#------------------------------------------------------------------------------ #$Date: 2016-04-02 21:53:42 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180808 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/39/2013920.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2013920_Fobs loop_ _publ_author_name 'Naumova, Marina I.' 'Kuratieva, Natalia V.' 'Podberezskaya, Nina V.' 'Naumov, Dmitry Yu.' _publ_section_title ; The alkali hypophosphites KH~2~PO~2~, RbH~2~PO~2~ and CsH~2~PO~2~ ; _journal_issue 5 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first i53 _journal_page_last i55 _journal_volume 60 _journal_year 2004 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 116.205 _cell_angle_gamma 90.000 _cell_length_a 7.3131 _cell_length_b 7.2952 _cell_length_c 7.1814 _exptl_crystal_F_000 208.00 _reflns_d_resolution_high 0.7121 _cod_data_source_file bc1035Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title 'KH2PO2 in C2/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 122.82 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 11550.44 8874.25 19.60 o 4 0 0 1389.42 1230.88 8.26 o 6 0 0 1216.60 1264.95 10.55 o 8 0 0 722.44 736.78 10.12 o 1 1 0 501.59 528.45 2.09 o 3 1 0 114.13 105.63 13.62 o 5 1 0 26.37 24.48 3.14 o 7 1 0 25.05 23.39 1.99 o 9 1 0 12.08 15.74 2.34 o 0 2 0 7083.55 6289.92 11.94 o 2 2 0 1388.82 1320.01 6.14 o 4 2 0 21.25 17.07 1.86 o 6 2 0 132.60 135.79 4.44 o 8 2 0 145.78 170.17 5.44 o 1 3 0 552.44 583.23 4.17 o 3 3 0 18.20 14.71 1.50 o 5 3 0 18.91 15.64 2.36 o 7 3 0 11.49 11.00 3.07 o 0 4 0 576.39 511.56 4.44 o 2 4 0 1272.82 1216.21 7.41 o 4 4 0 1303.97 1252.62 9.20 o 6 4 0 368.39 312.91 6.33 o 8 4 0 67.33 81.54 4.79 o 1 5 0 172.76 174.94 3.23 o 3 5 0 783.85 774.42 7.20 o 5 5 0 427.90 406.21 6.48 o 7 5 0 53.11 45.58 4.07 o 0 6 0 816.97 769.21 7.06 o 2 6 0 906.08 881.68 7.94 o 4 6 0 701.81 675.32 8.03 o 6 6 0 274.23 263.99 6.24 o 1 7 0 115.30 113.63 3.58 o 3 7 0 340.29 351.41 6.04 o 5 7 0 216.49 221.46 5.88 o 0 8 0 11.28 9.85 2.36 o 2 8 0 5.60 6.43 2.28 o 4 8 0 1.42 0.93 2.57 o 1 9 0 75.16 84.84 3.93 o 3 9 0 7.56 9.28 2.86 o 0 10 0 22.03 22.35 3.21 o 2 10 0 30.74 34.35 3.50 o -9 1 1 2.24 1.86 2.04 o -7 1 1 45.45 43.88 2.12 o -5 1 1 119.35 116.90 4.01 o -3 1 1 1595.85 1610.85 136.83 o -1 1 1 143.82 145.22 1.84 o 1 1 1 1665.08 1852.69 70.34 o 3 1 1 47.06 37.23 3.57 o 5 1 1 191.16 178.98 14.88 o 7 1 1 3.59 3.26 1.79 o -8 2 1 355.15 