#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2014308.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2014308_Fobs loop_ _publ_author_name 'Chen, Xue-An' 'Zhao, Ying-Hua' 'Chang, Xin-An' 'Zhang, Li' 'Xue, Hai-Ping' _publ_section_title ; Lead zinc borate, PbZn~2~(BO~3~)~2~ ; _journal_coeditor_code BC1089 _journal_issue 1 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first i11 _journal_page_last i12 _journal_volume 62 _journal_year 2006 _space_group_IT_number 56 _symmetry_space_group_name_Hall '-P 2ab 2ac' _symmetry_space_group_name_H-M 'P c c n' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 11.1709 _cell_length_b 4.9674 _cell_length_c 10.5987 _exptl_crystal_F_000 800.00 _reflns_d_resolution_high 0.6204 _[local]_cod_data_source_file bc1089Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' PbZn2B2O6 in Pccn' _shelx_refln_list_code 4 _shelx_f_calc_maximum 407.73 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y+1/2, z' '-x, y+1/2, -z+1/2' 'x+1/2, -y, -z+1/2' '-x, -y, -z' 'x-1/2, y-1/2, -z' 'x, -y-1/2, z-1/2' '-x-1/2, y, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 1117.70 721.50 50.82 o 4 0 0 131225.69 141771.58 1473.90 o 6 0 0 9125.39 8535.47 206.29 o 8 0 0 137374.56 147678.16 1502.80 o 10 0 0 4854.33 4369.88 155.46 o 12 0 0 39407.10 36718.98 543.12 o 14 0 0 4124.95 3827.76 180.38 o 16 0 0 29673.93 31468.14 582.98 o 18 0 0 1657.56 2251.21 217.25 o 1 1 0 61381.73 59115.51 637.79 o 3 1 0 112878.55 107609.76 1279.57 o 5 1 0 50163.35 56022.21 747.41 o 7 1 0 38111.13 43335.09 623.84 o 9 1 0 36565.94 38255.66 562.06 o 11 1 0 22997.62 23534.59 413.57 o 13 1 0 20143.33 19718.79 384.67 o 15 1 0 8350.07 7844.86 265.08 o 17 1 0 11301.53 12551.58 383.67 o 0 2 0 166241.83 152311.13 1558.61 o 2 2 0 11627.74 10455.83 237.18 o 4 2 0 107084.91 101648.38 1326.41 o 6 2 0 17545.74 19660.99 405.60 o 8 2 0 57903.92 68259.88 887.93 o 10 2 0 9370.28 9417.42 257.11 o 12 2 0 31116.45 28986.73 487.31 o 14 2 0 6724.03 6709.79 231.20 o 16 2 0 15272.42 15355.88 381.68 o 1 3 0 32891.07 37398.63 413.57 o 3 3 0 51041.19 44523.98 692.60 o 5 3 0 35704.45 33785.13 651.75 o 7 3 0 25020.06 29319.58 556.08 o 9 3 0 18018.14 20257.92 425.53 o 11 3 0 17622.26 16791.91 368.72 o 13 3 0 13581.51 11156.41 288.00 o 15 3 0 7836.48 6560.31 236.18 o 0 4 0 12455.39 14457.99 411.58 o 2 4 0 37314.43 37798.25 449.45 o 4 4 0 21633.68 16903.53 417.56 o 6 4 0 28272.80 29198.99 628.82 o 8 4 0 8521.68 