#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2014322.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2014322_Fobs loop_ _publ_author_name 'Janczak, Jan' 'Perp\'etuo, Genivaldo J\'ulio' _publ_section_title ; Bis{[phthalocyaninato(2--)]arsenic(III)} octaiododiarsenic(III) ; _journal_coeditor_code FA1174 _journal_issue 2 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first m45 _journal_page_last m47 _journal_volume 62 _journal_year 2006 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90.00 _cell_angle_beta 97.09 _cell_angle_gamma 90.00 _cell_length_a 19.3570 _cell_length_b 16.5370 _cell_length_c 21.7830 _exptl_crystal_F_000 4336.00 _reflns_d_resolution_high 0.7508 _[local]_cod_data_source_file fa1174Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' (AsPc)AsI4 in C2/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 2274.43 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 21020.86 20776.01 482.67 o 6 0 0 46131.46 43336.25 359.47 o 8 0 0 8468.31 9480.29 226.57 o 10 0 0 149571.92 157193.77 541.03 o 12 0 0 10259.07 10208.61 336.60 o 14 0 0 219889.25 234393.78 931.09 o 16 0 0 107595.02 116164.34 627.21 o 18 0 0 2629.62 2697.77 509.34 o 20 0 0 6103.76 5673.50 931.47 o 22 0 0 876.09 876.43 668.96 o 24 0 0 8.15 224.40 563.12 o 3 1 0 859.37 994.98 122.78 o 5 1 0 75420.13 81899.39 268.75 o 7 1 0 90191.38 88221.41 221.98 o 9 1 0 44768.30 38610.88 197.57 o 11 1 0 101728.01 105158.94 411.35 o 13 1 0 95.73 112.78 78.66 o 15 1 0 22877.75 26232.52 1304.29 o 17 1 0 24211.56 26990.34 590.10 o 19 1 0 4800.71 4326.38 536.36 o 21 1 0 56.66 135.50 367.66 o 23 1 0 1679.34 1872.10 643.26 o 25 1 0 4405.69 5240.16 699.88 o 2 2 0 11457.24 11368.16 169.36 o 4 2 0 82230.95 78298.02 421.62 o 6 2 0 420632.91 432430.78 588.49 o 8 2 0 471.89 447.71 53.62 o 10 2 0 28367.26 28285.28 982.03 o 12 2 0 8234.66 7529.81 409.58 o 14 2 0 2785.61 2433.40 172.69 o 16 2 0 1361.13 1686.99 332.60 o 18 2 0 2576.51 2531.90 300.87 o 20 2 0 30904.45 31559.50 1272.02 o 22 2 0 4733.27 4365.31 728.54 o 24 2 0 1709.92 1047.56 403.19 o 1 3 0 44464.49 41332.35 188.19 o 3 3 0 64801.10 59386.39 190.85 o 5 3 0 805084.63 776297.63 706.29 o 7 3 0 417348.66 392951.06 530.98 o 9 3 0 146275.19 158804.78 463.62 o 11 3 0 73404.27 83212.34 446.39 o 13 3 0 3649.83 3724.15 181.30 o 15 3 0 14232.75 12488.94 425.90 o 17 3 0 476.55 385.56 249.40 o 19 3 0 3115.84 2665.17 434.09 o 21 3 0 7459.22 