368.82 7.33 o -6 2 1 1151.99 1181.07 10.76 o -4 2 1 4187.56 3679.46 14.18 o -2 2 1 8335.66 8862.66 17.03 o 0 2 1 5898.09 5714.87 14.05 o 2 2 1 3600.04 3450.65 11.25 o 4 2 1 2437.38 2089.63 12.05 o 6 2 1 893.51 921.84 10.31 o 8 2 1 212.32 228.78 6.59 o -9 3 1 54.07 55.08 4.29 o -7 3 1 218.53 217.90 6.02 o -5 3 1 103.74 85.30 3.22 o -3 3 1 2.33 5.78 1.36 o -1 3 1 1044.37 1015.89 5.44 o 1 3 1 2675.35 2748.32 9.66 o 3 3 1 349.86 345.25 4.40 o 5 3 1 14.18 12.92 2.36 o 7 3 1 42.47 48.22 3.86 o -8 4 1 93.82 105.60 5.15 o -6 4 1 418.57 373.19 6.48 o -4 4 1 1930.28 1899.79 10.91 o -2 4 1 2376.49 2296.49 10.03 o 0 4 1 745.19 702.74 3.72 o 2 4 1 910.61 901.63 6.74 o 4 4 1 1130.38 1082.23 9.15 o 6 4 1 402.68 335.00 6.97 o -7 5 1 58.60 51.95 3.93 o -5 5 1 24.77 24.21 2.50 o -3 5 1 10.75 11.42 1.86 o -1 5 1 251.45 246.33 3.67 o 1 5 1 413.54 406.07 4.84 o 3 5 1 68.67 69.78 2.86 o 5 5 1 8.87 9.92 2.43 o 7 5 1 17.76 17.64 3.64 o -6 6 1 50.81 50.16 3.50 o -4 6 1 0.11 -1.71 2.00 o -2 6 1 16.04 15.57 2.07 o 0 6 1 390.40 374.62 3.59 o 2 6 1 213.74 205.25 4.23 o 4 6 1 4.17 1.78 2.21 o 6 6 1 3.97 3.86 2.86 o -7 7 1 42.17 40.22 4.00 o -5 7 1 122.75 117.89 4.36 o -3 7 1 236.83 238.30 5.02 o -1 7 1 265.58 266.14 4.95 o 1 7 1 210.18 214.56 4.66 o 3 7 1 151.51 156.05 4.44 o 5 7 1 82.70 83.35 4.15 o -6 8 1 111.76 124.85 5.15 o -4 8 1 85.73 89.57 4.00 o -2 8 1 187.34 188.02 4.73 o 0 8 1 482.32 478.13 5.07 o 2 8 1 331.21 321.96 6.25 o 4 8 1 80.13 83.13 4.07 o -3 9 1 175.32 182.19 5.44 o -1 9 1 263.85 276.34 6.17 o 1 9 1 262.63 272.88 6.31 o 3 9 1 152.13 164.08 5.44 o -2 10 1 6.42 6.28 2.93 o 0 10 1 34.39 34.37 2.47 o -8 0 2 1160.79 1139.98 11.44 o -6 0 2 3343.28 2996.84 15.30 o -4 0 2 2998.39 2912.85 12.80 o -2 0 2 4246.15 4868.26 11.43 o 0 0 2 15083.88 14708.72 19.79 o 2 0 2 9686.26 9864.30 25.21 o 4 0 2 1808.11 1826.91 11.77 o 6 0 2 447.11 471.83 7.41 o 8 0 2 229.31 259.84 6.95 o -9 1 2 12.25 11.48 2.14 o -7 1 2 58.90 52.10 2.47 o -5 1 2 88.99 88.63 2.07 o -3 1 2 13.97 11.14 1.01 o -1 1 2 142.33 157.43 1.37 o 1 1 2 596.53 680.35 18.57 o 3 1 2 135.60 111.52 2.23 o 5 1 2 11.56 13.93 1.76 o 7 1 2 8.41 9.56 1.97 o -8 2 2 239.01 240.95 5.88 o -6 2 2 742.22 763.17 8.49 o -4 2 2 120.89 105.76 2.72 o -2 2 2 0.68 2.57 1.07 o 0 2 2 2478.69 2660.46 30.61 o 2 2 2 2353.22 2470.14 10.43 o 4 2 2 199.35 177.00 4.30 o 6 2 2 20.28 22.99 3.07 o -9 3 2 3.56 4.57 3.07 o -7 3 2 42.86 44.58 3.50 o -5 3 2 8.17 9.42 2.00 o -3 3 2 