#------------------------------------------------------------------------------
#$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $
#$Revision: 26025 $
#$URL: file:///home/coder/svn-repositories/cod/hkl/2/2013955.hkl $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2013955_Fobs
loop_
_publ_author_name
'Okabe, Nobuo'
'Hagihara, Kana'
'Odoko, Mamiko'
'Muranishi, Yasunori'
_publ_section_title
;
 (2,2'-Bipyridine-\k^2^<i>N</i>,<i>N</i>')(2,3-naphthalenediolato-\k^2^<i>O</i>,<i>O</i>')palladium(II)
 and
 (2,2'-biquinoline-\k^2^<i>N</i>,<i>N</i>')(2,3-naphthalenediolato-\k^2^<i>O</i>,<i>O</i>')palladium(II)
;
_journal_issue                   4
_journal_name_full               'Acta Crystallographica Section C'
_journal_page_first              m150
_journal_page_last               m152
_journal_volume                  60
_journal_year                    2004
_space_group_IT_number           14
_symmetry_space_group_name_Hall  '-P 2ybc'
_symmetry_space_group_name_H-M   'P 1 21/c 1'
_[local]_cod_data_source_file    fg1730Isup2.hkl
_[local]_cod_data_source_block   I
loop_
_refln_index_h
_refln_index_k
_refln_index_l
_refln_F_squared_meas
_refln_F_squared_sigma
_refln_F_squared_calc
_refln_observed_status
0 0 2 29344.47 1925.17 42949.20 o
1 0 -2 44743.75 3606.40 85404.61 o
0 1 1 601.56 32.11 645.84 o
1 1 0 596.15 28.84 545.71 o
1 1 -1 1735.48 87.10 1725.81 o
1 1 1 169.60 9.13 153.37 o
1 0 2 6156.68 304.03 5967.64 o
2 0 0 8982.00 459.36 9215.32 o
0 1 2 11810.44 608.39 12275.03 o
1 1 -2 475.43 24.96 484.27 o
2 0 -2 5182.81 256.06 5008.12 o
2 1 -1 4731.02 235.02 4659.47 o
1 1 2 67.31 4.87 21.01 o
2 1 0 1255.72 57.70 1071.28 o
2 1 -2 6242.21 307.25 6068.92 o
1 1 -3 4890.29 234.62 4565.57 o
0 1 3 1159.95 57.70 1120.76 o
2 1 1 5486.51 268.95 5296.23 o
1 0 -4 12147.67 604.96 11970.50 o
0 2 0 1991.71 111.44 2318.53 o
2 1 -3 1302.02 63.70 1223.44 o
2 0 2 3659.91 183.26 3638.09 o
0 0 4 22273.47 1159.98 23560.53 o
0 2 1 22.58 2.28 20.52 o
3 0 -2 25261.97 1303.80 26374.86 o
2 0 -4 7038.01 350.07 6950.83 o
1 2 0 9168.39 481.96 9766.25 o
1 2 -1 -2.03 4.83 1.08 o
1 1 3 1848.98 92.81 1825.98 o
3 0 0 7992.51 406.69 8090.22 o
1 1 -4 8442.14 416.26 8233.99 o
1 2 1 19235.46 985.16 19823.59 o
0 2 2 11040.82 582.05 11830.44 o
2 1 2 10992.74 561.65 11237.93 o
1 2 -2 22568.74 1245.14 25958.65 o
3 1 -1 1596.20 77.96 1501.23 o
0 1 4 978.59 50.04 972.76 o
3 1 -2 3678.14 185.80 3698.91 o
2 1 -4 6197.09 304.61 6003.22 o
3 1 0 668.23 33.87 635.30 o
1 0 4 13347.09 676.59 13502.20 o
2 2 -1 3381.31 171.09 3404.41 o
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3 0 -4 22325.83 1102.97 21789.94 o
1 2 2 58610.88 3674.61 80596.79 o
2 2 0 59685.80 3818.50 84371.75 o
2 2 -2 15901.51 856.90 17629.74 o
1 2 -3 99.19 8.49 115.46 o
0 2 3 4.39 5.34 12.69 o
3 1 1 83.91 7.92 105.24 o
1 1 4 4510.53 226.81 4511.20 o
2 2 1 38404.82 2108.48 43636.06 o
2 1 3 77.47 6.98 79.62 o
1 1 -5 312.65 17.27 298.86 o
2 2 -3 36.23 3.75 40.22 o
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3 0 2 12213.09 613.90 12170.13 o
2 1 -5 3871.35 177.66 3347.84 o
4 0 -2 12837.32 644.39 12764.98 o
