#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/43/2014352.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2014352_Fobs loop_ _publ_author_name 'Din\,cer, Muharrem' '\"Ozdemir, Nam\?ik' 'Saydam, Sinan' 'Bekaro\(glu, \"Ozer' 'B\"uy\"ukg\"ung\"or, Orhan' _publ_section_title ; Hydrogen bonding in meso-4,5-diphenyl-3,6-diazaoctane-1,8-diol: the formation of one-dimensional linear chains of edge-fused rings ; _journal_coeditor_code GZ1025 _journal_issue 2 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first o89 _journal_page_last o91 _journal_volume 62 _journal_year 2006 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 103.035 _cell_angle_gamma 90.000 _cell_length_a 17.5849 _cell_length_b 6.8615 _cell_length_c 13.9453 _exptl_crystal_F_000 648.00 _reflns_d_resolution_high 0.8111 _[local]_cod_data_source_file gz1025Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' muh43 in C 2/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 161.72 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 6 0 0 51.86 47.19 5.17 o 8 0 0 1664.98 1484.89 6.52 o 10 0 0 1098.42 1042.29 5.93 o 12 0 0 105.38 108.02 3.11 o 14 0 0 225.61 189.18 4.04 o 16 0 0 72.77 61.66 2.62 o 18 0 0 72.14 67.18 2.43 o 20 0 0 178.08 215.49 3.82 o 1 1 0 1434.47 1466.16 15.30 o 3 1 0 349.54 236.99 18.14 o 5 1 0 20.26 14.88 2.77 o 7 1 0 59.99 56.20 2.89 o 9 1 0 319.42 283.75 4.63 o 11 1 0 1039.45 924.65 5.66 o 13 1 0 318.65 269.33 15.96 o 15 1 0 80.17 64.08 4.97 o 17 1 0 12.46 10.25 1.94 o 19 1 0 5.18 4.89 1.66 o 4 2 0 4575.39 4153.29 282.04 o 6 2 0 133.95 151.14 16.77 o 8 2 0 178.67 160.66 9.32 o 10 2 0 70.05 71.74 2.75 o 12 2 0 0.08 -2.03 2.62 o 14 2 0 900.95 807.66 4.41 o 16 2 0 0.33 0.30 1.66 o 18 2 0 16.53 19.98 1.66 o 20 2 0 59.99 71.44 3.23 o 1 3 0 1426.69 1669.54 17.15 o 3 3 0 7.87 6.59 1.56 o 5 3 0 76.60 83.97 5.89 o 7 3 0 206.09 169.96 13.84 o 9 3 0 537.68 527.80 69.12 o 11 3 0 400.41 396.70 43.14 o 13 3 0 204.87 203.54 12.78 o 15 3 0 5.65 6.37 3.16 o 17 3 0 1.17 2.55 2.25 o 19 3 0 15.48 18.57 6.55 o 0 4 0 2100.20 2290.55 36.12 o 2 4 0 2466.03 2619.01 38.23 o 4 4 0 0.31 -0.23 1.35 o 6 4 0 14.24 13.24 1.41 o 8 4 0 28.94 19.20 2.12 o 10 4 0 123.12 113.24 13.40 o 12 4 0 760.32 694.21 48.59 o 14 4 0 1.51 0.91 