#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2014336.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2014336_Fobs loop_ _publ_author_name 'Oh, Myeong-Jin' 'Lee, Yong-Min' 'Lee, Seung Jae' 'Kang, Sung Kwon' 'Choi, Sung-Nak' _publ_section_title ; Tris(1,10-phenanthroline)copper(II) di-\m-iodo-bis(diiodomercurate) dimethyl sulfoxide monohydrate ; _journal_coeditor_code GA1111 _journal_issue 2 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first m51 _journal_page_last m53 _journal_volume 62 _journal_year 2006 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 95.789 _cell_angle_gamma 90.000 _cell_length_a 12.6628 _cell_length_b 18.8367 _cell_length_c 20.1380 _exptl_crystal_F_000 3364.00 _reflns_d_resolution_high 0.8107 _[local]_cod_data_source_file ga1111Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' [Cu(Phen)3][I2HgI2HgI2] in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 1203.28 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 9652.50 12464.44 497.46 o 3 0 0 163061.55 166509.33 4733.56 o 4 0 0 165667.94 164060.09 2785.07 o 5 0 0 151037.00 160091.97 2772.27 o 6 0 0 83252.32 87309.16 1661.44 o 7 0 0 973.11 995.50 178.84 o 8 0 0 935.90 1204.72 201.57 o 9 0 0 16935.39 16004.15 600.24 o 10 0 0 59206.48 62961.36 1464.59 o 11 0 0 8.64 -215.77 322.58 o 12 0 0 3474.07 4135.23 700.76 o 13 0 0 2258.99 2124.17 784.84 o 14 0 0 536.48 70.23 332.69 o 15 0 0 71.17 314.59 383.30 o 1 1 0 104791.30 110654.14 3108.79 o 2 1 0 22206.01 24457.83 576.73 o 3 1 0 61.20 213.75 56.11 o 4 1 0 140158.72 137822.55 1833.54 o 5 1 0 738474.31 733002.81 9135.88 o 6 1 0 1474.76 1377.09 137.58 o 7 1 0 8939.20 8896.32 272.02 o 8 1 0 10506.20 10131.85 311.79 o 9 1 0 2129.93 1743.05 177.43 o 10 1 0 12086.05 12698.58 404.81 o 11 1 0 12336.91 12037.02 420.05 o 12 1 0 186.65 321.10 165.86 o 13 1 0 325.25 365.46 179.69 o 14 1 0 556.21 358.74 269.43 o 15 1 0 285.16 596.38 297.59 o 1 2 0 15055.18 15800.37 568.53 o 2 2 0 7049.41 8249.25 419.43 o 3 2 0 2051.17 2584.05 147.35 o 4 2 0 738.36 838.12 92.36 o 5 2 0 24880.61 27169.18 504.91 o 6 2 0 8282.30 7646.96 425.73 o 7 2 0 2409.03 2453.60 180.99 o 8 2 0 91.69 10.86 163.76 o 9 2 0 660.88 268.31 125.67 o 10 2 0 92.18 67.71 139.63 o 11 2 0 288.54 186.51 160.54 o 12 2 0 3043.48 3031.82 274.66 o 13 2 0 110.13 -61.06 189.07 o 14 2 0 53.08 217.20 275.36 o 15 2 0 148.55 337.71 235.45 o 1 3 0 4442.42 4585.86 275.90 o 2 3 0 40682.66 42675.28 843.07 o 3 3 0 2441.72 2888.46 150.75 o 4 3 0 6497.02 6138.72 196.35 o 5 3 0 8859.32 