#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/39/2013997.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2013997_Fobs loop_ _publ_author_name 'Perry, Christopher B.' 'Fernandes, Manuel A.' 'Marques, Helder M.' _publ_section_title ; Isoamylcobalamin--acetone--water (1/0.385/12.650) ; _journal_issue 4 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first m165 _journal_page_last m167 _journal_volume 60 _journal_year 2004 _space_group_IT_number 19 _symmetry_space_group_name_Hall 'P 2ac 2ab' _symmetry_space_group_name_H-M 'P 21 21 21' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 15.9588 _cell_length_b 20.7928 _cell_length_c 24.4030 _exptl_crystal_F_000 3539.15 _reflns_d_resolution_high 0.7965 _[local]_cod_data_source_file gd1306Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 3mcpisos in P2(1)2(1)2(1)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 410.55 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 22227.50 20539.62 325.59 o 4 0 0 43593.33 41080.68 630.83 o 6 0 0 4366.62 3787.86 98.84 o 8 0 0 60145.48 60421.14 933.16 o 10 0 0 9799.57 10008.97 152.07 o 12 0 0 10536.25 10822.70 199.86 o 14 0 0 4151.58 4422.09 125.73 o 16 0 0 196.84 53.78 77.04 o 18 0 0 21.78 13.08 91.57 o 1 1 0 42998.94 41197.96 345.74 o 2 1 0 2578.13 2100.68 23.55 o 3 1 0 7.72 66.54 11.45 o 4 1 0 516.18 280.73 15.28 o 5 1 0 900.46 846.16 30.12 o 6 1 0 5258.83 5590.87 71.57 o 7 1 0 24656.69 25527.96 245.41 o 8 1 0 2008.97 2375.74 51.14 o 9 1 0 4718.62 4772.55 74.37 o 10 1 0 385.42 478.78 41.59 o 11 1 0 5289.55 5283.52 85.86 o 12 1 0 326.56 326.93 30.24 o 13 1 0 958.12 971.41 55.39 o 14 1 0 35.56 69.19 37.44 o 15 1 0 145.25 209.95 42.98 o 16 1 0 729.69 822.02 71.22 o 17 1 0 7.43 -5.54 59.04 o 18 1 0 1075.81 1001.77 87.75 o 19 1 0 404.94 360.47 110.47 o 20 1 0 3.73 -114.83 114.83 o 0 2 0 9675.55 11139.63 131.71 o 1 2 0 252.11 749.29 18.67 o 2 2 0 26395.29 26549.99 210.44 o 3 2 0 10792.52 10319.71 99.23 o 4 2 0 22996.02 22099.04 176.57 o 5 2 0 2738.02 3165.38 47.35 o 6 2 0 5076.49 5849.82 73.44 o 7 2 0 19161.47 16793.07 209.87 o 8 2 0 1947.57 1733.98 46.51 o 9 2 0 3636.62 3824.09 65.63 o 10 2 0 109.76 165.27 26.40 o 11 2 0 6450.04 5704.39 88.60 o 12 2 0 1297.12 1391.96 54.38 o 13 2 0 799.04 718.65 43.15 o 14 2 0 1622.23 1679.14 94.82 o 15 2 0 12.87 -31.01 39.44 o 16 2 0 173.98 155.63 56.50 o 17 2 0 1256.24 1152.26 89.89 o 18 2 0 