2.36 o 16 4 0 6.71 2.87 1.49 o 18 4 0 0.94 0.96 1.52 o 1 5 0 69.60 56.20 1.40 o 3 5 0 117.18 133.95 2.38 o 5 5 0 92.20 123.15 7.87 o 7 5 0 164.92 173.18 17.50 o 9 5 0 121.63 104.97 10.94 o 11 5 0 296.80 311.74 35.42 o 13 5 0 53.47 56.94 6.39 o 15 5 0 53.92 49.06 4.87 o 17 5 0 7.15 10.31 2.22 o 0 6 0 4.96 11.96 2.07 o 2 6 0 71.81 88.50 1.56 o 4 6 0 239.62 194.81 9.96 o 6 6 0 44.92 36.08 3.07 o 8 6 0 5.93 8.45 1.19 o 10 6 0 3.99 3.12 1.47 o 12 6 0 30.33 27.54 4.44 o 14 6 0 18.44 18.59 1.58 o 1 7 0 0.23 1.17 1.31 o 3 7 0 0.02 0.22 1.42 o 5 7 0 51.21 53.22 3.57 o 7 7 0 1.42 -0.46 1.72 o 9 7 0 37.05 38.13 4.01 o 11 7 0 18.09 16.28 1.95 o 0 8 0 20.53 16.09 1.76 o 2 8 0 80.52 74.42 4.86 o 4 8 0 22.57 21.11 1.81 o 6 8 0 3.33 1.00 1.58 o -21 1 1 127.78 163.59 2.01 o -19 1 1 65.58 67.59 4.40 o -17 1 1 43.61 45.53 1.98 o -15 1 1 220.67 184.69 10.25 o -13 1 1 23.43 24.28 2.79 o -11 1 1 69.53 49.98 2.84 o -9 1 1 1352.91 1109.08 6.37 o -7 1 1 35.85 35.25 3.09 o -5 1 1 1039.16 770.52 31.22 o 1 1 1 4677.96 4577.18 135.52 o 3 1 1 7926.91 4231.67 2223.08 o 5 1 1 102.21 80.76 2.75 o 7 1 1 2487.26 2099.86 15.02 o 9 1 1 589.04 475.38 4.14 o 11 1 1 24.53 33.37 2.32 o 13 1 1 753.33 684.84 23.73 o 15 1 1 5.60 1.79 2.51 o 17 1 1 4.43 4.91 2.31 o 19 1 1 0.97 6.13 5.68 o -20 2 1 41.22 53.89 4.73 o -18 2 1 0.95 3.74 1.63 o -16 2 1 169.34 168.92 2.89 o -14 2 1 575.15 553.51 4.78 o -12 2 1 15.95 12.69 2.62 o -10 2 1 3.61 5.29 2.77 o -8 2 1 17.32 13.84 2.19 o -6 2 1 1038.16 964.40 79.64 o -4 2 1 27.56 25.44 2.38 o -2 2 1 4891.73 5077.99 160.70 o 0 2 1 2141.79 2271.72 92.37 o 2 2 1 67.80 95.41 4.36 o 4 2 1 38.92 35.44 3.12 o 6 2 1 2674.93 2331.44 304.67 o 8 2 1 99.60 88.97 4.95 o 10 2 1 2.90 5.05 4.41 o 12 2 1 10.30 17.44 3.60 o 14 2 1 106.62 119.18 2.21 o 16 2 1 108.74 111.72 4.67 o 18 2 1 51.92 47.40 1.71 o 20 2 1 1.96 8.12 1.70 o -19 3 1 22.83 23.42 2.72 o -17 3 1 7.46 10.46 2.35 o -15 3 1 64.59 64.11 2.45 o -13 3 1 215.04 207.70 3.85 o -11 3 1 165.04 151.31 6.52 o -9 3 1 207.16 213.61 17.91 o -7 3 1 353.26 411.44 40.20 o -5 3 1 558.25 656.20 53.47 o -3 3 1 326.85 373.15 7.17 o -1 3 1 3.20 5.71 1.21 o 1 3 1 2814.80 3012.33 40.92 o 3 3 1 2144.33 2462.87 73.01 o 5 3 1 82.99 64.91 4.76 o 7 3 1 85.51 113.90 17.66 o 9 3 1 764.76 