#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/41/2014107.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2014107_Fobs loop_ _publ_author_name 'Wen, Yi-Hang' 'Qin, Ye-Yan' 'Zhang, Jian' 'Li, Zhao-Ji' 'Cheng, Jian-Kai' 'Kang, Yao' 'Yao, Yuan-Gen' _publ_section_title ; catena-Poly[[[aquacopper(I)]-\m-4,4'-bipyridyl-\k^2^N:N'] hemi(isophthalate) monohydrate] ; _journal_issue 8 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first m371 _journal_page_last m372 _journal_volume 60 _journal_year 2004 _space_group_IT_number 60 _symmetry_space_group_name_Hall '-P 2n 2ab' _symmetry_space_group_name_H-M 'P b c n' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 21.6096 _cell_length_b 7.2160 _cell_length_c 17.6529 _exptl_crystal_F_000 1384.00 _reflns_d_resolution_high 0.8399 _[local]_cod_data_source_file bm1570Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' a in Pbcn' _shelx_refln_list_code 4 _shelx_f_calc_maximum 588.61 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y+1/2, z+1/2' '-x, y, -z+1/2' 'x+1/2, -y+1/2, -z' '-x, -y, -z' 'x-1/2, y-1/2, -z-1/2' 'x, -y, z-1/2' '-x-1/2, y-1/2, z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 621.60 654.47 19.91 o 4 0 0 3070.84 3121.51 84.20 o 6 0 0 37671.95 33300.08 843.04 o 8 0 0 1811.88 1665.33 53.70 o 10 0 0 44739.36 43803.31 1111.98 o 12 0 0 26416.73 24072.36 621.16 o 14 0 0 2713.97 2490.28 80.84 o 16 0 0 6296.81 5946.60 170.83 o 18 0 0 25308.05 25076.27 652.17 o 20 0 0 73.28 272.88 31.71 o 22 0 0 3887.34 3797.82 123.24 o 24 0 0 7108.45 8724.01 256.92 o 1 1 0 931.19 940.15 69.35 o 3 1 0 754.10 948.01 21.08 o 5 1 0 8967.76 9333.19 179.77 o 7 1 0 3163.23 3501.33 69.31 o 9 1 0 511.04 591.82 28.43 o 11 1 0 431.83 384.70 18.46 o 13 1 0 2438.29 2158.66 125.88 o 15 1 0 5.24 -1.71 10.91 o 17 1 0 240.56 240.48 18.58 o 19 1 0 8.80 -7.60 23.45 o 21 1 0 55.67 15.23 25.77 o 23 1 0 71.73 17.61 18.62 o 25 1 0 3.43 103.07 27.75 o 0 2 0 346461.03 343533.13 8610.41 o 2 2 0 2863.83 3082.39 77.83 o 4 2 0 8926.61 9366.08 174.13 o 6 2 0 48612.75 49078.31 953.82 o 8 2 0 15978.00 16164.39 348.10 o 10 2 0 36724.11 38772.89 697.98 o 12 2 0 21761.29 19308.15 355.19 o 14 2 0 1910.92 1670.46 112.87 o 16 2 0 4644.78 4297.66 93.96 o 18 2 0 8282.29 8118.12 163.64 