8257.55 446.68 o 23 3 0 2242.72 2108.51 249.34 o 25 3 0 18.44 160.39 346.95 o 0 4 0 189773.48 195986.80 546.37 o 2 4 0 58384.48 60685.25 217.76 o 4 4 0 22448.62 20947.21 144.34 o 6 4 0 22938.38 23165.78 274.44 o 8 4 0 3193.76 2724.64 117.11 o 10 4 0 78302.57 81238.52 305.35 o 12 4 0 3355.00 3319.90 172.93 o 14 4 0 48713.13 53522.70 1790.48 o 16 4 0 12411.35 12615.26 309.51 o 18 4 0 300.38 168.68 152.78 o 20 4 0 381.19 234.26 216.72 o 22 4 0 3669.84 3613.90 520.96 o 24 4 0 1129.12 432.30 425.50 o 1 5 0 10071.93 10049.89 139.06 o 3 5 0 29385.68 27087.16 730.19 o 5 5 0 12927.79 11914.69 253.78 o 7 5 0 72.18 50.60 46.97 o 9 5 0 11987.85 12734.46 330.07 o 11 5 0 31692.99 34148.32 1204.55 o 13 5 0 117334.07 136433.33 2916.08 o 15 5 0 413.04 512.31 98.36 o 17 5 0 4046.45 3595.60 274.73 o 19 5 0 371.94 222.60 226.90 o 21 5 0 115.52 157.89 230.46 o 23 5 0 170.60 46.34 243.88 o 0 6 0 40360.71 38128.42 427.63 o 2 6 0 176561.78 166891.41 306.62 o 4 6 0 163997.02 154654.69 416.87 o 6 6 0 98.83 65.96 45.45 o 8 6 0 81.84 71.05 45.13 o 10 6 0 19410.31 21007.79 591.70 o 12 6 0 71234.66 72107.85 572.78 o 14 6 0 2017.50 1784.58 197.92 o 16 6 0 1823.20 1708.64 243.38 o 18 6 0 10175.10 11792.25 798.63 o 20 6 0 184.13 44.84 203.06 o 22 6 0 40.92 268.55 410.47 o 24 6 0 261.48 168.12 246.12 o 1 7 0 81072.61 79052.64 337.82 o 3 7 0 13779.21 12144.76 279.45 o 5 7 0 216.47 148.18 62.22 o 7 7 0 341764.22 324927.41 522.68 o 9 7 0 88158.72 88096.36 2161.97 o 11 7 0 13864.64 13370.17 218.01 o 13 7 0 1331.35 1410.85 157.70 o 15 7 0 5603.58 5361.16 633.45 o 17 7 0 1811.70 1394.49 361.90 o 19 7 0 2772.04 2859.57 495.02 o 21 7 0 3486.86 4343.69 549.30 o 23 7 0 3271.76 4434.16 760.16 o 0 8 0 25739.98 30803.65 848.98 o 2 8 0 25528.57 22680.27 209.50 o 4 8 0 15784.80 16055.72 189.16 o 6 8 0 2495.13 2845.08 161.33 o 8 8 0 41944.48 37416.98 1003.63 o 10 8 0 967.09 986.52 104.45 o 12 8 0 28410.56 31537.08 485.45 o 14 8 0 5469.71 5827.52 300.63 o 16 8 0 1667.41 1581.04 231.22 o 18 8 0 27726.14 32739.71 708.57 o 20 8 0 455.20 164.24 198.75 o 22 8 0 182.34 263.73 215.83 o 1 9 0 142669.92 146696.47 469.59 o 3 9 0 49375.72 48861.37 660.41 o 5 9 0 12173.69 10697.51 158.52 o 7 9 0 11340.32 11706.31 344.71 o 9 9 0 8017.95 7875.27 203.06 o 11 9 0 165.74 4.23 102.45 o 13 9 0 38407.18 41420.11 1853.69 o 15 9 0 4061.46 4117.85 309.14 o 17 9 0 4853.76 4169.16 477.98 o 19 9 0 0.44 38.48 173.64 o 21 9 0 