#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2014311.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2014311_Fobs loop_ _publ_author_name 'Guo, Ming-Lin' 'Guo, Chen-Hu' _publ_section_title ; Poly[tetraaquadi-\m~4~-malonato-barium(II)zinc(II)] ; _journal_coeditor_code BM1619 _journal_issue 1 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first m7 _journal_page_last m9 _journal_volume 62 _journal_year 2006 _space_group_IT_number 56 _symmetry_space_group_name_Hall '-P 2ab 2ac' _symmetry_space_group_name_H-M 'P c c n' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 19.0140 _cell_length_b 6.8434 _cell_length_c 9.4203 _exptl_crystal_F_000 920.00 _reflns_d_resolution_high 0.8002 _[local]_cod_data_source_file bm1619Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' BM1619 in Pccn' _shelx_refln_list_code 4 _shelx_f_calc_maximum 290.66 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y+1/2, z' 'x+1/2, -y, -z+1/2' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, y-1/2, -z' '-x-1/2, y, z-1/2' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 270.14 263.34 16.69 o 4 0 0 84482.21 65882.41 2172.00 o 6 0 0 392.80 545.51 45.04 o 8 0 0 12657.97 10947.81 186.10 o 10 0 0 811.77 829.65 38.65 o 12 0 0 40311.84 41032.24 540.94 o 14 0 0 18817.42 20009.15 377.90 o 16 0 0 37714.15 37153.19 644.98 o 18 0 0 1676.72 1830.00 156.51 o 20 0 0 15919.05 15805.10 537.76 o 22 0 0 14.40 40.69 94.23 o 1 1 0 39824.85 38407.29 811.30 o 3 1 0 27249.30 28613.20 355.02 o 5 1 0 15242.79 14512.43 267.18 o 7 1 0 82933.66 77004.16 1034.87 o 9 1 0 10501.66 10021.27 110.85 o 11 1 0 27738.88 27676.86 267.79 o 13 1 0 19957.70 19885.76 231.80 o 15 1 0 9232.11 9592.99 202.97 o 17 1 0 9064.51 8963.79 333.47 o 19 1 0 3954.19 4344.45 177.58 o 21 1 0 6198.99 6136.28 217.66 o 23 1 0 5100.70 5277.73 206.71 o 0 2 0 1770.61 1944.49 52.03 o 2 2 0 77173.87 71739.77 1129.98 o 4 2 0 8835.53 8600.68 197.84 o 6 2 0 55307.79 53786.79 750.18 o 8 2 0 8012.70 8289.23 108.29 o 10 2 0 48985.86 48613.88 444.04 o 12 2 0 2750.09 2787.09 62.42 o 14 2 0 32369.53 32939.62 432.23 o 16 2 0 780.30 873.52 75.22 o 18 2 0 17880.06 19152.69 450.00 o 20 2 0 972.74 1220.81 113.06 o 22 2 0 10049.05 10589.21 437.88 o 1 3 0 35637.51 34751.36 524.82 o 3 3 0 52980.08 52584.67 510.13 o 5 3 0 14761.44 14571.47 255.54 o 7 3 0 2376.98 2251.60 78.86 o 9 3 0 15898.53 16511.41 194.54 o 11 3 0 11254.25 11474.48 180.35 o 13 3 0 12936.54 13201.98 176.23 o 15 3 0 12546.06 13048.79 212.28 o 17 3 0 11348.09 12063.61 359.16 o 19 3 0 6480.59 6624.70 