241.81 219.48 95.93 o 19 2 0 577.08 582.86 117.73 o 1 3 0 121.61 138.24 8.02 o 2 3 0 104.44 259.76 11.97 o 3 3 0 4681.27 3228.28 65.04 o 4 3 0 4884.61 5165.38 51.42 o 5 3 0 3440.34 3732.27 43.71 o 6 3 0 256.43 421.52 22.60 o 7 3 0 102.42 173.70 31.69 o 8 3 0 1285.77 1190.99 45.70 o 9 3 0 518.05 518.65 32.37 o 10 3 0 1766.35 1930.81 53.31 o 11 3 0 274.96 254.42 30.48 o 12 3 0 40.71 162.46 34.00 o 13 3 0 782.62 841.42 67.17 o 14 3 0 21.40 0.85 61.05 o 15 3 0 731.48 674.42 50.42 o 16 3 0 3845.37 3979.96 95.46 o 17 3 0 13.05 49.42 85.76 o 18 3 0 379.67 376.46 106.11 o 19 3 0 123.63 116.28 109.01 o 0 4 0 7564.48 9818.52 115.11 o 1 4 0 13230.16 12079.97 98.65 o 2 4 0 1983.64 1193.49 27.71 o 3 4 0 1686.39 1639.45 26.34 o 4 4 0 2630.85 1931.69 23.45 o 5 4 0 510.68 713.06 21.22 o 6 4 0 6042.92 6310.09 64.71 o 7 4 0 8855.26 8958.13 87.14 o 8 4 0 17668.34 17011.32 173.82 o 9 4 0 3031.59 3201.93 59.69 o 10 4 0 7467.90 7227.15 123.06 o 11 4 0 12590.71 12538.17 145.79 o 12 4 0 66.18 37.70 47.24 o 13 4 0 304.05 309.49 46.98 o 14 4 0 2448.87 2319.91 98.11 o 15 4 0 4652.48 4332.62 90.79 o 16 4 0 15.11 -16.82 58.06 o 17 4 0 193.20 219.63 64.23 o 18 4 0 144.87 100.29 100.29 o 19 4 0 750.40 979.67 129.36 o 1 5 0 1907.72 3716.00 54.31 o 2 5 0 23248.32 22174.80 201.63 o 3 5 0 1763.08 1384.31 32.57 o 4 5 0 10997.39 11980.18 102.98 o 5 5 0 12238.34 11040.73 79.17 o 6 5 0 5898.36 5892.11 71.98 o 7 5 0 6569.16 6652.78 93.99 o 8 5 0 5338.75 5655.78 59.23 o 9 5 0 3350.81 3975.78 57.93 o 10 5 0 658.48 733.04 37.07 o 11 5 0 2569.31 2317.72 51.31 o 12 5 0 7.18 -35.49 35.49 o 13 5 0 2938.95 2788.79 71.99 o 14 5 0 412.43 363.68 43.06 o 15 5 0 17.10 69.00 53.42 o 16 5 0 4052.39 3750.07 167.15 o 17 5 0 237.05 196.22 65.78 o 18 5 0 1304.68 1382.29 149.71 o 19 5 0 218.52 196.22 110.47 o 0 6 0 24678.54 29278.16 319.64 o 1 6 0 284.28 367.94 16.36 o 2 6 0 4909.94 4828.17 59.55 o 3 6 0 2557.19 2840.57 45.95 o 4 6 0 4953.97 4476.18 49.86 o 5 6 0 4308.05 3946.95 74.50 o 6 6 0 164.87 390.60 17.10 o 7 6 0 6499.46 7017.11 59.64 o 8 6 0 421.20 451.45 20.39 o 9 6 0 3660.19 3596.26 55.52 o 10 6 0 1429.01 1253.87 49.29 o 11 6 0 562.50 539.86 67.59 o 12 6 0 7249.17 7576.11 139.13 o 13 6 0 7075.60 7100.16 197.68 o 14 6 0 6315.36 5587.20 147.53 o 15 6 0 689.62 656.44 66.86 o 16 6 0 47.32 161.34 85.76 o 17 6 0 3053.39 3207.91 171.51 o 18 6 0 1201.32 1496.23 202.77 o 19 6 0 220.47 344.48 