#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/40/2014093.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2014093_Fobs loop_ _publ_author_name 'Liu, Zhao-Di' 'Zou, Ying' 'Tan, Min-Yu' 'Zhu, Hai-Liang' _publ_section_title ; catena-Poly[1,4-diazoniabicyclo[2.2.2]octane [silver(I)-tri-\m-thiocyanato-\k^6^S:S]] ; _journal_issue 9 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first m447 _journal_page_last m448 _journal_volume 60 _journal_year 2004 _space_group_IT_number 176 _symmetry_space_group_name_Hall '-P 6c' _symmetry_space_group_name_H-M 'P 63/m' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 120.000 _cell_length_a 10.2148 _cell_length_b 10.2148 _cell_length_c 7.1740 _exptl_crystal_F_000 396.00 _reflns_d_resolution_high 0.7840 _[local]_cod_data_source_file av1193Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' ZHL-42 in P6(3)/m' _shelx_refln_list_code 4 _shelx_f_calc_maximum 113.51 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-y, x-y, z' '-x+y, -x, z' '-x, -y, z+1/2' 'y, -x+y, z+1/2' 'x-y, x, z+1/2' '-x, -y, -z' 'y, -x+y, -z' 'x-y, x, -z' 'x, y, -z-1/2' '-y, x-y, -z-1/2' '-x+y, -x, -z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 0 1 0 6013.09 6640.78 503.93 o -1 2 0 12883.78 9464.51 917.97 o 0 2 0 1279.74 1789.26 154.21 o -2 3 0 2195.24 3596.42 184.89 o -1 3 0 2015.70 2168.90 288.49 o 0 3 0 2387.59 2751.93 209.02 o -3 4 0 6967.20 7646.94 250.34 o -2 4 0 2400.33 2693.81 301.73 o -1 4 0 5453.77 6373.57 544.28 o 0 4 0 4859.49 4911.65 281.52 o -4 5 0 5935.56 6378.06 192.87 o -3 5 0 286.08 311.30 25.68 o -2 5 0 2296.78 2620.37 364.97 o -1 5 0 11288.40 9986.16 400.98 o 0 5 0 10265.02 10305.95 559.24 o -5 6 0 1517.51 1405.84 214.83 o -4 6 0 2386.63 2872.76 96.01 o -3 6 0 915.68 935.03 72.62 o -2 6 0 357.64 375.93 31.02 o -1 6 0 2124.46 2633.36 436.53 o 0 6 0 5933.02 4632.21 3105.39 o -6 7 0 207.80 202.04 15.08 o -5 7 0 390.26 422.93 33.02 o -4 7 0 222.60 191.74 12.78 o -3 7 0 442.99 507.48 38.23 o -2 7 0 2173.57 1996.72 314.28 o -1 7 0 68.89 63.17 14.37 o 0 7 0 294.93 298.62 131.87 o -7 8 0 119.03 125.36 11.34 o -6 8 0 335.61 341.14 67.59 o -5 8 0 774.76 782.58 92.84 o -4 8 0 2893.39 2769.33 391.68 o -3 8 0 386.08 414.14 