9611.75 317.90 o 10 4 0 18106.53 18296.71 422.54 o 12 4 0 9008.67 7806.99 254.12 o 14 4 0 10126.67 8244.48 256.11 o 1 5 0 21225.72 27082.32 531.16 o 3 5 0 11525.40 9368.59 226.22 o 5 5 0 11109.96 8246.47 315.91 o 7 5 0 16393.94 16962.32 485.32 o 9 5 0 10055.95 10439.89 345.80 o 11 5 0 7478.65 6580.24 259.10 o 13 5 0 4051.28 3057.42 170.41 o 0 6 0 582.07 874.97 95.67 o 2 6 0 29537.54 31833.88 486.32 o 4 6 0 1084.86 934.77 73.74 o 6 6 0 19354.11 12984.08 424.53 o 8 6 0 1243.13 1180.91 98.66 o 10 6 0 14653.79 13975.66 388.66 o 1 7 0 7201.02 8194.65 364.74 o 3 7 0 3372.12 4316.07 197.32 o 5 7 0 4434.01 2918.90 176.39 o 7 7 0 5363.16 3295.60 224.22 o 0 8 0 103.36 -118.59 250.13 o 1 1 1 2461.43 2452.52 48.83 o 2 1 1 347.99 445.46 37.87 o 3 1 1 4434.29 4543.28 148.49 o 4 1 1 264.78 258.11 31.89 o 5 1 1 2628.93 2140.60 133.54 o 6 1 1 991.16 1140.06 113.61 o 7 1 1 910.93 923.80 73.74 o 8 1 1 55.78 61.79 34.88 o 9 1 1 610.40 730.47 66.77 o 10 1 1 37.01 -78.73 78.73 o 11 1 1 643.74 598.93 54.81 o 12 1 1 0.50 49.83 70.76 o 13 1 1 330.45 380.68 42.85 o 14 1 1 45.54 79.72 82.71 o 15 1 1 224.69 284.02 47.83 o 16 1 1 5.37 -117.59 117.59 o 17 1 1 178.59 93.68 140.51 o 1 2 1 8238.01 8797.57 128.56 o 2 2 1 3524.50 3637.42 107.63 o 3 2 1 11544.78 11573.96 288.00 o 4 2 1 0.78 9.97 87.70 o 5 2 1 10667.49 7661.50 299.96 o 6 2 1 1313.41 1561.60 107.63 o 7 2 1 7456.18 9943.60 314.91 o 8 2 1 1.83 -100.65 100.65 o 9 2 1 6277.55 7687.41 261.10 o 10 2 1 378.60 412.57 44.84 o 11 2 1 4401.22 4459.57 187.35 o 12 2 1 161.98 168.42 40.86 o 13 2 1 2038.89 1735.99 144.50 o 14 2 1 566.56 421.54 46.84 o 15 2 1 751.04 710.54 65.77 o 16 2 1 19.11 45.84 97.66 o 17 2 1 609.77 611.88 62.78 o 1 3 1 11885.43 11949.66 173.40 o 2 3 1 69.71 67.77 45.84 o 3 3 1 5701.96 5984.30 230.20 o 4 3 1 458.26 411.58 56.80 o 5 3 1 4343.68 4715.69 290.99 o 6 3 1 735.02 1273.59 124.57 o 7 3 1 5582.48 8833.44 345.80 o 8 3 1 237.75 487.31 55.81 o 9 3 1 2887.19 3627.45 202.30 o 10 3 1 8.55 38.87 92.68 o 11 3 1 989.71 1262.63 122.58 o 12 3 1 7.68 104.64 82.71 o 13 3 1 748.15 690.61 57.80 o 14 3 1 7.14 88.69 61.79 o 15 3 1 1577.79 1477.89 146.49 o 16 3 1 25.41 42.85 114.60 o 1 4 1 8128.08 8206.61 195.32 o 2 4 1 40.95 8.97 62.78 o 3 4 1 5180.90 5499.97 268.07 o 4 4 1 0.38 120.58 143.50 o 5 4 1 5476.85 8675.99 436.49 o 6 4 1 79.99 109.62 166.42 o 7 4 1 7412.02 12562.54 472.37 o 8 4 1 3.72 147.49 126.56 o 9 4 1 6393.33 8719.84 329.86 o 10 4 1 17.11 -36.87 