#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/39/2013931.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2013931_Fobs loop_ _publ_author_name 'Hardie, Michaele J.' 'Kilner, Colin A.' 'Halcrow, Malcolm A.' _publ_section_title ; {Tris[4-(1H-pyrazol-3-yl)-3-azabut-3-enyl]amine}iron(II) diperchlorate monohydrate ; _journal_issue 4 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first m177 _journal_page_last m179 _journal_volume 60 _journal_year 2004 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 101.986 _cell_angle_gamma 90.000 _cell_length_a 9.4086 _cell_length_b 22.5317 _cell_length_c 12.7279 _exptl_crystal_F_000 1344.00 _reflns_d_resolution_high 0.7702 _[local]_cod_data_source_file bm1561Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' mh104 at 100K' _shelx_refln_list_code 4 _shelx_f_calc_maximum 198.62 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 2392.28 1807.04 45.74 o 6 0 0 4516.72 4174.11 160.07 o 8 0 0 4447.46 4583.86 306.09 o 10 0 0 4727.76 5645.65 221.18 o 2 1 0 6867.12 6913.49 119.67 o 3 1 0 2489.86 2592.27 53.42 o 4 1 0 2.65 11.63 2.52 o 5 1 0 2961.63 3039.90 58.65 o 6 1 0 245.50 237.90 9.36 o 7 1 0 2368.26 2420.70 81.90 o 8 1 0 148.60 149.74 12.29 o 9 1 0 1564.40 1498.53 91.44 o 10 1 0 41.59 29.23 23.76 o 11 1 0 885.26 1027.70 73.15 o 0 2 0 1.83 -0.47 0.94 o 1 2 0 68.90 38.83 10.61 o 2 2 0 4206.02 4065.70 379.86 o 3 2 0 810.44 733.21 24.18 o 4 2 0 3524.42 3615.19 55.22 o 5 2 0 45.10 46.28 6.61 o 6 2 0 140.87 145.24 5.59 o 7 2 0 3.00 -3.57 5.70 o 8 2 0 70.02 63.05 30.42 o 9 2 0 28.86 19.56 11.06 o 10 2 0 155.11 168.35 14.91 o 11 2 0 293.54 374.68 47.09 o 2 3 0 165.27 164.59 15.17 o 3 3 0 4830.67 4162.62 70.48 o 4 3 0 1448.17 1338.08 52.19 o 5 3 0 735.33 590.39 19.87 o 6 3 0 1.18 -3.84 4.48 o 7 3 0 2563.73 2567.72 70.06 o 8 3 0 1100.40 1084.45 47.39 o 9 3 0 1357.67 1383.96 233.85 o 10 3 0 250.55 302.63 31.18 o 11 3 0 177.88 189.53 37.94 o 0 4 0 4083.63 3996.25 199.11 o 1 4 0 18.59 15.71 1.79 o 2 4 0 24728.92 24338.52 514.00 o 3 4 0 757.57 448.75 92.08 o 4 4 0 6710.73 6749.81 114.60 o 5 4 0 19.83 5.97 3.40 o 6 4 0 4810.07 5006.35 107.90 o 7 4 0 21.38 19.16 5.63 o 8 4 0 5.61 13.49 8.50 o 9 4 0 200.83 162.34 25.35 o 10 4 0 356.47 343.23 68.04 o 11 4 0 73.70 84.30 13.98 o 1 5 0 3095.18 3302.19 48.23 o 2 5 0 953.48 681.05 131.12 o 3 5 0 850.14 961.29 22.22 o 4 5 0 39.54 59.93 3.76 o 5 5 0 271.00 218.29 61.19 o 6 5 0 66.13 52.67 4.68 o 7 5 0 21.19 18.02 4.59 o 8 5 0 627.74 607.63 