29.94 o -2 8 0 46.29 57.85 8.81 o -1 8 0 867.98 788.56 399.52 o 0 8 0 70.50 62.49 7.45 o -8 9 0 1016.47 816.61 255.81 o -7 9 0 19.85 26.07 7.31 o -6 9 0 774.03 665.19 106.66 o -5 9 0 2430.23 2190.87 157.17 o -4 9 0 695.96 608.20 119.61 o -3 9 0 980.63 954.51 159.31 o -2 9 0 140.03 136.77 30.83 o -1 9 0 704.20 540.99 187.61 o 0 9 0 1392.37 1116.29 362.19 o -9 10 0 430.17 375.29 90.69 o -8 10 0 111.36 124.02 26.67 o -7 10 0 328.91 301.69 53.26 o -6 10 0 463.06 435.05 64.61 o -5 10 0 2386.38 2166.67 246.62 o -4 10 0 372.39 328.49 44.73 o -3 10 0 6.26 15.27 4.01 o -2 10 0 817.07 598.86 157.63 o -1 10 0 933.99 822.84 191.91 o 0 10 0 503.40 427.69 72.07 o -10 11 0 132.54 141.87 36.48 o -9 11 0 4.84 12.54 5.09 o -8 11 0 20.20 17.13 5.67 o -7 11 0 136.84 123.40 44.47 o -6 11 0 384.88 371.09 56.44 o -5 11 0 534.38 554.11 71.08 o -4 11 0 31.23 32.27 5.97 o -3 11 0 6.31 12.70 5.45 o -2 11 0 5.03 18.78 4.46 o -1 11 0 338.74 253.46 66.18 o 0 11 0 424.88 245.80 78.09 o -9 12 0 148.55 147.28 37.20 o -8 12 0 5.42 13.82 5.20 o -7 12 0 5.91 6.94 4.90 o -6 12 0 29.18 50.02 12.02 o -5 12 0 16.49 22.50 6.20 o -4 12 0 116.53 103.89 47.34 o -3 12 0 15.47 24.34 7.03 o -2 12 0 32.24 34.09 13.83 o -7 13 0 37.08 50.79 15.75 o -6 13 0 137.26 130.83 14.87 o 0 1 1 281.36 221.53 8.31 o -1 2 1 351.51 391.88 25.61 o 0 2 1 2978.62 3085.71 164.93 o -2 3 1 4417.07 4842.68 248.53 o -1 3 1 3765.53 3968.61 108.34 o 0 3 1 834.19 919.46 33.48 o -3 4 1 1455.46 1638.27 180.43 o -2 4 1 1.15 3.33 0.59 o -1 4 1 1077.74 1314.65 75.78 o 0 4 1 67.74 73.89 4.25 o -4 5 1 376.44 478.22 29.96 o -3 5 1 23.18 31.85 1.73 o -2 5 1 188.48 189.74 11.25 o -1 5 1 3.61 5.81 1.61 o 0 5 1 16.79 21.16 1.88 o -5 6 1 21.16 24.09 2.41 o -4 6 1 76.80 74.08 5.46 o -3 6 1 1494.60 1647.05 67.03 o -2 6 1 592.66 644.98 33.51 o -1 6 1 1.19 6.28 3.97 o 0 6 1 2.67 5.86 1.69 o -6 7 1 544.17 597.71 64.96 o -5 7 1 27.62 33.35 4.36 o -4 7 1 1343.27 1319.71 84.94 o -3 7 1 108.76 99.69 5.56 o -2 7 1 229.43 218.69 15.26 o -1 7 1 144.79 138.79 13.25 o 0 7 1 16.39 25.40 3.35 o -7 8 1 684.16 647.34 92.11 o -6 8 1 222.60 232.34 22.77 o -5 8 1 3.56 9.84 2.14 o -4 8 1 16.07 31.30 3.19 o -3 8 1 7.50 16.41 2.52 o -2 8 1 2623.25 2589.88 216.66 o -1 8 1 