197.68 o 21 3 0 4169.87 4710.82 192.53 o 0 4 0 6663.69 6352.19 144.33 o 2 4 0 2426.05 2640.18 59.35 o 4 4 0 51717.80 52291.32 1002.52 o 6 4 0 7076.48 7112.34 114.42 o 8 4 0 37561.31 37362.70 437.51 o 10 4 0 12585.35 13029.01 196.87 o 12 4 0 14506.90 14828.23 226.34 o 14 4 0 592.82 542.74 53.74 o 16 4 0 9248.56 9947.83 188.29 o 18 4 0 1674.16 1911.44 126.30 o 20 4 0 10414.46 11494.17 671.76 o 1 5 0 6863.70 6645.08 114.18 o 3 5 0 16456.42 16422.90 255.11 o 5 5 0 11526.41 11083.65 192.94 o 7 5 0 14575.54 14582.47 239.22 o 9 5 0 9937.62 9500.84 278.99 o 11 5 0 10084.74 9181.06 680.95 o 13 5 0 5207.76 5165.19 183.37 o 15 5 0 2708.13 2935.58 144.95 o 17 5 0 7350.18 8128.41 363.43 o 19 5 0 2295.05 2503.01 238.06 o 0 6 0 9833.48 9831.53 227.22 o 2 6 0 15359.33 14693.34 210.01 o 4 6 0 2557.93 2545.99 86.10 o 6 6 0 17417.59 17220.68 282.41 o 8 6 0 679.04 555.64 81.39 o 10 6 0 11876.53 11839.43 396.90 o 12 6 0 1191.94 1219.80 196.16 o 14 6 0 10202.37 10753.15 298.44 o 16 6 0 2324.96 2504.02 407.54 o 1 7 0 5016.66 4695.04 96.90 o 3 7 0 2460.31 2574.69 93.76 o 5 7 0 7235.52 6890.80 187.03 o 7 7 0 10224.92 9851.67 343.89 o 9 7 0 5648.76 5799.73 205.24 o 11 7 0 3318.56 3049.13 162.78 o 13 7 0 2693.98 2614.99 201.26 o 0 8 0 8539.61 8157.06 322.26 o 2 8 0 1812.08 1769.02 92.17 o 4 8 0 5430.02 5277.30 129.90 o 6 8 0 985.58 1006.07 189.98 o 8 8 0 9524.34 8802.63 331.81 o 1 1 1 15727.61 15822.68 145.86 o 2 1 1 346.75 337.53 10.70 o 3 1 1 9282.61 9230.30 112.56 o 4 1 1 641.38 618.38 13.74 o 5 1 1 3550.33 3408.11 38.37 o 6 1 1 6459.71 6766.18 80.15 o 7 1 1 5710.22 5654.44 62.77 o 8 1 1 3084.98 3233.95 38.76 o 9 1 1 13156.85 13240.26 122.58 o 10 1 1 895.52 943.16 22.06 o 11 1 1 6291.77 6133.03 79.30 o 12 1 1 187.58 187.20 15.09 o 13 1 1 3222.25 3112.31 49.76 o 14 1 1 241.22 216.71 23.18 o 15 1 1 2281.76 2214.58 54.49 o 16 1 1 0.98 -23.85 23.85 o 17 1 1 1411.54 1404.47 52.70 o 18 1 1 319.92 311.10 42.51 o 19 1 1 2768.31 3044.80 88.11 o 20 1 1 393.97 427.13 58.06 o 21 1 1 3018.20 3208.98 110.15 o 22 1 1 126.47 125.09 61.34 o 23 1 1 1137.37 1342.13 92.66 o 1 2 1 31394.81 32786.29 251.69 o 2 2 1 4981.98 5281.82 57.05 o 3 2 1 2147.44 2262.45 27.03 o 4 2 1 0.03 -6.92 6.92 o 5 2 1 2904.81 3087.95 38.54 o 6 2 1 146.93 139.01 15.30 o 7 2 1 477.57 544.32 16.52 o 8 2 1 127.39 93.50 11.05 o 9 2 1 746.52 793.25 17.83 o 10 2 1 87.50 57.15 11.94 o 11 2 1 1421.40 1579.51 30.26 o 12 2 1 1134.16 1084.73 25.82 o 13 2 1 1824.73 1855.13 40.99 o 14 2 1 581.62 616.31 32.39 o 15 2 1 4.83 -16.07 21.36 o 16 2 1 367.39 414.06 34.68 o 17 2 