114.60 o 11 4 1 3013.02 2924.88 177.39 o 12 4 1 128.69 172.40 44.84 o 13 4 1 1625.68 1491.84 128.56 o 14 4 1 43.08 11.96 94.67 o 15 4 1 1087.19 885.94 85.70 o 1 5 1 2538.93 2615.95 200.31 o 2 5 1 114.40 106.63 24.91 o 3 5 1 1291.24 1738.98 160.44 o 4 5 1 90.66 251.13 183.37 o 5 5 1 1191.35 2731.55 259.10 o 6 5 1 80.36 -115.60 250.13 o 7 5 1 1772.46 3360.38 220.24 o 8 5 1 90.32 170.41 75.74 o 9 5 1 624.26 704.56 79.72 o 10 5 1 28.87 -36.87 131.54 o 11 5 1 176.78 239.17 50.82 o 12 5 1 33.73 -23.92 99.66 o 13 5 1 247.88 188.35 44.84 o 14 5 1 24.11 1.99 85.70 o 1 6 1 295.45 610.89 112.61 o 2 6 1 28.62 -117.59 117.59 o 3 6 1 271.74 325.87 132.54 o 4 6 1 0.47 -283.02 365.73 o 5 6 1 350.68 861.02 137.52 o 6 6 1 85.96 376.70 290.99 o 7 6 1 437.48 804.22 123.57 o 8 6 1 19.31 215.26 189.35 o 9 6 1 538.32 668.69 86.70 o 10 6 1 0.92 -90.69 140.51 o 11 6 1 354.53 320.89 61.79 o 1 7 1 141.54 -511.23 511.23 o 2 7 1 9.56 6.98 469.38 o 3 7 1 69.54 4.98 344.81 o 4 7 1 1.69 -76.73 267.08 o 5 7 1 58.80 321.89 142.51 o 6 7 1 32.66 -92.68 269.07 o 7 7 1 70.94 209.28 264.09 o 8 7 1 0.27 -13.95 209.28 o 0 0 2 36995.63 36139.98 310.92 o 1 0 2 24844.34 25566.56 238.18 o 2 0 2 82228.82 80469.64 708.55 o 3 0 2 73589.05 77207.92 766.35 o 4 0 2 2333.42 2107.71 93.68 o 5 0 2 26478.37 25323.40 432.50 o 6 0 2 41106.48 31624.60 556.08 o 7 0 2 24429.86 16506.90 391.65 o 8 0 2 20626.46 16272.71 389.65 o 9 0 2 12901.30 13002.02 335.84 o 10 0 2 17383.17 18835.84 399.62 o 11 0 2 16623.63 17499.46 390.65 o 12 0 2 3521.07 3647.38 187.35 o 13 0 2 8496.33 8251.46 261.10 o 14 0 2 11784.26 11898.84 314.91 o 15 0 2 6845.75 6624.09 250.13 o 16 0 2 3892.19 4087.86 207.28 o 17 0 2 3808.91 3973.26 234.19 o 0 1 2 2213.68 2221.32 42.85 o 1 1 2 30530.59 31781.06 296.97 o 2 1 2 114449.65 120336.73 1021.47 o 3 1 2 34103.21 35247.07 405.60 o 4 1 2 2264.25 2646.84 105.63 o 5 1 2 37047.48 36761.83 576.01 o 6 1 2 94511.08 79159.17 1109.16 o 7 1 2 13280.25 9891.78 308.93 o 8 1 2 344.01 308.93 42.85 o 9 1 2 13339.56 14835.68 380.68 o 10 1 2 42320.80 50803.26 793.26 o 11 1 2 14964.88 17735.65 406.59 o 12 1 2 1495.05 1646.31 145.50 o 13 1 2 6557.05 7257.89 261.10 o 14 1 2 21544.01 23190.78 468.38 o 15 1 2 5617.55 5781.00 236.18 o 16 1 2 620.80 573.02 58.80 o 17 1 2 3542.58 3730.10 232.20 o 0 2 2 15720.23 14949.29 176.39 o 1 2 2 31375.86 33268.91 334.84 o 2 2 2 43596.45 44753.19 448.45 o 3 2 2 32309.98 31658.49 390.65 o 4 2 2 11854.94 12471.86 260.10 o 