#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/39/2013927.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2013927_Fobs loop_ _publ_author_name 'Lee, Clare' 'Harrison, William T. A.' _publ_section_title ; The catena-arsenite chain anion, [AsO~2~]~n~^n^{-}: (H~3~NCH~2~CH~2~NH~3~)~0.5~[AsO~2~] and NaAsO~2~ (revisited) ; _journal_issue 5 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first m215 _journal_page_last m218 _journal_volume 60 _journal_year 2004 _space_group_IT_number 61 _symmetry_space_group_name_Hall '-P 2ac 2ab' _symmetry_space_group_name_H-M 'P b c a' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 6.7762 _cell_length_b 5.0901 _cell_length_c 14.3098 _exptl_crystal_F_000 480.00 _reflns_d_resolution_high 0.6607 _[local]_cod_data_source_file bc1044IIsup3.hkl _[local]_cod_data_source_block II #BEGIN Tags that were not found in dictionaries: _shelx_title ' naast in Pbca' _shelx_refln_list_code 4 _shelx_f_calc_maximum 270.60 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' '-x, -y, -z' 'x-1/2, y, -z-1/2' 'x, -y-1/2, z-1/2' '-x-1/2, y-1/2, z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 4544.40 5989.84 75.79 o 4 0 0 35547.84 44550.04 936.36 o 6 0 0 13432.22 16451.45 999.94 o 8 0 0 1117.19 1124.13 78.60 o 10 0 0 4560.76 4951.19 231.88 o 2 1 0 48172.35 55400.64 840.54 o 4 1 0 7893.40 9390.43 81.14 o 6 1 0 14054.70 15687.01 261.82 o 8 1 0 6118.45 6450.33 116.16 o 10 1 0 645.76 552.89 75.57 o 0 2 0 73223.52 73497.20 589.56 o 2 2 0 9948.06 10959.96 121.35 o 4 2 0 29192.52 33502.38 162.17 o 6 2 0 11698.68 13211.91 232.61 o 8 2 0 1962.22 2082.78 78.41 o 2 3 0 34312.89 34772.42 367.17 o 4 3 0 2024.14 2322.00 69.56 o 6 3 0 5545.69 6289.64 91.29 o 8 3 0 4540.85 4524.22 107.38 o 0 4 0 27389.63 27958.29 216.35 o 2 4 0 2043.84 1973.83 40.78 o 4 4 0 11565.41 11927.54 175.61 o 6 4 0 4927.88 4953.36 91.87 o 8 4 0 1018.36 965.57 73.24 o 2 5 0 8806.19 8927.99 142.55 o 4 5 0 2388.77 2425.38 86.99 o 6 5 0 3539.92 3499.53 82.94 o 0 6 0 8468.17 8924.18 220.40 o 2 6 0 177.30 161.54 49.84 o 4 6 0 3260.25 3185.30 106.13 o 6 6 0 1116.45 872.05 107.09 o 2 7 0 2592.65 2729.41 105.62 o 4 7 0 417.66 469.27 69.52 o 1 1 1 118.76 113.91 11.80 o 2 1 1 1622.43 1823.15 45.06 o 3 1 1 624.35 745.74 21.63 o 4 1 1 34.37 44.72 16.52 o 5 1 1 102.99 141.72 23.04 o 6 1 1 8.07 41.86 40.13 o 7 1 1 21.61 16.90 27.68 o 8 1 1 106.23 293.60 