1 845.97 869.75 58.05 o 18 2 1 0.42 -35.71 35.71 o 19 2 1 56.93 65.45 40.84 o 20 2 1 148.54 151.97 44.97 o 21 2 1 96.83 108.53 52.21 o 22 2 1 6.07 74.95 49.85 o 23 2 1 36.93 35.41 53.61 o 1 3 1 9541.45 9343.07 88.69 o 2 3 1 1141.29 1271.28 33.28 o 3 3 1 10468.87 10973.27 106.25 o 4 3 1 453.26 476.02 14.60 o 5 3 1 12123.14 12303.84 113.96 o 6 3 1 296.00 273.03 18.49 o 7 3 1 6724.54 6925.06 71.66 o 8 3 1 52.43 56.20 12.10 o 9 3 1 2089.04 2090.19 36.02 o 10 3 1 408.57 365.58 23.13 o 11 3 1 2105.72 2137.51 42.23 o 12 3 1 139.27 99.72 20.05 o 13 3 1 1548.65 1576.43 41.38 o 14 3 1 18.83 11.99 21.43 o 15 3 1 2748.18 2799.68 70.28 o 16 3 1 453.43 479.88 40.25 o 17 3 1 1675.14 1717.75 64.71 o 18 3 1 4.54 0.51 38.57 o 19 3 1 1692.78 1710.78 77.60 o 20 3 1 8.74 24.64 44.95 o 21 3 1 1037.25 1177.05 128.04 o 22 3 1 96.54 157.92 57.88 o 1 4 1 860.22 935.06 24.90 o 2 4 1 177.18 155.38 16.44 o 3 4 1 12.66 16.56 13.16 o 4 4 1 357.30 357.02 18.19 o 5 4 1 8.44 3.48 11.29 o 6 4 1 1588.39 1610.43 36.59 o 7 4 1 601.03 582.25 27.65 o 8 4 1 359.63 331.43 32.08 o 9 4 1 47.40 28.79 17.07 o 10 4 1 214.44 169.82 21.12 o 11 4 1 65.52 32.56 23.58 o 12 4 1 73.90 55.68 25.59 o 13 4 1 63.59 39.67 27.13 o 14 4 1 87.26 83.35 26.22 o 15 4 1 220.63 168.96 34.38 o 16 4 1 32.24 37.45 37.06 o 17 4 1 15.17 76.20 39.00 o 18 4 1 1.11 -10.06 44.33 o 19 4 1 8.04 -51.70 51.70 o 20 4 1 82.55 44.13 65.44 o 1 5 1 873.84 864.98 31.19 o 2 5 1 43.11 43.40 17.39 o 3 5 1 1608.03 1594.33 40.10 o 4 5 1 1386.40 1404.22 37.86 o 5 5 1 4978.89 4991.71 80.28 o 6 5 1 430.46 385.76 30.44 o 7 5 1 3284.22 3310.58 65.17 o 8 5 1 255.74 196.90 25.28 o 9 5 1 1522.87 1457.40 53.23 o 10 5 1 86.23 98.94 39.13 o 11 5 1 2170.39 2191.59 80.13 o 12 5 1 192.11 213.45 46.02 o 13 5 1 3536.61 3686.82 108.28 o 14 5 1 2.79 -4.35 45.98 o 15 5 1 1800.09 1726.21 117.99 o 16 5 1 69.80 76.23 60.30 o 17 5 1 2737.15 3077.92 190.45 o 18 5 1 34.74 -85.20 85.20 o 19 5 1 239.87 346.23 104.22 o 1 6 1 121.25 69.51 21.73 o 2 6 1 287.90 297.22 27.30 o 3 6 1 300.39 280.82 25.61 o 4 6 1 0.41 9.59 22.74 o 5 6 1 20.71 42.81 24.92 o 6 6 1 159.74 132.62 28.13 o 7 6 1 193.42 174.21 30.13 o 8 6 1 83.02 75.52 32.53 o 9 6 1 762.56 777.88 63.35 o 10 6 1 147.10 143.64 48.36 o 11 6 1 837.45 889.50 72.18 o 12 6 1 332.79 337.37 57.37 o 13 6 1 5.77 9.89 50.17 o 14 6 1 22.46 -33.18 54.23 o 15 6 1 29.56 -10.23 59.10 o 16 6 1 73.38 -10.45 61.57 o 1 7 1 1463.29 1439.98 47.48 o 2 7 1 196.51 160.10 28.99 o 3 7 1 1098.85 1105.78 50.41 o 4 7 1 46.97 23.77 29.09 o 5 7 1 401.06 332.25 51.65 o 6 7 1 85.38 