o 20 2 0 246.55 244.44 46.92 o 22 2 0 3886.73 3824.39 104.01 o 24 2 0 6294.80 6359.12 194.39 o 1 3 0 1653.95 1761.46 91.43 o 3 3 0 1237.00 1230.04 87.38 o 5 3 0 522.54 572.23 21.65 o 7 3 0 486.75 516.02 21.27 o 9 3 0 976.51 1160.82 41.01 o 11 3 0 1274.27 1267.57 152.50 o 13 3 0 61.16 57.42 21.14 o 15 3 0 93.70 75.00 31.05 o 17 3 0 187.78 136.64 19.29 o 19 3 0 175.53 131.54 20.56 o 21 3 0 85.99 186.33 38.98 o 23 3 0 3.37 -10.57 27.75 o 0 4 0 87606.76 93522.70 2366.76 o 2 4 0 6817.91 6208.15 404.81 o 4 4 0 604.74 565.02 40.33 o 6 4 0 7366.99 7546.52 155.90 o 8 4 0 1625.64 1817.51 48.90 o 10 4 0 9144.06 10448.00 203.65 o 12 4 0 7594.76 7952.84 160.42 o 14 4 0 541.00 580.97 33.71 o 16 4 0 1311.94 1470.77 48.74 o 18 4 0 4728.15 4906.00 114.62 o 20 4 0 377.45 370.74 49.56 o 22 4 0 914.61 946.01 65.45 o 1 5 0 76.06 145.85 18.88 o 3 5 0 819.32 748.69 30.78 o 5 5 0 177.45 211.87 16.83 o 7 5 0 292.25 260.83 23.02 o 9 5 0 348.91 432.11 25.93 o 11 5 0 1155.96 1272.59 42.32 o 13 5 0 1068.83 1036.21 38.05 o 15 5 0 63.04 120.39 20.00 o 17 5 0 381.77 475.92 42.63 o 19 5 0 295.97 442.75 50.88 o 0 6 0 11773.82 13244.99 373.11 o 2 6 0 589.23 449.99 39.33 o 4 6 0 1816.45 1834.62 56.52 o 6 6 0 526.52 422.46 31.31 o 8 6 0 1030.39 1106.18 77.70 o 10 6 0 1534.71 1499.61 145.86 o 12 6 0 1527.41 1628.76 53.07 o 14 6 0 512.39 498.53 154.66 o 16 6 0 100.67 155.82 26.52 o 18 6 0 1637.19 1997.40 92.59 o 1 7 0 0.32 -21.20 51.53 o 3 7 0 100.14 106.77 24.97 o 5 7 0 91.22 130.35 30.27 o 7 7 0 136.14 87.63 58.81 o 9 7 0 230.39 266.82 30.11 o 11 7 0 113.86 57.07 23.90 o 13 7 0 193.49 354.56 51.54 o 0 8 0 1668.43 1346.69 71.44 o 2 8 0 184.45 254.54 71.36 o 4 8 0 88.19 137.26 163.20 o 6 8 0 153.45 173.87 132.15 o 8 8 0 40.38 -45.41 112.32 o 1 1 1 160.93 288.79 7.63 o 2 1 1 13440.77 14888.81 452.26 o 3 1 1 6464.17 5940.08 77.26 o 4 1 1 3939.64 4295.76 57.10 o 5 1 1 1613.38 1459.90 23.55 o 6 1 1 102.73 102.52 12.11 o 7 1 1 1467.60 1462.37 24.48 o 8 1 1 21731.15 20514.89 262.82 o 9 1 1 3921.02 4009.25 76.76 o 10 1 1 58928.89 56690.46 717.25 o 11 1 1 2213.96 2205.14 40.36 o 12 1 1 277.05 290.18 11.82 o 13 1 1 421.57 363.64 13.47 o 14 1 1 10709.48 9360.12 127.77 o 15 1 1 6279.95 5973.85 98.46 o 16 1 1 7874.43 7745.07 114.33 o 17 1 1 1.52 -5.30 38.43 o 18 1 1 277.68 280.16 15.44 o 19 1 1 60.46 46.69 12.14 o 20 1 1 3191.09 3212.91 54.28 o 21 1 1 1776.44 1615.56 34.10 o 22 1 1 5077.12 4751.15 112.87 o 23 1 1 235.41 302.79 24.73 o 24 1 1 276.97 282.22 35.02 o 25 1 1 256.03 236.57 32.38 o 0 2 1 544.90 651.34 37.05 o 1 2 1 872.92 1028.87 18.82 o 2 2 1 3126.12 3297.38 47.15 o 3 2 1 138.71 109.97 6.47 o 4 2 1 604.10 642.47 26.83 o 5 2 1 35.22 44.02 21.39 o 6 2 1 3897.22 4170.23 59.46 o 7 2 1 277.09 282.83 23.28 o 8 2 1 512.94 540.03 12.87 o 9 2 1 0.12 39.01 9.63 o 10 2 1 3.17 14.76 21.05 o 11 2 1 359.50 348.44 29.38 o 12 2 1 819.64 965.45 23.96 o 13 2 1 16.36 45.73 8.10 o 14 2 1 96.06 69.26 11.83 o 15 2 1 7.01 -9.54 9.54 o 16 2 1 16.68 1.69 19.26 o 17 2 1 56.59 79.40 30.42 o 18 2 1 195.07 126.29 21.36 o 19 2 1 28.66 -5.35 10.49 o 20 2 1 2.97 44.16 35.16 o 21 2 1 21.50 68.26 46.61 o 22 2 1 62.00 102.92 16.16 o 23 2 1 24.43 -10.46 25.25 o 24 2 1 28.38 72.16 114.30 o 1 3 1 991.93 1165.91 49.10 o 2 3 1 7388.75 7839.53 107.16 o 3 3 1 1199.14 1267.19 27.62 o 4 3 1 4546.49 4511.92 75.19 o 5 3 1 1261.11 1245.45 28.58 o 6 3 1 27.77 31.48 14.69 o 7 3 1 936.75 967.76 34.76 o 8 3 1 10020.51 10788.25 144.56 o 9 3 1 4388.85 4599.41 67.60 o 10 3 1 25439.57 27805.12 358.29 o 11 3 1 363.19 349.43 25.47 o 12 3 1 27.77 51.07 25.90 o 13 3 1 303.23 363.74 28.24 o 14 3 1 7253.35 7209.86 103.00 o 15 3 1 1925.85 1814.44 36.14 o 16 3 1 3254.16 3527.75 103.76 o 17 3 1 223.20 199.67 26.74 o 18 3 1 72.04 90.01 23.65 o 19 3 1 83.95 69.42 29.28 o 20 3 1 1838.07 1798.42 45.31 o 21 3 1 836.24 785.25 42.67 o 22 3 1 3070.49 2914.59 113.27 o 23 3 1 101.14 24.84 22.48 o 0 4 1 1945.42 2304.71 89.08 o 1 4 1 1006.00 984.78 27.98 o 2 4 1 221.73 185.37 13.74 o 3 4 1 6.85 4.23 8.38 o 4 4 1 2127.81 1978.83 57.72 o 5 4 1 144.05 156.40 21.75 o 6 4 1 91.93 95.66 26.51 o 7 4 1 305.23 303.43 15.17 o 8 4 1 212.96 273.04 30.81 o 9 4 1 14.87 27.88 15.73 o 10 4 1 400.14 361.17 17.66 o 11 4 1 469.98 430.59 60.02 o 12 4 1 133.25 150.39 14.40 o 13 4 1 36.22 19.57 23.96 o 14 4 1 14.51 40.68 18.69 o 15 4 1 6.81 -2.71 43.56 o 16 4 1 1.68 -6.72 43.20 o 17 4 1 126.47 206.05 34.33 o 18 4 1 317.62 391.77 39.74 o 19 4 1 70.97 174.94 115.05 o 20 4 1 96.58 174.62 67.17 o 21 4 1 30.10 15.11 31.91 o 22 4 