57.52 o 9 1 1 24.99 46.45 39.94 o 10 1 1 0.16 -41.39 42.39 o 0 2 1 41.99 78.01 15.18 o 1 2 1 25.69 30.63 9.21 o 2 2 1 359.14 544.18 70.86 o 3 2 1 1019.52 1115.19 24.98 o 4 2 1 631.91 855.20 70.01 o 5 2 1 20.88 14.83 24.35 o 6 2 1 237.49 659.01 106.11 o 7 2 1 160.65 234.71 31.34 o 8 2 1 168.62 268.22 42.05 o 9 2 1 0.23 -47.64 47.64 o 1 3 1 14.39 44.03 17.62 o 2 3 1 2008.48 3001.24 175.32 o 3 3 1 43.09 99.93 19.31 o 4 3 1 730.33 852.01 30.28 o 5 3 1 199.36 310.65 26.02 o 6 3 1 361.76 608.23 45.49 o 7 3 1 31.67 18.54 27.32 o 8 3 1 266.72 526.72 53.12 o 9 3 1 74.13 94.48 44.04 o 0 4 1 3140.36 3890.47 183.03 o 1 4 1 1068.67 1034.29 22.51 o 2 4 1 4.35 74.08 17.96 o 3 4 1 453.95 542.82 23.96 o 4 4 1 886.36 1304.62 92.22 o 5 4 1 6.31 18.37 25.47 o 6 4 1 247.02 454.98 38.66 o 7 4 1 66.43 107.17 35.67 o 8 4 1 63.66 92.36 41.99 o 1 5 1 83.72 164.91 23.65 o 2 5 1 1928.13 2087.14 42.26 o 3 5 1 29.95 47.04 27.56 o 4 5 1 789.42 920.22 40.12 o 5 5 1 305.62 376.98 32.28 o 6 5 1 486.60 643.49 47.21 o 7 5 1 20.94 58.98 40.70 o 0 6 1 1258.50 1585.96 210.12 o 1 6 1 132.20 185.11 35.18 o 2 6 1 137.76 157.77 35.51 o 3 6 1 650.04 703.61 46.02 o 4 6 1 966.92 1102.08 66.13 o 5 6 1 0.95 32.27 41.00 o 6 6 1 342.53 410.09 53.40 o 1 7 1 166.41 223.80 40.78 o 2 7 1 1551.46 1551.91 61.36 o 3 7 1 143.92 132.14 41.34 o 4 7 1 179.13 230.45 44.60 o 0 0 2 2278.24 2076.86 34.42 o 1 0 2 15814.91 16175.31 421.77 o 2 0 2 15.07 15.32 16.89 o 3 0 2 3062.60 3014.15 147.37 o 4 0 2 2268.88 2598.15 118.09 o 5 0 2 1325.08 1503.56 80.60 o 6 0 2 430.19 442.11 45.48 o 7 0 2 3644.47 3859.61 96.33 o 8 0 2 600.04 580.98 65.49 o 9 0 2 233.90 153.05 54.49 o 10 0 2 423.94 447.81 70.95 o 1 1 2 20879.87 22184.02 317.40 o 2 1 2 5858.21 6827.06 43.43 o 3 1 2 936.46 1008.66 21.22 o 4 1 2 1021.80 1207.82 27.06 o 5 1 2 11974.69 12663.37 182.19 o 6 1 2 895.24 983.20 35.44 o 7 1 2 100.30 91.62 29.30 o 8 1 2 689.07 650.89 36.90 o 9 1 2 1588.31 1466.23 52.05 o 10 1 2 40.03 -26.58 58.21 o 0 2 2 2277.55 2182.50 45.70 o 1 2 2 1393.96 1204.50 19.15 o 2 2 2 7.92 11.64 11.98 o 3 2 2 6937.86 7352.65 68.69 o 4 2 2 1805.10 1932.07 30.09 o 5 2 2 786.77 823.10 27.23 o 6 2 2 378.00 403.42 25.15 o 7 2 2 4426.01 4655.16 60.51 o 8 2 2 443.30 482.08 39.38 o 9 2 2 8.75 -16.04 41.15 o 1 3 2 10904.44 11042.03 137.04 o 2 3 2 2878.76 2866.51 29.41 o 3 3 2 2806.61 2786.57 35.23 o 4 3 2 612.63 732.74 29.91 o 5 3 2 4023.68 