#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2014296.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2014296_Fobs loop_ _publ_author_name 'Mohanu, Antoneta' 'Trombe, Jean-Christian' _publ_section_title ; VF(C~4~O~4~)(H~2~O)~2~: a new layer type of diaquavanadium(III) fluoride squarate ; _journal_coeditor_code AV1268 _journal_issue 1 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first m16 _journal_page_last m18 _journal_volume 62 _journal_year 2006 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 102.019 _cell_angle_gamma 90.000 _cell_length_a 3.7790 _cell_length_b 11.2070 _cell_length_c 7.8410 _exptl_crystal_F_000 216.00 _reflns_d_resolution_high 0.6710 _[local]_cod_data_source_file av1268Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title 'VF(H2O)2_(C4O4) en P21/n - Sortav' _shelx_refln_list_code 4 _shelx_f_calc_maximum 59.25 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 2923.06 3010.52 39.49 o 4 0 0 145.61 147.76 11.75 o 2 1 0 154.36 170.03 7.62 o 3 1 0 138.82 146.63 5.07 o 4 1 0 2.15 0.29 6.47 o 5 1 0 4.08 -0.04 25.69 o 1 2 0 1025.35 1039.76 24.63 o 2 2 0 1996.93 2043.53 35.80 o 3 2 0 24.47 25.84 4.67 o 4 2 0 105.73 108.94 7.22 o 5 2 0 0.01 -6.41 21.55 o 1 3 0 72.15 72.08 2.30 o 2 3 0 416.65 442.57 9.05 o 3 3 0 151.24 146.53 7.49 o 4 3 0 44.87 41.52 6.64 o 5 3 0 9.63 17.65 24.05 o 0 4 0 1373.19 1259.01 24.98 o 1 4 0 56.77 48.73 2.39 o 2 4 0 970.70 959.09 18.28 o 3 4 0 373.40 365.94 9.66 o 4 4 0 200.41 194.01 9.87 o 5 4 0 8.62 -19.39 42.03 o 1 5 0 717.24 674.59 14.03 o 2 5 0 316.33 333.65 10.53 o 3 5 0 183.82 177.14 5.54 o 4 5 0 70.40 61.56 11.50 o 5 5 0 91.49 93.36 31.66 o 0 6 0 2560.55 2564.68 52.41 o 1 6 0 210.30 215.10 6.31 o 2 6 0 698.77 662.38 9.69 o 3 6 0 44.05 40.19 4.16 o 4 6 0 405.78 418.44 18.57 o 5 6 0 1.97 23.34 29.85 o 1 7 0 67.89 62.55 4.36 o 2 7 0 24.33 20.08 3.52 o 3 7 0 291.06 283.66 9.24 o 4 7 0 3.70 6.92 11.56 o 5 7 0 77.45 120.37 32.47 o 0 8 0 4.84 15.07 5.83 o 1 8 0 0.14 2.42 3.80 o 2 8 0 424.48 387.99 8.20 o 3 8 0 28.50 18.12 5.68 o 4 8 0 187.61 218.23 16.55 o 1 9 0 0.79 -2.77 4.91 o 2 9 0 73.79 72.05 5.95 o 3 9 0 102.78 101.40 9.92 o 4 9 0 1.22 -4.62 16.59 o 0 10 0 299.69 293.85 15.84 o 1 10 0 97.42 94.59 8.85 o 2 10 0 209.30 200.06 9.05 