246.86 233.96 42.87 o 0 8 1 234.17 190.07 33.02 o -8 9 1 14.96 18.86 3.47 o -7 9 1 14.55 24.84 4.12 o -6 9 1 355.07 346.44 35.68 o -5 9 1 3.00 8.14 2.59 o -4 9 1 33.88 43.65 4.00 o -3 9 1 2.84 8.93 3.07 o -2 9 1 8.72 15.44 2.77 o -1 9 1 141.35 123.31 12.91 o 0 9 1 37.96 44.50 7.71 o -9 10 1 22.92 25.43 4.19 o -8 10 1 16.94 34.51 5.64 o -7 10 1 58.39 73.09 9.85 o -6 10 1 48.51 59.69 5.98 o -5 10 1 0.41 3.20 2.52 o -4 10 1 172.86 186.27 16.91 o -3 10 1 0.08 8.21 2.36 o -2 10 1 23.37 30.60 5.79 o -1 10 1 0.07 12.46 2.85 o 0 10 1 4.36 18.71 4.04 o -10 11 1 29.84 40.62 10.00 o -9 11 1 101.72 111.10 9.76 o -8 11 1 559.19 463.98 68.90 o -7 11 1 50.45 70.10 7.33 o -6 11 1 67.46 78.34 7.07 o -5 11 1 3.40 14.99 3.78 o -4 11 1 187.83 167.93 25.71 o -3 11 1 194.38 197.85 28.82 o -2 11 1 173.44 143.98 24.16 o -1 11 1 58.47 66.92 10.51 o 0 11 1 26.25 39.75 9.59 o -10 12 1 77.33 65.72 13.65 o -9 12 1 38.03 47.85 6.56 o -8 12 1 120.44 118.54 9.22 o -7 12 1 110.35 94.69 7.78 o -6 12 1 75.65 83.01 9.72 o -5 12 1 0.22 14.22 5.04 o -4 12 1 90.26 107.72 12.76 o -3 12 1 12.53 26.04 5.22 o -2 12 1 74.32 76.17 24.44 o 0 0 2 2216.97 2721.25 338.31 o 0 1 2 1670.71 1957.46 109.54 o -1 2 2 8894.42 8245.87 451.30 o 0 2 2 8301.69 8883.69 314.73 o -2 3 2 3315.97 3357.06 77.32 o -1 3 2 6412.37 6139.61 332.29 o 0 3 2 8205.24 7990.80 297.00 o -3 4 2 2558.01 2524.50 134.19 o -2 4 2 6492.84 5532.51 375.34 o -1 4 2 1564.61 1645.47 121.40 o 0 4 2 425.30 414.29 21.47 o -4 5 2 1513.61 1718.34 58.87 o -3 5 2 3112.38 3208.72 197.99 o -2 5 2 2685.13 2751.44 126.12 o -1 5 2 192.55 203.17 17.38 o 0 5 2 67.74 82.06 6.85 o -5 6 2 606.19 662.72 37.81 o -4 6 2 1204.91 1112.34 85.80 o -3 6 2 4940.87 5720.03 209.47 o -2 6 2 2434.13 2696.48 167.30 o -1 6 2 440.21 511.74 18.98 o 0 6 2 225.09 243.25 23.30 o -6 7 2 1408.38 1405.13 129.57 o -5 7 2 3178.48 3027.53 327.30 o -4 7 2 1805.02 1645.54 136.90 o -3 7 2 1258.30 1246.93 149.01 o -2 7 2 1802.99 1889.98 179.49 o -1 7 2 1468.01 1400.88 115.73 o 0 7 2 998.46 894.68 148.18 o -7 8 2 1780.33 1601.13 133.68 o -6 8 2 1046.20 1027.03 75.07 o -5 8 2 354.03 335.83 30.51 o -4 8 2 344.34 328.61 15.68 o -3 8 2 685.31 635.68 46.58 o -2 8 2 1935.90 2043.40 224.62 o -1 8 2 1259.25 