4234.24 50.91 o 6 3 2 701.85 720.30 30.95 o 7 3 2 250.17 237.68 31.93 o 8 3 2 443.56 473.37 41.38 o 9 3 2 1219.28 1122.18 63.40 o 0 4 2 1508.86 1633.39 67.05 o 1 4 2 1913.32 1849.21 28.75 o 2 4 2 39.69 32.50 19.92 o 3 4 2 3471.89 3418.46 44.90 o 4 4 2 1060.52 1147.45 49.30 o 5 4 2 248.99 288.87 28.31 o 6 4 2 254.04 288.75 31.96 o 7 4 2 2203.26 2212.37 55.76 o 8 4 2 237.23 295.69 42.44 o 1 5 2 2497.66 2314.76 43.82 o 2 5 2 1212.57 1304.36 58.35 o 3 5 2 242.50 242.35 26.36 o 4 5 2 181.00 229.30 37.95 o 5 5 2 3225.10 3096.00 65.68 o 6 5 2 313.10 407.91 39.94 o 7 5 2 3.51 53.43 34.48 o 0 6 2 632.13 851.71 100.64 o 1 6 2 1329.99 1265.96 50.64 o 2 6 2 27.59 66.47 29.82 o 3 6 2 1074.11 1103.55 44.69 o 4 6 2 407.90 542.41 70.39 o 5 6 2 95.00 66.62 50.84 o 6 6 2 113.03 262.53 55.70 o 1 7 2 687.91 698.32 48.99 o 2 7 2 325.37 483.56 63.15 o 3 7 2 189.47 209.46 43.49 o 4 7 2 49.96 66.72 77.02 o 1 1 3 658.00 586.28 19.21 o 2 1 3 546.80 596.60 14.10 o 3 1 3 529.43 557.17 17.06 o 4 1 3 154.22 165.93 19.80 o 5 1 3 6.12 3.36 23.61 o 6 1 3 152.59 159.96 25.48 o 7 1 3 42.26 51.63 29.00 o 8 1 3 15.96 61.73 33.27 o 9 1 3 48.51 89.39 37.05 o 10 1 3 4.52 12.62 41.91 o 0 2 3 1583.03 1613.69 29.66 o 1 2 3 58.24 51.83 10.97 o 2 2 3 43.69 35.17 11.94 o 3 2 3 1573.05 1548.08 28.00 o 4 2 3 0.11 12.71 18.07 o 5 2 3 0.74 -20.05 20.45 o 6 2 3 3.79 40.64 21.43 o 7 2 3 502.63 516.39 32.59 o 8 2 3 56.29 53.99 34.66 o 9 2 3 4.76 -14.96 40.33 o 1 3 3 1285.87 1249.50 23.97 o 2 3 3 24.49 48.67 15.60 o 3 3 3 177.50 191.39 20.74 o 4 3 3 156.81 138.74 21.82 o 5 3 3 1238.53 1267.89 34.47 o 6 3 3 4.03 13.06 29.08 o 7 3 3 2.89 -26.09 29.66 o 8 3 3 0.59 23.51 37.99 o 9 3 3 221.18 199.38 56.61 o 0 4 3 0.31 56.79 32.43 o 1 4 3 1909.72 1764.49 28.74 o 2 4 3 330.96 369.94 23.04 o 3 4 3 1552.23 1552.26 37.13 o 4 4 3 48.13 86.66 23.07 o 5 4 3 14.50 49.86 24.47 o 6 4 3 92.95 107.19 35.37 o 7 4 3 575.09 598.04 41.53 o 8 4 3 2.91 47.85 37.94 o 1 5 3 1429.63 1368.89 37.13 o 2 5 3 0.34 54.18 23.13 o 3 5 3 176.87 187.80 25.86 o 4 5 3 114.73 151.14 30.19 o 5 5 3 1599.92 1629.86 57.54 o 6 5 3 2.91 77.60 39.46 o 7 5 3 5.53 3.50 34.05 o 0 6 3 202.71 299.39 41.59 o 1 6 3 647.48 671.51 38.02 o 2 6 3 1.03 -10.04 29.31 o 3 6 3 1754.43 1717.32 53.01 o 4 6 3 4.28 43.91 47.71 o 5 6 3 14.39 -14.86 50.88 o 6 6 3 22.95 15.05 51.78 o 1 7 3 1082.21 1063.33 52.76 o 2 7 3 21.23 80.84 40.65 o 3 7 3 310.73 344.30 