113.37 o 1 7 0 1613.30 1567.03 29.25 o 2 7 0 1183.97 1353.01 35.19 o 3 7 0 20791.91 19937.27 263.94 o 4 7 0 1566.33 1832.46 41.50 o 5 7 0 6779.90 6422.43 66.82 o 6 7 0 124.45 146.73 21.61 o 7 7 0 8968.36 7772.90 71.51 o 8 7 0 4082.91 4289.60 46.16 o 9 7 0 150.69 124.76 17.12 o 10 7 0 6336.10 6500.41 70.14 o 11 7 0 20.57 0.57 25.82 o 12 7 0 5313.66 5457.65 117.52 o 13 7 0 1757.87 1819.48 83.23 o 14 7 0 535.48 467.88 58.93 o 15 7 0 112.63 129.62 54.98 o 16 7 0 30.33 34.88 88.66 o 17 7 0 41.12 7.27 94.48 o 18 7 0 279.32 351.75 109.01 o 19 7 0 32.62 5.81 113.37 o 0 8 0 122791.88 129350.92 1349.32 o 1 8 0 732.26 1170.52 34.41 o 2 8 0 8513.06 8363.59 79.08 o 3 8 0 631.97 530.89 28.56 o 4 8 0 1163.17 791.50 34.92 o 5 8 0 11135.49 10720.97 118.14 o 6 8 0 65.61 98.07 16.92 o 7 8 0 52.04 36.88 17.98 o 8 8 0 1118.73 1155.77 31.32 o 9 8 0 4346.47 4819.78 78.88 o 10 8 0 2040.83 1967.31 48.07 o 11 8 0 56.69 28.91 31.43 o 12 8 0 2371.13 2352.17 86.48 o 13 8 0 490.05 376.41 54.44 o 14 8 0 34.71 93.77 52.57 o 15 8 0 10.23 35.43 56.42 o 16 8 0 409.74 354.43 65.68 o 17 8 0 2.36 101.75 95.93 o 18 8 0 119.13 222.39 113.37 o 19 8 0 78.66 210.76 122.10 o 1 9 0 444.79 757.19 39.44 o 2 9 0 78.66 65.42 14.94 o 3 9 0 46.00 33.35 19.36 o 4 9 0 1538.61 1362.97 66.02 o 5 9 0 4586.84 5478.65 77.28 o 6 9 0 846.52 684.27 54.74 o 7 9 0 4204.28 3794.06 53.90 o 8 9 0 11.11 -20.30 20.30 o 9 9 0 2973.10 3165.08 67.20 o 10 9 0 6588.19 7277.03 104.09 o 11 9 0 6248.35 6093.33 96.79 o 12 9 0 387.88 318.08 52.30 o 13 9 0 508.25 738.59 118.46 o 14 9 0 223.14 279.98 57.90 o 15 9 0 351.66 302.38 64.08 o 16 9 0 2226.25 2575.57 119.19 o 17 9 0 1414.70 1251.48 146.80 o 18 9 0 3784.12 3982.63 203.49 o 0 10 0 8846.65 10114.19 156.98 o 1 10 0 11452.46 10984.26 101.18 o 2 10 0 6844.09 7444.39 75.99 o 3 10 0 4537.46 4628.17 76.78 o 4 10 0 13999.34 13164.63 163.80 o 5 10 0 78.59 72.66 23.27 o 6 10 0 1340.58 1387.57 61.88 o 7 10 0 8312.01 7273.59 98.79 o 8 10 0 37.41 47.35 27.54 o 9 10 0 4531.83 4261.55 81.16 o 10 10 0 13.64 -21.64 33.11 o 11 10 0 5982.49 5791.63 125.19 o 12 10 0 708.10 593.61 59.09 o 13 10 0 28.44 -4.88 51.90 o 14 10 0 1555.84 1689.11 91.20 o 15 10 0 839.38 914.10 76.52 o 16 10 0 2570.19 2755.46 183.14 o 17 10 0 1820.63 1752.94 156.98 o 18 10 0 146.70 255.82 116.28 o 1 11 0 7053.94 7262.92 89.67 o 2 11 0 104.62 105.19 17.97 o 3 11 0 7902.27 7621.53 96.14 o 4 11 0 4491.29 