66.92 34.05 o 7 7 1 651.36 539.35 50.55 o 8 7 1 53.79 -2.91 47.49 o 9 7 1 274.01 305.70 57.63 o 10 7 1 13.50 -21.08 53.06 o 11 7 1 676.47 690.94 76.66 o 12 7 1 134.13 109.55 63.21 o 13 7 1 284.70 314.42 73.86 o 1 8 1 204.08 159.71 38.47 o 2 8 1 73.99 50.48 38.98 o 3 8 1 5.39 -35.42 35.42 o 4 8 1 6.46 37.80 38.26 o 5 8 1 0.03 -42.03 42.03 o 6 8 1 15.53 -18.93 44.27 o 7 8 1 22.29 30.33 54.91 o 8 8 1 0.18 -46.28 57.54 o 0 0 2 40362.90 39210.40 831.45 o 1 0 2 2189.28 2202.01 41.16 o 2 0 2 13232.08 13868.88 158.63 o 3 0 2 12271.92 12970.50 150.15 o 4 0 2 60999.65 58336.21 619.23 o 5 0 2 7379.54 7612.42 97.78 o 6 0 2 10010.81 10585.65 148.47 o 7 0 2 1304.87 1285.39 46.68 o 8 0 2 61513.07 59973.74 645.88 o 9 0 2 748.42 739.26 21.53 o 10 0 2 1299.78 1316.95 56.59 o 11 0 2 5573.92 5535.78 78.49 o 12 0 2 42818.40 40780.26 479.59 o 13 0 2 70.19 67.75 27.73 o 14 0 2 2069.45 2097.26 122.29 o 15 0 2 1561.38 1473.74 82.50 o 16 0 2 13923.78 14034.78 254.15 o 17 0 2 2893.69 2899.22 100.71 o 18 0 2 3325.36 3248.34 159.12 o 19 0 2 1151.53 1246.46 78.83 o 20 0 2 15633.63 15055.73 371.06 o 21 0 2 1496.55 1499.36 157.76 o 22 0 2 393.77 342.39 84.77 o 23 0 2 658.88 644.44 99.14 o 0 1 2 4443.97 4529.14 73.79 o 1 1 2 15491.56 15815.50 163.42 o 2 1 2 53.70 40.57 7.59 o 3 1 2 25071.35 25421.93 199.35 o 4 1 2 13680.25 14387.72 119.57 o 5 1 2 42616.23 42993.63 309.80 o 6 1 2 1714.81 1754.24 27.11 o 7 1 2 38530.98 39103.33 305.32 o 8 1 2 2884.55 2953.58 40.20 o 9 1 2 22539.71 22663.64 297.31 o 10 1 2 7407.97 7497.32 86.76 o 11 1 2 12984.80 12951.21 155.23 o 12 1 2 1153.67 1154.88 33.08 o 13 1 2 10719.14 10213.85 148.97 o 14 1 2 1025.55 1021.32 35.60 o 15 1 2 4398.32 4243.95 80.04 o 16 1 2 986.11 999.39 47.10 o 17 1 2 7189.86 7226.00 118.56 o 18 1 2 818.51 920.17 52.71 o 19 1 2 9567.92 9253.55 144.23 o 20 1 2 559.14 581.58 54.38 o 21 1 2 6936.70 7099.10 167.83 o 22 1 2 596.88 622.65 67.59 o 23 1 2 2934.53 3000.70 111.88 o 0 2 2 10205.48 10782.21 157.75 o 1 2 2 700.40 737.50 20.50 o 2 2 2 43572.41 42419.74 345.95 o 3 2 2 9682.84 10367.66 92.03 o 4 2 2 7566.69 7995.17 70.65 o 5 2 2 17.37 18.88 7.77 o 6 2 2 63037.39 61184.88 466.63 o 7 2 2 12235.27 12710.00 178.96 o 8 2 2 2064.33 2152.25 33.14 o 9 2 2 1120.20 1087.86 23.43 o 10 2 2 46786.43 45881.61 366.19 o 11 2 2 2102.29 2213.07 41.25 o 12 2 2 419.38 404.95 33.58 o 13 2 2 2724.24 2667.19 49.72 o 14 2 2 23689.21 23190.63 418.68 o 15 2 2 274.91 343.16 30.86 o 16 2 2 1456.43 1420.57 48.40 o 17 2 2 1521.79 1516.67 55.92 o 18 2 2 15804.41 15964.88 336.41 o 19 2 2 230.41 245.82 