104.25 o 4 7 3 4.03 -19.19 49.42 o 0 0 4 25011.93 25415.70 208.45 o 1 0 4 29117.36 28355.65 333.27 o 2 0 4 3.51 30.55 16.27 o 3 0 4 51057.24 52252.80 988.88 o 4 0 4 1978.24 2240.43 53.48 o 5 0 4 89.23 144.57 40.33 o 6 0 4 958.88 1076.42 53.09 o 7 0 4 11732.67 11802.69 154.26 o 8 0 4 4.99 -11.99 46.02 o 9 0 4 871.11 927.50 125.09 o 10 0 4 551.72 453.76 64.75 o 1 1 4 28514.18 27633.87 250.59 o 2 1 4 1111.61 973.49 16.31 o 3 1 4 7367.82 7929.46 95.54 o 4 1 4 414.46 459.34 22.59 o 5 1 4 20166.59 20817.96 97.94 o 6 1 4 1368.45 1417.34 40.56 o 7 1 4 16.22 26.24 33.48 o 8 1 4 346.09 383.25 38.68 o 9 1 4 4713.95 4733.31 115.85 o 0 2 4 3429.76 3063.89 39.14 o 1 2 4 20571.75 20295.24 234.08 o 2 2 4 1670.29 1710.68 34.21 o 3 2 4 33418.19 34018.82 342.52 o 4 2 4 2299.29 2287.84 31.13 o 5 2 4 100.37 130.29 20.28 o 6 2 4 1198.86 1231.64 34.27 o 7 2 4 8940.42 9073.74 87.89 o 8 2 4 184.56 150.73 40.46 o 9 2 4 746.72 696.68 65.24 o 1 3 4 15253.49 14671.64 104.70 o 2 3 4 2636.84 2546.97 34.38 o 3 3 4 3471.13 3525.01 41.85 o 4 3 4 20.14 33.19 20.28 o 5 3 4 12418.15 12962.04 136.80 o 6 3 4 211.11 226.70 30.96 o 7 3 4 6.29 8.01 31.74 o 8 3 4 408.28 503.28 61.44 o 9 3 4 2969.90 2790.08 96.81 o 0 4 4 1996.71 1851.01 45.76 o 1 4 4 7145.73 6970.20 81.14 o 2 4 4 217.99 225.70 22.38 o 3 4 4 13021.93 13016.92 168.26 o 4 4 4 884.03 879.90 30.22 o 5 4 4 101.63 144.73 29.11 o 6 4 4 500.03 465.69 36.31 o 7 4 4 4493.95 4520.37 72.74 o 8 4 4 86.17 64.09 42.33 o 1 5 4 5540.60 5462.47 94.43 o 2 5 4 419.11 387.46 26.50 o 3 5 4 1325.42 1260.07 36.91 o 4 5 4 325.80 307.25 32.80 o 5 5 4 4436.17 4376.18 78.61 o 6 5 4 480.45 473.65 44.85 o 7 5 4 12.04 27.64 40.06 o 0 6 4 1059.88 1005.80 53.79 o 1 6 4 1806.71 1836.95 47.91 o 2 6 4 0.72 12.89 28.49 o 3 6 4 3500.63 3568.27 111.61 o 4 6 4 255.82 243.36 44.72 o 5 6 4 58.97 -24.71 52.25 o 6 6 4 68.00 33.85 54.86 o 1 7 4 1376.79 1330.16 74.74 o 2 7 4 229.08 266.48 44.28 o 3 7 4 302.23 422.22 57.54 o 1 1 5 71.42 74.54 11.49 o 2 1 5 524.97 491.09 16.44 o 3 1 5 212.40 221.99 15.74 o 4 1 5 54.02 60.81 24.38 o 5 1 5 562.41 555.41 33.45 o 6 1 5 0.59 0.67 29.75 o 7 1 5 9.41 18.81 31.53 o 8 1 5 51.79 56.09 35.75 o 9 1 5 2.30 -9.46 36.99 o 0 2 5 242.33 199.66 21.06 o 1 2 5 724.21 634.99 18.11 o 2 2 5 334.21 292.70 18.15 o 3 2 5 6.80 -0.52 15.87 o 4 2 5 377.55 387.47 21.34 o 5 2 5 56.94 59.48 23.07 o 6 2 5 217.54 199.28 29.08 o 7 2 5 47.70 