657.34 98.54 o 11 3 1 5.83 4.38 2.07 o 13 3 1 333.53 348.34 21.16 o 15 3 1 9.23 7.82 2.28 o 17 3 1 0.00 -3.51 2.22 o 19 3 1 0.73 1.82 5.52 o -18 4 1 3.31 3.27 1.68 o -16 4 1 1.55 5.96 1.48 o -14 4 1 8.88 11.85 1.66 o -12 4 1 27.66 31.43 2.72 o -10 4 1 137.16 147.62 13.08 o -8 4 1 32.60 30.40 3.56 o -6 4 1 6.60 9.16 2.08 o -4 4 1 173.66 163.63 6.93 o -2 4 1 1572.54 1879.05 42.65 o 0 4 1 764.46 821.59 11.48 o 2 4 1 52.42 60.98 3.45 o 4 4 1 15.64 6.75 1.52 o 6 4 1 256.81 272.73 19.67 o 8 4 1 382.66 393.27 36.74 o 10 4 1 173.99 153.82 18.93 o 12 4 1 48.77 67.06 8.21 o 14 4 1 3.15 2.01 1.31 o 16 4 1 22.51 27.49 4.10 o 18 4 1 0.43 0.43 1.69 o -17 5 1 5.19 3.21 1.79 o -15 5 1 7.52 7.54 1.59 o -13 5 1 126.90 121.59 11.60 o -11 5 1 78.03 80.89 10.05 o -9 5 1 9.69 10.10 1.49 o -7 5 1 9.88 8.02 1.37 o -5 5 1 551.69 526.62 40.78 o -3 5 1 2.42 1.18 1.04 o -1 5 1 191.33 209.66 2.08 o 1 5 1 853.39 863.68 31.07 o 3 5 1 0.65 4.28 1.68 o 5 5 1 217.89 243.90 17.25 o 7 5 1 609.02 604.36 47.85 o 9 5 1 540.36 549.17 49.39 o 11 5 1 73.97 60.36 5.08 o 13 5 1 0.12 1.23 1.73 o 15 5 1 13.87 19.74 1.40 o -14 6 1 2.38 1.43 1.39 o -12 6 1 21.76 24.08 2.09 o -10 6 1 30.08 29.31 4.22 o -8 6 1 18.62 24.53 2.25 o -6 6 1 57.31 58.46 4.37 o -4 6 1 131.35 132.17 6.77 o -2 6 1 1.27 1.82 1.14 o 0 6 1 260.33 288.71 3.24 o 2 6 1 185.36 201.01 2.91 o 4 6 1 320.69 325.35 21.44 o 6 6 1 197.08 199.04 13.96 o 8 6 1 49.78 59.50 4.51 o 10 6 1 6.75 7.61 1.49 o 12 6 1 21.40 20.59 3.43 o 14 6 1 11.08 11.09 2.22 o -11 7 1 0.17 1.07 1.52 o -9 7 1 47.15 48.84 4.18 o -7 7 1 6.27 7.72 1.72 o -5 7 1 26.41 20.87 1.72 o -3 7 1 6.31 5.43 1.29 o -1 7 1 2.60 6.75 1.18 o 1 7 1 10.07 14.49 3.06 o 3 7 1 2.97 0.07 1.29 o 5 7 1 78.55 85.10 4.83 o 7 7 1 94.79 95.07 10.25 o 9 7 1 169.04 177.11 19.46 o 11 7 1 81.72 100.76 15.06 o -6 8 1 10.63 12.23 1.43 o -4 8 1 5.65 2.60 1.26 o -2 8 1 1.49 0.81 1.52 o 0 8 1 6.13 2.34 1.54 o 2 8 1 15.33 18.70 2.73 o 4 8 1 1.41 5.14 1.77 o 6 8 1 13.26 14.05 2.37 o -20 0 2 0.71 6.22 2.35 o -18 0 2 272.20 224.22 2.99 o -16 0 2 667.51 589.87 4.65 o -14 0 2 1890.25 1517.38 5.68 o -12 0 2 1761.93 1678.53 6.76 o -2 0 2 948.55 1063.91 17.27 o 0 0 2 2842.50 2847.36 69.38 o 2 0 2 8013.97 5083.47 108.85 o 4 0 2 1339.30 1057.52 22.36 o 6 0 2 