45.27 o 20 2 2 1651.20 1728.27 83.49 o 21 2 2 983.59 1059.60 70.50 o 22 2 2 9464.93 9845.42 223.66 o 0 3 2 15217.60 15451.67 221.30 o 1 3 2 23501.08 24060.56 228.86 o 2 3 2 1442.53 1420.09 30.59 o 3 3 2 26053.72 26572.54 215.21 o 4 3 2 1796.72 1792.49 33.34 o 5 3 2 8256.36 8230.19 79.67 o 6 3 2 3826.85 3847.09 47.39 o 7 3 2 16379.71 16802.25 150.56 o 8 3 2 656.29 703.72 22.80 o 9 3 2 9666.27 9713.33 110.58 o 10 3 2 1533.85 1580.63 37.48 o 11 3 2 14817.29 15098.77 186.74 o 12 3 2 6.62 -8.54 16.77 o 13 3 2 9215.08 9226.59 149.24 o 14 3 2 5182.03 5313.25 86.94 o 15 3 2 10442.84 10609.63 223.87 o 16 3 2 224.57 287.25 31.37 o 17 3 2 9567.01 9777.50 229.27 o 18 3 2 1466.58 1544.69 88.40 o 19 3 2 1705.19 1798.55 76.91 o 20 3 2 1839.30 1953.27 84.17 o 21 3 2 3763.53 3877.98 112.78 o 0 4 2 43908.41 42214.86 547.14 o 1 4 2 3654.60 3719.65 55.54 o 2 4 2 1980.05 1982.21 56.47 o 3 4 2 839.79 916.22 28.42 o 4 4 2 38708.62 37812.07 346.40 o 5 4 2 449.17 496.67 21.53 o 6 4 2 949.03 924.16 24.83 o 7 4 2 4253.16 4444.35 59.79 o 8 4 2 30063.29 30542.45 332.08 o 9 4 2 885.34 829.89 32.85 o 10 4 2 2095.39 2115.05 56.14 o 11 4 2 700.59 676.17 34.17 o 12 4 2 16562.28 16016.17 444.52 o 13 4 2 3213.09 3223.92 82.94 o 14 4 2 1544.77 1477.18 47.36 o 15 4 2 577.24 578.97 48.75 o 16 4 2 17243.30 17430.43 222.63 o 17 4 2 769.66 833.02 56.34 o 18 4 2 495.17 585.70 66.95 o 19 4 2 115.23 71.28 56.36 o 20 4 2 7131.51 7718.09 371.33 o 0 5 2 1710.91 1924.67 144.58 o 1 5 2 14044.03 13740.72 156.66 o 2 5 2 1420.95 1362.28 37.21 o 3 5 2 11175.31 11002.84 123.83 o 4 5 2 549.45 532.14 28.93 o 5 5 2 7437.34 7443.65 95.06 o 6 5 2 2227.06 2219.62 53.19 o 7 5 2 5954.08 5978.66 92.24 o 8 5 2 1122.40 1165.64 45.79 o 9 5 2 7670.94 7710.29 127.76 o 10 5 2 821.42 849.36 49.40 o 11 5 2 6454.01 6728.17 180.68 o 12 5 2 1310.30 1305.19 84.89 o 13 5 2 5601.32 5764.35 185.33 o 14 5 2 713.85 714.34 65.60 o 15 5 2 9171.50 9078.33 291.51 o 16 5 2 633.96 542.87 78.17 o 17 5 2 2565.26 2599.66 122.84 o 18 5 2 338.88 291.82 98.98 o 0 6 2 1953.10 1895.16 74.04 o 1 6 2 1710.95 1707.49 48.64 o 2 6 2 20375.46 19367.27 198.09 o 3 6 2 845.22 923.16 37.83 o 4 6 2 1357.29 1342.13 42.38 o 5 6 2 1667.72 1589.22 50.07 o 6 6 2 10546.19 10541.31 142.35 o 7 6 2 110.51 110.36 32.66 o 8 6 2 1622.40 1591.50 60.63 o 9 6 2 468.35 567.10 48.59 o 10 6 2 9004.67 9030.50 202.96 o 11 6 2 940.27 936.67 71.24 o 12 6 2 2641.66 2697.25 101.75 o 13 6 2 203.91 161.23 61.44 o 14 6 2 10443.33 11621.67 686.85 o 15 6 2 839.11 1073.09 120.19 o 16 6 2 793.11 924.83 144.36 o 0 7 2 