5 2 2 15396.45 15234.30 349.79 o 6 2 2 26083.53 23110.06 510.23 o 7 2 2 21978.69 17817.37 458.41 o 8 2 2 12225.57 12825.63 381.68 o 9 2 2 14923.27 18060.53 447.45 o 10 2 2 12432.99 15420.66 402.61 o 11 2 2 10744.49 13840.12 366.73 o 12 2 2 5892.60 6508.49 247.15 o 13 2 2 6066.21 6035.12 238.18 o 14 2 2 8160.75 8217.57 272.06 o 15 2 2 5972.65 5971.34 237.18 o 16 2 2 2952.22 2891.00 190.34 o 17 2 2 4446.62 4199.47 221.23 o 0 3 2 25064.93 24624.82 296.97 o 1 3 2 17730.04 17128.75 222.23 o 2 3 2 26633.35 28197.46 339.82 o 3 3 2 17811.55 17956.88 287.01 o 4 3 2 7769.60 7576.79 212.27 o 5 3 2 18045.37 18787.01 426.52 o 6 3 2 21839.48 20130.37 505.25 o 7 3 2 10502.36 8917.15 342.81 o 8 3 2 10926.08 12008.46 415.56 o 9 3 2 9275.52 11363.69 384.67 o 10 3 2 13055.92 15566.15 428.52 o 11 3 2 7839.68 9131.41 313.91 o 12 3 2 3684.95 3883.57 203.30 o 13 3 2 5479.35 5799.94 235.19 o 14 3 2 6980.28 6629.07 252.13 o 15 3 2 4141.95 3649.38 194.33 o 16 3 2 3436.17 2757.46 175.39 o 0 4 2 10807.98 11286.96 217.25 o 1 4 2 14807.31 14295.55 219.24 o 2 4 2 10261.63 12454.92 217.25 o 3 4 2 11842.84 12676.15 254.12 o 4 4 2 15992.95 15566.15 343.81 o 5 4 2 10939.04 10842.49 339.82 o 6 4 2 7920.80 8189.67 346.80 o 7 4 2 9208.67 8189.67 355.77 o 8 4 2 6850.45 8948.05 377.69 o 9 4 2 8768.47 12229.70 435.49 o 10 4 2 5269.47 7021.71 308.93 o 11 4 2 5341.96 5958.39 272.06 o 12 4 2 6711.86 7523.97 279.03 o 13 4 2 4643.88 4621.02 220.24 o 14 4 2 2839.44 2763.44 176.39 o 15 4 2 2879.48 2619.94 171.41 o 0 5 2 20332.60 19607.17 374.70 o 1 5 2 9498.56 8534.48 194.33 o 2 5 2 1311.42 1325.42 85.70 o 3 5 2 5581.56 6343.06 196.32 o 4 5 2 21450.89 19941.02 430.51 o 5 5 2 4851.67 4409.75 244.16 o 6 5 2 921.84 841.09 75.74 o 7 5 2 7010.50 6198.56 344.81 o 8 5 2 13735.45 19101.92 612.88 o 9 5 2 5858.55 9366.60 414.57 o 10 5 2 900.16 1099.20 105.63 o 11 5 2 2285.83 3073.37 216.25 o 12 5 2 8501.69 9191.21 321.89 o 13 5 2 2675.80 2696.67 183.37 o 0 6 2 7512.57 7783.08 289.00 o 1 6 2 4437.33 4258.27 166.42 o 2 6 2 1886.02 2032.97 109.62 o 3 6 2 4472.08 5371.42 190.34 o 4 6 2 7824.43 8482.66 303.95 o 5 6 2 6599.36 6144.74 301.96 o 6 6 2 1843.44 2016.03 164.43 o 7 6 2 2611.72 3007.60 288.00 o 8 6 2 4055.14 6145.74 369.72 o 9 6 2 2747.00 3669.31 296.97 o 10 6 2 1755.40 3054.43 258.11 o 11 6 2 2478.04 3097.29 245.15 o 0 7 2 8922.20 8402.93 337.83 o 1 7 2 2912.43 2551.18 166.42 o 2 7 2 60.93 112.61 77.73 o 3 7 2 2192.63 2575.09 159.45 o 4 7 