23.53 o 9 5 0 66.16 84.38 9.10 o 10 5 0 6.05 11.21 10.86 o 11 5 0 80.38 39.45 30.38 o 0 6 0 5719.61 6055.01 129.94 o 1 6 0 13558.82 13797.40 217.51 o 2 6 0 831.32 850.04 71.78 o 3 6 0 2243.04 2261.23 104.86 o 4 6 0 6727.83 7070.58 150.77 o 5 6 0 2804.15 2929.91 45.20 o 6 6 0 1.68 2.15 2.97 o 7 6 0 1883.17 1996.20 49.66 o 8 6 0 695.45 678.93 20.77 o 9 6 0 942.55 795.73 86.48 o 10 6 0 268.20 271.55 19.46 o 11 6 0 179.47 250.12 41.18 o 1 7 0 17.27 13.06 2.55 o 2 7 0 5045.68 5263.51 206.46 o 3 7 0 3505.79 3594.89 211.79 o 4 7 0 96.92 84.48 2.85 o 5 7 0 189.91 160.03 5.69 o 6 7 0 1383.41 1617.88 37.33 o 7 7 0 257.77 253.27 10.55 o 8 7 0 83.44 78.36 9.76 o 9 7 0 110.80 102.63 13.82 o 10 7 0 8.93 25.72 20.57 o 11 7 0 260.95 244.22 42.77 o 0 8 0 10727.70 11179.12 225.78 o 1 8 0 41.93 85.30 3.52 o 2 8 0 5620.73 5341.33 79.12 o 3 8 0 1405.61 1495.22 26.20 o 4 8 0 3280.45 3183.83 64.07 o 5 8 0 8.25 9.44 5.67 o 6 8 0 277.92 284.64 18.14 o 7 8 0 319.42 335.16 11.02 o 8 8 0 40.38 53.66 5.87 o 9 8 0 629.54 647.08 80.28 o 10 8 0 998.46 979.46 227.80 o 11 8 0 13.49 10.66 30.24 o 1 9 0 485.18 360.74 7.88 o 2 9 0 1.97 0.20 4.18 o 3 9 0 3153.05 2938.83 54.76 o 4 9 0 3588.26 3961.09 72.91 o 5 9 0 3672.54 3679.12 112.49 o 6 9 0 1551.02 1552.39 56.18 o 7 9 0 4.72 -11.61 14.43 o 8 9 0 218.74 185.90 16.81 o 9 9 0 457.58 446.27 33.99 o 10 9 0 234.91 198.27 71.13 o 11 9 0 86.07 104.83 24.91 o 0 10 0 228.03 263.24 14.64 o 1 10 0 2557.59 2597.62 37.49 o 2 10 0 1563.57 1607.65 29.15 o 3 10 0 5366.98 5951.36 121.73 o 4 10 0 1219.24 1359.27 25.04 o 5 10 0 250.67 256.42 16.64 o 6 10 0 2538.88 2797.09 82.77 o 7 10 0 570.38 576.15 25.93 o 8 10 0 90.39 132.81 21.34 o 9 10 0 69.69 53.01 22.01 o 10 10 0 48.65 23.47 32.04 o 1 11 0 15258.53 15205.30 224.25 o 2 11 0 11307.44 12437.55 180.58 o 3 11 0 7926.33 8172.94 157.12 o 4 11 0 139.94 137.85 10.45 o 5 11 0 11032.93 11301.86 324.52 o 6 11 0 542.04 461.27 20.96 o 7 11 0 2804.15 3086.47 184.34 o 8 11 0 118.58 102.80 19.17 o 9 11 0 1958.29 2271.06 103.39 o 10 11 0 275.62 195.69 77.25 o 11 11 0 483.48 466.55 46.43 o 0 12 0 11436.50 12703.72 367.15 o 1 12 0 556.99 577.76 11.53 o 2 12 0 4007.66 4038.41 71.59 o 3 12 0 78.98 75.08 5.82 o 4 12 0 5795.31 5856.10 619.61 o 5 12 0 234.77 218.98 28.54 o 6 12 0 7559.10 7437.62 341.76 o 7 12 0 375.28 346.84 22.42 o 8 12 0 2409.68 2490.54 108.36 o 9 12 0 0.89 -18.42 20.45 o 1 13 0 2.25 13.71 3.87 o 2 13 0 819.76 917.30 15.85 o 3 13 0 746.13 740.80 15.45 o 4 13 0 281.00 