#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/41/2014186.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2014186_Fobs loop_ _publ_author_name 'Harvey, Miguel Angel' 'Baggio, Sergio' 'Iba\~nez, Andr\'es' 'Baggio, Ricardo' _publ_section_title ; Bis(acetato-\k^2^O,O')(2,9-dimethyl-1,10-phenanthroline-\k^2^N,N')mercury(II) in two differently hydrated crystal forms ; _journal_issue 8 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first m382 _journal_page_last m385 _journal_volume 60 _journal_year 2004 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 93.110 _cell_angle_beta 90.850 _cell_angle_gamma 118.930 _cell_length_a 13.7384 _cell_length_b 14.0765 _cell_length_c 20.6146 _exptl_crystal_F_000 1832.00 _reflns_d_resolution_high 0.7567 _[local]_cod_data_source_file hj1012IIsup3.hkl _[local]_cod_data_source_block II #BEGIN Tags that were not found in dictionaries: _shelx_title ' hg_1 in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 739.12 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 112590.65 70537.34 2113.47 o 2 0 0 8882.23 8684.55 227.02 o 3 0 0 3598.21 3739.84 121.18 o 4 0 0 19484.17 20217.06 522.69 o 5 0 0 1103.45 1152.57 59.03 o 6 0 0 100.76 157.81 44.84 o 7 0 0 356.44 417.34 48.50 o 8 0 0 8689.24 8569.67 258.44 o 9 0 0 8920.07 9749.88 293.21 o 10 0 0 406.58 496.71 94.30 o 11 0 0 957.58 992.96 119.70 o 12 0 0 2069.80 2464.66 575.06 o 13 0 0 2028.99 2148.76 242.44 o 14 0 0 3.67 174.81 149.90 o 15 0 0 30.86 162.95 175.21 o -15 1 0 255.17 78.70 156.22 o -14 1 0 6.97 -70.79 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3 0 82.40 156.62 124.58 o -12 3 0 125.04 162.55 131.70 o -11 3 0 193.08 118.45 55.56 o -10 3 0 6785.99 6610.89 218.71 o -9 3 0 5489.56 6066.73 319.50 o -8 3 0 6496.00 6452.29 200.63 o -7 3 0 3286.36 3462.43 121.87 o -6 3 0 66971.88 69335.45 1745.38 o -5 3 0 26450.51 28467.02 727.38 o -4 3 0 18360.96 20538.45 527.33 o -3 3 0 238.89 195.39 22.16 o -2 3 0 28439.69 27718.47 699.02 o -1 3 0 2204.67 2611.75 77.91 o 0 3 0 1669.11 1402.44 50.05 o 1 3 0 158.55 185.02 39.70 o 2 3 0 24568.07 25372.53 648.30 o 3 3 0 63488.75 62554.48 1572.39 o 4 3 0 3490.53 3476.92 117.70 o 5 3 0 5829.73 6166.77 188.92 o 6 3 0 5851.92 5868.99 187.14 o 7 3 0 22320.71 22123.88 593.15 o 8 3 0 669.52 828.04 176.79 o 9 3 0 501.44 753.18 180.35 o 10 3 0 27.41 -5.29 73.43 o 11 3 0 111.89 124.93 84.44 o 12 3 0 228.39 324.18 105.62 o 13 3 0 59.43 16.89 111.82 o 14 3 0 44.39 -128.14 161.76 o -16 4 0 816.58 906.09 242.44 o -15 4 0 1097.10 1047.29 230.58 o -14 4 0 17.88 -89.78 109.16 o -13 4 0 14.75 -83.06 83.06 o -12 4 0 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559.09 722.89 101.54 o -9 5 0 5733.13 6081.01 198.89 o -8 5 0 1574.88 1624.47 81.82 o -7 5 0 12280.44 12906.63 356.81 o -6 5 0 42382.38 44482.28 1132.57 o -5 5 0 1678.12 1547.64 98.17 o -4 5 0 11662.48 11553.93 310.43 o -3 5 0 3257.12 2957.75 97.89 o -2 5 0 52739.51 53432.80 1156.91 o -1 5 0 147.45 93.13 23.36 o 0 5 0 43731.38 45790.45 1155.16 o 1 5 0 10511.51 11156.98 302.92 o 2 5 0 4425.33 4444.27 141.91 o 3 5 0 7077.92 6879.56 204.82 o 4 5 0 843.04 806.32 60.00 o 5 5 0 573.23 603.22 58.97 o 6 5 0 5040.65 5393.52 184.01 o 7 5 0 4654.73 4319.70 236.31 o 8 5 0 1128.76 1189.18 117.21 o 9 5 0 2117.08 1989.29 151.89 o 10 5 0 230.61 242.84 165.32 o 11 5 0 263.88 460.76 194.59 o 12 5 0 128.80 379.68 204.87 o -16 6 0 880.05 779.53 215.55 o -15 6 0 755.75 1235.94 238.09 o -14 6 0 395.88 332.22 170.07 o -13 6 0 48.54 -110.74 123.00 o -12 6 0 13789.14 13604.92 524.36 o -11 6 0 6392.39 6751.69 389.37 o -10 6 0 308.09 309.65 79.03 o -9 6 0 68.62 51.19 43.64 o -8 6 0 520.44 490.64 51.47 o -7 6 0 1614.87 1483.09 74.74 o -6 6 0 1400.19 1519.12 165.00 o -5 6 0 184.06 213.18 35.94 o -4 6 0 16822.50 18143.16 475.42 o -3 6 0 82883.63 81573.40 2041.88 o -2 6 0 9265.76 9704.02 227.08 o -1 6 0 9639.96 10037.98 275.67 o 0 6 0 459.37 450.50 39.26 o 1 6 0 24100.76 24307.92 633.08 o 2 6 0 1980.42 1924.75 84.16 o 3 6 0 2439.97 2556.26 244.74 o 4 6 0 14.59 17.07 40.64 o 5 6 0 1767.15 1655.25 179.56 o 6 6 0 1873.35 2198.42 139.14 o 7 6 0 646.20 751.93 99.18 o 8 6 0 410.75 387.20 162.55 o 9 6 0 1859.78 2213.23 249.17 o 10 6 0 1527.22 1743.77 253.91 o 11 6 0 18.74 252.33 181.14 o -17 7 0 34.78 -45.88 149.50 o -16 7 0 30.75 -18.98 156.62 o -15 7 0 686.59 615.01 206.85 o -14 7 0 74.46 96.11 153.45 o -13 7 0 3979.66 3627.94 213.16 o -12 7 0 2514.64 2614.32 291.29 o -11 7 0 1256.78 1362.76 133.50 o -10 7 0 228.97 176.24 77.16 o -9 7 0 20603.49 22195.56 603.60 o -8 7 0 11868.02 11562.69 338.07 o -7 7 0 1951.82 1944.82 90.14 o -6 7 0 7328.02 6682.19 202.75 o -5 7 0 1094.81 1233.91 69.14 o -4 7 0 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