o 3 10 0 0.72 4.57 9.06 o 4 10 0 75.82 88.10 20.68 o 1 11 0 340.41 330.97 16.62 o 2 11 0 2.33 5.44 8.17 o 3 11 0 52.99 54.72 12.06 o 4 11 0 5.72 22.56 21.97 o 0 12 0 826.38 751.57 47.69 o 1 12 0 3.66 3.14 12.32 o 2 12 0 238.03 242.16 14.03 o 3 12 0 0.29 11.11 12.49 o 1 13 0 193.68 191.52 18.27 o 2 13 0 0.03 -6.78 10.21 o 3 13 0 55.64 41.58 14.83 o 0 14 0 87.33 84.89 25.12 o 1 14 0 0.23 -1.10 17.28 o 2 14 0 112.90 118.61 16.80 o 3 14 0 0.21 4.26 17.13 o 1 15 0 29.22 23.79 16.85 o 2 15 0 0.67 -9.84 19.12 o 0 16 0 86.80 81.67 39.35 o 1 16 0 0.51 2.44 22.32 o -5 0 1 86.93 65.06 31.82 o -3 0 1 1008.50 1080.69 18.37 o 1 0 1 144.38 116.44 6.34 o 3 0 1 27.12 28.06 6.52 o 5 0 1 31.22 -3.69 27.67 o -5 1 1 0.21 -1.14 18.42 o -4 1 1 437.84 435.55 35.51 o -3 1 1 15.51 17.86 2.53 o -2 1 1 2676.77 2671.60 21.39 o 1 1 1 1068.73 1067.78 19.72 o 2 1 1 418.82 376.91 7.02 o 3 1 1 19.94 25.17 4.47 o 4 1 1 116.80 140.66 10.22 o 5 1 1 8.25 -24.05 26.87 o -5 2 1 56.41 34.69 24.10 o -4 2 1 0.59 -3.34 5.90 o -3 2 1 84.52 87.60 3.40 o -2 2 1 371.54 389.20 6.66 o -1 2 1 288.00 290.24 5.03 o 1 2 1 422.49 468.40 6.43 o 2 2 1 162.41 159.58 3.93 o 3 2 1 1.45 2.08 4.61 o 4 2 1 45.22 38.04 10.23 o 5 2 1 30.38 15.30 22.71 o -5 3 1 1.84 -5.12 25.83 o -4 3 1 139.40 154.75 10.03 o -3 3 1 13.73 14.70 2.31 o -2 3 1 422.65 392.18 8.06 o -1 3 1 496.44 516.23 9.00 o 0 3 1 1142.48 1095.61 23.55 o 1 3 1 209.21 209.91 4.16 o 2 3 1 11.09 6.92 1.68 o 3 3 1 84.31 81.70 5.97 o 4 3 1 125.63 133.86 10.34 o 5 3 1 8.09 6.45 28.40 o -5 4 1 30.12 22.17 19.44 o -4 4 1 9.09 -3.68 9.04 o -3 4 1 50.56 55.41 2.94 o -2 4 1 1.68 1.81 1.86 o -1 4 1 200.67 182.26 3.87 o 0 4 1 2459.73 2578.94 26.73 o 1 4 1 57.62 48.51 2.31 o 2 4 1 14.52 13.72 2.61 o 3 4 1 40.98 41.48 5.73 o 4 4 1 24.62 22.60 9.08 o 5 4 1 6.28 14.03 29.81 o -5 5 1 0.00 0.98 18.28 o -4 5 1 223.51 232.47 13.52 o -3 5 1 6.80 8.02 2.95 o -2 5 1 1100.98 1108.79 18.70 o -1 5 1 298.31 326.65 9.33 o 0 5 1 1904.24 1772.76 32.74 o 1 5 1 657.98 686.88 11.06 o 2 5 1 1449.50 1416.77 27.19 o 3 5 1 17.21 17.28 3.14 o 4 5 1 53.47 64.40 16.28 o 5 5 1 1.18 -20.62 26.18 o -5 6 1 25.79 27.27 23.19 o -4 6 1 0.07 6.12 6.37 o -3 6 1 317.02 303.48 6.87 o -2 6 1 99.56 104.41 3.68 o -1 6 1 393.77 391.16 10.44 o 0 6 1 79.10 