5094.28 76.43 o 5 11 0 1614.85 1238.25 46.63 o 6 11 0 7000.19 6878.58 94.79 o 7 11 0 511.89 601.34 41.52 o 8 11 0 126.82 88.44 29.88 o 9 11 0 4377.11 4031.44 78.00 o 10 11 0 10080.02 9892.26 130.46 o 11 11 0 847.59 789.57 76.31 o 12 11 0 2175.86 1981.23 87.36 o 13 11 0 152.70 195.60 57.53 o 14 11 0 596.31 511.09 67.81 o 15 11 0 543.33 573.15 96.66 o 16 11 0 144.27 162.34 71.43 o 17 11 0 84.57 90.12 109.01 o 0 12 0 3072.56 2658.33 64.68 o 1 12 0 8159.44 7968.27 137.21 o 2 12 0 15521.88 15114.69 134.67 o 3 12 0 6836.74 6708.99 90.82 o 4 12 0 20.15 16.01 39.06 o 5 12 0 26.68 70.65 27.09 o 6 12 0 6135.49 5843.90 93.37 o 7 12 0 8571.84 8478.25 112.93 o 8 12 0 1574.01 1310.54 73.88 o 9 12 0 32.19 101.07 60.11 o 10 12 0 4491.01 4088.99 83.72 o 11 12 0 1106.65 1118.98 84.30 o 12 12 0 406.76 450.41 59.04 o 13 12 0 985.29 1049.87 82.50 o 14 12 0 841.64 865.36 164.97 o 15 12 0 2645.87 2292.03 105.73 o 16 12 0 557.32 574.17 96.66 o 17 12 0 19.03 68.70 77.00 o 1 13 0 97.70 72.83 20.65 o 2 13 0 1566.74 1843.99 56.23 o 3 13 0 7.22 25.48 26.16 o 4 13 0 1363.57 1367.83 49.38 o 5 13 0 4292.43 4040.07 96.09 o 6 13 0 521.34 540.76 47.98 o 7 13 0 228.78 312.06 35.46 o 8 13 0 2166.28 1989.29 62.12 o 9 13 0 1991.53 1974.23 64.72 o 10 13 0 1809.49 1543.13 105.38 o 11 13 0 3.40 98.11 58.87 o 12 13 0 188.04 130.09 55.50 o 13 13 0 67.34 153.02 59.51 o 14 13 0 757.60 838.52 76.04 o 15 13 0 251.38 276.96 94.48 o 16 13 0 1888.98 1943.80 109.74 o 17 13 0 18.78 -5.81 113.37 o 0 14 0 4529.26 3791.65 138.81 o 1 14 0 123.96 74.16 22.72 o 2 14 0 5249.27 5175.73 82.35 o 3 14 0 137.02 155.19 30.27 o 4 14 0 1477.86 1356.69 87.92 o 5 14 0 11879.79 11442.27 138.63 o 6 14 0 3258.92 3299.43 72.82 o 7 14 0 2400.75 2280.57 66.24 o 8 14 0 4099.23 3790.34 80.29 o 9 14 0 180.72 54.82 37.88 o 10 14 0 417.12 309.02 58.48 o 11 14 0 134.55 16.04 54.44 o 12 14 0 1261.67 1096.96 83.23 o 13 14 0 4112.17 4255.46 164.97 o 14 14 0 9.49 10.91 66.78 o 15 14 0 1262.85 1394.64 101.61 o 16 14 0 331.46 407.22 81.67 o 1 15 0 1985.45 1774.79 53.86 o 2 15 0 132.27 139.37 31.80 o 3 15 0 412.77 444.70 48.29 o 4 15 0 70.40 45.72 31.19 o 5 15 0 1380.63 1319.77 57.03 o 6 15 0 850.55 793.59 50.85 o 7 15 0 6532.13 6608.38 105.15 o 8 15 0 6849.40 6307.16 103.72 o 9 15 0 2312.31 2298.20 72.23 o 10 15 0 217.05 225.60 57.90 o 11 15 0 1356.72 1242.95 84.56 o 12 15 0 558.15 620.63 69.37 o 13 15 0 156.98 169.84 