347.23 88.58 195.06 o 23 9 0 8.19 106.63 235.79 o 0 10 0 63141.63 61618.44 2014.36 o 2 10 0 166990.34 163922.94 1218.00 o 4 10 0 39358.11 39792.37 612.11 o 6 10 0 17468.86 14815.36 483.83 o 8 10 0 816.57 643.66 104.02 o 10 10 0 874.37 957.95 109.41 o 12 10 0 38856.28 40855.17 550.77 o 14 10 0 11679.26 13725.06 444.14 o 16 10 0 1771.40 1661.06 261.55 o 18 10 0 5174.30 6245.85 614.17 o 20 10 0 7.57 80.73 168.91 o 22 10 0 250.27 215.85 267.40 o 1 11 0 3092.02 2548.82 144.46 o 3 11 0 17.05 176.66 90.31 o 5 11 0 18824.78 22040.26 287.95 o 7 11 0 52493.57 49597.88 501.99 o 9 11 0 13982.52 18490.87 1554.35 o 11 11 0 3888.88 3920.21 217.98 o 13 11 0 3344.12 3466.53 329.16 o 15 11 0 510.42 271.46 165.01 o 17 11 0 467.27 150.11 177.95 o 19 11 0 694.45 280.41 223.50 o 21 11 0 599.51 751.11 308.01 o 0 12 0 49897.67 57476.88 1493.57 o 2 12 0 1104.47 1306.19 104.22 o 4 12 0 30514.75 30313.10 906.13 o 6 12 0 25.86 210.49 103.31 o 8 12 0 1083.77 909.78 48.62 o 10 12 0 11504.48 10968.82 338.85 o 12 12 0 1685.95 1961.88 251.78 o 14 12 0 476.89 319.23 148.21 o 16 12 0 1648.94 1635.97 266.67 o 18 12 0 1552.66 1852.57 407.03 o 20 12 0 5436.93 5899.91 907.14 o 1 13 0 2428.46 2554.28 226.86 o 3 13 0 26199.38 28668.71 1108.99 o 5 13 0 84331.86 94333.79 1199.20 o 7 13 0 26080.48 25981.00 610.33 o 9 13 0 13904.10 12541.60 1097.24 o 11 13 0 6560.71 6531.28 579.40 o 13 13 0 2896.36 2877.40 318.16 o 15 13 0 274.59 813.04 208.83 o 17 13 0 2110.34 1757.07 465.45 o 19 13 0 2253.04 2239.15 553.92 o 0 14 0 68781.99 78524.07 903.63 o 2 14 0 17508.07 17022.83 463.60 o 4 14 0 237.64 113.89 100.46 o 6 14 0 2247.99 1836.03 219.59 o 8 14 0 2324.32 2036.67 222.96 o 10 14 0 498.48 323.26 182.86 o 12 14 0 126.74 62.83 128.39 o 14 14 0 10204.23 10633.57 390.59 o 16 14 0 3415.75 4236.49 409.36 o 18 14 0 166.15 187.62 261.79 o 1 15 0 5520.93 5495.61 278.84 o 3 15 0 120.29 25.13 102.68 o 5 15 0 5756.58 6151.15 272.00 o 7 15 0 8883.03 8040.23 398.25 o 9 15 0 81.19 77.41 136.42 o 11 15 0 3180.20 2985.27 300.18 o 13 15 0 13.72 26.08 153.65 o 15 15 0 6800.32 8313.94 1274.18 o 17 15 0 3824.77 2929.72 729.98 o 0 16 0 54739.61 60308.27 878.82 o 2 16 0 4625.60 4035.02 280.51 o 4 16 0 732.56 817.65 255.53 o 6 16 0 22742.57 23184.65 488.59 o 8 16 0 2419.02 2857.10 338.50 o 10 16 0 20723.86 21404.77 496.65 o 12 16 0 1112.67 784.43 217.29 o 14 16 0 1323.82 1448.32 202.97 o 16 16 0 1911.47 1428.16 258.47 o 1 17 