#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/43/2014355.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2014355_Fobs loop_ _publ_author_name 'Bourne, Susan A.' 'De Villiers, Katherine' 'Egan, Timothy J.' _publ_section_title ; Three 4-aminoquinolines of antimalarial interest ; _journal_coeditor_code HJ1079 _journal_issue 2 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first o53 _journal_page_last o57 _journal_volume 62 _journal_year 2006 _space_group_IT_number 61 _symmetry_space_group_name_Hall '-P 2ac 2ab' _symmetry_space_group_name_H-M 'P b c a' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 13.2379 _cell_length_b 7.8883 _cell_length_c 29.4118 _exptl_crystal_F_000 1472.00 _reflns_d_resolution_high 0.7787 _[local]_cod_data_source_file hj1079Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' qia in Pbca (absorption correction)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 382.38 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' 'x+1/2, -y+1/2, -z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, y, -z-1/2' '-x-1/2, y-1/2, z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 83307.10 79201.22 1471.47 o 4 0 0 65849.84 65958.34 1018.93 o 6 0 0 74084.37 74377.76 1032.45 o 8 0 0 483.35 375.55 26.93 o 10 0 0 4224.98 4010.34 105.54 o 12 0 0 13165.24 13265.24 388.58 o 14 0 0 1525.05 1575.56 152.32 o 16 0 0 78.05 312.93 242.89 o 2 1 0 146217.55 142647.22 1814.23 o 4 1 0 54872.72 53851.85 607.68 o 6 1 0 9331.15 10422.55 126.57 o 8 1 0 24143.57 25101.28 281.11 o 10 1 0 7413.54 7185.46 116.79 o 12 1 0 387.36 246.33 67.44 o 14 1 0 2847.05 2758.38 98.28 o 16 1 0 2724.73 2754.92 191.96 o 0 2 0 3610.52 3360.02 81.60 o 2 2 0 2038.31 1920.30 27.03 o 4 2 0 2633.37 2856.67 55.51 o 6 2 0 74757.75 77213.44 970.61 o 8 2 0 12256.10 12214.05 182.32 o 10 2 0 73.05 61.80 24.40 o 12 2 0 4976.22 5322.21 132.94 o 14 2 0 982.75 1470.32 225.81 o 16 2 0 1044.41 968.45 177.37 o 2 3 0 5327.22 5241.07 67.29 o 4 3 0 20616.47 21017.12 289.23 o 6 3 0 6565.73 7084.84 118.58 o 8 3 0 5127.39 5341.55 97.76 o 10 3 0 17007.37 18595.70 334.00 o 12 3 0 869.51 679.83 123.29 o 14 3 0 1503.94 1778.24 196.61 o 16 3 0 707.52 888.36 140.49 o 0 4 0 3400.87 3473.72 77.79 o 2 4 0 4263.52 4398.73 85.66 o 4 4 0 679.68 831.11 25.60 o 6 4 0 231.25 369.45 34.33 o 8 4 0 774.64 645.38 43.67 o 10 4 0 4081.26 4107.75 103.36 o 12 4 0 616.12 629.52 145.33 o 14 4 0 281.78 108.46 213.71 o 2 5 0 65.77 265.95 50.86 o 4 5 0 1107.02 1248.18 56.54 o 6 5 0 153.43 186.45 37.65 o 8 5 0 431.44 456.63 98.27 o 10 5 0 164.23 29.40 175.09 o 12 5 0 731.29 920.91 265.25 o 14 5 0 32.39 447.04 254.82 o 0 6 0 11463.04 11933.70 329.80 o 2 6 0 371.46 418.02 38.76 o 4 6 0 161.77 284.55 35.53 o 6 6 0 2163.15 2178.47 139.44 o 8 6 0 1.58 -146.03 146.03 o 10 6 0 313.55 341.24 248.86 o 12 6 0 299.56 649.20 212.56 o 2 7 0 11829.29 11703.36 545.39 o 4 7 0 10107.06 10484.70 490.26 o 6 7 0 147.07 193.28 83.83 o 8 7 0 5966.49 5872.68 409.79 o 10 7 0 1439.74 1494.83 258.42 o 12 7 0 736.51 648.11 270.76 o 4 8 0 857.62 710.80 144.54 o 4 9 0 5034.63 4367.63 555.83 o 0 10 0 3259.95 3087.59 414.26 o 2 10 0 1020.66 734.64 269.72 o 1 1 1 2081.96 1875.52 20.90 o 2 1 1 4571.51 4355.30 39.14 o 3 1 1 1431.45 1501.77 13.81 o 4 1 1 9840.39 9667.69 69.82 o 5 1 1 12653.67 13239.70 105.57 o 6 1 1 3180.45 3351.85 31.56 o 7 1 1 472.80 552.20 13.61 o 8 1 1 828.67 792.92 13.86 o 9 1 1 4872.77 