1 2 3 10710.66 525.46 10368.29 o
0 1 5 23.59 2.87 24.38 o
1 2 -4 6829.01 350.60 7062.83 o
2 2 2 22435.76 1189.05 24313.71 o
3 1 2 31.35 3.49 46.91 o
3 2 -1 147.20 10.75 158.53 o
2 0 4 9203.72 461.39 9198.75 o
4 0 0 16386.13 822.65 16332.72 o
0 2 4 10020.03 518.82 10514.52 o
3 2 -2 11152.37 580.34 11792.27 o
4 1 -2 5082.94 246.68 4812.99 o
2 2 -4 9066.08 456.47 9117.23 o
4 1 -1 445.46 22.94 400.80 o
3 2 0 10380.03 542.54 11044.23 o
1 0 -6 3477.26 165.16 3168.70 o
4 0 -4 12750.65 641.84 12716.63 o
3 1 -5 10.16 2.61 8.29 o
2 0 -6 2.11 5.77 31.80 o
4 1 -3 61.62 5.19 50.61 o
3 2 -3 371.53 20.58 365.98 o
2 1 4 4752.78 239.59 4767.09 o
4 1 0 153.20 9.73 127.37 o
0 3 1 178.85 12.93 237.27 o
1 1 5 76.19 7.11 48.80 o
1 3 0 34.02 3.57 26.54 o
1 3 -1 485.15 27.83 535.11 o
0 0 6 1820.36 93.63 1850.56 o
3 2 1 520.85 27.29 497.13 o
1 1 -6 14526.80 708.12 13933.60 o
4 1 -4 2800.50 142.56 2826.92 o
1 2 4 12971.02 670.27 13579.42 o
2 1 -6 5581.07 282.87 5648.49 o
2 2 3 182.10 12.52 201.12 o
3 0 -6 1634.98 84.50 1666.11 o
1 2 -5 290.78 16.96 289.25 o
1 3 1 5966.22 291.40 5711.10 o
3 2 -4 5726.21 299.02 6060.44 o
0 3 2 1315.26 68.98 1363.43 o
1 3 -2 774.90 41.27 793.58 o
3 1 3 563.04 27.97 494.94 o
2 2 -5 1457.41 71.16 1350.63 o
4 1 1 424.22 21.71 371.43 o
0 1 6 14571.84 736.83 14772.61 o
0 2 5 169.14 10.23 125.01 o
2 3 -1 1098.86 55.83 1067.32 o
3 1 -6 8771.71 439.04 8734.83 o
1 3 2 201.24 13.18 212.86 o
2 3 0 69.65 7.46 57.77 o
4 1 -5 233.66 13.56 193.56 o
3 2 2 3068.00 167.71 3450.72 o
2 3 -2 1452.35 77.04 1531.02 o
1 3 -3 749.97 39.24 740.40 o
4 0 2 2843.17 145.00 2877.43 o
0 3 3 228.64 13.99 228.52 o
4 2 -2 18754.96 952.65 19151.78 o
1 0 6 8248.09 403.17 7920.58 o
4 2 -1 2104.06 97.79 1820.62 o
5 0 -2 11339.91 573.67 11489.13 o
3 2 -5 1271.45 64.03 1225.56 o
3 0 4 4522.78 227.24 4504.69 o
4 2 -3 868.53 44.59 837.85 o
2 3 1 898.97 49.24 970.54 o
2 3 -3 380.66 21.97 394.80 o
2 1 5 2696.71 127.30 2412.70 o
4 0 -6 6549.84 318.33 6218.86 o
4 1 2 725.85 41.33 820.54 o
2 2 4 10132.56 514.33 10313.68 o
4 2 0 13038.67 668.32 13479.19 o
1 2 5 8.72 6.56 5.60 o
5 0 -4 17543.24 853.09 16765.98 o
1 1 6 12499.11 621.35 12339.15 o
5 1 -2 319.64 19.56 341.42 o
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1 2 -6 5244.69 256.09 5005.19 o
4 2 -4 7464.78 377.49 7537.55 o
5 1 -3 92.41 8.82 68.78 o
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3 1 4 7818.33 388.85 7703.72 o
2 2 -6 5125.11 256.19 5067.77 o
1 3 -4 3297.53 172.11 3460.81 o
5 0 0 12702.56 620.09 12196.27 o
1 1 -7 342.81 19.74 313.22 o
5 1 -1 742.08 38.86 723.64 o
2 3 2 1259.99 64.42 1243.14 o
4 1 -6 1447.04 78.82 1582.63 o
3 2 3 6.55 4.41 6.24 o
3 3 -1 306.00 20.03 365.02 o
0 3 4 9884.07 495.75 9877.12 o
3 3 -2 33.80 3.51 13.11 o
5 1 -4 3970.90 193.60 3762.10 o
2 3 -4 3792.38 195.99 3926.71 o
4 2 1 9.33 2.80 4.63 o
0 2 6 2440.08 121.61 2370.81 o
3 3 0 381.55 20.37 335.45 o
3 1 -7 395.07 20.94 340.63 o
3 3 -3 916.22 47.18 886.22 o
5 1 0 87.67 8.20 68.44 o
3 2 -6 7676.83 368.87 7167.01 o
0 1 -7 -54.31 16.83 187.83 o
4 2 -5 4631.04 217.49 4144.98 o
2 0 6 9381.57 454.84 8896.75 o
4 1 3 34.84 3.79 30.93 o
5 1 -5 302.53 18.02 280.95 o