9604.46 311.65 o 6 3 0 171.67 164.62 102.43 o 7 3 0 6348.82 6722.36 267.27 o 8 3 0 1715.01 1381.73 212.14 o 9 3 0 3842.87 3801.73 271.76 o 10 3 0 430.72 589.62 161.83 o 11 3 0 2941.40 3164.13 258.27 o 12 3 0 151.69 178.71 188.50 o 13 3 0 371.81 363.08 211.07 o 14 3 0 2793.42 2443.22 319.38 o 15 3 0 453.27 235.72 243.77 o 0 4 0 58759.94 61707.69 1856.08 o 1 4 0 1564.84 1389.97 156.21 o 2 4 0 378.15 427.20 104.38 o 3 4 0 6146.76 6328.23 231.26 o 4 4 0 25267.89 23981.79 442.91 o 5 4 0 2127.10 2518.38 151.97 o 6 4 0 15811.38 15873.71 388.63 o 7 4 0 243.72 167.07 105.48 o 8 4 0 3712.00 4095.05 274.96 o 9 4 0 7512.79 7662.39 331.96 o 10 4 0 115.46 585.61 211.36 o 11 4 0 2576.52 2714.46 285.17 o 12 4 0 82.32 167.57 179.57 o 13 4 0 0.13 13.13 190.37 o 14 4 0 26.74 -186.16 211.45 o 15 4 0 7.78 -12.17 233.62 o 1 5 0 37492.25 37257.81 1617.98 o 2 5 0 2387.32 2464.78 277.80 o 3 5 0 3366.18 3494.30 215.37 o 4 5 0 11616.04 11948.64 286.57 o 5 5 0 8491.08 10130.25 301.08 o 6 5 0 32840.59 32532.76 615.82 o 7 5 0 670.08 637.03 126.67 o 8 5 0 125.41 21.92 113.52 o 9 5 0 1320.49 1396.32 233.29 o 10 5 0 5521.70 7077.95 419.91 o 11 5 0 7452.82 6247.94 419.77 o 12 5 0 320.59 -5.56 163.15 o 13 5 0 540.17 127.42 203.53 o 14 5 0 648.72 335.59 234.54 o 15 5 0 1330.51 1353.89 304.35 o 0 6 0 161901.19 172828.53 5873.40 o 1 6 0 284.08 117.35 134.96 o 2 6 0 108.53 207.78 147.76 o 3 6 0 681.30 634.64 135.04 o 4 6 0 4619.14 4801.09 353.40 o 5 6 0 56113.30 56091.71 897.32 o 6 6 0 8503.95 9198.55 378.70 o 7 6 0 1861.17 2165.27 177.32 o 8 6 0 1890.05 1506.96 220.04 o 9 6 0 538.72 531.87 259.86 o 10 6 0 6127.15 6200.19 402.26 o 11 6 0 3745.04 3838.54 453.54 o 12 6 0 2143.72 1954.67 308.61 o 13 6 0 1228.19 1390.81 367.61 o 14 6 0 257.77 626.17 247.73 o 15 6 0 338.44 451.58 245.09 o 1 7 0 116011.16 113733.02 2044.98 o 2 7 0 3473.82 3609.17 310.08 o 3 7 0 64.20 84.44 108.84 o 4 7 0 35903.07 35462.28 862.62 o 5 7 0 194061.70 196448.25 3488.55 o 6 7 0 18047.31 17422.54 460.70 o 7 7 0 134.84 429.32 246.30 o 8 7 0 465.79 181.85 165.39 o 9 7 0 605.43 310.58 179.17 o 10 7 0 4929.92 5190.59 386.34 o 11 7 0 6767.13 6939.50 452.28 o 12 7 0 246.74 -33.22 207.53 o 13 7 0 177.80 566.92 256.92 o 14 7 0 885.83 509.16 265.54 o 0 8 0 1043667.06 1040792.31 20390.97 o 1 8 0 48556.23 48380.24 872.19 o 2 8 0 660.89 390.09 140.71 o 3 8 0 2585.70 3322.19 259.18 o 4 8 0 90225.95 91517.09 1807.41 o 5 8 0 35096.23 35533.61 918.85 o 6 8 0 27510.31 27348.14 876.66 o 7 8 0 56.56 -97.88 145.01 o 8 8 0 1433.09 1103.17 224.27 o 