200.26 232.28 73.11 o 5 24 0 88.16 100.68 29.48 o 6 24 0 590.42 631.97 74.58 o 1 25 0 5.39 22.01 23.56 o 2 25 0 46.93 94.21 41.22 o 3 25 0 73.29 100.10 40.23 o 4 25 0 14.58 21.59 37.29 o 1 0 1 108.58 144.58 4.15 o 2 0 1 59324.77 57761.91 822.30 o 3 0 1 6731.12 6831.18 97.29 o 4 0 1 724.10 713.46 11.69 o 5 0 1 2887.25 3019.52 42.12 o 6 0 1 20103.52 18831.69 231.64 o 7 0 1 915.19 854.60 14.45 o 8 0 1 15981.78 15884.63 207.69 o 9 0 1 225.24 234.34 9.46 o 10 0 1 21.08 28.64 5.69 o 11 0 1 1731.01 1810.97 35.35 o 12 0 1 9.63 -6.07 7.54 o 13 0 1 572.81 512.21 21.43 o 14 0 1 0.16 -9.74 9.74 o 15 0 1 27.01 6.55 13.67 o 16 0 1 28.59 11.55 27.48 o 17 0 1 18.07 0.77 22.77 o -17 1 1 149.38 166.83 43.18 o -16 1 1 50.73 26.74 16.14 o -15 1 1 600.46 610.13 29.56 o -14 1 1 67.81 37.35 11.62 o -13 1 1 76.77 66.11 9.11 o -12 1 1 166.07 170.51 11.15 o -11 1 1 668.54 676.09 18.27 o -10 1 1 155.89 175.34 9.25 o -9 1 1 751.92 811.90 19.46 o -8 1 1 1961.51 1960.02 35.89 o -7 1 1 2431.96 2408.30 44.55 o -6 1 1 9325.07 9377.70 150.55 o -5 1 1 3439.08 3725.18 65.71 o -4 1 1 372.48 315.99 18.65 o -3 1 1 48459.48 52758.96 1007.10 o -2 1 1 1390.02 1566.92 32.17 o -1 1 1 51.18 94.48 6.80 o 0 1 1 8.18 13.86 1.70 o 1 1 1 54.69 96.90 2.24 o 2 1 1 1436.93 1584.37 23.50 o 3 1 1 48922.14 52739.70 788.10 o 4 1 1 261.08 263.13 8.62 o 5 1 1 3651.68 3903.60 52.30 o 6 1 1 9258.54 9222.67 115.99 o 7 1 1 2297.24 2330.03 34.43 o 8 1 1 2103.91 2084.43 31.10 o 9 1 1 898.71 975.39 17.62 o 10 1 1 184.35 207.07 8.51 o 11 1 1 700.93 704.97 22.68 o 12 1 1 153.95 152.40 12.87 o 13 1 1 76.71 43.61 14.16 o 14 1 1 73.73 71.33 12.94 o 15 1 1 583.15 540.26 24.29 o 16 1 1 45.76 36.85 18.39 o 17 1 1 172.86 222.76 45.14 o -17 2 1 20.47 30.19 20.27 o -16 2 1 207.93 224.80 28.24 o -15 2 1 344.69 356.74 20.43 o -14 2 1 577.68 544.05 19.00 o -13 2 1 388.57 375.13 14.90 o -12 2 1 893.60 859.04 22.08 o -11 2 1 446.54 433.03 15.73 o -10 2 1 269.96 273.08 11.10 o -9 2 1 668.65 625.37 19.83 o -8 2 1 8016.18 7775.13 142.26 o -7 2 1 3253.53 3484.72 53.02 o -6 2 1 47786.73 48912.78 687.39 o -5 2 1 2271.27 2465.09 41.72 o -4 2 1 42449.81 45440.44 763.74 o -3 2 1 7546.52 8302.37 144.15 o -2 2 1 47666.43 48022.71 1094.03 o -1 2 1 11033.50 10929.35 191.19 o 0 2 1 71.72 95.99 7.51 o 1 2 1 11114.48 11155.25 192.24 o 2 2 1 47752.77 48364.31 1362.31 o 3 2 1 7544.21 8228.67 126.83 o 4 2 1 41653.54 43738.16 617.81 o 5 2 1 2325.49 2505.02 35.25 o 6 2 1 47747.20 48028.36 597.40 o 7 2 1 3200.49 3373.65 48.30 o 8 2 1 7306.93 7221.37 94.14 o 9 2 1 621.10 676.35 18.87 o 10 2 1 215.14 229.96 10.47 o 11 2 1 396.92 389.88 12.82 o 12 2 1 865.41 845.85 23.96 o 13 2 1 375.75 350.20 18.97 o 14 2 1 570.63 525.65 26.39 o 15 2 1 363.68 368.03 23.33 o 16 2 1 176.21 197.41 25.26 o 17 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