0 5.50 73.10 98.02 o 3 17 0 4152.86 4204.44 350.61 o 5 17 0 10108.51 12093.96 628.32 o 7 17 0 2223.11 1667.97 307.39 o 9 17 0 6555.80 7355.51 434.19 o 11 17 0 1909.03 1346.08 323.49 o 13 17 0 1233.06 1128.62 346.31 o 15 17 0 5.22 139.02 318.58 o 0 18 0 11.43 146.04 229.55 o 2 18 0 1510.78 971.20 209.43 o 4 18 0 1500.33 2099.17 336.84 o 6 18 0 1476.08 1747.08 290.89 o 8 18 0 1339.00 1185.06 277.34 o 10 18 0 1448.09 1197.07 265.86 o 12 18 0 2824.07 3391.84 495.59 o 14 18 0 0.58 419.34 423.11 o 1 19 0 184.53 44.58 136.86 o 3 19 0 1165.64 1246.90 288.71 o 5 19 0 7375.93 8136.40 458.44 o 7 19 0 630.04 298.66 191.12 o 9 19 0 96.70 305.29 187.81 o 11 19 0 2968.51 3829.02 685.69 o 0 20 0 2409.97 2196.97 594.00 o 2 20 0 3427.52 2775.35 408.18 o 4 20 0 2634.08 2814.24 397.03 o 6 20 0 2.52 49.85 126.09 o 8 20 0 542.74 210.54 218.47 o 10 20 0 466.83 249.98 268.55 o 1 21 0 213.82 232.66 244.25 o 3 21 0 516.13 218.17 198.48 o 5 21 0 17.53 68.42 151.25 o 7 21 0 102.59 194.90 274.30 o 0 22 0 18.63 326.01 635.09 o -25 1 1 1338.73 965.06 602.22 o -23 1 1 1644.47 678.77 490.04 o -21 1 1 11883.30 11638.77 806.57 o -19 1 1 15797.01 15601.23 540.70 o -17 1 1 1424.45 1132.13 243.83 o -15 1 1 21642.71 22345.90 960.49 o -13 1 1 9953.93 9650.07 213.23 o -11 1 1 15679.70 14943.24 183.35 o -9 1 1 24508.15 21902.79 510.29 o -7 1 1 156836.19 165547.14 424.56 o -5 1 1 356978.31 385788.25 465.07 o -3 1 1 5948.99 6079.96 326.01 o 3 1 1 447.42 414.30 120.67 o 5 1 1 47296.43 47673.78 279.44 o 7 1 1 74682.62 77829.73 312.34 o 9 1 1 205.88 106.59 77.58 o 11 1 1 243.37 152.70 50.24 o 13 1 1 26597.27 29851.47 489.04 o 15 1 1 127809.17 148942.45 3493.81 o 17 1 1 6479.65 6580.19 385.60 o 19 1 1 12060.26 13063.52 1234.20 o 21 1 1 1739.70 859.97 512.87 o 23 1 1 38.61 233.88 364.61 o 25 1 1 61.60 177.65 288.29 o -24 2 1 41.73 178.43 232.01 o -22 2 1 2485.66 2479.28 533.02 o -20 2 1 1071.31 1635.73 680.27 o -18 2 1 732.46 574.15 201.79 o -16 2 1 43197.50 44816.39 571.83 o -14 2 1 366.67 305.73 100.83 o -12 2 1 17380.84 17818.13 200.60 o -10 2 1 90214.18 89123.13 385.14 o -8 2 1 148967.72 155167.47 367.85 o -6 2 1 287277.94 289787.44 449.89 o -4 2 1 1317.39 1441.06 231.75 o 2 2 1 407.92 454.37 96.94 o 4 2 1 2027.22 1655.57 93.07 o 6 2 1 182817.16 202276.16 532.90 o 8 2 1 167294.11 164339.25 361.58 o 10 2 1 30052.93 31139.38 628.62 o 12 2 1 6862.88 5617.38 222.09 o 14 2 1 2330.60 2000.24 242.05 o 