8696.40 6590.76 13.18 o 8 0 2 5522.16 4551.96 10.07 o 10 0 2 806.33 646.24 5.14 o 12 0 2 115.55 138.20 4.12 o 14 0 2 140.75 130.95 2.92 o 16 0 2 40.18 42.53 2.52 o 18 0 2 183.41 177.18 2.84 o 20 0 2 24.27 48.36 2.47 o -21 1 2 5.54 4.84 1.97 o -19 1 2 50.44 43.83 1.97 o -17 1 2 300.91 282.10 8.73 o -15 1 2 371.35 333.19 3.50 o -13 1 2 191.62 178.75 3.26 o -11 1 2 52.55 52.35 4.14 o -9 1 2 376.22 330.00 3.94 o -7 1 2 56.85 44.29 4.34 o -5 1 2 124.11 105.75 16.93 o -3 1 2 1881.97 1967.31 190.79 o -1 1 2 210.11 229.66 3.64 o 1 1 2 60.48 62.03 2.90 o 3 1 2 204.26 190.94 13.66 o 5 1 2 1148.94 934.31 51.35 o 7 1 2 2679.19 2259.15 64.49 o 9 1 2 4.09 2.01 2.00 o 11 1 2 27.41 34.76 2.94 o 13 1 2 444.46 394.37 2.78 o 15 1 2 473.92 414.26 15.23 o 17 1 2 15.47 12.65 3.45 o 19 1 2 10.29 12.29 2.30 o -20 2 2 12.04 12.24 1.95 o -18 2 2 8.65 8.84 3.33 o -16 2 2 640.61 565.73 3.87 o -14 2 2 1591.92 1429.84 6.32 o -12 2 2 136.31 130.41 4.12 o -10 2 2 207.60 157.53 3.33 o -8 2 2 11.68 12.51 2.09 o -6 2 2 2030.04 2023.48 211.05 o -4 2 2 9.95 8.46 1.54 o -2 2 2 2838.15 3027.33 46.52 o 0 2 2 2202.46 2408.65 26.08 o 2 2 2 1042.34 1237.83 54.66 o 4 2 2 14.52 11.90 2.88 o 6 2 2 1344.36 1305.23 188.73 o 8 2 2 1201.78 1229.76 115.78 o 10 2 2 1998.71 1768.17 161.96 o 12 2 2 8.54 6.03 1.57 o 14 2 2 3.21 -0.18 1.69 o 16 2 2 213.79 201.95 18.12 o 18 2 2 40.94 37.81 2.05 o -19 3 2 0.91 1.61 1.53 o -17 3 2 4.92 5.19 1.66 o -15 3 2 227.03 229.28 11.72 o -13 3 2 23.01 21.97 1.58 o -11 3 2 844.85 839.95 33.47 o -9 3 2 0.48 1.08 1.68 o -7 3 2 234.88 242.31 23.56 o -5 3 2 2555.12 2692.45 244.10 o -3 3 2 26.20 29.22 1.88 o -1 3 2 494.74 575.26 4.46 o 1 3 2 3337.25 3779.65 39.94 o 3 3 2 3.14 2.00 1.58 o 5 3 2 3100.92 3186.47 216.24 o 7 3 2 607.09 612.66 88.43 o 9 3 2 1865.32 1806.75 298.29 o 11 3 2 0.28 1.50 1.72 o 13 3 2 68.85 76.58 6.73 o 15 3 2 84.77 97.16 12.58 o 17 3 2 1.12 1.61 1.87 o 19 3 2 45.40 65.45 11.49 o -18 4 2 71.50 79.92 9.10 o -16 4 2 16.44 14.33 4.45 o -14 4 2 308.63 327.02 4.70 o -12 4 2 404.31 366.25 25.01 o -10 4 2 214.36 223.18 21.54 o -8 4 2 1.23 0.98 1.40 o -6 4 2 38.57 39.95 3.25 o -4 4 2 162.35 155.10 8.16 o -2 4 2 9.51 12.71 1.45 o 0 4 2 58.46 69.15 1.42 o 2 4 2 20.88 14.01 1.77 o 4 4 2 38.36 32.12 1.77 o 6 