1200.60 225.59 o 0 8 2 521.86 466.48 102.79 o -8 9 2 33.03 32.85 4.26 o -7 9 2 682.52 610.31 52.88 o -6 9 2 362.57 331.27 34.88 o -5 9 2 11.01 13.47 2.91 o -4 9 2 55.10 68.28 5.15 o -3 9 2 853.22 906.03 84.63 o -2 9 2 304.81 264.36 35.79 o -1 9 2 15.24 15.61 3.27 o 0 9 2 7.02 9.77 2.85 o -9 10 2 7.08 17.64 3.57 o -8 10 2 460.51 410.88 40.90 o -7 10 2 290.05 246.59 47.01 o -6 10 2 39.77 43.52 4.98 o -5 10 2 12.54 15.79 3.20 o -4 10 2 75.49 74.64 10.95 o -3 10 2 495.54 476.69 64.70 o -2 10 2 138.76 140.55 23.50 o -1 10 2 14.13 19.27 3.59 o 0 10 2 11.93 22.18 3.87 o -10 11 2 144.50 157.61 12.98 o -9 11 2 307.93 266.44 43.53 o -8 11 2 447.01 425.32 52.84 o -7 11 2 320.04 313.12 26.81 o -6 11 2 18.73 24.72 6.04 o -5 11 2 8.36 8.73 5.66 o -4 11 2 655.16 557.12 97.82 o -3 11 2 458.18 373.39 87.66 o -2 11 2 183.90 166.22 37.67 o -1 11 2 16.20 26.54 6.65 o 0 11 2 0.97 10.24 10.77 o -9 12 2 156.99 247.35 43.26 o -8 12 2 170.98 191.24 21.13 o -7 12 2 225.16 226.81 29.39 o -6 12 2 311.76 290.87 48.05 o -5 12 2 258.34 246.18 51.70 o -4 12 2 87.26 93.34 17.21 o -3 12 2 232.28 175.38 50.18 o 0 1 3 1996.51 1985.39 43.88 o -1 2 3 385.91 363.71 11.51 o 0 2 3 54.92 64.38 3.62 o -2 3 3 1700.98 1589.93 71.13 o -1 3 3 1081.32 968.94 48.15 o 0 3 3 0.71 4.52 1.18 o -3 4 3 153.12 147.47 4.06 o -2 4 3 471.95 442.64 20.82 o -1 4 3 607.85 643.54 36.05 o 0 4 3 3.15 5.77 0.98 o -4 5 3 49.62 56.01 2.65 o -3 5 3 10.65 13.32 1.37 o -2 5 3 423.31 436.43 47.10 o -1 5 3 29.40 36.81 2.39 o 0 5 3 277.50 316.72 33.75 o -5 6 3 47.30 57.55 3.98 o -4 6 3 434.30 418.91 23.76 o -3 6 3 421.45 381.77 22.54 o -2 6 3 56.96 56.89 3.29 o -1 6 3 152.61 203.55 14.37 o 0 6 3 9.21 19.04 2.36 o -6 7 3 169.76 162.70 22.26 o -5 7 3 29.10 37.94 4.87 o -4 7 3 424.54 445.21 35.92 o -3 7 3 562.42 654.46 37.58 o -2 7 3 147.44 153.14 9.14 o -1 7 3 722.82 669.60 65.26 o 0 7 3 300.40 269.92 40.24 o -7 8 3 195.62 256.12 23.06 o -6 8 3 280.64 271.22 36.71 o -5 8 3 10.97 15.28 3.15 o -4 8 3 60.83 54.74 9.22 o -3 8 3 300.77 311.62 30.69 o -2 8 3 458.43 437.15 42.26 o -1 8 3 240.28 171.45 25.06 o 0 8 3 45.14 47.06 6.79 o -8 9 3 70.62 100.27 10.88 o -7 9 3 70.80 65.12 9.62 o -6 9 3 40.37 45.00 5.79 o -5 9 3 111.53 91.22 11.38 o -4 9 