1 20.73 -14.24 30.39 o 1 5 1 429.84 454.89 17.95 o 2 5 1 2040.55 2119.26 90.02 o 3 5 1 1336.66 1302.10 32.47 o 4 5 1 2002.09 1970.23 47.44 o 5 5 1 80.83 101.20 23.01 o 6 5 1 0.88 10.13 10.38 o 7 5 1 622.10 614.90 32.32 o 8 5 1 3078.70 3233.05 55.36 o 9 5 1 40.56 49.29 27.94 o 10 5 1 6921.83 7480.55 109.58 o 11 5 1 445.07 541.31 78.04 o 12 5 1 3.09 7.16 11.86 o 13 5 1 226.47 294.04 24.90 o 14 5 1 3041.62 3268.20 57.69 o 15 5 1 582.85 723.15 30.05 o 16 5 1 540.13 572.54 23.27 o 17 5 1 113.68 93.56 64.57 o 18 5 1 0.82 -56.79 56.79 o 19 5 1 36.24 64.17 66.94 o 20 5 1 724.31 983.94 49.95 o 0 6 1 1.55 108.72 65.08 o 1 6 1 444.25 368.54 18.41 o 2 6 1 281.37 187.88 24.90 o 3 6 1 32.59 17.30 27.71 o 4 6 1 36.77 38.59 11.98 o 5 6 1 121.80 183.69 32.62 o 6 6 1 9.57 -18.82 36.24 o 7 6 1 134.53 143.45 16.41 o 8 6 1 293.37 312.30 49.70 o 9 6 1 17.97 28.78 31.28 o 10 6 1 203.36 259.53 31.67 o 11 6 1 209.27 202.79 30.04 o 12 6 1 150.60 186.10 48.48 o 13 6 1 20.74 86.05 86.78 o 14 6 1 27.00 -71.78 71.78 o 15 6 1 28.22 -25.90 25.90 o 16 6 1 9.15 -3.28 19.64 o 17 6 1 107.65 131.26 48.38 o 18 6 1 35.97 202.22 124.13 o 1 7 1 14.93 -44.44 44.44 o 2 7 1 425.52 343.68 19.79 o 3 7 1 204.83 286.78 55.13 o 4 7 1 574.35 609.06 28.05 o 5 7 1 11.13 -38.74 38.74 o 6 7 1 4.68 23.83 44.44 o 7 7 1 8.15 2.31 35.57 o 8 7 1 501.17 573.44 27.91 o 9 7 1 216.73 264.07 49.86 o 10 7 1 1195.88 1268.34 47.72 o 11 7 1 77.63 61.71 19.47 o 12 7 1 12.85 -36.35 53.59 o 13 7 1 52.68 98.83 38.35 o 14 7 1 968.32 983.63 62.62 o 0 8 1 0.11 37.86 23.51 o 1 8 1 119.05 37.30 56.55 o 2 8 1 36.72 -10.01 17.10 o 3 8 1 3.88 -31.61 31.61 o 4 8 1 54.01 -22.10 35.45 o 5 8 1 19.94 3.55 63.32 o 6 8 1 4.85 -99.81 118.93 o 7 8 1 45.48 -3.16 35.48 o 8 8 1 5.57 -46.63 46.63 o 9 8 1 4.90 65.76 59.46 o 0 0 2 42932.70 38527.61 1346.22 o 1 0 2 18434.93 16971.69 350.49 o 2 0 2 4362.85 4259.53 63.38 o 3 0 2 523.47 502.31 11.60 o 4 0 2 43.14 24.19 5.29 o 5 0 2 16662.77 14390.45 260.24 o 6 0 2 11481.74 9138.56 168.52 o 7 0 2 14032.88 12069.61 221.69 o 8 0 2 5559.78 4817.84 94.09 o 9 0 2 13.29 36.44 7.43 o 10 0 2 12283.26 11843.96 583.13 o 11 0 2 6434.88 5717.05 213.59 o 12 0 2 10263.28 9323.01 177.66 o 13 0 2 4986.68 4888.26 99.58 o 14 0 2 1329.55 1310.72 35.68 o 15 0 2 152.33 