9 8 0 3049.57 3754.08 334.38 o 10 8 0 16512.26 17932.10 647.94 o 11 8 0 42.41 170.12 215.01 o 12 8 0 1370.78 952.48 398.05 o 13 8 0 203.65 -102.80 266.70 o 14 8 0 883.63 688.99 258.82 o 1 9 0 79405.70 74885.19 1268.96 o 2 9 0 10959.02 10688.38 314.33 o 3 9 0 319.26 440.31 156.47 o 4 9 0 52229.28 53814.66 1220.69 o 5 9 0 255646.42 244388.47 4308.85 o 6 9 0 17779.70 16181.81 612.29 o 7 9 0 6784.00 6957.53 441.76 o 8 9 0 2013.90 2052.25 495.22 o 9 9 0 5411.95 6086.28 467.73 o 10 9 0 663.05 1227.91 255.40 o 11 9 0 78.53 271.39 219.72 o 12 9 0 246.24 43.74 349.76 o 13 9 0 112.55 74.66 244.10 o 14 9 0 4.30 96.23 252.58 o 0 10 0 203559.58 196791.05 4199.55 o 1 10 0 34280.28 33157.55 695.08 o 2 10 0 12888.05 12591.88 365.16 o 3 10 0 7448.96 7642.50 432.42 o 4 10 0 708.27 670.40 198.68 o 5 10 0 664.10 1026.43 227.68 o 6 10 0 1812.44 1519.69 262.55 o 7 10 0 4029.07 3776.56 366.30 o 8 10 0 15.02 -129.15 183.28 o 9 10 0 1.36 -10.83 206.17 o 10 10 0 10048.23 10340.13 614.48 o 11 10 0 5059.85 5407.12 510.26 o 12 10 0 815.56 579.60 260.18 o 13 10 0 577.33 600.81 267.82 o 14 10 0 81.42 -86.53 241.20 o 1 11 0 81865.16 79675.13 1378.80 o 2 11 0 3223.48 2252.30 618.67 o 3 11 0 509.80 57.73 174.26 o 4 11 0 10894.38 11300.70 511.95 o 5 11 0 5488.94 5616.05 485.66 o 6 11 0 24990.57 25927.90 850.68 o 7 11 0 4377.39 3778.37 657.71 o 8 11 0 10.29 -200.26 200.26 o 9 11 0 238.09 194.45 223.55 o 10 11 0 4024.19 4030.40 578.84 o 11 11 0 1893.64 2422.99 429.22 o 12 11 0 559.75 645.10 432.21 o 13 11 0 172.04 381.60 289.41 o 0 12 0 11784.34 10416.87 531.28 o 1 12 0 100.25 164.69 130.40 o 2 12 0 674.05 134.54 161.41 o 3 12 0 2280.55 2213.16 286.42 o 4 12 0 26291.06 26412.66 830.28 o 5 12 0 15311.42 14873.96 699.63 o 6 12 0 28784.55 29539.97 928.09 o 7 12 0 468.58 505.30 225.08 o 8 12 0 5768.96 5968.86 476.33 o 9 12 0 11052.55 10672.22 1185.94 o 10 12 0 1026.27 1193.73 357.89 o 11 12 0 2999.36 2396.55 395.80 o 12 12 0 432.35 188.09 279.25 o 13 12 0 142.36 -131.73 306.92 o 1 13 0 43922.42 42963.62 1102.51 o 2 13 0 405.21 1117.21 354.45 o 3 13 0 14328.49 14508.35 612.75 o 4 13 0 14594.96 14907.05 637.67 o 5 13 0 258.95 405.71 226.29 o 6 13 0 11009.74 11827.57 591.27 o 7 13 0 1048.11 596.53 249.55 o 8 13 0 87.86 96.81 232.54 o 9 13 0 463.82 540.68 263.20 o 10 13 0 2386.49 2903.27 453.74 o 11 13 0 170.84 337.20 292.17 o 12 13 0 1.90 -73.87 267.33 o 0 14 0 3450.62 3217.48 681.40 o 1 14 0 376.01 317.23 226.74 o 2 14 0 2042.40 1957.06 296.62 o 3 14 0 338.90 -83.49 232.56 o 4 14 0 1548.25 1623.47 