66.71 o 14 15 0 160.23 94.29 73.40 o 15 15 0 1.61 182.93 76.04 o 16 15 0 8.48 -45.41 80.68 o 0 16 0 550.80 566.87 71.22 o 1 16 0 59.63 -10.80 31.48 o 2 16 0 1674.42 1367.80 55.16 o 3 16 0 831.95 802.44 49.50 o 4 16 0 1084.93 990.99 63.65 o 5 16 0 33.31 122.47 50.11 o 6 16 0 8020.09 7698.10 114.21 o 7 16 0 1329.22 1303.98 83.64 o 8 16 0 870.20 843.25 53.84 o 9 16 0 6261.77 6352.89 139.73 o 10 16 0 2053.71 2107.89 128.64 o 11 16 0 193.00 236.92 63.20 o 12 16 0 54.11 -35.40 62.12 o 13 16 0 664.96 642.02 74.94 o 14 16 0 899.60 936.75 85.78 o 15 16 0 25.67 122.10 77.00 o 1 17 0 5603.27 5200.92 127.91 o 2 17 0 783.19 669.88 45.85 o 3 17 0 660.63 596.32 42.08 o 4 17 0 14.63 -22.17 35.68 o 5 17 0 343.78 296.69 40.12 o 6 17 0 1197.04 1191.77 62.21 o 7 17 0 127.69 173.70 42.58 o 8 17 0 236.70 228.48 51.32 o 9 17 0 4.18 51.82 57.53 o 10 17 0 5608.68 5515.57 136.65 o 11 17 0 256.81 134.47 63.70 o 12 17 0 975.40 903.69 78.62 o 13 17 0 315.11 472.44 98.84 o 14 17 0 979.59 984.26 116.28 o 15 17 0 39.53 78.43 125.73 o 0 18 0 12.39 26.16 63.95 o 1 18 0 235.75 200.80 119.19 o 2 18 0 657.29 628.55 56.98 o 3 18 0 227.37 149.82 38.58 o 4 18 0 386.57 573.41 50.53 o 5 18 0 125.02 130.54 41.05 o 6 18 0 27.28 82.88 41.24 o 7 18 0 588.08 423.14 49.08 o 8 18 0 51.38 49.27 44.87 o 9 18 0 74.34 90.45 64.68 o 10 18 0 1921.17 1689.13 97.62 o 11 18 0 2533.10 2362.01 106.89 o 12 18 0 28.43 123.61 70.90 o 13 18 0 630.64 617.79 84.75 o 14 18 0 132.82 85.08 81.18 o 1 19 0 568.02 510.92 58.06 o 2 19 0 285.40 170.54 51.83 o 3 19 0 470.35 399.05 54.36 o 4 19 0 2390.26 2167.28 88.23 o 5 19 0 42.85 50.18 47.10 o 6 19 0 864.51 796.63 68.54 o 7 19 0 35.96 163.88 47.15 o 8 19 0 985.48 968.15 77.06 o 9 19 0 421.16 458.58 71.38 o 10 19 0 1931.63 2084.02 105.85 o 11 19 0 199.95 343.73 73.35 o 12 19 0 343.50 358.96 80.15 o 13 19 0 6.54 23.98 79.14 o 0 20 0 920.85 883.74 95.93 o 1 20 0 1174.79 833.26 67.27 o 2 20 0 345.14 291.95 56.42 o 3 20 0 2.30 -53.42 53.42 o 4 20 0 3.31 76.34 53.78 o 5 20 0 26.16 110.65 56.50 o 6 20 0 1.39 46.00 47.47 o 7 20 0 940.64 935.60 60.92 o 8 20 0 297.97 136.70 95.93 o 9 20 0 309.73 329.10 71.38 o 10 20 0 15.49 129.83 72.41 o 11 20 0 118.56 67.33 73.98 o 12 20 0 347.09 428.97 83.25 o 1 21 0 1646.20 1616.77 159.89 o 2 21 0 4502.02 3808.84 110.99 o 3 21 0 1500.38 1385.93 130.82 o 4 21 0 3174.52 3081.66 184.60 o 5 21 0 1749.51 1793.66 108.29 o 6 21 0 168.35 