75.36 43.26 o 8 2 5 61.61 79.44 52.36 o 9 2 5 29.05 24.37 44.47 o 1 3 5 1294.22 1181.07 26.52 o 2 3 5 708.54 628.94 24.29 o 3 3 5 112.93 81.88 21.33 o 4 3 5 169.51 160.25 24.82 o 5 3 5 456.30 416.51 32.25 o 6 3 5 289.89 260.45 31.70 o 7 3 5 89.46 122.83 33.92 o 8 3 5 134.90 72.07 49.41 o 9 3 5 64.24 129.57 57.07 o 0 4 5 2471.05 2178.79 49.61 o 1 4 5 7.03 34.66 20.94 o 2 4 5 15.76 0.43 20.27 o 3 4 5 582.44 531.68 24.76 o 4 4 5 572.51 532.42 31.07 o 5 4 5 56.16 81.39 29.13 o 6 4 5 241.25 272.78 35.33 o 7 4 5 441.04 415.48 42.77 o 8 4 5 11.80 -2.92 48.99 o 1 5 5 1140.78 1013.21 32.35 o 2 5 5 832.02 774.88 31.84 o 3 5 5 166.31 169.44 30.45 o 4 5 5 270.31 255.56 33.42 o 5 5 5 504.22 550.43 41.86 o 6 5 5 384.12 444.95 44.45 o 7 5 5 78.55 144.23 40.33 o 0 6 5 1053.83 1032.29 56.49 o 1 6 5 346.61 288.52 31.46 o 2 6 5 134.37 133.61 31.80 o 3 6 5 250.23 319.44 40.10 o 4 6 5 619.72 595.75 51.08 o 5 6 5 32.15 68.52 47.97 o 1 7 5 448.00 415.41 46.15 o 2 7 5 808.05 679.82 58.20 o 3 7 5 9.77 40.55 43.33 o 0 0 6 13498.84 12015.61 91.94 o 1 0 6 1462.18 1404.25 30.64 o 2 0 6 376.55 344.13 25.61 o 3 0 6 112.86 109.18 24.91 o 4 0 6 11165.24 11442.00 323.92 o 5 0 6 2.86 -7.39 40.48 o 6 0 6 2396.45 2270.47 119.68 o 7 0 6 56.96 59.79 43.17 o 8 0 6 2226.96 2132.36 85.50 o 9 0 6 53.78 112.53 71.49 o 1 1 6 238.63 229.72 12.08 o 2 1 6 26318.86 26162.00 224.68 o 3 1 6 69.76 68.43 17.29 o 4 1 6 4996.23 4956.56 62.50 o 5 1 6 228.55 236.20 27.58 o 6 1 6 3791.32 3889.00 64.35 o 7 1 6 9.46 41.65 32.85 o 8 1 6 3085.20 3061.13 69.38 o 9 1 6 7.61 36.51 42.76 o 0 2 6 13601.57 12500.14 171.48 o 1 2 6 200.59 189.60 12.22 o 2 2 6 178.75 192.15 15.40 o 3 2 6 117.84 137.04 17.61 o 4 2 6 8415.50 8325.38 127.04 o 5 2 6 0.56 31.31 23.93 o 6 2 6 1943.99 1851.07 61.96 o 7 2 6 13.92 -14.82 43.97 o 8 2 6 1586.20 1440.51 62.78 o 9 2 6 15.27 35.16 45.98 o 1 3 6 251.66 266.50 21.28 o 2 3 6 13261.88 12793.41 122.15 o 3 3 6 173.03 169.19 24.60 o 4 3 6 2962.67 2905.64 49.87 o 5 3 6 65.74 56.50 31.75 o 6 3 6 2829.07 2625.55 66.11 o 7 3 6 103.10 60.26 45.48 o 8 3 6 1895.02 1770.74 81.28 o 9 3 6 3.00 68.54 68.50 o 0 4 6 7163.44 6735.61 104.25 o 1 4 6 5.21 -0.51 20.48 o 2 4 6 244.12 253.23 22.96 o 3 4 6 3.28 21.25 24.17 o 4 4 6 4402.75 4230.01 84.67 o 5 4 6 4.89 7.95 28.77 o 6 4 6 1146.76 1051.26 50.14 o 7 4 6 2.19 24.85 45.35 o 8 4 6 832.41 738.26 58.50 o 1 5 6 3.64 39.42 22.78 o 2 5 6 5041.87 