304.03 o 5 14 0 5593.27 6020.32 730.26 o 6 14 0 605.51 795.69 271.65 o 7 14 0 33.04 -9.69 230.92 o 8 14 0 2970.71 2836.61 390.19 o 9 14 0 36.75 342.50 259.83 o 10 14 0 2468.79 2720.81 433.12 o 11 14 0 1122.78 1258.81 369.52 o 12 14 0 409.30 18.47 286.88 o 1 15 0 16680.06 20113.88 1008.74 o 2 15 0 5.70 -120.55 375.25 o 3 15 0 540.18 278.07 224.53 o 4 15 0 1220.05 501.15 380.12 o 5 15 0 831.95 1136.43 307.16 o 6 15 0 3991.97 3730.13 447.04 o 7 15 0 29.54 -303.08 303.08 o 8 15 0 1738.81 1753.15 353.88 o 9 15 0 72.54 17.87 248.49 o 10 15 0 47.08 392.46 312.54 o 11 15 0 958.77 640.21 335.05 o 0 16 0 17146.53 17871.04 1368.37 o 1 16 0 1571.31 1665.57 439.25 o 2 16 0 71.90 -294.33 294.33 o 3 16 0 222.99 56.60 148.71 o 4 16 0 6904.32 8513.63 558.26 o 5 16 0 7.53 -81.50 233.86 o 6 16 0 1044.26 1116.33 303.29 o 7 16 0 730.59 303.36 263.99 o 8 16 0 45.58 319.39 278.59 o 9 16 0 280.81 201.81 355.64 o 10 16 0 1142.77 1120.61 367.88 o 11 16 0 59.72 485.23 363.84 o 1 17 0 3674.55 4129.43 650.05 o 2 17 0 2812.08 3275.87 520.60 o 3 17 0 63.75 -265.73 302.86 o 4 17 0 289.44 842.04 305.05 o 5 17 0 19957.75 19740.22 898.48 o 6 17 0 2569.17 2292.49 385.93 o 7 17 0 192.44 -253.19 302.59 o 8 17 0 248.03 465.75 293.66 o 9 17 0 2416.83 2286.06 450.76 o 10 17 0 488.51 343.41 384.42 o 0 18 0 14037.77 15084.13 1355.83 o 1 18 0 3350.29 3695.68 570.45 o 2 18 0 880.13 1179.03 410.90 o 3 18 0 1529.32 1690.19 480.29 o 4 18 0 719.49 740.07 396.60 o 5 18 0 2495.71 2707.62 459.78 o 6 18 0 622.20 906.46 334.49 o 7 18 0 2483.02 1982.85 395.57 o 8 18 0 8.30 187.54 417.97 o 9 18 0 31.54 -264.35 282.17 o 1 19 0 3922.81 5267.76 1413.66 o 2 19 0 859.34 1015.68 427.88 o 3 19 0 716.06 1042.49 415.24 o 4 19 0 116.20 -279.52 820.05 o 5 19 0 1830.12 2001.16 546.93 o 6 19 0 5380.18 7073.16 808.29 o 7 19 0 443.70 702.40 304.52 o 8 19 0 184.59 -71.96 372.57 o 0 20 0 190.34 890.42 595.00 o 1 20 0 46.09 389.92 366.34 o 2 20 0 276.26 394.43 379.47 o 3 20 0 32.04 -276.11 325.27 o 4 20 0 419.81 910.35 436.69 o 5 20 0 2886.60 3895.73 626.98 o 6 20 0 2530.03 3164.25 626.42 o 7 20 0 162.91 -85.36 437.24 o 1 21 0 2449.78 2073.35 850.70 o 2 21 0 11.36 -322.42 322.42 o 3 21 0 1100.19 1155.02 600.58 o 4 21 0 1344.17 1351.72 494.80 o 5 21 0 15.68 364.88 409.46 o 6 21 0 904.15 1938.47 530.21 o 0 22 0 165.54 713.45 634.02 o 1 22 0 287.02 -304.91 368.57 o 2 22 0 1064.07 1427.73 475.08 o 3 22 0 357.73 570.29 450.78 o 4 22 0 3.77 76.41 399.57 o 5 22 0 29.77 -23.97 482.13 o 1 23 0 262.35 684.72 457.40 o 2 23 0 49.03 216.01 716.93 