101.04 99.84 2.36 o -1 3 2 4.26 8.50 1.21 o 1 3 2 356.15 361.73 3.90 o 3 3 2 39.62 36.87 2.22 o 5 3 2 3.84 -1.36 2.50 o 7 3 2 0.42 0.36 3.00 o -8 4 2 111.93 118.86 5.36 o -6 4 2 251.08 225.00 5.09 o -4 4 2 1350.44 1373.15 9.15 o -2 4 2 2639.15 2629.79 10.92 o 0 4 2 981.84 899.70 7.06 o 2 4 2 382.82 355.31 4.69 o 4 4 2 484.38 474.83 6.56 o 6 4 2 264.74 249.04 6.60 o -7 5 2 37.71 34.29 3.36 o -5 5 2 267.56 268.31 4.95 o -3 5 2 1185.94 1165.15 8.59 o -1 5 2 779.27 761.72 6.48 o 1 5 2 115.50 117.48 3.08 o 3 5 2 177.91 178.77 4.23 o 5 5 2 218.96 211.97 5.45 o -8 6 2 125.39 116.15 5.72 o -6 6 2 310.64 310.36 6.32 o -4 6 2 776.63 751.85 8.12 o -2 6 2 1166.72 1153.48 9.01 o 0 6 2 887.93 872.89 5.56 o 2 6 2 544.35 550.52 6.86 o 4 6 2 352.28 346.17 6.61 o 6 6 2 161.26 159.73 5.94 o -7 7 2 24.73 23.92 3.43 o -5 7 2 136.10 133.59 4.58 o -3 7 2 522.53 506.23 7.07 o -1 7 2 356.96 360.77 5.61 o 1 7 2 68.04 69.55 3.15 o 3 7 2 94.28 102.75 4.00 o 5 7 2 128.05 135.26 5.22 o -6 8 2 1.50 1.07 2.86 o -4 8 2 2.76 2.57 2.43 o -2 8 2 5.81 4.57 2.28 o 0 8 2 8.22 8.70 1.69 o 2 8 2 3.56 4.71 2.43 o 4 8 2 0.42 -3.00 3.00 o -3 9 2 2.53 2.14 2.57 o -1 9 2 19.15 21.07 2.93 o 1 9 2 65.37 72.25 3.86 o 3 9 2 25.19 27.92 3.43 o -9 1 3 14.90 16.36 2.17 o -7 1 3 86.10 75.76 7.26 o -5 1 3 139.83 140.43 11.36 o -3 1 3 789.40 970.68 39.90 o -1 1 3 1146.09 1490.96 81.11 o 1 1 3 112.08 129.29 5.91 o 3 1 3 111.12 110.76 9.27 o 5 1 3 16.30 16.80 1.94 o 7 1 3 20.15 23.58 2.35 o -8 2 3 602.27 638.78 8.95 o -6 2 3 1157.46 1234.61 10.69 o -4 2 3 3523.67 3463.05 13.91 o -2 2 3 7053.89 8361.46 18.28 o 0 2 3 4155.34 4446.09 44.60 o 2 2 3 1643.28 1695.43 9.76 o 4 2 3 954.02 806.87 9.10 o 6 2 3 423.49 457.49 8.48 o -9 3 3 23.17 17.92 3.36 o -7 3 3 322.27 314.76 6.68 o -5 3 3 593.76 550.80 6.30 o -3 3 3 26.62 20.00 1.64 o -1 3 3 41.21 40.67 1.79 o 1 3 3 842.89 903.00 6.80 o 3 3 3 452.04 459.16 6.06 o 5 3 3 42.13 37.65 3.43 o 7 3 3 7.27 8.57 3.43 o -8 4 3 218.06 231.14 6.81 o -6 4 3 292.12 273.80 5.46 o -4 4 3 1158.50 1192.40 8.66 o -2 4 3 2823.93 2847.02 11.90 o 0 4 3 1487.75 1512.93 6.35 o 2 4 3 408.94 414.81 5.48 o 4 4 3 323.20 323.20 6.03 o 6 4 3 192.24 199.71 6.66 o -7 5 3 75.60 66.55 3.86 o -5 5 3 132.63 126.41 3.65 o -3 5 3 28.20 27.00 2.14 o -1 5 3 16.54 19.14 2.00 o 1 5 3 135.07 140.55 3.51 o 3 5 3 111.42 115.03 3.79 o 5 5 3 21.47 19.64 3.07 o -8 6 3 30.65 30.21 3.93 o -6 6 3 150.87 142.58 4.58 o -4 6 3 44.64 54.87 2.93 o -2 