16 2 1 12068.54 10366.89 388.25 o 18 2 1 11.83 56.78 181.56 o 20 2 1 2883.29 3307.61 582.14 o 22 2 1 12723.25 15167.55 949.69 o 24 2 1 18.69 71.41 262.34 o -25 3 1 1822.16 1082.94 413.94 o -23 3 1 3241.40 3321.85 475.94 o -21 3 1 6674.20 6573.81 536.46 o -19 3 1 2075.46 1365.41 379.31 o -17 3 1 3853.36 4469.06 401.63 o -15 3 1 475.60 294.78 144.75 o -13 3 1 175.90 399.80 117.64 o -11 3 1 1943.75 2418.09 209.45 o -9 3 1 98607.78 109100.07 402.53 o -7 3 1 84994.49 91186.79 367.00 o -5 3 1 154541.13 154650.48 346.81 o -3 3 1 58768.64 52709.04 176.73 o -1 3 1 176.90 275.95 57.61 o 1 3 1 5872.19 5664.62 340.71 o 3 3 1 208449.97 223365.83 363.53 o 5 3 1 86664.45 72902.12 284.96 o 7 3 1 29705.29 25488.10 246.41 o 9 3 1 261051.52 268621.50 427.12 o 11 3 1 676.98 508.87 115.86 o 13 3 1 46454.04 49588.25 1124.98 o 15 3 1 79.24 33.43 78.15 o 17 3 1 1719.62 1259.45 233.53 o 19 3 1 470.49 211.29 202.29 o 21 3 1 2972.07 2998.79 520.92 o 23 3 1 1043.63 673.01 367.73 o 25 3 1 2576.18 2342.93 677.35 o -24 4 1 15.62 153.42 282.34 o -22 4 1 346.08 226.48 215.44 o -20 4 1 3514.76 2561.79 377.29 o -18 4 1 11.21 87.45 129.13 o -16 4 1 5233.00 4824.21 299.34 o -14 4 1 101428.30 107740.05 613.68 o -12 4 1 57682.21 58143.56 381.47 o -10 4 1 297.53 287.24 105.35 o -8 4 1 1047.68 834.37 83.89 o -6 4 1 50800.18 50270.04 1037.61 o -4 4 1 238659.69 233956.09 548.15 o -2 4 1 3535.21 3337.78 257.71 o 0 4 1 92431.14 86134.73 212.11 o 2 4 1 549452.69 511711.53 544.13 o 4 4 1 55280.39 55069.73 227.64 o 6 4 1 122525.52 120526.27 359.08 o 8 4 1 20390.24 18981.22 180.97 o 10 4 1 84093.06 80155.05 430.89 o 12 4 1 680.20 962.75 99.18 o 14 4 1 37472.70 38999.07 783.72 o 16 4 1 18028.79 18851.72 1061.51 o 18 4 1 693.17 605.01 241.02 o 20 4 1 14416.11 15515.53 633.12 o 22 4 1 290.48 194.70 185.83 o 24 4 1 36.51 29.21 97.90 o -25 5 1 74.07 131.25 406.46 o -23 5 1 19.69 100.45 243.12 o -21 5 1 3416.07 4697.04 482.26 o -19 5 1 1877.85 1724.50 268.61 o -17 5 1 806.86 562.57 128.45 o -15 5 1 29544.53 30513.98 1727.44 o -13 5 1 12595.05 15252.36 903.61 o -11 5 1 156858.33 173632.72 2543.76 o -9 5 1 27313.82 25617.65 527.33 o -7 5 1 10435.56 9948.75 210.84 o -5 5 1 14926.54 15094.80 429.95 o -3 5 1 163708.19 164778.80 318.05 o -1 5 1 18276.06 17314.04 335.66 o 1 5 1 20221.54 18104.79 295.64 o 3 5 1 181639.16 158959.50 326.41 o 5 5 1 69109.34 71590.98 244.68 o 7 5 1 19575.42 23547.58 966.78 o 9 5 1 8160.93 