4945.10 96.79 o 3 5 6 65.13 60.43 28.88 o 4 5 6 788.53 699.76 39.10 o 5 5 6 54.34 86.17 33.35 o 6 5 6 1135.71 1006.06 53.30 o 7 5 6 5.30 17.80 46.11 o 0 6 6 2503.13 2382.57 83.21 o 1 6 6 39.66 60.27 29.15 o 2 6 6 129.52 122.44 35.93 o 3 6 6 18.65 24.47 37.98 o 4 6 6 1551.21 1551.19 69.35 o 5 6 6 0.14 60.50 47.59 o 1 7 6 1.06 13.38 40.45 o 2 7 6 1230.73 1207.04 69.90 o 3 7 6 0.58 -14.34 42.92 o 1 1 7 179.62 169.61 12.73 o 2 1 7 2.00 -0.78 15.52 o 3 1 7 98.85 97.16 19.41 o 4 1 7 307.66 284.67 23.45 o 5 1 7 3.88 9.07 27.67 o 6 1 7 263.06 239.71 33.13 o 7 1 7 29.49 -5.78 31.12 o 8 1 7 4.99 40.18 34.67 o 9 1 7 1.62 -23.96 43.48 o 0 2 7 2992.57 2696.84 53.44 o 1 2 7 32.48 21.01 12.36 o 2 2 7 1.16 23.69 17.22 o 3 2 7 67.98 79.25 20.12 o 4 2 7 369.18 342.86 26.38 o 5 2 7 6.18 -13.88 35.25 o 6 2 7 177.08 176.14 36.40 o 7 2 7 72.04 44.13 40.69 o 8 2 7 1.21 -16.39 40.74 o 9 2 7 3.92 -44.21 44.21 o 1 3 7 283.88 256.93 22.07 o 2 3 7 1048.51 973.65 27.92 o 3 3 7 1.26 10.25 21.18 o 4 3 7 56.43 70.58 26.52 o 5 3 7 178.15 176.03 29.96 o 6 3 7 243.59 230.09 44.18 o 7 3 7 13.95 -3.41 49.22 o 8 3 7 230.08 216.29 48.62 o 0 4 7 1439.08 1331.66 45.50 o 1 4 7 180.77 142.97 22.11 o 2 4 7 574.68 536.80 28.85 o 3 4 7 18.45 25.73 24.41 o 4 4 7 1119.95 1051.01 36.43 o 5 4 7 21.12 22.45 29.61 o 6 4 7 668.17 567.01 45.02 o 7 4 7 31.84 40.12 49.99 o 8 4 7 120.14 95.91 53.23 o 1 5 7 222.18 244.23 26.47 o 2 5 7 1414.09 1347.66 50.07 o 3 5 7 0.42 -15.00 28.68 o 4 5 7 90.64 86.28 30.78 o 5 5 7 232.51 243.77 35.56 o 6 5 7 317.58 305.34 44.05 o 7 5 7 12.62 59.67 51.46 o 0 6 7 2231.65 2289.37 78.17 o 1 6 7 20.41 37.56 33.12 o 2 6 7 80.91 137.84 35.76 o 3 6 7 85.31 88.81 39.53 o 4 6 7 740.06 784.40 46.68 o 5 6 7 10.96 -4.24 37.35 o 1 7 7 162.77 184.65 44.81 o 2 7 7 656.86 709.90 54.60 o 0 0 8 17856.11 15901.20 215.38 o 1 0 8 4498.49 4127.72 51.08 o 2 0 8 3477.39 3335.12 51.75 o 3 0 8 11125.13 10710.42 96.33 o 4 0 8 10731.07 10959.90 199.00 o 5 0 8 2.09 42.36 40.54 o 6 0 8 4181.35 4001.52 94.59 o 7 0 8 2805.97 2667.81 141.64 o 8 0 8 1178.85 1035.14 66.60 o 9 0 8 263.56 215.52 58.76 o 1 1 8 3120.80 2940.25 29.85 o 2 1 8 18702.52 17686.42 91.96 o 3 1 8 1555.21 1531.16 30.81 o 4 1 8 2125.74 2130.01 42.51 o 5 1 8 3392.90 3380.36 71.74 o 6 1 8 3088.26 3054.45 75.28 o 7 1 8 10.71 -2.06 30.41 o 8 1 8 2426.67 2232.93 70.52 o 9 1 8 1354.75 1165.77 59.96 o 0 2 8 22240.92 19809.08 237.72 