87.77 4.38 o 1 6 1 1561.83 1616.41 36.33 o 2 6 1 0.15 2.49 3.07 o 3 6 1 135.67 133.23 6.31 o 4 6 1 4.47 -0.09 12.17 o -5 7 1 0.71 -35.42 29.25 o -4 7 1 111.41 92.62 10.56 o -3 7 1 3.95 -0.59 4.41 o -2 7 1 594.25 567.80 9.08 o -1 7 1 86.97 84.84 3.92 o 0 7 1 1715.05 1765.91 31.06 o 1 7 1 85.69 88.88 4.65 o 2 7 1 830.64 829.35 11.73 o 3 7 1 0.13 -0.42 4.32 o 4 7 1 58.26 51.25 13.57 o -4 8 1 1.05 -8.83 15.42 o -3 8 1 0.48 1.40 5.12 o -2 8 1 10.90 10.81 4.37 o -1 8 1 217.85 233.13 8.69 o 0 8 1 6.54 6.09 4.11 o 1 8 1 216.46 216.83 7.12 o 2 8 1 1.59 -2.81 4.29 o 3 8 1 73.47 80.08 7.18 o 4 8 1 3.93 18.94 15.67 o -4 9 1 49.53 50.47 17.02 o -3 9 1 0.15 3.07 7.08 o -2 9 1 26.33 20.53 6.35 o -1 9 1 2.02 0.79 4.89 o 0 9 1 452.34 451.31 9.85 o 1 9 1 72.26 77.05 5.99 o 2 9 1 233.12 226.59 9.39 o 3 9 1 1.96 2.72 8.35 o 4 9 1 105.36 105.31 19.61 o -4 10 1 12.67 13.07 18.37 o -3 10 1 32.22 28.66 9.52 o -2 10 1 12.78 8.72 6.77 o -1 10 1 7.69 12.30 6.47 o 0 10 1 53.71 62.31 7.60 o 1 10 1 152.85 158.52 10.06 o 2 10 1 36.01 38.63 7.37 o 3 10 1 141.94 143.12 11.19 o 4 10 1 8.26 22.28 18.85 o -4 11 1 128.98 171.81 24.79 o -3 11 1 12.65 11.09 10.36 o -2 11 1 231.43 237.83 14.18 o -1 11 1 0.80 1.08 7.90 o 0 11 1 195.62 187.46 10.73 o 1 11 1 12.54 16.87 11.28 o 2 11 1 471.51 492.11 15.05 o 3 11 1 22.24 29.79 10.58 o 4 11 1 81.47 108.37 43.81 o -3 12 1 163.98 164.58 16.27 o -2 12 1 28.71 19.83 13.81 o -1 12 1 144.30 146.49 9.85 o 0 12 1 28.19 32.37 11.41 o 1 12 1 236.88 221.45 15.41 o 2 12 1 0.19 5.68 11.63 o 3 12 1 87.04 89.43 13.70 o -3 13 1 20.70 18.61 15.25 o -2 13 1 229.72 215.14 16.90 o -1 13 1 1.78 -3.90 11.27 o 0 13 1 289.52 299.94 25.75 o 1 13 1 58.50 78.51 17.19 o 2 13 1 99.04 90.21 12.71 o 3 13 1 0.07 -6.81 17.81 o -3 14 1 22.60 -15.68 24.26 o -2 14 1 11.47 10.71 15.92 o -1 14 1 144.97 140.16 20.40 o 0 14 1 7.93 6.36 15.32 o 1 14 1 26.90 7.94 12.13 o 2 14 1 8.59 -7.70 13.52 o -2 15 1 65.66 75.42 17.27 o -1 15 1 0.79 2.50 20.53 o 0 15 1 97.79 94.08 23.72 o 1 15 1 1.27 -23.66 15.77 o 2 15 1 44.78 65.51 17.99 o -1 16 1 64.75 52.66 26.76 o 0 16 1 14.21 19.01 17.50 o 1 16 1 67.84 86.33 27.90 o -4 0 2 282.29 320.50 28.96 o -2 0 2 3510.15 3648.61 56.78 o 2 0 2 622.63 624.59 16.34 o 4 0 2 298.81 272.09 38.70 o -5 1 2 16.79 -2.84 