105.48 62.59 o 7 21 0 69.91 -77.04 93.02 o 8 21 0 986.02 983.56 81.67 o 9 21 0 1.29 -24.43 72.41 o 10 21 0 922.21 1076.19 89.40 o 11 21 0 590.41 540.14 85.31 o 0 22 0 964.96 803.79 104.65 o 1 22 0 74.48 17.38 61.15 o 2 22 0 1521.70 1463.05 89.40 o 3 22 0 103.27 37.97 69.04 o 4 22 0 3430.23 3289.91 110.87 o 5 22 0 90.78 150.36 65.21 o 6 22 0 1790.07 1810.68 101.23 o 7 22 0 51.48 -52.33 98.84 o 8 22 0 640.81 675.88 119.19 o 9 22 0 99.17 117.73 110.47 o 10 22 0 13.18 -76.81 79.12 o 1 23 0 1698.31 1516.26 93.51 o 2 23 0 13.80 -16.12 64.23 o 3 23 0 1452.35 1174.77 96.66 o 4 23 0 149.68 170.38 87.21 o 5 23 0 2768.32 2917.54 113.54 o 6 23 0 8.58 -53.78 100.29 o 7 23 0 24.70 -33.43 109.01 o 8 23 0 156.34 42.15 110.47 o 0 24 0 80.08 79.94 98.84 o 1 24 0 17.65 -17.10 75.58 o 2 24 0 1679.61 1747.20 112.65 o 3 24 0 99.50 18.36 72.45 o 4 24 0 3.52 -32.31 70.40 o 5 24 0 497.08 530.88 81.59 o 6 24 0 519.64 517.45 119.19 o 1 25 0 267.91 222.39 78.11 o 2 25 0 81.53 38.18 76.57 o 3 25 0 153.98 73.88 77.59 o 4 25 0 386.33 389.46 83.65 o 0 26 0 589.34 675.88 125.00 o 1 26 0 269.91 268.90 117.73 o 1 0 1 1877.74 2105.40 33.40 o 2 0 1 1798.35 2595.28 32.67 o 3 0 1 7.32 4.36 11.31 o 4 0 1 958.52 874.98 35.61 o 5 0 1 1779.75 1661.25 44.70 o 6 0 1 2092.02 2029.83 85.76 o 7 0 1 5634.93 6542.34 101.74 o 8 0 1 118.46 302.34 25.73 o 9 0 1 3816.51 3923.44 86.92 o 10 0 1 5687.46 5587.28 85.57 o 11 0 1 8380.83 8665.39 115.77 o 12 0 1 577.36 587.92 34.83 o 13 0 1 1056.60 1061.94 47.41 o 14 0 1 1939.48 1825.65 57.87 o 15 0 1 3697.62 4201.26 91.17 o 16 0 1 4.33 80.64 54.92 o 17 0 1 1636.79 1765.02 97.12 o 18 0 1 393.17 313.14 68.84 o 19 0 1 171.72 97.55 73.48 o -19 1 1 355.06 395.36 113.37 o -18 1 1 106.53 115.69 65.75 o -17 1 1 461.41 394.28 92.30 o -16 1 1 82.22 98.93 100.29 o -15 1 1 364.82 413.95 45.30 o -14 1 1 1390.98 1571.46 66.41 o -13 1 1 88.73 53.59 28.97 o -12 1 1 392.85 299.58 29.64 o -11 1 1 609.55 604.86 33.01 o -10 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4329.64 86.42 o 12 2 12 4870.88 4477.82 115.62 o 13 2 12 220.69 260.80 53.89 o 14 2 12 417.90 389.54 60.12 o 15 2 12 738.05 677.38 70.40 o 16 2 12 1573.05 1538.73 96.46 o 17 2 12 1159.27 1098.93 90.01 o 18 2 12 1326.27 1709.33 154.07 o -18 3 12 164.29 147.33 65.96 o -17 3 12 37.29 128.28 52.49 o -16 3 12 922.44 931.36 59.58 o -15 3 12 2666.37 2585.24 74.29 o -14 3 12 684.36 817.90 52.45 o -13 