o 1 2 8 4364.31 4103.00 53.43 o 2 2 8 576.82 549.14 21.25 o 3 2 8 7195.94 6882.80 80.86 o 4 2 8 7031.82 6896.39 85.57 o 5 2 8 2.36 14.68 28.81 o 6 2 8 2548.22 2320.91 86.51 o 7 2 8 2097.37 2140.27 67.70 o 8 2 8 455.45 482.74 51.84 o 9 2 8 274.99 269.76 48.65 o 1 3 8 2249.44 2077.88 34.02 o 2 3 8 7743.01 7210.85 64.94 o 3 3 8 687.12 672.14 28.97 o 4 3 8 2597.73 2509.47 45.03 o 5 3 8 2659.08 2483.79 46.65 o 6 3 8 2932.10 2863.62 75.91 o 7 3 8 12.60 43.84 41.67 o 8 3 8 1253.18 1279.39 66.27 o 0 4 8 7822.84 7814.65 130.95 o 1 4 8 1652.52 1578.87 34.47 o 2 4 8 398.46 389.28 28.03 o 3 4 8 3246.16 3117.99 49.17 o 4 4 8 3461.03 3443.97 54.42 o 5 4 8 14.02 26.35 29.85 o 6 4 8 1218.69 1110.16 60.36 o 7 4 8 1177.70 1190.05 66.61 o 1 5 8 1218.28 1196.15 41.53 o 2 5 8 3840.62 3910.82 66.10 o 3 5 8 388.05 364.14 34.51 o 4 5 8 311.84 317.21 35.05 o 5 5 8 987.75 907.64 43.61 o 6 5 8 600.55 547.27 53.88 o 0 6 8 1535.15 1511.30 84.68 o 1 6 8 446.63 445.13 40.94 o 2 6 8 247.04 284.69 39.05 o 3 6 8 989.69 1044.39 55.15 o 4 6 8 1144.43 1177.00 53.21 o 5 6 8 15.52 18.29 34.94 o 1 7 8 375.02 386.59 49.92 o 2 7 8 831.48 796.03 115.22 o 1 1 9 50.78 54.12 15.50 o 2 1 9 3.63 -8.66 16.58 o 3 1 9 50.65 72.06 26.65 o 4 1 9 114.84 86.37 30.32 o 5 1 9 403.90 393.07 33.69 o 6 1 9 21.96 42.46 31.73 o 7 1 9 11.52 -13.55 33.39 o 8 1 9 0.81 11.88 40.73 o 9 1 9 10.12 8.92 42.79 o 0 2 9 74.99 87.86 22.12 o 1 2 9 637.38 584.48 19.43 o 2 2 9 48.47 46.36 18.68 o 3 2 9 160.30 127.27 20.75 o 4 2 9 17.32 24.22 28.35 o 5 2 9 17.50 4.82 27.22 o 6 2 9 1.79 28.39 35.80 o 7 2 9 85.21 53.47 39.70 o 8 2 9 3.31 31.11 44.10 o 1 3 9 904.87 788.20 28.00 o 2 3 9 257.79 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10163.09 58.74 o 2 1 10 4412.66 4473.94 61.30 o 3 1 10 2182.11 2113.03 41.11 o 4 1 10 1069.37 1020.47 35.43 o 5 1 10 6631.70 6593.61 79.17 o 6 1 10 332.88 323.69 34.53 o 7 1 10 80.49 41.28 38.48 o 8 1 10 548.27 499.29 48.66 o 9 1 10 1572.57 1378.35 123.59 o 0 2 10 2058.36 2020.40 42.59 o 1 2 10 5215.74 4975.49 45.31 o 2 2 10 17.77 15.28 20.72 o 3 2 10 5700.39 5441.11 84.58 o 4 2 10 963.21 986.34 38.50 o 5 2 10 401.03 382.36 36.07 o 6 2 10 242.90 268.99 40.61 o 7 2 10 3102.15 2917.55 133.56 o 8 2 10 148.25 159.42 50.23 o 1 3 10 5344.99 4854.18 50.49 o 2 3 10 1909.30 1813.98 36.76 o 3 3 10 614.73 582.12 28.51 o 4 3 10 708.78 694.19 37.66 o 5 3 10 5755.16 5313.34 86.70 o 6 