338.00 12.18 o 5 13 0 162.72 181.50 8.52 o 6 13 0 952.69 879.73 39.22 o 7 13 0 3.39 9.70 16.02 o 8 13 0 218.06 228.23 34.81 o 9 13 0 1334.09 1273.56 59.69 o 0 14 0 1266.00 1236.46 30.22 o 1 14 0 1462.24 1480.57 35.90 o 2 14 0 833.87 854.86 15.85 o 3 14 0 3.50 4.79 3.78 o 4 14 0 1207.37 1192.90 24.71 o 5 14 0 820.18 840.91 41.61 o 6 14 0 1911.63 1894.99 57.18 o 7 14 0 94.53 78.24 19.47 o 8 14 0 1377.11 1343.02 57.28 o 9 14 0 9.87 3.32 63.21 o 10 14 0 798.63 818.91 91.37 o 1 15 0 6783.03 7074.56 99.78 o 2 15 0 1563.67 1704.75 30.78 o 3 15 0 2682.64 2718.46 51.65 o 4 15 0 1312.89 1155.23 120.03 o 5 15 0 4431.54 4635.20 97.85 o 6 15 0 133.36 148.08 31.75 o 7 15 0 640.37 623.32 40.72 o 8 15 0 1315.51 1416.61 137.80 o 9 15 0 325.78 354.50 51.62 o 10 15 0 414.80 421.27 38.20 o 0 16 0 1744.81 1828.16 50.26 o 1 16 0 287.19 306.71 22.61 o 2 16 0 2418.14 2758.48 56.09 o 3 16 0 102.85 103.35 6.73 o 4 16 0 136.08 111.25 8.46 o 5 16 0 16.47 10.28 7.08 o 6 16 0 56.67 39.89 22.48 o 7 16 0 199.09 233.10 27.65 o 8 16 0 9.61 -23.18 23.18 o 9 16 0 209.22 256.75 64.08 o 1 17 0 165.31 163.83 8.42 o 2 17 0 313.43 327.54 12.63 o 3 17 0 239.46 227.91 8.75 o 4 17 0 12.51 2.19 6.16 o 5 17 0 541.70 606.67 22.02 o 6 17 0 255.75 268.32 27.78 o 7 17 0 1252.93 1234.18 70.27 o 8 17 0 332.71 371.66 28.49 o 0 18 0 45.30 44.45 11.73 o 1 18 0 2.63 3.15 6.44 o 2 18 0 1523.57 1574.58 35.21 o 3 18 0 951.58 1024.24 35.62 o 4 18 0 167.67 167.33 8.20 o 5 18 0 226.35 211.74 19.45 o 7 18 0 3.58 0.39 42.33 o 8 18 0 426.60 350.86 36.43 o 1 19 0 10.78 5.68 10.15 o 2 19 0 183.37 197.78 14.10 o 3 19 0 26.20 20.85 8.86 o 4 19 0 172.34 173.11 20.27 o 5 19 0 6.14 12.99 9.80 o 6 19 0 191.94 201.29 39.89 o 7 19 0 345.20 364.25 40.68 o 8 19 0 230.91 136.91 39.01 o 9 19 0 214.50 224.34 45.34 o 0 20 0 1653.55 1930.30 54.86 o 1 20 0 1.94 3.39 8.82 o 2 20 0 935.07 983.32 28.17 o 3 20 0 1061.23 987.98 37.33 o 4 20 0 2033.00 1963.03 78.91 o 5 20 0 5.60 -21.39 26.40 o 6 20 0 961.25 969.17 47.09 o 7 20 0 13.77 14.40 48.67 o 8 20 0 164.12 193.37 44.57 o 1 21 0 2.26 7.63 9.39 o 2 21 0 1170.42 1098.89 36.30 o 3 21 0 129.63 144.91 18.64 o 4 21 0 507.82 507.28 30.26 o 5 21 0 516.44 497.11 44.64 o 6 21 0 21.98 11.75 24.77 o 7 21 0 201.09 191.23 30.23 o 8 21 0 18.28 1.82 22.41 o 0 22 0 1873.45 2108.62 113.65 o 1 22 0 4.06 14.64 10.91 o 2 22 0 3433.54 3661.89 104.62 o 3 22 0 411.08 401.13 24.14 o 4 22 0 834.08 869.37 41.60 o 5 22 0 332.59 280.50 32.15 o 6 22 0 387.10 473.06 40.89 o 7 22 0 