2 11133.65 12551.58 405.60 o 5 7 2 1524.40 1683.18 141.51 o 6 7 2 67.41 -106.63 192.33 o 7 7 2 2568.81 2804.30 214.26 o 8 7 2 7572.04 12618.35 565.05 o 1 1 3 6203.52 6399.86 93.68 o 2 1 3 3384.37 3650.37 70.76 o 3 1 3 10003.56 9751.27 148.49 o 4 1 3 40.62 85.70 14.95 o 5 1 3 6386.92 7064.56 185.36 o 6 1 3 1025.94 1274.59 102.64 o 7 1 3 1732.71 1874.52 145.50 o 8 1 3 7.44 83.71 73.74 o 9 1 3 1094.52 962.67 85.70 o 10 1 3 204.66 306.94 47.83 o 11 1 3 1553.87 1700.12 115.60 o 12 1 3 0.59 50.82 91.68 o 13 1 3 1199.98 1321.43 103.64 o 14 1 3 157.98 71.75 126.56 o 15 1 3 427.10 442.47 55.81 o 16 1 3 2.14 92.68 78.73 o 17 1 3 251.94 173.40 140.51 o 1 2 3 2426.47 2565.13 64.78 o 2 2 3 253.64 262.09 20.93 o 3 2 3 2791.91 2805.30 80.72 o 4 2 3 109.75 142.51 16.94 o 5 2 3 1082.15 977.62 87.70 o 6 2 3 542.90 733.46 63.78 o 7 2 3 199.88 242.16 40.86 o 8 2 3 2.32 -9.97 101.65 o 9 2 3 626.46 598.93 59.79 o 10 2 3 532.87 542.12 57.80 o 11 2 3 781.11 1022.46 98.66 o 12 2 3 230.92 162.44 117.59 o 13 2 3 265.91 358.76 49.83 o 14 2 3 16.24 -119.59 119.59 o 15 2 3 20.75 90.69 106.63 o 16 2 3 37.22 43.85 78.73 o 17 2 3 146.65 -97.66 145.50 o 1 3 3 19205.06 18173.13 235.19 o 2 3 3 645.88 650.75 46.84 o 3 3 3 23057.76 22737.35 303.95 o 4 3 3 167.68 229.21 22.92 o 5 3 3 16062.21 16503.91 327.87 o 6 3 3 135.59 126.56 35.88 o 7 3 3 6301.18 6532.40 264.09 o 8 3 3 70.06 52.82 106.63 o 9 3 3 4048.80 3371.34 226.22 o 10 3 3 0.42 -134.53 134.53 o 11 3 3 4662.60 5851.76 286.01 o 12 3 3 8.47 -134.53 134.53 o 13 3 3 3888.33 3923.43 237.18 o 14 3 3 54.31 52.82 59.79 o 15 3 3 1734.74 1751.94 152.47 o 16 3 3 30.58 74.74 83.71 o 1 4 3 4243.31 4118.75 113.61 o 2 4 3 23.24 77.73 18.93 o 3 4 3 297.97 281.03 24.91 o 4 4 3 120.94 209.28 23.92 o 5 4 3 69.98 54.81 61.79 o 6 4 3 274.13 254.12 40.86 o 7 4 3 971.84 1197.86 97.66 o 8 4 3 0.88 -78.73 109.62 o 9 4 3 1273.40 998.55 82.71 o 10 4 3 285.85 462.40 63.78 o 11 4 3 119.64 118.59 145.50 o 12 4 3 123.82 213.26 57.80 o 13 4 3 70.95 155.46 52.82 o 14 4 3 31.09 52.82 103.64 o 15 4 3 206.26 280.03 52.82 o 1 5 3 5620.87 5081.42 138.52 o 2 5 3 0.04 -4.98 53.81 o 3 5 3 4806.29 5197.02 168.42 o 4 5 3 96.31 106.63 28.90 o 5 5 3 3390.31 2858.11 161.44 o 6 5 3 33.56 10.96 78.73 o 7 5 3 1942.63 1735.99 172.40 o 8 5 3 29.00 27.90 136.53 o 9 5 3 1385.93 1136.07 104.64 o 10 5 3 86.98 215.26 154.47 o 11 5 3 1110.28 1400.16 137.52 o 12 5 3 26.05 -152.47 152.47 o 13 5 3 1005.11 1115.14 108.62 o 1 6 