3 10 315.05 275.86 46.71 o 7 3 10 0.45 -8.23 50.88 o 8 3 10 285.64 316.59 59.01 o 0 4 10 851.00 787.86 50.80 o 1 4 10 2151.70 2007.84 39.56 o 2 4 10 38.09 35.59 24.34 o 3 4 10 3326.11 3106.38 50.51 o 4 4 10 483.73 479.92 36.21 o 5 4 10 201.91 174.41 34.18 o 6 4 10 144.17 135.79 48.96 o 7 4 10 1735.30 1573.10 72.17 o 1 5 10 2416.53 2269.35 55.06 o 2 5 10 705.09 775.28 37.74 o 3 5 10 718.10 701.49 37.87 o 4 5 10 112.80 132.09 33.94 o 5 5 10 1514.38 1398.59 57.10 o 6 5 10 76.73 98.82 49.05 o 0 6 10 244.51 246.06 59.55 o 1 6 10 453.02 394.81 45.35 o 2 6 10 27.21 70.72 33.58 o 3 6 10 1388.51 1456.39 50.53 o 4 6 10 162.94 195.32 37.39 o 1 1 11 7.26 16.26 18.46 o 2 1 11 0.99 -6.82 24.41 o 3 1 11 0.19 -2.93 25.02 o 4 1 11 161.21 144.57 26.99 o 5 1 11 82.38 62.89 30.77 o 6 1 11 93.30 103.01 32.21 o 7 1 11 6.22 13.10 38.47 o 8 1 11 0.59 -5.69 40.28 o 0 2 11 661.72 579.53 35.65 o 1 2 11 302.44 289.95 22.88 o 2 2 11 7.75 -2.07 23.02 o 3 2 11 300.97 274.78 31.96 o 4 2 11 91.46 95.88 31.36 o 5 2 11 0.92 30.16 30.78 o 6 2 11 29.75 18.28 37.21 o 7 2 11 55.41 73.39 44.50 o 8 2 11 0.32 -17.92 44.75 o 1 3 11 161.94 148.58 22.49 o 2 3 11 419.99 392.98 26.32 o 3 3 11 93.20 102.02 30.14 o 4 3 11 46.80 46.69 31.10 o 5 3 11 182.14 148.77 37.71 o 6 3 11 40.40 22.02 47.19 o 7 3 11 1.51 31.34 51.31 o 0 4 11 216.84 158.59 41.14 o 1 4 11 214.81 188.98 29.76 o 2 4 11 152.69 143.45 25.87 o 3 4 11 810.17 768.99 33.91 o 4 4 11 334.09 362.62 37.96 o 5 4 11 3.66 4.06 34.79 o 6 4 11 177.38 193.40 48.93 o 7 4 11 250.26 263.12 58.95 o 1 5 11 269.65 249.03 34.76 o 2 5 11 542.30 510.25 33.66 o 3 5 11 138.33 137.78 32.30 o 4 5 11 52.77 61.42 38.33 o 5 5 11 230.62 203.87 41.66 o 0 6 11 605.42 649.74 69.67 o 1 6 11 293.46 254.24 43.72 o 2 6 11 8.33 13.91 42.18 o 3 6 11 550.50 547.20 41.45 o 0 0 12 8793.43 8218.57 118.96 o 1 0 12 1434.25 1324.45 39.16 o 2 0 12 1508.40 1495.06 47.42 o 3 0 12 1565.66 1433.92 48.18 o 4 0 12 4896.79 5118.12 82.29 o 5 0 12 67.46 102.16 44.28 o 6 0 12 2423.06 2281.92 109.52 o 7 0 12 724.65 703.59 60.82 o 8 0 12 508.41 493.82 80.00 o 1 1 12 2633.88 2403.94 39.10 o 2 1 12 6178.66 6067.91 60.77 o 3 1 12 295.83 271.26 27.65 o 4 1 12 553.70 538.22 31.85 o 5 1 12 1921.95 1902.07 50.38 o 6 1 12 1813.01 1737.47 59.16 o 7 1 12 39.34 92.35 40.79 o 8 1 12 1190.78 1025.17 57.40 o 0 2 12 9999.81 9984.32 172.04 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