188.74 35.68 o 16 0 2 1745.00 1751.06 45.83 o 17 0 2 1097.08 1096.45 33.98 o 18 0 2 1265.57 1266.05 84.99 o 19 0 2 313.23 435.15 97.15 o 20 0 2 1097.60 1117.78 37.66 o 21 0 2 16.62 105.28 32.04 o 22 0 2 1816.05 1524.90 66.16 o 23 0 2 2434.09 2143.62 82.73 o 24 0 2 4504.74 4996.78 165.01 o 25 0 2 1562.09 1923.25 86.64 o 1 1 2 638.96 643.92 12.81 o 2 1 2 1044.00 1023.18 22.80 o 3 1 2 1672.34 1735.95 40.37 o 4 1 2 182.25 181.08 5.63 o 5 1 2 6572.79 6754.99 99.94 o 6 1 2 1254.55 1309.87 31.22 o 7 1 2 3109.90 3583.12 72.88 o 8 1 2 577.99 663.61 13.93 o 9 1 2 156.08 151.21 13.16 o 10 1 2 29.12 39.06 17.86 o 11 1 2 1426.83 1368.36 23.28 o 12 1 2 278.56 292.21 12.90 o 13 1 2 534.12 501.27 14.94 o 14 1 2 101.32 97.48 15.45 o 15 1 2 1.17 -6.05 8.01 o 16 1 2 0.06 -15.83 15.83 o 17 1 2 1.53 38.16 17.64 o 18 1 2 0.80 -14.38 18.35 o 19 1 2 146.78 123.80 14.62 o 20 1 2 130.68 107.26 23.46 o 21 1 2 60.04 70.32 15.82 o 22 1 2 0.22 57.80 24.06 o 23 1 2 22.22 124.46 22.63 o 24 1 2 17.09 70.95 23.35 o 25 1 2 11.94 -19.28 19.28 o 0 2 2 230534.75 267411.06 4740.79 o 1 2 2 28432.19 31788.13 403.91 o 2 2 2 2634.11 2575.79 39.42 o 3 2 2 38.68 51.81 6.20 o 4 2 2 143.69 129.90 8.67 o 5 2 2 7255.49 7616.13 102.97 o 6 2 2 864.12 634.63 14.64 o 7 2 2 4105.68 3990.85 56.60 o 8 2 2 329.61 393.83 11.06 o 9 2 2 22.11 60.42 18.20 o 10 2 2 4575.39 4444.01 82.84 o 11 2 2 3508.51 3509.79 52.73 o 12 2 2 7258.90 7206.65 99.82 o 13 2 2 3334.57 3200.04 50.43 o 14 2 2 1125.20 1005.45 22.51 o 15 2 2 64.21 95.22 20.43 o 16 2 2 878.43 790.12 64.90 o 17 2 2 1430.91 1285.82 37.29 o 18 2 2 6015.07 5707.06 85.69 o 19 2 2 654.19 576.30 22.76 o 20 2 2 414.95 400.05 61.27 o 21 2 2 14.58 -19.95 36.31 o 22 2 2 860.46 858.70 28.67 o 23 2 2 1705.80 1553.86 44.41 o 24 2 2 3187.51 3119.82 103.28 o 1 3 2 1886.56 2085.97 34.53 o 2 3 2 1111.27 1048.59 39.45 o 3 3 2 11.27 -1.64 16.98 o 4 3 2 1555.73 1494.80 39.76 o 5 3 2 1129.65 1278.82 35.26 o 6 3 2 0.61 0.87 13.92 o 7 3 2 13.47 4.93 10.97 o 8 3 2 721.56 807.35 18.99 o 9 3 2 20.69 41.68 24.30 o 10 3 2 24.72 61.06 34.81 o 11 3 2 8.74 58.15 22.13 o 12 3 2 0.26 50.79 21.34 o 13 3 2 1355.36 1366.28 28.56 o 14 3 2 1263.80 1314.25 28.51 o 15 3 2 5.04 -29.64 37.67 o 16 3 2 6.42 35.97 26.13 o 17 3 2 468.93 444.07 