3 3 1 2941.08 153.62 3080.36 o
1 3 4 19968.76 1006.52 20156.16 o
2 3 3 277.08 17.86 315.78 o
1 3 -5 1248.70 62.11 1170.05 o
3 3 -4 6540.52 322.60 6345.69 o
2 2 5 114.97 10.88 155.89 o
4 2 2 4574.52 237.15 4769.44 o
2 0 -8 6361.43 287.61 5380.81 o
5 0 -6 10759.04 522.61 10235.77 o
2 3 -5 1700.13 84.52 1616.56 o
5 1 1 4.41 6.60 2.36 o
2 1 6 23382.55 1159.97 23050.38 o
1 2 6 5337.25 260.35 5080.89 o
5 2 -2 24338.73 1209.65 24059.78 o
4 1 -7 6335.91 280.86 5187.54 o
0 3 5 6670.03 320.70 6223.32 o
1 0 -8 368.11 21.37 365.32 o
5 2 -3 4328.97 196.80 3668.18 o
2 2 -7 1186.85 56.45 1021.13 o
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3 1 5 957.75 47.07 852.77 o
1 2 -7 -9.70 7.25 3.64 o
3 0 -8 24.28 3.19 2.92 o
5 2 -1 2.71 7.70 6.60 o
0 4 0 7186.16 370.58 7463.43 o
4 2 -6 5516.11 277.26 5495.50 o
3 3 2 581.60 32.88 616.53 o
0 4 1 260.39 16.14 262.19 o
1 1 7 1907.62 87.62 1594.84 o
2 1 -8 8623.94 432.13 8589.94 o
5 1 -6 10615.47 516.24 10114.06 o
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5 2 -4 22415.49 1112.09 22091.85 o
4 3 -2 260.45 15.51 224.90 o
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1 4 -1 123.78 10.00 107.10 o
4 3 -1 1757.16 91.24 1790.66 o
1 1 -8 18896.71 917.68 18019.40 o
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3 3 -5 309.68 19.12 319.47 o
4 3 -3 921.98 47.24 872.08 o
6 0 -2 31097.02 1541.59 30636.21 o
5 2 0 7025.68 365.66 7395.73 o
3 1 -8 4562.69 230.64 4572.13 o
1 4 1 4.65 6.54 0.11 o
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0 2 7 407.43 22.90 393.67 o
0 4 2 3925.01 208.04 4218.85 o
1 4 -2 7471.72 385.51 7766.07 o
6 0 -4 16161.51 788.97 15522.21 o
2 3 4 339.00 22.44 421.35 o
4 3 0 601.23 30.53 526.53 o
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1 3 5 3255.18 155.22 2959.67 o
4 2 3 226.99 13.74 195.70 o
5 2 -5 1620.03 77.74 1442.68 o
4 0 -8 424.62 24.69 437.72 o
6 1 -3 98.52 10.39 80.90 o
1 3 -6 9313.90 462.33 9148.47 o
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1 4 -3 84.62 9.27 77.73 o
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2 7 -7 94.87 10.30 98.26 o
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1 2 -15 36.26 8.84 76.28 o
1 7 -7 303.48 23.52 312.11 o
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1 5 -12 1611.00 86.70 1624.67 o
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11 3 -7 10.32 14.38 0.35 o
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1 8 -3 174.00 14.77 180.46 o
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1 5 -13 215.28 22.39 227.41 o
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1 7 -9 -11.72 14.24 1.29 o
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10 2 4 830.35 49.44 847.33 o
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11 2 -11 85.06 9.29 84.80 o
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1 8 -5 360.96 26.95 358.53 o
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4 1 -17 10.59 16.63 29.19 o
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10 3 3 27.68 6.91 34.53 o
2 1 15 509.13 35.81 513.50 o
4 3 -16 305.00 23.92 268.81 o