3 203.63 207.28 26.91 o 2 6 3 51.61 135.53 26.91 o 3 6 3 55.22 103.64 33.88 o 4 6 3 55.38 69.76 82.71 o 5 6 3 17.75 -53.81 88.69 o 6 6 3 9.52 -4.98 92.68 o 7 6 3 5.74 70.76 104.64 o 8 6 3 9.70 130.55 90.69 o 9 6 3 55.09 95.67 121.58 o 10 6 3 3.87 111.61 162.44 o 11 6 3 19.37 19.93 154.47 o 1 7 3 10.56 64.78 26.91 o 2 7 3 67.86 89.69 60.79 o 3 7 3 18.97 37.87 91.68 o 4 7 3 9.35 61.79 88.69 o 5 7 3 36.64 95.67 93.68 o 6 7 3 26.96 140.51 104.64 o 7 7 3 5.34 43.85 81.72 o 8 7 3 4.03 62.78 142.51 o 0 0 4 28652.63 28221.38 277.04 o 1 0 4 64960.82 69526.49 613.88 o 2 0 4 18971.41 18211.00 208.28 o 3 0 4 52906.32 50116.64 492.30 o 4 0 4 23393.63 24298.95 310.92 o 5 0 4 70061.48 77373.35 845.08 o 6 0 4 11527.69 13034.91 284.02 o 7 0 4 26672.90 28411.71 506.25 o 8 0 4 11103.83 11385.61 331.85 o 9 0 4 31620.99 27254.72 575.01 o 10 0 4 5077.59 3967.28 219.24 o 11 0 4 23125.61 19048.11 482.33 o 12 0 4 5459.35 5172.11 256.11 o 13 0 4 14737.54 16082.37 428.52 o 14 0 4 1834.69 1821.70 169.41 o 15 0 4 11229.85 11273.00 352.78 o 16 0 4 1525.80 1571.56 121.58 o 17 0 4 8797.67 9032.75 330.86 o 0 1 4 84514.78 84783.72 729.48 o 1 1 4 1479.03 1649.29 48.83 o 2 1 4 29801.45 30113.83 306.94 o 3 1 4 112.60 118.59 11.96 o 4 1 4 102926.32 104473.60 981.60 o 5 1 4 10.04 10.96 40.86 o 6 1 4 16350.33 18130.28 337.83 o 7 1 4 230.28 187.35 35.88 o 8 1 4 58089.38 58366.10 893.91 o 9 1 4 820.29 993.56 92.68 o 10 1 4 7467.52 6166.67 273.06 o 11 1 4 25.74 18.93 103.64 o 12 1 4 35672.02 39840.18 754.39 o 13 1 4 9.67 -104.64 111.61 o 14 1 4 7466.98 8886.26 310.92 o 15 1 4 27.99 -120.58 120.58 o 16 1 4 11630.00 12374.20 371.71 o 17 1 4 331.64 223.23 68.76 o 0 2 4 6011.86 5776.02 101.65 o 1 2 4 56052.27 57562.88 541.13 o 2 2 4 4625.05 4893.07 97.66 o 3 2 4 35390.94 34216.64 374.70 o 4 2 4 9179.53 8946.05 166.42 o 5 2 4 41041.47 43245.41 539.14 o 6 2 4 2499.14 2589.04 134.53 o 7 2 4 26757.24 28366.87 513.22 o 8 2 4 2830.94 3063.40 181.37 o 9 2 4 28074.76 25342.34 576.01 o 10 2 4 1547.93 1314.45 109.62 o 11 2 4 17436.64 16587.62 477.35 o 12 2 4 2344.79 2515.30 200.31 o 13 2 4 10773.62 12555.57 388.66 o 14 2 4 359.13 347.80 62.78 o 15 2 4 10376.25 11201.25 357.76 o 16 2 4 430.11 317.90 64.78 o 0 3 4 47520.56 44600.71 458.41 o 1 3 4 22.45 43.85 30.89 o 2 3 4 30562.91 31641.54 364.74 o 3 3 4 547.04 543.12 48.83 o 4 3 4 26935.00 25043.37 343.81 o 5 3 4 382.92 362.75 34.88 o 6 3 4 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