o -15 1 1 267.77 342.96 260.50 o -14 1 1 284.48 266.41 197.36 o -13 1 1 2242.66 2102.16 251.78 o -12 1 1 318.13 367.76 164.92 o -11 1 1 3798.87 4435.82 290.72 o -10 1 1 213.60 495.78 178.43 o -9 1 1 457.72 558.11 138.22 o -8 1 1 10502.99 11167.39 325.58 o -7 1 1 26741.77 27570.99 514.09 o -6 1 1 56829.10 59317.70 857.34 o -5 1 1 18.27 -9.25 82.54 o -4 1 1 98285.64 108677.61 1476.32 o -3 1 1 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-1 2 1 42052.92 45676.01 1404.60 o 1 2 1 151970.19 163304.64 3223.47 o 2 2 1 33406.51 35086.84 553.11 o 3 2 1 281.92 481.36 68.43 o 4 2 1 2484.45 2190.48 125.18 o 5 2 1 109579.51 112416.72 1565.72 o 6 2 1 12869.52 12472.22 335.80 o 7 2 1 40133.89 39182.56 721.67 o 8 2 1 6946.94 7386.62 373.31 o 9 2 1 1376.53 861.72 171.15 o 10 2 1 46656.73 46000.75 838.28 o 11 2 1 16128.57 16529.05 479.32 o 12 2 1 433.10 390.75 173.05 o 13 2 1 4292.04 4334.44 370.38 o 14 2 1 422.33 456.10 230.77 o 15 2 1 20.63 448.18 238.84 o -15 3 1 1347.56 1358.09 287.67 o -14 3 1 725.67 579.09 248.50 o -13 3 1 66.11 179.03 191.82 o -12 3 1 722.64 680.61 203.48 o -11 3 1 4117.34 5083.00 306.40 o -10 3 1 54903.69 55121.49 943.00 o -9 3 1 4819.05 4854.49 276.03 o -8 3 1 572.35 590.56 158.41 o -7 3 1 2302.08 2320.50 222.63 o -6 3 1 329336.59 335797.34 4342.45 o -5 3 1 6053.15 6222.17 340.04 o -4 3 1 24.55 -19.47 63.70 o -3 3 1 1007.89 1453.14 98.98 o -2 3 1 1362.71 1613.73 174.72 o -1 3 1 188755.36 195477.83 5479.06 o 0 3 1 24.10 -32.55 41.59 o 1 3 1 855.38 912.00 98.04 o 2 3 1 5796.79 5763.26 167.96 o 3 3 1 69490.61 79859.53 1108.08 o 4 3 1 2808.55 2499.09 164.92 o 5 3 1 73195.05 69465.73 1041.89 o 6 3 1 108911.14 104671.98 1513.45 o 7 3 1 10.48 -80.50 91.13 o 8 3 1 40222.41 36630.68 721.31 o 9 3 1 13798.87 12667.70 461.85 o 10 3 1 3718.24 4127.15 288.36 o 11 3 1 15950.62 15759.41 529.33 o 12 3 1 421.74 330.65 214.05 o 13 3 1 1132.34 1350.31 315.05 o 14 3 1 983.56 840.14 253.41 o 15 3 1 3421.78 3682.83 402.11 o -15 4 1 1653.61 1744.25 318.42 o -14 4 1 1735.03 2273.17 318.08 o -13 4 1 121.19 223.44 193.56 o -12 4 1 4361.68 4451.32 627.81 o -11 4 1 59556.29 58208.89 1143.60 o -10 4 1 4937.72 4871.51 309.94 o -9 4 1 25916.89 24902.34 595.56 o -8 4 1 10135.85 10545.56 353.94 o -7 4 1 2181.49 2152.57 174.71 o -6 4 1 186519.92 190242.14 2574.92 o -5 4 1 265654.22 268646.94 3495.45 o -4 4 1 4868.12 5163.44 187.21 o -3 4 1 35202.46 36007.94 580.05 o -2 4 1 18698.15 18015.33 452.25 o -1 4 1 84714.29 89094.27 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