4 2 5.34 2.42 1.33 o 8 4 2 1170.08 1131.58 99.05 o 10 4 2 53.75 72.75 8.36 o 12 4 2 2.42 4.08 3.00 o 14 4 2 83.54 94.11 14.61 o 16 4 2 0.01 0.00 1.56 o -17 5 2 6.14 5.79 1.82 o -15 5 2 24.69 29.41 1.73 o -13 5 2 167.14 160.14 15.44 o -11 5 2 184.25 180.65 18.47 o -9 5 2 92.56 95.27 11.10 o -7 5 2 62.13 78.08 6.50 o -5 5 2 4.40 7.47 1.22 o -3 5 2 961.75 944.15 26.09 o -1 5 2 405.61 409.12 4.80 o 1 5 2 2.18 3.21 1.28 o 3 5 2 829.65 801.31 21.42 o 5 5 2 460.41 428.40 18.48 o 7 5 2 720.35 712.92 58.24 o 9 5 2 416.40 462.32 45.42 o 11 5 2 170.07 157.99 19.69 o 13 5 2 0.04 -0.99 1.37 o 15 5 2 1.57 2.09 1.58 o -14 6 2 2.35 3.45 1.39 o -12 6 2 0.13 0.34 1.23 o -10 6 2 4.01 4.64 1.47 o -8 6 2 155.70 140.99 12.62 o -6 6 2 0.99 1.52 1.84 o -4 6 2 4.47 6.40 1.09 o -2 6 2 127.73 127.56 2.56 o 0 6 2 83.02 84.12 1.55 o 2 6 2 75.02 51.15 2.27 o 4 6 2 387.46 368.78 17.94 o 6 6 2 0.01 1.25 1.41 o 8 6 2 3.13 3.45 1.33 o 10 6 2 32.01 33.62 2.48 o 12 6 2 18.41 24.71 2.80 o 14 6 2 2.68 7.09 1.87 o -11 7 2 12.95 14.18 2.08 o -9 7 2 3.29 4.83 1.34 o -7 7 2 8.62 8.68 1.85 o -5 7 2 12.99 17.33 2.04 o -3 7 2 124.39 117.30 3.55 o -1 7 2 71.88 69.77 2.44 o 1 7 2 9.79 11.03 1.31 o 3 7 2 73.73 70.09 1.66 o 5 7 2 214.40 211.36 11.51 o 7 7 2 118.94 126.74 10.21 o 9 7 2 62.03 68.43 7.37 o 11 7 2 52.78 53.26 3.50 o -6 8 2 40.71 33.47 3.07 o -4 8 2 12.34 14.32 3.59 o -2 8 2 32.91 33.48 1.40 o 0 8 2 3.06 4.94 1.54 o 2 8 2 82.50 75.87 3.40 o 4 8 2 88.00 80.97 4.03 o -21 1 3 26.09 22.51 3.87 o -19 1 3 37.35 29.62 2.60 o -17 1 3 5.80 6.53 1.73 o -15 1 3 1665.98 1471.25 6.35 o -13 1 3 1189.74 968.97 5.07 o -11 1 3 3435.53 2766.54 8.28 o -9 1 3 7.48 7.15 3.87 o -7 1 3 428.80 483.71 61.36 o -5 1 3 989.07 877.28 148.86 o -3 1 3 108.64 126.91 11.48 o 1 1 3 85.57 88.92 8.48 o 3 1 3 222.45 174.00 12.69 o 5 1 3 294.26 250.76 12.12 o 7 1 3 1662.78 1530.53 33.92 o 9 1 3 77.07 68.28 5.30 o 11 1 3 34.60 43.73 2.58 o 13 1 3 227.94 185.53 2.18 o 15 1 3 2.11 1.71 3.44 o 17 1 3 38.51 30.70 2.38 o 19 1 3 0.08 0.31 5.21 o -20 2 3 26.49 26.22 4.67 o -18 2 3 193.61 194.87 3.77 o -16 2 3 2.16 9.60 3.36 o -14 2 3 9.38 8.01 3.58 o -12 2 3 5.05 7.47 3.80 o -10 2 3 32.85 34.06 2.45 o -8 2 3 575.72 621.02 80.27 o -6 2 3 410.23 398.24 50.39 o -4 2 3 441.34 454.79 