21.65 o -4 1 2 2.13 8.80 10.63 o -3 1 2 293.78 294.98 5.46 o -2 1 2 207.64 215.11 4.02 o -1 1 2 1229.49 1244.00 12.00 o 1 1 2 82.11 80.22 3.43 o 2 1 2 367.68 373.22 5.49 o 3 1 2 245.07 233.15 15.89 o 4 1 2 4.90 6.51 9.96 o 5 1 2 52.06 13.37 31.04 o -5 2 2 4.13 0.35 16.56 o -4 2 2 210.09 214.51 15.65 o -3 2 2 44.52 48.03 2.61 o -2 2 2 622.54 584.05 11.14 o -1 2 2 5.34 4.42 1.19 o 0 2 2 1065.38 1042.85 22.62 o 1 2 2 177.43 176.43 3.86 o 2 2 2 1295.29 1292.29 17.18 o 3 2 2 91.43 78.42 7.32 o 4 2 2 243.30 226.04 18.37 o 5 2 2 0.25 7.32 23.05 o -5 3 2 1.50 4.87 23.08 o -4 3 2 16.08 14.10 6.73 o -3 3 2 60.88 60.28 3.04 o -2 3 2 49.19 47.97 2.04 o -1 3 2 346.42 407.15 9.24 o 0 3 2 0.31 -2.84 1.89 o 1 3 2 791.31 830.85 10.33 o 2 3 2 13.44 13.74 2.00 o 3 3 2 201.72 203.60 11.26 o 4 3 2 0.67 4.89 9.63 o 5 3 2 72.03 4.29 23.45 o -5 4 2 26.53 11.18 20.49 o -4 4 2 80.16 87.18 6.83 o -3 4 2 28.36 27.14 2.95 o -2 4 2 386.99 370.12 6.91 o -1 4 2 229.12 230.89 4.84 o 0 4 2 1369.43 1380.68 17.03 o 1 4 2 4.05 5.89 1.61 o 2 4 2 989.11 972.70 17.14 o 3 4 2 15.80 7.14 7.10 o 4 4 2 262.89 254.89 21.28 o 5 4 2 0.00 -56.19 48.23 o -5 5 2 17.34 23.39 18.63 o -4 5 2 17.81 13.47 5.60 o -3 5 2 23.15 29.00 3.16 o -2 5 2 191.98 183.21 5.63 o -1 5 2 1034.17 1045.05 22.43 o 0 5 2 0.04 0.64 2.38 o 1 5 2 266.92 251.30 6.30 o 2 5 2 7.43 6.90 2.85 o 3 5 2 245.80 236.79 8.91 o 4 5 2 0.04 -5.81 12.64 o -5 6 2 1.45 -9.92 23.73 o -4 6 2 88.95 85.79 7.86 o -3 6 2 14.18 14.75 3.37 o -2 6 2 944.45 929.56 18.53 o -1 6 2 0.66 9.71 2.49 o 0 6 2 2242.75 2187.00 35.72 o 1 6 2 63.36 60.64 3.36 o 2 6 2 633.26 614.24 9.58 o 3 6 2 44.80 44.92 4.73 o 4 6 2 196.47 193.39 25.28 o -5 7 2 25.54 33.44 31.00 o -4 7 2 0.01 0.14 8.31 o -3 7 2 37.17 35.65 4.26 o -2 7 2 176.66 168.83 6.13 o -1 7 2 421.77 396.10 9.62 o 0 7 2 42.83 44.02 3.83 o 1 7 2 578.49 548.50 9.44 o 2 7 2 341.23 343.74 7.70 o 3 7 2 142.12 137.26 7.40 o 4 7 2 5.78 0.45 13.33 o -4 8 2 68.47 70.38 10.39 o -3 8 2 9.45 6.60 6.01 o -2 8 2 128.98 132.90 5.86 o -1 8 2 195.58 186.49 5.62 o 0 8 2 897.78 870.14 13.71 o 1 8 2 260.59 257.60 7.15 o 2 8 2 609.54 584.24 11.86 o 3 8 2 45.38 31.28 7.92 o 4 8 2 59.91 63.28 16.40 o -4 9 2 1.28 12.75 12.47 o -3 9 2 22.90 26.17 6.88 o -2 9 2 6.02 0.97 5.26 o -1 9 