516.35 488.95 41.96 o 1 23 0 1222.99 1266.42 90.32 o 2 23 0 1211.49 1251.52 65.32 o 3 23 0 3056.68 3040.91 101.72 o 4 23 0 386.99 397.56 37.33 o 5 23 0 1594.69 1701.50 133.17 o 6 23 0 110.70 140.20 31.48 o 7 23 0 1471.67 1547.57 147.60 o 0 24 0 254.06 274.02 65.73 o 1 24 0 3.65 -0.78 11.56 o 2 24 0 133.80 119.12 20.60 o 3 24 0 166.60 189.10 33.57 o 4 24 0 72.63 77.33 20.30 o 5 24 0 478.11 475.02 31.49 o 6 24 0 100.55 77.82 35.67 o 1 25 0 423.80 399.99 22.51 o 2 25 0 602.53 724.63 37.13 o 3 25 0 1138.24 1151.53 54.54 o 4 25 0 64.34 27.88 19.92 o 5 25 0 324.78 441.59 56.04 o 6 25 0 0.02 16.16 64.29 o 0 26 0 261.97 364.31 49.97 o 1 26 0 41.91 27.48 25.01 o 2 26 0 584.90 583.98 57.75 o 3 26 0 7.19 4.61 13.85 o 4 26 0 585.49 609.79 38.92 o 5 26 0 86.43 91.94 36.50 o 1 27 0 476.47 500.96 60.89 o 2 27 0 48.42 5.46 21.34 o 3 27 0 416.29 427.17 33.12 o 4 27 0 60.08 67.16 28.04 o 0 28 0 55.83 29.52 38.73 o 1 28 0 155.47 201.18 25.25 o 2 28 0 12.87 35.83 27.89 o 3 28 0 107.04 180.86 25.93 o 1 29 0 145.34 121.86 35.10 o -11 0 1 73.93 65.81 31.10 o -9 0 1 2004.69 2062.59 166.82 o -7 0 1 1715.65 1730.28 46.25 o -5 0 1 131.28 74.78 5.15 o -3 0 1 289.21 255.78 10.49 o 1 0 1 175.68 106.80 29.97 o 3 0 1 774.41 861.56 33.03 o 5 0 1 1625.31 1608.27 40.95 o 7 0 1 5949.19 5774.84 251.12 o 9 0 1 1164.39 994.58 72.86 o 11 0 1 282.96 349.48 31.25 o -12 1 1 27.66 22.86 16.68 o -11 1 1 26.09 49.10 20.02 o -10 1 1 163.91 179.38 20.91 o -9 1 1 111.04 96.16 7.98 o -8 1 1 14.71 11.69 4.90 o -7 1 1 424.91 401.56 12.59 o -6 1 1 29.92 25.93 3.56 o -5 1 1 1940.49 2048.69 33.30 o -4 1 1 69.48 92.91 4.44 o -3 1 1 1312.50 1279.43 19.69 o -2 1 1 2233.01 2425.93 209.55 o 1 1 1 1362.99 1091.61 177.09 o 2 1 1 22143.48 21384.71 528.73 o 3 1 1 15950.36 16272.19 486.64 o 4 1 1 1382.13 1069.85 29.69 o 5 1 1 121.11 106.30 5.08 o 6 1 1 115.68 112.80 7.19 o 7 1 1 200.44 192.03 11.48 o 8 1 1 1054.99 959.18 43.66 o 9 1 1 791.11 765.64 122.76 o 10 1 1 435.35 568.78 40.03 o 11 1 1 60.50 41.88 19.99 o -12 2 1 36.36 100.08 32.83 o -11 2 1 65.50 105.68 20.70 o -10 2 1 944.49 1093.85 65.95 o -9 2 1 48.31 36.41 7.51 o -8 2 1 180.10 190.14 7.67 o -7 2 1 471.19 444.47 17.79 o -6 2 1 2398.39 2273.52 54.27 o -5 2 1 6147.59 6399.05 165.13 o -4 2 1 3276.44 3254.01 89.57 o -3 2 1 12837.45 13562.40 274.46 o -2 2 1 18527.20 18412.29 1050.52 o -1 2 1 37.93 40.61 7.03 o 1 2 1 2721.24 2536.63 111.89 o 2 2 1 5650.78 5629.64 98.58 o 3 2 1 843.68 781.58 15.86 o 4 2 1 8469.07 8237.03 294.27 o 