298.48 296.65 47.40 o 1 7 2 4599.40 4481.14 110.28 o 2 7 2 666.17 657.25 44.01 o 3 7 2 4560.94 4457.01 87.90 o 4 7 2 1314.46 1283.79 53.67 o 5 7 2 5484.11 5319.15 98.53 o 6 7 2 169.63 103.58 39.51 o 7 7 2 4039.02 3916.46 97.52 o 8 7 2 409.10 409.13 49.17 o 9 7 2 3829.67 3780.84 118.60 o 10 7 2 964.95 1046.56 83.15 o 11 7 2 3204.89 3190.61 148.12 o 12 7 2 715.88 872.50 121.49 o 13 7 2 4138.10 4404.40 270.87 o 0 8 2 6243.46 6228.41 159.82 o 1 8 2 85.49 56.42 38.37 o 2 8 2 1344.23 1394.78 77.56 o 3 8 2 1186.33 1176.47 65.94 o 4 8 2 5232.49 5114.25 160.24 o 5 8 2 265.81 274.33 56.51 o 6 8 2 1932.08 1899.63 98.24 o 7 8 2 336.55 254.73 51.86 o 1 1 3 5589.16 5509.21 65.13 o 2 1 3 845.34 862.63 25.24 o 3 1 3 29285.59 29567.98 294.81 o 4 1 3 6424.64 6945.65 68.44 o 5 1 3 1293.41 1192.59 22.90 o 6 1 3 470.34 590.86 17.17 o 7 1 3 7628.08 7484.83 98.10 o 8 1 3 744.53 729.06 20.79 o 9 1 3 11276.01 11096.22 133.25 o 10 1 3 799.30 772.67 23.89 o 11 1 3 4877.00 4632.41 59.24 o 12 1 3 135.70 84.40 19.35 o 13 1 3 15694.81 15091.24 277.56 o 14 1 3 584.13 487.94 32.84 o 15 1 3 4637.26 4541.62 90.81 o 16 1 3 164.60 157.45 31.89 o 17 1 3 1480.75 1382.70 57.84 o 18 1 3 889.64 869.66 55.29 o 19 1 3 2421.30 2346.97 74.88 o 20 1 3 8.77 25.47 35.81 o 21 1 3 556.44 538.85 58.32 o 22 1 3 40.22 72.80 46.49 o 1 2 3 202.96 187.50 14.84 o 2 2 3 1674.64 1806.78 34.34 o 3 2 3 533.16 497.95 19.61 o 4 2 3 30.23 48.68 25.65 o 5 2 3 666.08 648.89 18.93 o 6 2 3 3216.65 3241.50 43.15 o 7 2 3 797.25 918.40 22.45 o 8 2 3 53.02 39.53 10.39 o 9 2 3 2.73 -12.05 12.05 o 10 2 3 1508.29 1555.01 34.08 o 11 2 3 330.35 299.67 22.57 o 12 2 3 57.96 59.01 16.74 o 13 2 3 105.29 96.72 20.99 o 14 2 3 360.86 324.12 29.36 o 15 2 3 226.46 195.73 32.88 o 16 2 3 20.07 0.28 26.90 o 17 2 3 744.09 669.62 46.09 o 18 2 3 102.73 60.43 37.54 o 19 2 3 27.64 38.42 35.50 o 20 2 3 747.41 956.31 100.19 o 21 2 3 301.05 312.33 51.97 o 22 2 3 50.72 -46.98 46.98 o 1 3 3 4502.19 4668.12 76.59 o 2 3 3 778.94 830.12 26.82 o 3 3 3 852.48 850.36 26.87 o 4 3 3 645.34 627.89 22.55 o 5 3 3 5198.15 4953.52 58.09 o 6 3 3 1031.76 1083.29 23.64 o 7 3 3 4188.36 4235.42 67.64 o 8 3 3 1343.73 1378.96 30.78 o 9 3 3 2791.66 2775.50 51.16 o 10 3 3 25.21 11.54 16.91 o 11 3 3 5274.71 5315.32 72.24 o 12 3 3 64.10 74.57 19.17 o 13 3 3 1479.68 1417.62 47.26 o 14 3 3 335.10 297.95 30.89 o 15 3 3 2595.26 2693.92 68.48 o 16 3 3 847.95 798.24 48.51 o 17 3 3 2679.49 2748.29 74.62 o 18 3 3 57.49 39.24 35.83 o 19 3 3 934.60 1135.53 106.96 o 20 3 3 137.79 128.09 48.33 o 21 3 3 366.96 474.29 59.87 