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10 0 -14 876.10 51.67 883.74 o
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10 5 -4 619.18 40.38 661.50 o
10 5 -5 399.95 30.61 429.19 o
12 2 -7 19.08 16.62 26.36 o
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4 8 -2 764.34 47.25 794.86 o
11 3 0 166.91 15.00 167.80 o
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3 8 -5 262.28 21.98 258.81 o
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11 3 -10 2166.94 119.40 2299.11 o
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3 5 -14 1596.28 87.40 1612.21 o
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11 4 -6 941.33 58.33 1062.39 o
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1 8 5 836.53 48.42 813.16 o
12 2 -8 472.92 34.18 515.92 o
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1 8 -6 344.97 26.10 331.12 o
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10 5 -2 4.39 16.85 17.96 o
1 4 -15 231.93 26.27 307.32 o
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10 5 -7 252.34 24.52 289.95 o
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1 3 15 6.80 16.35 23.18 o
11 4 -7 169.08 14.99 159.43 o
3 7 -10 818.00 47.69 779.78 o
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1 7 9 -16.33 14.56 6.06 o
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5 5 -14 327.58 26.74 352.45 o
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1 1 16 1246.63 69.50 1240.85 o
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12 2 -2 2439.83 133.94 2597.25 o
1 5 13 274.65 24.22 280.26 o
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11 1 3 66.15 7.85 64.91 o
1 7 -10 1175.85 67.21 1210.85 o
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4 0 14 495.39 34.60 539.57 o
8 6 2 684.48 43.86 733.39 o
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1 3 -16 676.83 43.05 700.82 o
3 8 -6 221.30 22.07 246.63 o
12 2 -9 159.45 16.26 188.58 o
4 4 12 585.13 38.59 602.41 o
4 8 -5 264.11 23.32 255.86 o
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10 2 5 192.25 20.28 191.49 o
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11 4 -2 1631.10 91.27 1711.22 o
6 7 3 442.31 31.06 444.69 o
7 7 0 24.41 6.81 23.80 o
5 4 11 497.48 32.87 460.75 o
11 1 -13 27.13 7.65 24.82 o
12 0 0 1119.55 65.15 1148.47 o
4 7 -10 1417.65 79.00 1437.88 o
11 3 1 130.67 11.86 132.36 o
8 3 8 1480.67 84.03 1573.59 o
10 2 -14 700.28 44.79 739.28 o
0 6 12 102.16 10.79 104.48 o
1 5 -14 1203.38 66.23 1148.80 o
10 3 4 563.64 34.99 518.39 o
11 4 -8 364.10 26.65 328.45 o
3 6 10 103.45 10.24 108.24 o
4 6 9 789.94 47.83 804.03 o
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10 5 -1 546.07 37.12 575.07 o
1 1 -17 71.66 9.22 82.33 o
5 1 13 25.63 7.12 39.10 o
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1 3 16 155.96 14.57 147.89 o
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1 1 17 45.26 9.45 74.17 o
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12 3 0 55.10 8.03 50.77 o
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1 8 8 15.18 16.23 0.10 o
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1 1 -18 27.15 7.54 29.01 o