3 12 1044.81 993.72 55.20 o -12 3 12 2893.79 2853.07 68.57 o -11 3 12 1891.84 2113.58 60.80 o -10 3 12 804.51 727.71 40.58 o -9 3 12 508.39 492.44 42.17 o -8 3 12 1994.06 1835.09 52.99 o -7 3 12 4809.77 4649.40 59.78 o -6 3 12 2280.88 2412.47 43.25 o -5 3 12 9655.68 9631.00 99.87 o -4 3 12 1795.96 1696.91 40.20 o -3 3 12 8546.60 8877.73 92.02 o -2 3 12 1186.71 1120.57 35.88 o -1 3 12 13853.30 14735.09 133.89 o 0 3 12 12998.99 14550.87 132.14 o 1 3 12 12672.26 13417.74 112.51 o 2 3 12 1303.28 1255.79 38.80 o 3 3 12 9039.13 9445.41 97.58 o 4 3 12 1809.37 1681.96 41.74 o 5 3 12 10339.27 10371.26 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19.67 o -4 5 12 640.46 627.90 33.23 o -3 5 12 944.04 1161.28 37.44 o -2 5 12 3666.49 3810.87 56.27 o -1 5 12 17632.27 18931.24 166.22 o 0 5 12 458.01 499.83 28.12 o 1 5 12 18440.98 19678.69 170.46 o 2 5 12 3773.62 3865.73 55.22 o 3 5 12 933.90 1193.60 32.17 o 4 5 12 546.31 582.39 31.38 o 5 5 12 15.34 15.39 20.66 o 6 5 12 1656.78 1620.24 53.92 o 7 5 12 774.60 860.51 40.21 o 8 5 12 2002.19 1997.85 62.36 o 9 5 12 176.80 243.17 36.36 o 10 5 12 238.33 243.24 49.80 o 11 5 12 789.64 948.59 72.41 o 12 5 12 927.21 1022.97 85.03 o 13 5 12 50.66 -31.05 51.27 o 14 5 12 783.78 737.37 131.54 o 15 5 12 89.65 23.67 60.07 o 16 5 12 2527.19 2962.23 113.57 o 17 5 12 105.16 145.35 106.11 o 18 5 12 1601.89 1600.32 164.25 o -17 6 12 1642.83 1709.21 80.53 o -16 6 12 121.03 70.51 50.58 o -15 6 12 274.02 181.19 66.72 o -14 6 12 1178.86 1078.93 62.16 o -13 6 12 3998.24 3840.97 84.26 o -12 6 12 42.42 57.60 38.25 o -11 6 12 796.25 836.87 49.33 o -10 6 12 1675.13 1430.05 55.80 o -9 6 12 3432.71 3712.47 71.31 o -8 6 12 1379.06 1326.54 43.55 o -7 6 12 154.23 171.89 23.93 o -6 6 12 6024.16 5853.11 69.78 o -5 6 12 1212.10 1382.26 38.95 o -4 6 12 80.63 132.05 20.07 o -3 6 12 2539.63 2689.77 50.31 o -2 6 12 456.07 539.76 29.74 o -1 6 12 3793.93 3827.25 56.48 o 0 6 12 1914.12 2193.74 44.51 o 1 6 12 3737.75 3727.29 54.87 o 2 6 12 550.77 759.80 33.69 o 3 6 12 2424.03 2535.09 72.38 o 4 6 12 50.80 79.29 20.60 o 5 6 12 1250.63 1343.46 41.52 o 6 6 12 5976.62 5685.76 93.96 o 7 6 12 175.51 230.00 32.96 o 8 6 12 1471.79 1368.08 56.76 o 9 6 12 3402.40 3622.75 137.24 o 10 6 12 1509.22 1422.56 59.83 o 11 6 12 909.42 924.43 119.91 o 12 6 12 22.99 1.18 49.21 o 13 6 12 4264.96 4110.59 115.62 o 14 6 12 1066.98 920.85 80.09 o 15 6 12 390.99 388.29 