7885.13 130.54 o 11 5 1 51326.65 49574.84 407.40 o 13 5 1 8069.55 7669.60 667.04 o 15 5 1 1570.95 1538.32 217.51 o 17 5 1 5623.80 5355.59 361.82 o 19 5 1 3958.22 4039.90 404.44 o 21 5 1 3138.34 2699.81 525.52 o 23 5 1 0.91 -25.23 209.39 o -24 6 1 1.10 128.74 259.04 o -22 6 1 3283.44 3449.86 514.41 o -20 6 1 1873.51 1109.09 435.36 o -18 6 1 14722.12 16558.78 999.62 o -16 6 1 1803.58 2165.31 231.48 o -14 6 1 198.48 71.34 113.84 o -12 6 1 40795.99 41513.50 396.70 o -10 6 1 6050.45 5084.50 139.76 o -8 6 1 36486.37 40106.21 993.52 o -6 6 1 258.94 226.16 72.15 o -4 6 1 27346.01 32085.03 551.11 o -2 6 1 33175.13 39871.04 881.14 o 0 6 1 40.10 63.79 62.46 o 2 6 1 15214.59 16126.54 593.90 o 4 6 1 186080.94 178730.19 353.41 o 6 6 1 73480.84 65702.85 258.48 o 8 6 1 287018.06 258386.63 471.48 o 10 6 1 7820.78 7590.41 208.72 o 12 6 1 12297.36 11500.69 837.87 o 14 6 1 28343.32 30830.13 1553.71 o 16 6 1 3137.40 3357.02 384.97 o 18 6 1 468.49 703.95 306.46 o 20 6 1 492.44 203.32 195.61 o 22 6 1 2535.48 2178.85 657.72 o 24 6 1 1772.66 2408.69 542.91 o -23 7 1 6.30 103.84 287.51 o -21 7 1 621.74 619.92 408.43 o -19 7 1 4170.75 5462.60 510.63 o -17 7 1 6531.29 6774.29 511.30 o -15 7 1 1303.09 1168.19 204.46 o -13 7 1 3862.70 4092.00 187.75 o -11 7 1 1021.63 991.92 70.97 o -9 7 1 57779.58 58027.94 341.69 o -7 7 1 23736.39 25513.14 235.71 o -5 7 1 10749.07 11928.85 269.65 o -3 7 1 125363.05 120903.39 1449.22 o -1 7 1 20626.63 18012.22 167.11 o 1 7 1 16242.15 14085.56 85.78 o 3 7 1 45462.71 46121.29 793.18 o 5 7 1 5420.64 5274.92 84.06 o 7 7 1 6228.30 6361.35 128.04 o 9 7 1 9455.77 8333.73 325.11 o 11 7 1 9.01 74.90 83.33 o 13 7 1 19.05 -9.41 79.66 o 15 7 1 10.33 -8.65 114.24 o 17 7 1 699.86 200.20 233.51 o 19 7 1 8.32 172.74 315.81 o 21 7 1 337.75 255.34 341.73 o 23 7 1 4.57 329.13 306.19 o -22 8 1 941.95 469.36 237.11 o -20 8 1 225.51 244.17 215.57 o -18 8 1 3968.47 3954.28 593.68 o -16 8 1 293.36 85.25 132.12 o -14 8 1 13941.88 11794.40 460.12 o -12 8 1 28074.60 28225.35 902.24 o -10 8 1 2006.07 2200.51 116.08 o -8 8 1 7312.24 8447.38 876.71 o -6 8 1 11311.69 13375.27 270.48 o -4 8 1 11167.29 12270.57 227.95 o -2 8 1 2922.66 2126.79 301.20 o 0 8 1 25992.96 22950.53 196.13 o 2 8 1 148794.58 155180.97 463.77 o 4 8 1 17662.71 17707.62 190.29 o 6 8 1 9418.63 9814.25 269.71 o 8 8 1 2541.83 1933.89 274.81 o 10 8 1 1640.65 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