37.73 o -2 2 3 149.75 179.56 2.59 o 0 2 3 619.91 699.32 7.47 o 2 2 3 1383.56 1460.81 83.92 o 4 2 3 6.14 4.25 3.32 o 6 2 3 29.41 23.22 2.22 o 8 2 3 0.45 2.35 1.83 o 10 2 3 75.51 76.07 1.78 o 12 2 3 785.96 709.55 26.63 o 14 2 3 104.85 102.64 10.30 o 16 2 3 0.00 4.55 1.86 o 18 2 3 30.71 34.34 4.92 o -19 3 3 23.51 23.54 3.28 o -17 3 3 0.00 1.42 1.87 o -15 3 3 512.24 514.28 3.00 o -13 3 3 784.29 732.83 24.81 o -11 3 3 45.48 45.50 1.70 o -9 3 3 310.80 286.66 18.54 o -7 3 3 756.97 843.47 85.11 o -5 3 3 0.56 1.66 1.39 o -3 3 3 740.41 834.76 22.34 o -1 3 3 49.86 41.28 1.78 o 1 3 3 868.86 1065.36 24.99 o 3 3 3 0.78 4.98 1.43 o 5 3 3 477.60 534.38 71.87 o 7 3 3 29.30 49.65 11.21 o 9 3 3 441.27 438.95 68.99 o 11 3 3 42.90 28.20 4.96 o 13 3 3 32.71 25.30 2.58 o 15 3 3 19.16 22.89 1.66 o 17 3 3 28.47 39.78 3.81 o -18 4 3 0.17 -0.40 2.98 o -16 4 3 20.60 22.91 1.80 o -14 4 3 104.06 118.34 1.80 o -12 4 3 28.23 31.14 1.78 o -10 4 3 157.11 156.21 16.32 o -8 4 3 29.34 35.60 2.90 o -6 4 3 49.09 54.79 3.63 o -4 4 3 96.26 92.17 2.82 o -2 4 3 148.77 155.16 15.97 o 0 4 3 340.29 428.22 2.93 o 2 4 3 7.18 9.53 1.64 o 4 4 3 22.18 23.73 3.21 o 6 4 3 85.33 82.94 5.02 o 8 4 3 324.31 335.27 27.70 o 10 4 3 5.89 9.85 1.91 o 12 4 3 30.98 30.61 8.53 o 14 4 3 0.00 3.09 1.84 o 16 4 3 26.40 44.78 3.35 o -17 5 3 0.11 1.81 3.34 o -15 5 3 1.81 2.78 1.71 o -13 5 3 338.49 328.80 32.86 o -11 5 3 13.35 12.51 1.45 o -9 5 3 5.96 6.07 1.54 o -7 5 3 44.81 45.85 3.62 o -5 5 3 637.29 598.21 40.91 o -3 5 3 56.21 60.72 3.39 o -1 5 3 81.93 82.75 1.35 o 1 5 3 26.28 33.73 1.77 o 3 5 3 624.04 616.05 20.40 o 5 5 3 64.13 63.77 3.88 o 7 5 3 0.83 -2.58 2.09 o 9 5 3 10.90 12.73 1.64 o 11 5 3 56.59 48.08 5.08 o 13 5 3 64.30 72.36 7.13 o 15 5 3 24.10 30.67 4.92 o -14 6 3 7.08 6.77 1.79 o -12 6 3 10.84 11.50 1.84 o -10 6 3 27.94 29.95 3.67 o -8 6 3 66.89 66.61 7.78 o -6 6 3 274.70 276.95 25.08 o -4 6 3 65.95 61.77 2.93 o -2 6 3 235.59 223.43 4.72 o 0 6 3 45.04 39.20 1.55 o 2 6 3 4.58 5.00 1.47 o 4 6 3 103.12 109.33 3.90 o 6 6 3 33.23 29.47 3.66 o 8 6 3 6.22 6.16 1.43 o 10 6 3 139.39 150.14 19.23 o 12 6 3 42.45 42.68 5.30 o -11 7 3 7.92 9.18 2.16 o -9 7 3 32.00 33.26 3.99 o -7 7 3 33.93 36.87 3.18 o -5 7 3 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