2 39.86 47.50 4.95 o 0 9 2 249.74 238.12 9.49 o 1 9 2 458.38 445.77 17.07 o 2 9 2 10.16 17.75 6.63 o 3 9 2 34.89 51.38 9.25 o 4 9 2 0.06 -4.11 19.75 o -4 10 2 38.42 53.47 20.95 o -3 10 2 0.94 -0.63 9.01 o -2 10 2 298.77 299.94 11.84 o -1 10 2 36.38 33.50 6.37 o 0 10 2 597.18 588.22 17.35 o 1 10 2 7.55 1.40 7.28 o 2 10 2 166.63 177.02 9.91 o 3 10 2 12.89 12.86 9.73 o 4 10 2 44.73 58.48 31.98 o -4 11 2 1.92 -18.35 18.33 o -3 11 2 90.55 98.80 11.54 o -2 11 2 13.86 18.74 10.20 o -1 11 2 574.61 565.48 20.19 o 0 11 2 8.81 12.65 9.27 o 1 11 2 82.50 88.94 12.93 o 2 11 2 15.85 21.18 8.74 o 3 11 2 31.36 33.20 10.84 o -3 12 2 46.14 53.47 12.59 o -2 12 2 448.00 431.10 36.23 o -1 12 2 38.11 48.11 9.97 o 0 12 2 419.39 408.13 19.13 o 1 12 2 1.57 16.10 12.10 o 2 12 2 88.60 97.83 12.24 o 3 12 2 1.06 5.90 16.87 o -3 13 2 152.68 147.33 17.62 o -2 13 2 118.88 109.81 15.19 o -1 13 2 141.93 101.76 14.60 o 0 13 2 5.42 21.28 14.48 o 1 13 2 94.35 100.74 15.16 o 2 13 2 11.01 21.84 12.55 o 3 13 2 11.75 11.05 18.95 o -3 14 2 10.40 5.57 21.46 o -2 14 2 102.46 90.66 22.98 o -1 14 2 44.44 23.05 16.43 o 0 14 2 77.27 83.11 15.31 o 1 14 2 7.87 -3.47 17.22 o 2 14 2 64.76 44.87 20.66 o -2 15 2 0.17 3.44 26.85 o -1 15 2 12.41 10.85 20.70 o 0 15 2 9.76 3.11 15.12 o 1 15 2 24.38 34.05 20.69 o 2 15 2 10.00 -4.11 25.62 o -1 16 2 2.95 8.93 30.42 o 0 16 2 30.70 19.01 20.88 o 1 16 2 12.39 8.06 23.97 o -5 0 3 194.13 125.37 29.03 o -3 0 3 152.83 164.44 8.23 o -1 0 3 9.54 21.35 2.06 o 1 0 3 1756.04 1883.40 84.56 o 3 0 3 144.39 149.44 12.75 o -5 1 3 0.15 38.16 18.46 o -4 1 3 448.14 457.45 10.80 o -3 1 3 31.93 29.47 3.20 o -2 1 3 392.07 369.85 6.80 o -1 1 3 1426.57 1575.89 29.49 o 0 1 3 2490.30 2463.56 65.45 o 1 1 3 391.91 384.06 9.90 o 2 1 3 1365.30 1394.90 24.93 o 3 1 3 1.75 6.10 7.36 o 4 1 3 153.46 163.53 13.64 o -5 2 3 71.39 59.24 23.12 o -4 2 3 25.96 19.74 4.15 o -3 2 3 105.14 113.53 4.56 o -2 2 3 22.65 26.59 2.17 o -1 2 3 316.32 300.10 6.54 o 0 2 3 2636.30 2816.02 94.42 o 1 2 3 434.13 417.82 7.20 o 2 2 3 32.04 31.71 2.45 o 3 2 3 340.36 321.16 29.79 o 4 2 3 1.78 -2.50 11.33 o -5 3 3 18.55 11.19 15.04 o -4 3 3 158.71 161.08 6.32 o -3 3 3 43.84 49.07 4.48 o -2 3 3 1534.18 1510.00 24.84 o -1 3 3 86.21 95.08 3.04 o 0 3 3 1274.08 1215.78 25.41 o 1 3 