36.16 o 18 3 2 15.42 38.69 14.84 o 19 3 2 438.35 427.64 23.63 o 20 3 2 352.95 334.42 22.75 o 21 3 2 45.06 71.63 63.76 o 22 3 2 0.60 -31.34 58.15 o 23 3 2 25.72 179.50 54.30 o 0 4 2 35514.88 38315.91 694.83 o 1 4 2 5349.13 5983.26 163.20 o 2 4 2 308.03 291.51 20.31 o 3 4 2 133.06 136.26 10.89 o 4 4 2 2797.43 2835.85 50.33 o 5 4 2 3521.06 3694.80 70.36 o 6 4 2 2595.72 2761.57 60.92 o 7 4 2 2137.40 2220.46 39.16 o 8 4 2 791.57 885.10 23.19 o 9 4 2 2.14 25.94 28.89 o 10 4 2 2582.38 2619.73 45.07 o 11 4 2 1836.60 2099.25 39.12 o 12 4 2 4446.27 4502.85 91.84 o 13 4 2 1866.93 1813.72 36.08 o 14 4 2 721.79 754.63 28.15 o 15 4 2 11.78 9.68 31.73 o 16 4 2 328.63 327.54 20.44 o 17 4 2 465.11 507.38 50.68 o 18 4 2 2432.61 2919.36 63.65 o 19 4 2 325.27 418.78 28.04 o 20 4 2 50.08 153.65 105.05 o 21 4 2 43.22 79.21 62.12 o 22 4 2 917.57 1101.84 40.96 o 1 5 2 8.76 47.16 20.48 o 2 5 2 190.91 178.31 29.95 o 3 5 2 0.96 42.58 14.51 o 4 5 2 419.39 411.11 17.72 o 5 5 2 6.55 -5.20 28.87 o 6 5 2 8.29 -2.58 15.64 o 7 5 2 0.49 -25.27 25.27 o 8 5 2 722.52 677.84 32.54 o 9 5 2 1770.27 2028.28 65.78 o 10 5 2 157.10 190.52 28.90 o 11 5 2 24.00 38.42 34.74 o 12 5 2 2.35 21.95 43.34 o 13 5 2 50.61 36.88 20.41 o 14 5 2 441.06 410.93 33.63 o 15 5 2 103.18 125.46 57.70 o 16 5 2 1.55 -37.12 37.12 o 17 5 2 141.09 189.98 57.86 o 18 5 2 16.31 17.39 43.81 o 19 5 2 205.40 221.73 46.19 o 20 5 2 238.83 279.73 55.81 o 0 6 2 6776.43 6631.49 141.80 o 1 6 2 1225.51 1202.33 46.66 o 2 6 2 1038.47 1099.13 38.08 o 3 6 2 10.48 9.38 30.84 o 4 6 2 125.10 116.05 20.70 o 5 6 2 628.32 704.67 30.72 o 6 6 2 1134.48 1375.28 41.62 o 7 6 2 458.19 504.98 30.63 o 8 6 2 25.21 36.80 34.14 o 9 6 2 0.56 4.13 23.79 o 10 6 2 817.92 911.38 43.61 o 11 6 2 569.49 757.31 63.44 o 12 6 2 1705.43 1936.28 85.07 o 13 6 2 498.83 521.95 39.11 o 14 6 2 19.66 -4.14 16.73 o 15 6 2 29.90 6.02 23.03 o 16 6 2 94.69 180.34 29.74 o 17 6 2 93.27 -17.17 54.51 o 18 6 2 646.83 694.89 40.87 o 1 7 2 74.89 20.95 38.53 o 2 7 2 71.91 32.31 52.47 o 3 7 2 34.17 37.51 30.80 o 4 7 2 112.64 107.25 20.89 o 5 7 2 9.78 -28.28 33.19 o 6 7 2 2.65 16.80 15.24 o 7 7 2 1.43 -26.45 58.74 o 8 7 2 58.08 50.91 36.52 o 9 7 2 3.07 15.20 17.02 o 10 7 2 20.74 89.93 38.72 o 11 7 2 36.68 25.97 36.37 o 12 7 2 3.74 87.56 