6 3 2.84 2.21 1.93 o 0 6 3 59.91 55.25 1.95 o 2 6 3 186.06 185.33 4.51 o 4 6 3 40.42 38.15 3.29 o -7 7 3 58.88 61.45 4.14 o -5 7 3 120.13 115.67 4.29 o -3 7 3 216.73 210.37 4.87 o -1 7 3 250.19 252.49 5.09 o 1 7 3 162.02 167.40 4.58 o 3 7 3 76.76 85.13 4.00 o -6 8 3 209.36 223.16 6.23 o -4 8 3 183.13 182.81 5.30 o -2 8 3 101.53 99.47 3.93 o 0 8 3 202.84 204.35 6.41 o 2 8 3 253.64 253.61 6.09 o -3 9 3 172.63 182.96 5.51 o -1 9 3 193.15 193.92 5.66 o 1 9 3 185.21 201.39 5.94 o -10 0 4 188.01 191.73 6.16 o -8 0 4 847.43 789.04 9.64 o -6 0 4 4173.22 4167.79 19.58 o -4 0 4 6266.49 7673.53 20.74 o -2 0 4 2266.97 2504.44 9.75 o 0 0 4 2349.06 2556.11 38.74 o 2 0 4 3362.76 3408.06 17.33 o 4 0 4 1327.39 1416.85 12.59 o 6 0 4 248.25 278.73 6.88 o -9 1 4 6.95 6.85 2.04 o -7 1 4 44.05 42.92 2.24 o -5 1 4 122.55 123.97 8.34 o -3 1 4 73.78 80.11 4.19 o -1 1 4 54.68 70.03 11.84 o 1 1 4 92.18 96.23 2.08 o 3 1 4 55.48 53.29 2.82 o 5 1 4 15.18 15.75 2.12 o -10 2 4 6.45 3.14 3.21 o -8 2 4 93.93 97.18 4.15 o -6 2 4 940.99 992.62 9.84 o -4 2 4 1083.16 1059.85 8.08 o -2 2 4 48.16 45.18 1.86 o 0 2 4 145.14 166.85 6.70 o 2 2 4 652.43 683.65 7.10 o 4 2 4 250.35 229.58 5.74 o 6 2 4 22.70 24.28 3.71 o -9 3 4 2.19 0.86 2.86 o -7 3 4 16.13 15.28 3.21 o -5 3 4 110.29 111.07 3.36 o -3 3 4 0.57 0.86 1.43 o -1 3 4 73.26 73.32 2.29 o 1 3 4 11.71 10.35 1.86 o 3 3 4 45.79 44.51 2.86 o 5 3 4 4.63 4.35 3.14 o -8 4 4 272.30 285.78 7.46 o -6 4 4 226.22 234.05 5.09 o -4 4 4 521.89 570.65 6.29 o -2 4 4 1608.63 1643.93 9.80 o 0 4 4 1179.38 1200.88 13.20 o 2 4 4 300.09 297.86 5.24 o 4 4 4 137.35 130.38 4.58 o -7 5 4 93.15 84.94 4.15 o -5 5 4 75.87 75.57 3.29 o -3 5 4 532.56 524.58 6.28 o -1 5 4 915.82 929.10 8.08 o 1 5 4 249.79 253.85 4.81 o 3 5 4 48.25 50.51 3.22 o 5 5 4 48.97 47.01 4.07 o -8 6 4 206.47 201.74 6.52 o -6 6 4 322.29 319.81 6.39 o -4 6 4 533.98 537.35 7.14 o -2 6 4 864.91 834.59 8.42 o 0 6 4 734.77 727.38 5.73 o 2 6 4 333.29 317.97 6.25 o 4 6 4 140.01 145.31 5.37 o -7 7 4 56.15 52.23 4.14 o -5 7 4 47.83 45.72 3.29 o -3 7 4 252.97 253.51 5.45 o -1 7 4 408.65 418.42 6.62 o 1 7 4 136.70 141.46 4.58 o 3 7 4 35.16 37.86 3.50 o -6 8 4 2.66 2.86 2.93 o -4 8 4 2.85 3.07 2.57 o -2 8 4 1.92 2.21 2.43 o 0 8 4 3.15 1.54 1.76 o 2 8 4 2.10 1.57 2.86 o -3 9 4 15.28 16.71 3.14 o -1 9 4 1.84 3.64 2.71 o -9 1 5 69.68 62.55 3.68 o -7 1 5 3.22 6.26 2.03 o -5 1 5 297.35 303.64 6.47 o -3 1 5 22.42 22.87 1.57 o -1 1 5 393.83 