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3 8 -9 811.25 49.39 805.68 o
8 7 -8 939.30 56.16 958.54 o
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1 7 -12 954.55 57.97 1000.02 o
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1 6 -14 491.26 35.78 517.22 o
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3 9 -3 724.06 46.53 761.49 o
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12 2 -13 94.31 10.44 91.73 o
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10 5 3 163.43 16.14 169.95 o
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11 3 -14 812.97 49.81 821.23 o
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10 7 -12 335.02 35.73 332.21 o
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13 5 -11 37.10 26.88 0.10 o
1 3 19 26.86 20.34 24.29 o
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10 8 -5 96.67 13.47 106.63 o
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14 2 -14 279.55 26.19 261.49 o
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2 1 -21 14.41 19.93 27.42 o
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5 9 6 191.74 19.12 175.50 o
7 9 2 4.88 26.85 28.63 o
8 9 -3 647.59 46.24 555.67 o
10 4 9 153.98 15.91 149.04 o
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11 4 -17 102.42 13.53 98.54 o
10 8 -3 16.55 26.51 32.88 o
3 8 -14 429.48 33.10 428.32 o
10 8 -6 83.53 12.93 80.14 o
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1 9 -11 29.31 8.62 20.03 o
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9 8 2 240.39 23.95 215.74 o
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5 1 17 -9.61 26.87 15.32 o
8 9 -2 11.85 26.84 7.61 o
8 5 11 4.07 26.04 6.90 o
12 4 5 108.20 13.87 99.99 o
4 5 -19 221.13 23.07 210.93 o
0 5 18 3.46 18.89 9.49 o
1 3 -20 0.79 17.41 0.03 o
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5 5 -19 172.06 18.10 160.61 o
8 1 -21 28.90 24.89 4.89 o
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10 3 -19 123.26 14.40 113.76 o
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12 2 7 26.92 25.05 0.49 o
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14 4 -2 579.87 45.55 573.18 o
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1 10 6 17.18 19.31 26.01 o
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12 3 -17 -26.15 25.81 7.61 o
2 8 -14 29.43 9.03 35.15 o
9 6 -16 365.61 39.11 365.99 o
5 4 -20 479.19 37.98 382.97 o
2 7 -16 189.61 19.96 229.49 o
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14 3 -13 151.63 15.73 101.84 o
5 10 -3 61.89 12.72 59.72 o
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4 4 -20 695.76 49.04 668.91 o
2 10 -7 198.25 18.72 190.61 o
3 10 4 92.76 12.86 93.93 o
11 7 -10 455.61 38.84 386.00 o
4 0 18 971.19 61.60 919.96 o
6 9 -10 533.50 46.22 570.37 o
10 8 -2 343.48 37.18 361.12 o
1 10 -7 518.14 37.37 510.99 o
10 8 -7 248.40 25.27 252.79 o
14 1 -15 3.95 29.62 33.45 o
1 0 20 829.15 54.14 887.24 o
7 6 11 121.60 13.39 118.32 o
8 3 13 26.21 18.29 35.87 o
13 4 -14 210.66 22.48 184.14 o
5 10 -1 -13.50 26.18 2.19 o
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9 6 8 28.35 11.63 37.91 o