5 2 1 4147.87 4479.97 94.52 o 6 2 1 1670.60 1684.45 41.16 o 7 2 1 330.67 343.07 15.33 o 8 2 1 401.52 408.79 18.34 o 9 2 1 291.34 263.50 33.73 o 10 2 1 857.93 1028.47 43.39 o 11 2 1 42.60 53.00 23.19 o -12 3 1 0.26 23.62 23.62 o -11 3 1 66.61 74.66 16.33 o -10 3 1 762.36 903.48 45.65 o -9 3 1 4249.18 4227.35 282.50 o -8 3 1 602.10 566.46 29.29 o -7 3 1 5516.31 5614.32 111.43 o -6 3 1 346.60 299.43 17.06 o -5 3 1 15988.81 15118.86 1617.99 o -4 3 1 21.68 15.96 12.26 o -3 3 1 13890.65 13017.58 545.06 o -2 3 1 1083.74 1061.12 29.14 o -1 3 1 24986.26 20593.98 12297.46 o 0 3 1 1477.09 1474.26 160.16 o 1 3 1 10620.48 10921.51 171.73 o 2 3 1 9927.56 10085.82 162.99 o 3 3 1 7898.94 7266.51 137.83 o 4 3 1 9.19 28.31 3.62 o 5 3 1 11.38 20.44 3.93 o 6 3 1 347.92 386.11 17.23 o 7 3 1 798.13 798.41 18.24 o 8 3 1 1932.35 1798.27 53.56 o 9 3 1 893.69 879.96 108.06 o 10 3 1 615.61 624.80 46.80 o 11 3 1 204.97 233.21 25.76 o -11 4 1 59.95 44.93 39.60 o -10 4 1 413.06 424.36 25.06 o -9 4 1 353.15 262.16 109.37 o -8 4 1 564.23 507.15 24.44 o -7 4 1 1.48 -3.91 5.98 o -6 4 1 1045.85 1074.61 33.54 o -5 4 1 2.87 5.72 4.39 o -4 4 1 23.65 38.42 8.36 o -3 4 1 1.93 -5.78 12.73 o -2 4 1 3.07 5.53 3.71 o -1 4 1 142.68 137.56 5.42 o 0 4 1 2209.95 2268.40 31.59 o 1 4 1 3610.47 3982.54 72.49 o 2 4 1 19.28 24.68 2.93 o 3 4 1 2819.09 2804.84 44.24 o 4 4 1 0.40 6.80 3.29 o 5 4 1 519.63 549.50 11.39 o 6 4 1 7.01 8.22 6.13 o 7 4 1 30.02 28.14 4.76 o 8 4 1 418.11 433.65 29.74 o 9 4 1 0.57 6.16 12.89 o 10 4 1 77.13 102.81 25.56 o 11 4 1 0.54 2.38 29.09 o -11 5 1 1171.94 1333.11 77.90 o -10 5 1 5.57 64.51 32.26 o -9 5 1 206.05 226.89 15.83 o -8 5 1 93.18 114.09 14.17 o -7 5 1 2595.34 2815.16 50.44 o -6 5 1 280.27 290.77 7.00 o -5 5 1 4205.81 4144.69 70.62 o -4 5 1 2099.38 2276.12 45.59 o -3 5 1 4026.79 3899.56 84.47 o -2 5 1 1381.43 1469.54 31.03 o -1 5 1 12.02 13.52 2.02 o 0 5 1 28452.13 27944.96 595.63 o 1 5 1 430.34 410.68 11.43 o 2 5 1 11280.87 11921.93 198.84 o 3 5 1 2099.99 2029.65 33.07 o 4 5 1 86.89 87.93 4.61 o 5 5 1 3912.62 3805.07 72.92 o 6 5 1 35.48 27.78 4.74 o 7 5 1 2166.17 2224.56 60.06 o 8 5 1 48.58 47.96 7.38 o 9 5 1 843.19 897.61 69.29 o 10 5 1 306.89 270.97 30.60 o 11 5 1 631.61 618.55 30.48 o -11 6 1 2.87 -17.86 43.05 o -10 6 1 1963.43 2308.04 226.36 o -9 6 1 40.64 33.16 9.19 o -8 6 1 3117.20 3057.53 96.45 o -7 6 1 1215.52 1390.02 34.50 o -6 6 1 9038.91 9396.10 198.30 o -5 6 1 228.54 196.48 12.82 o -4 6 1 8205.88 7650.81 144.32 o -3 6 1 322.82 