65.68 o 16 6 12 149.05 11.63 97.39 o 17 6 12 1713.79 1776.19 155.53 o -17 7 12 156.60 222.65 73.01 o -16 7 12 481.47 541.38 59.99 o -15 7 12 675.24 580.11 62.27 o -14 7 12 651.55 773.78 73.35 o -13 7 12 2435.81 2626.77 117.73 o -12 7 12 2009.88 2008.63 94.14 o -11 7 12 3644.32 3504.26 169.33 o -10 7 12 153.92 177.05 37.09 o -9 7 12 962.91 982.75 49.71 o -8 7 12 148.61 179.07 26.98 o -7 7 12 715.92 744.93 35.41 o -6 7 12 447.36 385.76 26.70 o -5 7 12 5289.41 5228.47 65.05 o -4 7 12 6747.99 7166.77 75.82 o -3 7 12 1869.57 1996.06 38.94 o -2 7 12 1211.32 1312.38 38.79 o -1 7 12 4399.59 4832.24 64.85 o 0 7 12 4228.82 4297.81 59.93 o 1 7 12 4588.01 5124.65 65.27 o 2 7 12 1094.01 1192.61 38.03 o 3 7 12 1575.86 1589.58 39.46 o 4 7 12 6481.82 6941.26 121.28 o 5 7 12 4872.00 4840.57 82.72 o 6 7 12 390.20 391.12 34.96 o 7 7 12 631.71 720.82 47.24 o 8 7 12 183.76 175.37 45.69 o 9 7 12 847.14 787.09 48.95 o 10 7 12 118.26 188.62 37.96 o 11 7 12 3507.07 3423.39 82.79 o 12 7 12 2169.88 2057.15 89.40 o 13 7 12 2395.47 2597.61 321.23 o 14 7 12 688.18 769.26 67.74 o 15 7 12 617.90 424.43 98.84 o 16 7 12 439.39 511.64 109.01 o -17 8 12 439.69 459.86 86.26 o -16 8 12 133.30 88.19 75.01 o -15 8 12 138.33 153.82 70.72 o -14 8 12 855.96 882.81 79.41 o -13 8 12 2202.74 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o -11 14 12 163.38 84.75 72.68 o -10 14 12 914.92 883.31 82.32 o -9 14 12 3510.76 3600.12 94.64 o -8 14 12 489.80 645.43 54.16 o -7 14 12 934.70 856.10 57.25 o -6 14 12 60.40 40.85 41.84 o -5 14 12 146.82 97.05 40.82 o -4 14 12 444.88 371.59 31.89 o -3 14 12 3370.02 3289.30 79.92 o -2 14 12 1730.89 1762.97 76.43 o -1 14 12 402.24 448.02 35.02 o 0 14 12 3135.49 3331.74 76.35 o 1 14 12 407.82 417.06 43.14 o 2 14 12 1917.78 1946.61 66.20 o 3 14 12 3512.91 3489.22 79.99 o 4 14 12 534.83 519.79 44.95 o 5 14 12 139.02 140.37 39.89 o 6 14 12 19.00 38.77 40.12 o 7 14 12 1020.79 894.09 51.20 o 8 14 12 578.47 805.54 53.92 o 9 14 12 3578.61 3579.44 103.33 o 10 14 12 881.32 969.32 63.48 o 11 14 12 191.91 145.78 64.99 o 12 14 12 926.71 996.17 70.14 o 13 14 12 243.33 265.69 61.91 o 14 14 12 1120.49 1190.99 78.44 o -13 15 12 664.60 717.03 86.91 o -12 15 12 717.04 625.33 82.50 o -11 15 12 1580.06 1485.44 167.88 o -10 15 12 22.20 105.92 52.26 o -9 15 12 398.30 424.35 53.34 o -8 15 12 71.84 35.60 46.81 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