4 10 -6 24.83 25.49 10.63 o
8 9 -6 182.58 19.49 150.41 o
13 5 0 -49.51 25.91 4.92 o
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3 5 -19 46.73 8.34 43.82 o
5 10 -4 132.87 14.49 126.62 o
8 9 -1 837.16 51.70 648.95 o
5 8 -14 229.63 24.19 165.65 o
13 1 -17 -5.68 30.12 15.43 o
8 8 -12 2.68 27.28 0.71 o
15 1 -12 552.97 44.34 560.30 o
6 4 -20 619.27 44.73 548.80 o
6 5 -19 182.67 19.72 198.62 o
14 4 -11 163.65 17.36 164.76 o
7 8 -13 471.49 40.60 421.56 o
12 4 -16 395.53 37.33 363.36 o
1 8 13 262.13 25.01 228.00 o
3 10 -7 290.59 26.54 258.62 o
11 2 -19 -53.68 30.05 0.78 o
10 5 8 362.21 37.08 368.57 o
11 5 6 536.13 44.61 526.15 o
7 9 -9 37.80 26.49 7.06 o
4 1 18 35.73 24.59 9.85 o
6 7 -16 136.79 14.32 117.14 o
14 2 2 756.61 51.75 652.04 o
5 10 0 177.99 17.70 128.91 o
9 7 -14 249.75 25.54 253.03 o
13 3 4 501.05 42.27 457.89 o
15 2 -11 15.14 26.58 22.70 o
1 1 20 4.55 18.08 11.36 o
3 3 18 69.21 10.04 85.64 o
3 4 -20 806.55 51.51 802.34 o
10 5 -17 116.58 13.71 108.76 o
5 9 -11 -2.30 27.79 0.29 o
12 2 -18 846.37 57.33 840.46 o
0 6 17 3.88 19.24 14.86 o
0 10 7 479.14 36.78 472.29 o
2 4 18 217.80 19.66 226.83 o
8 1 14 603.04 47.91 610.70 o
15 3 -7 194.63 19.83 169.73 o
1 7 15 296.66 27.94 268.14 o
9 4 -19 -27.50 29.49 2.03 o
15 3 -6 284.23 28.43 340.24 o
11 6 4 247.05 25.20 238.93 o
0 9 11 42.40 8.97 42.02 o
8 8 5 136.65 14.36 113.40 o
9 7 6 295.60 25.94 290.85 o
13 5 -12 711.40 49.31 638.46 o
8 7 -15 188.60 20.37 181.63 o
6 9 5 328.74 34.23 249.19 o
13 2 5 -0.97 26.75 16.59 o
1 8 -14 61.55 9.91 66.58 o
4 6 -18 475.38 42.84 516.84 o
12 6 1 202.10 20.47 205.37 o
15 3 -8 370.70 31.15 403.64 o
10 8 -1 -24.65 27.35 7.07 o
4 10 3 128.82 13.26 102.23 o
10 8 -8 38.62 12.21 15.99 o
8 6 -17 165.45 18.34 165.16 o
2 2 -21 4.21 25.16 73.21 o
5 10 -5 295.72 26.35 255.66 o
11 5 -16 65.73 12.86 82.75 o
3 9 9 -10.52 17.90 0.08 o
7 9 3 374.21 34.47 298.19 o
8 9 -7 300.10 27.38 275.10 o
9 4 11 37.10 26.37 43.45 o
5 6 -18 526.17 42.37 481.05 o
14 3 1 93.11 13.68 98.96 o
6 2 16 498.92 41.93 474.40 o
15 1 -1 -44.02 30.29 36.94 o
15 3 -5 114.12 13.64 95.73 o
11 6 -14 236.81 24.24 221.19 o
1 7 -16 174.92 18.77 170.39 o
2 6 16 227.16 20.62 278.91 o
4 9 8 240.19 23.55 220.91 o
15 2 -2 351.65 39.08 408.18 o
8 9 0 10.63 28.00 17.06 o
1 1 -21 29.03 19.66 38.27 o
7 8 7 146.44 15.88 146.52 o
14 4 -1 6.02 26.29 6.03 o
3 6 -18 397.64 30.75 370.72 o
13 6 -6 248.04 24.07 230.60 o
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2 5 -19 142.31 14.97 164.94 o
12 6 -12 14.75 26.92 5.43 o
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13 6 -5 -10.27 27.39 20.89 o
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5 10 1 30.34 25.82 26.54 o
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8 7 8 184.52 18.73 194.35 o
9 3 -20 -41.11 27.21 1.23 o
9 8 -11 384.09 37.90 346.69 o
10 2 -20 773.25 52.85 753.31 o
15 3 -9 13.83 29.20 30.10 o
7 4 -20 964.57 63.12 946.97 o
8 2 -21 -18.66 28.65 11.83 o
9 5 -18 184.98 20.50 174.75 o
10 7 4 255.67 23.42 207.19 o
2 9 10 225.38 18.79 202.95 o
13 6 -7 59.28 11.97 48.13 o
2 10 6 168.64 18.23 185.07 o
10 7 -13 -3.30 26.25 5.00 o
14 1 3 -25.08 28.51 3.39 o