3 31.16 46.81 7.30 o -3 9 3 0.05 5.66 2.52 o -2 9 3 323.60 278.98 30.70 o -1 9 3 0.92 4.18 2.71 o 0 9 3 38.56 39.07 5.59 o -9 10 3 19.43 35.80 9.42 o -8 10 3 109.26 101.89 13.71 o -7 10 3 5.30 6.58 3.40 o -6 10 3 14.52 14.69 4.26 o -5 10 3 4.75 6.37 3.39 o -4 10 3 3.12 10.09 2.93 o -3 10 3 119.49 129.85 16.42 o -2 10 3 31.78 39.68 5.35 o -1 10 3 41.25 42.14 6.41 o 0 10 3 0.46 9.04 3.43 o -10 11 3 56.69 42.94 10.17 o -9 11 3 16.47 23.21 4.85 o -8 11 3 374.26 330.53 50.85 o -7 11 3 98.62 97.37 10.33 o -6 11 3 80.19 78.05 11.19 o -5 11 3 14.57 12.50 5.16 o -4 11 3 42.82 44.72 8.85 o -3 11 3 62.90 73.50 8.82 o -2 11 3 112.40 96.15 17.88 o -1 11 3 2.79 10.62 5.87 o -8 12 3 13.07 12.65 12.58 o -7 12 3 21.22 53.32 22.57 o -6 12 3 174.80 234.51 30.21 o -5 12 3 9.41 24.10 12.40 o -4 12 3 109.43 86.72 45.67 o 0 0 4 7437.40 5262.99 36.57 o 0 1 4 5955.23 5381.03 261.43 o -1 2 4 559.66 566.39 19.38 o 0 2 4 686.79 620.25 15.82 o -2 3 4 2485.13 2318.93 69.56 o -1 3 4 616.64 569.75 11.60 o 0 3 4 957.06 852.45 14.58 o -3 4 4 257.35 254.12 12.10 o -2 4 4 1086.04 937.93 50.52 o -1 4 4 1480.43 1470.29 58.48 o 0 4 4 3605.53 3847.95 258.95 o -4 5 4 2118.52 1981.85 131.99 o -3 5 4 1190.61 1192.26 77.56 o -2 5 4 339.13 324.41 15.65 o -1 5 4 3310.24 3568.16 193.78 o 0 5 4 2774.10 2605.37 105.41 o -5 6 4 1417.10 1403.21 61.66 o -4 6 4 266.83 245.68 9.84 o -3 6 4 86.43 90.81 9.16 o -2 6 4 514.51 531.85 31.55 o -1 6 4 1637.74 1679.68 122.51 o 0 6 4 1259.12 1334.47 107.18 o -6 7 4 195.99 190.31 19.85 o -5 7 4 87.83 100.29 5.43 o -4 7 4 288.42 254.75 15.30 o -3 7 4 469.42 410.54 26.85 o -2 7 4 13.46 16.79 2.50 o -1 7 4 331.52 311.61 33.12 o 0 7 4 173.55 178.61 23.91 o -7 8 4 21.76 29.13 5.77 o -6 8 4 4.34 6.84 2.71 o -5 8 4 682.90 632.43 67.82 o -4 8 4 470.69 491.81 79.42 o -3 8 4 495.19 475.40 59.57 o -2 8 4 81.93 85.86 10.90 o -1 8 4 6.10 12.55 2.91 o 0 8 4 236.70 223.20 27.63 o -8 9 4 186.03 165.67 31.84 o -7 9 4 179.38 147.90 23.34 o -6 9 4 454.37 437.85 64.31 o -5 9 4 686.42 593.85 85.52 o -4 9 4 849.51 724.03 100.73 o -3 9 4 3.21 8.05 2.94 o -2 9 4 369.22 324.47 42.19 o -1 9 4 583.24 487.00 79.20 o 0 9 4 462.85 410.60 33.93 o -9 10 4 234.12 197.48 40.05 o -8 10 4 111.77 106.48 17.29 o -7 10 4 0.53 8.05 3.63 o -6 10 4 463.66 381.42 42.81 o -5 10 4 770.26 697.99 85.78 o -4 10 4 363.19 313.66 59.71 o -3 10 4 51.61 53.53 6.11 o -2 10 4 113.52 131.60 23.41 o -1 10 4 273.73 195.38 23.24 o 0 10 4 405.39 438.71 55.36 o -9 11 4 0.35 10.76 5.02 o -8 11 4 11.45 10.15 6.62 o -7 11 4 68.70 76.27 8.35 o -6 11 4 195.00 198.78 36.57 o -5 11 4 148.30 123.59 14.42 o -4 11 4 0.30 7.84 3.14 o -3 11 4 0.14 10.19 3.44 o -2 11 4 45.12 65.15 28.65 o 0 1 5 291.81 243.51 8.37 o -1 2 5 154.19 120.09 7.06 o 0 2 5 122.99 116.46 5.73 o -2 3 5 181.04 170.26 11.34 o -1 3 5 779.97 706.35 46.15 o 0 3 5 10.03 12.47 1.81 o -3 4 5 276.82 240.58 13.21 o -2 4 5 322.32 295.50 17.01 o -1 4 5 24.12 23.79 2.29 o 0 4 5 260.99 258.60 14.15 o -4 5 5 135.81 125.19 8.21 o -3 5 5 319.16 303.89 26.02 o -2 5 5 21.67 23.06 2.85 o -1 5 5 28.55 34.14 3.01 o 0 5 5 11.21 14.61 2.34 o -5 6 5 59.04 66.23 6.47 o -4 6 5 15.15 20.55 3.60 o -3 6 5 78.63 95.25 7.02 o -2 6 5 136.70 145.50 8.19 o -1 6 5 7.59 16.49 2.68 o 0 6 5 16.86 22.49 3.29 o -6 7 5 259.49 243.01 31.34 o -5 7 5 7.87 11.76 2.56 o -4 7 5 467.75 491.89 36.82 o -3 7 5 171.18 181.86 11.51 o -2 7 5 78.21 83.64 6.97 o -1 7 5 304.48 303.13 42.90 o 0 7 5 79.84 84.41 12.36 o -7 8 5 27.85 32.15 7.01 o -6 8 5 31.73 38.60 8.13 o -5 8 5 39.90 45.24 6.80 o -4 8 5 34.14 40.27 5.00 o -3 8 5 121.98 131.60 14.16 o -2 8 5 191.75 195.57 35.44 o -1 8 5 100.13 111.02 23.33 o 0 8 5 92.79 103.48 27.62 o -8 9 5 1.10 10.71 4.80 o -7 9 5 245.71 247.38 42.43 o -6 9 5 2.16 9.74 2.64 o -5 9 5 14.89 18.50 4.31 o -4 9 5 1.89 6.87 3.51 o -3 9 5 0.04 6.11 2.78 o -2 9 5 125.35 112.51 25.09 o -1 9 5 9.21 16.71 3.46 o 0 9 5 17.50 27.06 6.60 o -8 10 5 108.81 107.77 49.48 o -7 10 5 31.19 46.73 6.50 o -6 10 5 33.14 52.14 6.70 o -5 10 5 4.57 12.52 3.99 o -4 10 5 31.83 45.35 6.73 o -3 10 5 20.16 20.65 4.14 o -2 10 5 24.98 30.42 11.80 o 0 0 6 122.45 126.75 8.00 o 0 1 6 247.01 214.49 14.57 o -1 2 6 746.58 635.57 32.88 o 0 2 6 1379.54 1222.60 39.53 o -2 3 6 541.81 471.70 35.88 o -1 3 6 1208.33 1100.96 47.71 o 0 3 6 463.14 445.62 28.68 o -3 4 6 1126.07 931.34 44.58 o -2 4 6 273.56 244.97 10.48 o -1 4 6 469.57 428.39 28.40 o 0 4 6 81.56 88.04 5.26 o -4 5 6 2.77 13.11 2.55 o -3 5 6 487.78 