365.50 10.61 o -2 6 1 14600.02 13333.84 260.48 o -1 6 1 337.35 322.77 7.26 o 1 6 1 2419.52 2278.34 34.42 o 2 6 1 13862.06 13360.00 219.95 o 3 6 1 379.42 423.03 9.49 o 4 6 1 6340.03 5884.75 214.10 o 5 6 1 114.40 120.53 7.49 o 6 6 1 6155.45 6134.28 356.28 o 7 6 1 723.04 656.67 54.93 o 8 6 1 2333.11 2035.49 129.41 o 9 6 1 8.04 7.76 21.32 o 10 6 1 859.70 891.54 70.49 o 11 6 1 265.06 338.97 58.89 o -11 7 1 443.95 391.67 60.91 o -10 7 1 19.02 17.86 33.98 o -9 7 1 643.30 636.33 50.60 o -8 7 1 228.34 201.32 21.45 o -7 7 1 811.68 823.78 31.37 o -6 7 1 97.75 103.03 14.51 o -5 7 1 89.35 120.94 8.84 o -4 7 1 2005.76 2044.52 48.84 o -3 7 1 397.11 341.01 10.35 o -2 7 1 217.49 217.99 19.82 o -1 7 1 756.94 850.92 19.96 o 0 7 1 2928.16 3044.86 44.68 o 1 7 1 8265.41 8079.61 112.31 o 2 7 1 14.65 28.81 5.37 o 3 7 1 12.29 7.19 2.87 o 4 7 1 1060.13 1139.13 56.33 o 5 7 1 374.85 349.72 12.42 o 6 7 1 74.87 62.12 9.17 o 7 7 1 67.82 32.60 23.17 o 8 7 1 97.90 62.68 23.79 o 9 7 1 795.77 749.52 69.51 o 10 7 1 93.93 45.87 50.61 o 11 7 1 366.59 427.09 55.29 o -11 8 1 0.80 -3.60 33.98 o -10 8 1 793.85 832.79 79.49 o -9 8 1 523.21 362.19 23.50 o -8 8 1 2006.62 2011.94 72.61 o -7 8 1 62.81 54.28 15.71 o -6 8 1 9190.15 9567.10 205.29 o -5 8 1 381.96 365.43 16.83 o -4 8 1 8182.67 8392.23 193.21 o -3 8 1 320.70 324.64 7.89 o -2 8 1 281.85 226.63 9.69 o -1 8 1 2445.49 2639.35 38.74 o 0 8 1 1453.10 1471.79 26.95 o 1 8 1 1130.08 1193.01 18.56 o 2 8 1 1579.14 1548.64 26.91 o 3 8 1 278.38 278.69 7.07 o 4 8 1 191.63 119.52 5.88 o 5 8 1 56.97 39.02 13.03 o 6 8 1 7191.92 6872.28 462.87 o 7 8 1 522.43 507.61 21.81 o 8 8 1 3701.48 3410.88 208.20 o 9 8 1 227.61 175.78 17.02 o 10 8 1 1258.82 1181.92 242.27 o 11 8 1 69.79 147.31 47.95 o -11 9 1 221.32 153.50 53.57 o -10 9 1 123.43 148.31 23.34 o -9 9 1 545.37 436.04 34.65 o -8 9 1 82.69 74.55 15.01 o -7 9 1 4642.15 4555.20 298.43 o -6 9 1 54.33 41.95 12.28 o -5 9 1 5045.87 4869.16 106.19 o -4 9 1 126.11 94.56 9.47 o -3 9 1 4009.81 3668.74 72.21 o -2 9 1 1654.86 1592.52 25.74 o -1 9 1 4166.11 3735.31 53.40 o 0 9 1 3133.49 3402.23 48.18 o 1 9 1 32553.98 31625.03 541.49 o 2 9 1 2652.69 2616.77 46.67 o 3 9 1 3882.63 3733.98 58.29 o 4 9 1 3504.20 2973.66 417.28 o 5 9 1 4272.44 4195.20 267.05 o 6 9 1 480.77 443.48 10.58 o 7 9 1 4590.47 4835.19 149.57 o 8 9 1 198.79 172.05 24.84 o 9 9 1 845.28 592.82 116.42 o 10 9 1 79.95 77.68 18.50 o 11 9 1 24.68 56.73 23.04 o -11 10 1 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