3 246.34 286.14 7.74 o 2 3 3 1069.53 1081.47 25.93 o 3 3 3 3.67 -6.64 6.58 o 4 3 3 147.30 147.35 15.07 o -5 4 3 45.29 28.69 18.25 o -4 4 3 60.53 55.21 6.51 o -3 4 3 236.59 241.09 9.05 o -2 4 3 61.31 68.01 2.68 o -1 4 3 921.42 991.90 23.81 o 0 4 3 81.54 76.44 3.96 o 1 4 3 362.99 377.73 9.41 o 2 4 3 11.52 14.92 3.38 o 3 4 3 73.99 77.79 4.16 o 4 4 3 58.24 57.96 14.50 o -5 5 3 10.16 29.97 20.02 o -4 5 3 444.06 427.41 24.30 o -3 5 3 51.20 49.51 4.04 o -2 5 3 1335.94 1391.16 16.99 o -1 5 3 161.96 170.47 4.67 o 0 5 3 2556.26 2675.51 31.29 o 1 5 3 1.42 1.47 2.33 o 2 5 3 237.18 252.51 6.50 o 3 5 3 51.30 45.18 5.26 o 4 5 3 14.59 51.04 17.30 o -5 6 3 57.48 54.56 30.17 o -4 6 3 7.11 5.61 6.99 o -3 6 3 661.46 633.26 15.26 o -2 6 3 10.40 5.73 3.47 o -1 6 3 956.56 1009.34 20.08 o 0 6 3 70.05 75.98 4.83 o 1 6 3 344.94 351.66 7.03 o 2 6 3 37.21 39.99 4.26 o 3 6 3 11.81 6.83 5.87 o 4 6 3 16.00 6.97 17.27 o -5 7 3 17.65 22.15 25.75 o -4 7 3 274.32 255.52 14.21 o -3 7 3 1.63 -4.73 4.62 o -2 7 3 1678.07 1683.67 29.98 o -1 7 3 193.70 189.09 6.37 o 0 7 3 1185.00 1183.94 17.64 o 1 7 3 4.05 0.43 3.37 o 2 7 3 60.34 57.88 4.58 o 3 7 3 17.81 15.64 6.70 o 4 7 3 21.62 30.77 19.84 o -4 8 3 37.53 31.33 10.41 o -3 8 3 242.38 215.77 12.29 o -2 8 3 6.50 12.12 6.07 o -1 8 3 883.18 843.95 13.16 o 0 8 3 0.06 -1.88 4.54 o 1 8 3 15.11 28.31 4.65 o 2 8 3 50.15 53.25 5.62 o 3 8 3 34.26 37.18 8.81 o 4 8 3 0.54 -15.57 24.81 o -4 9 3 35.92 36.33 12.50 o -3 9 3 39.42 34.57 8.69 o -2 9 3 613.82 612.70 15.53 o -1 9 3 164.69 145.37 7.48 o 0 9 3 369.08 364.26 14.15 o 1 9 3 176.43 193.90 8.30 o 2 9 3 185.18 196.41 9.99 o 3 9 3 15.14 11.25 10.04 o 4 9 3 75.31 65.24 26.62 o -4 10 3 22.00 14.62 18.79 o -3 10 3 28.04 32.60 10.50 o -2 10 3 15.39 11.50 8.70 o -1 10 3 128.34 118.99 10.98 o 0 10 3 607.83 663.15 26.19 o 1 10 3 153.00 166.58 8.39 o 2 10 3 68.16 70.38 8.85 o 3 10 3 66.13 61.50 14.19 o -4 11 3 83.94 115.30 32.31 o -3 11 3 3.33 -0.85 12.21 o -2 11 3 53.87 54.47 12.48 o -1 11 3 165.42 144.94 9.75 o 0 11 3 308.69 301.62 17.55 o 1 11 3 193.05 183.35 11.24 o 2 11 3 170.65 176.30 11.76 o 3 11 3 25.93 18.00 16.86 o -3 12 3 39.91 47.37 16.26 o -2 12 3 0.61 -2.16 14.00 o -1 12 3 20.53 17.65 8.59 o 0 12 3 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