495.60 40.40 o -2 5 6 879.61 879.61 32.60 o -1 5 6 9.92 23.67 3.16 o 0 5 6 27.62 35.64 3.71 o -5 6 6 132.88 137.81 8.62 o -4 6 6 685.11 739.96 43.83 o -3 6 6 405.17 452.74 37.58 o -2 6 6 465.57 528.54 37.28 o -1 6 6 66.38 89.45 6.58 o 0 6 6 0.58 9.73 2.56 o -6 7 6 350.77 370.97 44.86 o -5 7 6 225.98 225.68 26.40 o -4 7 6 399.92 436.38 28.99 o -3 7 6 296.28 331.20 33.34 o -2 7 6 405.38 433.98 41.36 o -1 7 6 284.86 299.14 25.28 o 0 7 6 270.52 303.02 46.22 o -7 8 6 164.38 192.52 39.24 o -6 8 6 570.13 546.80 72.88 o -5 8 6 69.78 91.95 9.63 o -4 8 6 18.04 22.06 3.31 o -3 8 6 109.26 154.24 13.46 o -2 8 6 337.85 434.47 50.63 o -1 8 6 282.12 307.12 45.02 o 0 8 6 130.85 169.67 60.05 o -7 9 6 83.68 93.58 18.63 o -6 9 6 1.27 15.51 3.60 o -5 9 6 27.92 37.62 5.86 o -4 9 6 18.14 33.12 5.25 o -3 9 6 210.12 252.45 35.12 o -2 9 6 47.41 120.40 21.18 o 0 1 7 15.23 10.33 1.92 o -1 2 7 32.56 33.22 2.64 o 0 2 7 66.07 71.74 4.14 o -2 3 7 123.21 113.28 4.07 o -1 3 7 163.94 163.04 7.03 o 0 3 7 6.02 12.66 2.31 o -3 4 7 65.50 70.92 6.16 o -2 4 7 36.11 36.94 3.60 o -1 4 7 32.86 36.07 3.55 o 0 4 7 14.91 19.64 2.96 o -4 5 7 1.49 12.63 2.17 o -3 5 7 14.88 17.05 3.01 o -2 5 7 17.59 22.86 2.97 o -1 5 7 3.59 10.80 2.26 o 0 5 7 5.57 12.77 2.56 o -5 6 7 0.83 11.61 2.57 o -4 6 7 1.82 14.85 2.82 o -3 6 7 57.71 85.08 6.14 o -2 6 7 43.10 62.40 5.21 o -1 6 7 3.36 16.02 2.90 o 0 6 7 1.80 18.77 3.37 o -6 7 7 50.59 68.22 10.01 o -5 7 7 0.15 16.04 3.01 o -4 7 7 118.44 135.64 10.31 o -3 7 7 30.91 59.05 5.94 o -2 7 7 26.29 41.15 4.91 o -1 7 7 62.77 65.96 6.28 o 0 7 7 20.21 37.17 8.56 o -6 8 7 12.27 25.34 7.78 o -5 8 7 2.51 17.97 5.10 o -4 8 7 5.68 17.19 5.53 o 0 0 8 1153.26 1100.84 39.56 o 0 1 8 286.50 244.98 8.03 o -1 2 8 62.37 86.03 7.00 o 0 2 8 66.33 78.54 6.23 o -2 3 8 139.81 134.28 6.35 o -1 3 8 88.14 90.40 4.39 o 0 3 8 11.42 20.02 3.02 o -3 4 8 185.44 181.94 14.92 o -2 4 8 28.22 34.46 3.58 o -1 4 8 204.53 199.40 10.91 o 0 4 8 211.23 203.71 13.70 o -4 5 8 64.29 75.92 8.48 o -3 5 8 45.05 65.30 6.61 o -2 5 8 91.33 126.11 6.38 o -1 5 8 172.96 204.17 11.46 o 0 5 8 456.98 588.91 40.97 o -3 6 8 0.30 13.71 5.31 o -2 6 8 29.35 51.20 8.09 o 0 1 9 2.89 7.68 3.68 o -1 2 9 2.81 4.94 4.46 o 0 2 9 12.34 15.36 4.44 o