413.29 10.96 o 1 1 5 54.68 58.24 3.68 o 3 1 5 18.81 20.50 2.07 o 5 1 5 0.42 -1.61 2.11 o -10 2 5 341.27 352.78 7.97 o -8 2 5 884.25 928.29 10.80 o -6 2 5 1242.08 1423.87 12.01 o -4 2 5 1747.09 1874.44 11.76 o -2 2 5 2841.42 3035.95 13.00 o 0 2 5 2342.40 2593.23 117.32 o 2 2 5 938.38 936.43 9.16 o 4 2 5 344.56 327.15 7.40 o -9 3 5 4.97 5.35 3.28 o -7 3 5 96.05 93.83 4.58 o -5 3 5 668.40 662.41 7.39 o -3 3 5 472.67 494.23 5.70 o -1 3 5 29.38 35.86 2.21 o 1 3 5 67.55 71.84 2.93 o 3 3 5 154.96 156.20 4.72 o 5 3 5 50.46 56.94 4.79 o -8 4 5 430.63 433.63 8.84 o -6 4 5 363.16 351.43 6.25 o -4 4 5 446.94 456.98 6.05 o -2 4 5 1258.23 1256.23 9.32 o 0 4 5 1123.56 1156.42 27.94 o 2 4 5 316.65 329.22 6.03 o 4 4 5 95.70 89.66 4.58 o -7 5 5 27.08 22.93 3.14 o -5 5 5 147.70 144.46 4.15 o -3 5 5 106.76 105.31 3.43 o -1 5 5 12.00 13.64 2.21 o 1 5 5 22.52 23.78 2.57 o 3 5 5 49.28 48.80 3.57 o -8 6 5 1.74 2.36 3.28 o -6 6 5 93.61 95.88 4.15 o -4 6 5 177.31 171.74 4.73 o -2 6 5 16.29 17.28 2.43 o 0 6 5 1.19 -0.41 1.59 o 2 6 5 41.05 41.86 3.36 o -7 7 5 75.87 73.90 4.43 o -5 7 5 105.53 106.12 4.29 o -3 7 5 126.28 128.06 4.36 o -1 7 5 139.48 137.60 4.51 o 1 7 5 97.26 101.31 4.29 o -4 8 5 268.73 254.08 6.24 o -2 8 5 126.20 125.04 4.65 o 0 8 5 66.76 66.01 2.80 o -10 0 6 356.09 343.25 7.97 o -8 0 6 487.12 451.94 8.28 o -6 0 6 1962.94 2299.87 14.40 o -4 0 6 4575.70 5340.42 19.01 o -2 0 6 2707.68 2975.48 13.87 o 0 0 6 951.74 977.28 16.79 o 2 0 6 776.53 771.64 10.35 o 4 0 6 479.34 524.26 9.28 o -9 1 6 5.91 6.16 2.28 o -7 1 6 11.98 11.34 2.03 o -5 1 6 76.45 86.44 7.87 o -3 1 6 101.76 108.67 2.97 o -1 1 6 24.40 27.12 1.68 o 1 1 6 13.19 14.87 2.36 o 3 1 6 20.18 20.10 2.34 o -8 2 6 12.95 15.42 3.14 o -6 2 6 275.90 293.78 6.10 o -4 2 6 1099.33 1094.65 10.16 o -2 2 6 440.97 549.36 6.70 o 0 2 6 38.56 42.05 2.11 o 2 2 6 79.99 73.92 3.72 o 4 2 6 89.31 90.21 5.43 o -9 3 6 3.59 -0.36 3.50 o -7 3 6 3.99 4.85 3.21 o -5 3 6 46.11 46.51 3.00 o -3 3 6 46.75 48.95 2.64 o -1 3 6 5.43 6.21 2.14 o 1 3 6 2.12 1.93 2.21 o 3 3 6 10.84 9.42 3.00 o -8 4 6 389.30 370.91 8.55 o -6 4 6 396.07 409.19 6.90 o -4 4 6 238.03 255.32 5.02 o -2 4 6 449.74 437.62 6.27 o 0 4 6 590.59 599.09 25.33 o 2 4 6 244.23 237.05 5.95 o -7 5 6 232.52 218.21 6.02 o -5 5 6 86.77 88.23 3.72 o -3 5 6 109.45 106.94 3.72 o -1 5 6 332.83 336.27 6.03 o 1 5 6 214.21 219.67 5.52 o 3 5 6 37.38 36.43 3.71 o -6 6 6 348.60 340.31 7.11 o -4 6 6 354.21 339.87 6.46 o -2 6 6 