o 1 4 3 457.14 501.80 27.19 o 2 4 3 1827.78 1893.82 43.40 o 3 4 3 2837.96 2896.32 59.99 o 4 4 3 48.75 48.32 16.20 o 5 4 3 88.27 100.64 17.13 o 6 4 3 1735.71 1788.08 35.44 o 7 4 3 6.61 32.19 16.29 o 8 4 3 375.75 390.41 29.53 o 9 4 3 33.07 15.92 17.95 o 10 4 3 577.06 583.39 46.28 o 11 4 3 1265.26 1298.26 41.53 o 12 4 3 31.68 45.51 22.83 o 13 4 3 37.93 65.95 26.02 o 14 4 3 535.74 565.24 50.26 o 15 4 3 11.62 -30.60 30.60 o 16 4 3 95.85 61.09 37.12 o 17 4 3 90.87 66.18 37.40 o 18 4 3 13.92 -44.72 44.72 o 19 4 3 165.97 148.74 54.73 o 20 4 3 64.88 50.34 58.47 o 1 5 3 3257.45 3262.39 62.85 o 2 5 3 19.70 19.91 19.49 o 3 5 3 396.71 344.56 34.18 o 4 5 3 1487.49 1420.97 41.90 o 5 5 3 4091.22 4041.53 66.07 o 6 5 3 77.03 93.92 23.92 o 7 5 3 1474.35 1521.16 53.47 o 8 5 3 10.26 26.18 27.39 o 9 5 3 1311.53 1328.62 61.40 o 10 5 3 315.15 345.24 38.39 o 11 5 3 1002.05 1045.35 78.53 o 12 5 3 4.09 -24.63 43.30 o 13 5 3 27.41 55.76 47.31 o 14 5 3 356.45 352.37 46.89 o 15 5 3 471.35 526.79 53.66 o 16 5 3 18.34 31.20 48.49 o 17 5 3 1540.04 1724.55 313.31 o 18 5 3 398.48 323.89 96.07 o 1 6 3 11.70 12.74 23.55 o 2 6 3 54.34 51.74 24.82 o 3 6 3 199.83 207.60 29.24 o 4 6 3 77.53 92.68 27.51 o 5 6 3 91.60 78.36 27.84 o 6 6 3 1.12 31.06 26.84 o 7 6 3 160.38 136.86 35.53 o 8 6 3 0.19 -6.67 32.21 o 9 6 3 0.85 -18.77 34.10 o 10 6 3 247.15 208.69 40.52 o 11 6 3 180.01 248.20 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6428.23 6614.73 199.78 o 2 0 10 10036.17 9972.79 206.02 o 3 0 10 6497.72 6572.97 160.68 o 4 0 10 1709.83 1630.75 83.37 o 5 0 10 5719.31 5641.00 254.88 o 6 0 10 2619.49 2862.38 133.79 o 7 0 10 10760.87 10607.22 271.41 o 8 0 10 1139.10 1200.34 106.17 o 9 0 10 5441.21 5728.71 195.02 o 10 0 10 691.90 806.95 99.95 o 11 0 10 2796.31 2836.09 140.47 o 12 0 10 8.01 -14.15 93.03 o 0 1 10 6583.47 6505.47 225.86 o 1 1 10 79.10 86.09 38.44 o 2 1 10 5251.08 5282.25 110.58 o 3 1 10 8.89 46.47 35.90 o 4 1 10 6053.34 5985.68 119.62 o 5 1 10 1477.51 1537.26 64.15 o 6 1 10 8345.89 8330.33 222.78 o 7 1 10 76.26 36.92 46.56 o 8 1 10 7681.88 7586.01 159.92 o 9 1 10 1088.03 1194.77 134.57 o 10 1 10 4495.54 4496.37 123.81 o 11 1 10 83.68 85.17 51.60 o 12 1 10 3901.05 3766.98 142.84 o 0 2 10 2206.41 2074.38 94.36 o 1 2 10 6027.31 6086.63 123.25 o 2 2 10 655.87 855.35 92.84 o 3 2 10 5204.64 5391.11 152.17 o 4 2 10 2619.78 2717.21 83.27 o 5 2 10 7492.39 7559.75 140.33 o 6 2 10 186.38 148.36 45.95 o 7 2 10 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102.25 o 6 2 11 115.40 83.93 58.24 o 1 3 11 1564.76 1587.94 96.01 o