69.14 o 13 7 2 90.07 112.55 51.29 o 14 7 2 155.66 90.97 47.29 o 0 8 2 898.05 766.90 42.31 o 1 8 2 165.26 187.72 31.59 o 2 8 2 158.07 79.38 81.64 o 3 8 2 1.93 -45.77 45.77 o 4 8 2 342.74 308.17 54.94 o 5 8 2 95.48 108.72 38.89 o 6 8 2 16.52 46.16 35.22 o 7 8 2 66.49 84.99 31.09 o 8 8 2 110.81 29.32 56.08 o 1 1 3 32166.71 36029.88 453.72 o 2 1 3 1877.67 2487.92 89.92 o 3 1 3 10003.59 11410.99 174.98 o 4 1 3 22.48 60.66 11.39 o 5 1 3 4994.91 5034.05 54.46 o 6 1 3 73.08 53.07 7.29 o 7 1 3 2621.89 2505.56 33.79 o 8 1 3 62.17 109.29 7.89 o 9 1 3 42845.04 42532.82 481.80 o 10 1 3 9051.64 8744.15 103.97 o 11 1 3 747.14 606.79 14.13 o 12 1 3 117.35 127.09 22.49 o 13 1 3 3390.89 3272.23 49.35 o 14 1 3 1460.66 1363.68 27.25 o 15 1 3 20525.56 18397.70 273.99 o 16 1 3 14.36 19.98 38.53 o 17 1 3 1332.18 1260.12 26.98 o 18 1 3 3.17 -5.37 9.25 o 19 1 3 1536.97 1551.84 63.63 o 20 1 3 216.40 308.65 28.80 o 21 1 3 7501.00 7062.47 149.60 o 22 1 3 1236.08 1380.35 89.27 o 23 1 3 480.66 512.54 121.61 o 24 1 3 17.05 -18.62 18.62 o 25 1 3 1408.84 1458.70 139.53 o 0 2 3 4449.08 4856.90 192.41 o 1 2 3 374.66 346.16 23.95 o 2 2 3 3326.15 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13 249.74 325.61 17.96 o 5 1 13 1278.53 1357.61 44.03 o 6 1 13 298.78 263.72 25.64 o 7 1 13 858.49 859.97 35.00 o 8 1 13 1114.03 1175.17 41.34 o 9 1 13 3325.18 3582.75 53.36 o 10 1 13 606.93 699.52 40.47 o 11 1 13 395.26 423.02 23.52 o 12 1 13 0.04 10.74 14.02 o 13 1 13 859.71 825.46 64.62 o 14 1 13 73.20 76.20 40.76 o 15 1 13 1730.24 1635.27 95.74 o 16 1 13 2.63 177.50 117.05 o 17 1 13 223.15 291.14 30.33 o 18 1 13 44.16 115.56 95.47 o 19 1 13 924.64 1080.76 140.48 o 0 2 13 17.40 -16.85 16.85 o 1 2 13 3.51 -3.48 15.21 o 2 2 13 24.11 53.79 11.92 o 3 2 13 41.68 9.28 40.43 o 4 2 13 140.17 134.11 14.97 o 5 2 13 0.60 9.96 22.92 o 6 2 13 89.04 122.51 18.12 o 7 2 13 4.65 7.87 24.65 o 8 2 13 63.80 25.25 27.44 o 9 2 13 1.21 12.30 17.86 o 10 2 13 93.54 108.41 22.13 o 11 2 13 23.28 76.21 38.24 o 12 2 13 98.97 67.14 24.32 o 13 2 13 3.12 -11.63 12.92 o 14 2 13 162.75 192.99 39.88 o 15 2 13 31.14 40.13 20.83 o 16 2 13 35.53 101.38 27.50 o 17 2 13 37.58 30.26 24.73 o 18 2 13 4.60 128.29 29.20 o 19 2 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