392.38 381.08 6.68 o 0 6 6 357.38 356.90 16.98 o 2 6 6 180.24 184.12 5.80 o -5 7 6 53.16 51.44 3.72 o -3 7 6 59.61 54.38 3.64 o -1 7 6 177.85 175.97 5.37 o 1 7 6 132.25 139.84 5.29 o -4 8 6 2.48 1.57 2.78 o -2 8 6 0.38 0.57 2.86 o -9 1 7 15.63 13.58 2.64 o -7 1 7 106.41 113.56 4.15 o -5 1 7 5.38 4.79 1.53 o -3 1 7 124.77 117.37 2.48 o -1 1 7 1.94 0.81 1.58 o 1 1 7 54.25 56.67 4.93 o 3 1 7 4.83 5.88 2.50 o -8 2 7 813.21 844.70 11.14 o -6 2 7 1169.56 1268.04 12.83 o -4 2 7 1002.81 980.00 12.23 o -2 2 7 1018.49 1070.90 12.30 o 0 2 7 909.51 901.79 10.88 o 2 2 7 428.03 384.23 7.76 o -9 3 7 26.60 28.85 4.07 o -7 3 7 8.30 8.64 3.57 o -5 3 7 183.81 193.68 5.01 o -3 3 7 422.09 398.73 6.19 o -1 3 7 113.72 133.77 4.51 o 1 3 7 15.18 15.49 2.86 o -8 4 7 415.47 404.55 8.91 o -6 4 7 526.95 537.23 8.36 o -4 4 7 290.51 286.90 5.67 o -2 4 7 326.76 321.69 5.96 o 0 4 7 408.05 415.51 17.07 o 2 4 7 185.84 197.60 5.80 o -7 5 7 5.15 5.14 3.07 o -5 5 7 42.23 38.08 3.14 o -3 5 7 103.62 90.68 3.93 o -1 5 7 44.60 45.58 3.36 o 1 5 7 11.04 9.28 2.93 o -6 6 7 9.08 12.42 3.00 o -4 6 7 111.65 101.98 4.22 o -2 6 7 73.58 73.47 3.93 o 0 6 7 5.32 2.93 3.14 o -5 7 7 86.46 88.35 4.50 o -3 7 7 68.58 70.25 4.07 o -8 0 8 523.34 586.87 9.65 o -6 0 8 635.04 714.30 8.88 o -4 0 8 1613.84 1507.69 12.05 o -2 0 8 1677.10 1668.69 13.01 o 0 0 8 610.10 590.48 6.30 o 2 0 8 203.98 205.95 7.23 o -9 1 8 12.96 13.65 2.73 o -7 1 8 6.63 5.50 3.03 o -5 1 8 22.27 23.64 2.93 o -3 1 8 47.30 45.01 2.10 o -1 1 8 25.29 25.18 2.11 o 1 1 8 9.02 8.87 2.37 o -8 2 8 39.90 44.29 4.21 o -6 2 8 28.52 25.78 4.14 o -4 2 8 282.69 319.70 6.24 o -2 2 8 353.36 310.51 7.69 o 0 2 8 72.47 79.67 3.00 o -7 3 8 9.36 8.42 3.93 o -5 3 8 0.24 1.64 2.64 o -3 3 8 35.80 33.29 3.07 o -1 3 8 11.25 14.71 3.50 o 1 3 8 0.13 2.14 2.71 o -6 4 8 424.95 439.69 8.05 o -4 4 8 243.83 236.61 5.66 o -2 4 8 138.11 139.73 4.79 o 0 4 8 162.98 155.87 10.31 o -5 5 8 158.26 147.71 5.08 o -3 5 8 42.96 39.07 3.50 o -1 5 8 58.63 59.95 4.07 o -4 6 8 242.95 229.15 6.16 o -7 1 9 40.55 38.65 4.43 o -5 1 9 50.99 49.75 2.45 o -3 1 9 5.41 1.75 2.64 o -1 1 9 6.64 8.57 2.19 o -6 2 9 752.29 922.02 12.50 o -4 2 9 622.45 570.34 8.44 o -2 2 9 389.35 287.40 7.90 o -7 3 9 18.38 18.71 4.64 o -5 3 9 17.35 17.07 3.43 o -3 3 9 109.48 108.19 5.01 o -1 3 9 95.38 92.51 5.65 o -6 4 9 387.96 389.22 8.04 o -4 4 9 244.31 219.70 6.02 o -2 4 9 105.05 104.46 5.01 o -4 0 10 398.74 316.10 7.04 o -5 1 10 7.35 3.86 2.12 o