4915.03 57.87 o 10 1 1 336.61 377.85 20.51 o 11 1 1 767.04 755.63 27.82 o 12 1 1 82.91 112.58 39.51 o 13 1 1 594.01 603.04 52.44 o 14 1 1 196.03 177.54 52.79 o 15 1 1 640.01 646.09 74.22 o 16 1 1 557.95 585.37 110.85 o 0 2 1 15495.03 14776.21 211.69 o 1 2 1 564.05 616.89 19.07 o 2 2 1 113.19 131.52 6.49 o 3 2 1 2175.79 2160.75 22.84 o 4 2 1 6551.97 6548.39 67.40 o 5 2 1 8758.34 8216.76 70.43 o 6 2 1 3165.19 3235.78 33.53 o 7 2 1 13545.89 13584.79 116.11 o 8 2 1 70.72 79.76 13.10 o 9 2 1 69.21 65.68 18.31 o 10 2 1 76.30 70.24 19.42 o 11 2 1 7810.74 7990.58 116.36 o 12 2 1 1732.70 1672.78 59.43 o 13 2 1 852.15 916.68 66.67 o 14 2 1 144.92 266.91 97.80 o 15 2 1 186.74 214.28 110.16 o 16 2 1 452.41 193.71 130.56 o 1 3 1 11734.57 11874.44 122.11 o 2 3 1 18732.07 18719.21 171.82 o 3 3 1 46874.56 46451.69 402.14 o 4 3 1 4246.96 4037.59 42.11 o 5 3 1 8168.86 8338.94 76.71 o 6 3 1 404.50 420.35 23.50 o 7 3 1 9081.46 9088.76 108.19 o 8 3 1 4823.90 4784.12 64.09 o 9 3 1 18044.19 18283.94 210.35 o 10 3 1 7469.30 7738.93 105.65 o 11 3 1 531.11 514.17 45.18 o 12 3 1 10.96 -17.11 60.85 o 13 3 1 1418.72 1245.71 96.59 o 14 3 1 1337.94 1272.93 159.07 o 15 3 1 1333.18 1235.97 103.62 o 16 3 1 324.75 164.87 145.05 o 0 4 1 5485.01 5199.59 80.93 o 1 4 1 37770.63 38491.18 365.43 o 2 4 1 1615.03 1552.72 21.70 o 3 4 1 129.73 131.45 12.71 o 4 4 1 1762.58 1706.97 24.66 o 5 4 1 30249.78 32091.32 327.66 o 6 4 1 9972.63 10368.81 127.87 o 7 4 1 9835.76 9621.90 115.48 o 8 4 1 214.51 225.94 26.64 o 9 4 1 458.47 410.85 36.26 o 10 4 1 5083.38 5487.52 103.78 o 11 4 1 9604.43 9951.32 218.09 o 12 4 1 4476.05 4801.18 168.82 o 13 4 1 2343.41 2433.47 121.98 o 14 4 1 267.66 295.64 234.48 o 15 4 1 4.18 -189.14 189.14 o 1 5 1 9928.94 10591.86 121.24 o 2 5 1 11301.99 11868.20 132.93 o 3 5 1 24163.43 24940.41 240.82 o 4 5 1 12375.45 12847.78 147.12 o 5 5 1 3718.15 3537.57 58.76 o 6 5 1 151.03 116.16 23.51 o 7 5 1 4041.16 4170.77 80.06 o 8 5 1 4569.50 4780.00 105.20 o 9 5 1 7096.38 7438.55 166.12 o 10 5 1 739.57 760.63 94.41 o 11 5 1 1106.92 1193.21 111.45 o 12 5 1 17.82 103.81 105.85 o 14 5 1 1005.07 851.14 215.45 o 0 6 1 8870.18 9399.56 141.07 o 1 6 1 9987.43 10356.53 172.08 o 2 6 1 1401.85 1504.29 38.26 o 3 6 1 312.06 284.51 28.20 o 4 6 1 3908.26 4111.16 69.32 o 5 6 1 10132.75 10586.43 154.87 o 6 6 1 5294.12 5291.45 103.97 o 7 6 1 5128.58 5277.59 160.24 o 8 6 1 361.54 213.94 94.70 o 9 6 1 181.78 300.83 89.51 o 10 6 1 963.94 619.90 293.56 o 11 6 1 2022.76 2406.59 312.93 o 12 6 1 1154.07 1351.89 213.63 o 13 6 1 2020.55 2056.62 277.94 o 1 7 1 4056.53 3899.06 114.08 o 2 7 1 719.20 761.78 124.43 o 3 7 1 6645.15 5995.07 268.04 o 4 7 1 712.50 816.44 103.11 o 5 7 1 862.26 787.75 96.92 o 6 7 1 31.68 68.52 49.63 o 8 7 1 1471.83 1715.54 202.59 o 9 7 1 1345.99 1008.83 251.84 o 10 7 1 461.74 821.75 147.55 o 11 7 1 872.95 731.59 253.77 o 12 7 1 143.73 609.00 267.05 o 0 8 1 152.76 247.36 186.27 o 4 8 1 55.60 205.23 90.17 o 5 8 1 1204.78 1363.49 153.18 o 10 8 1 23.22 -338.26 618.41 o 3 9 1 82.15 428.40 250.95 o 4 9 1 137.31 264.10 271.95 o 7 9 1 17.73 108.78 306.97 o 1 10 1 387.33 892.60 335.28 o 2 10 1 50.35 148.59 173.62 o 2 0 2 2890.52 2754.42 32.48 o 3 0 2 8837.04 8259.81 96.71 o 4 0 2 772.24 664.92 12.75 o 5 0 2 48142.92 46973.80 541.39 o 6 0 2 24778.39 24560.83 280.78 o 7 0 2 69420.61 71180.05 787.08 o 8 0 2 21.42 29.03 14.45 o 9 0 2 52.00 14.01 21.02 o 10 0 2 26.66 0.89 26.17 o 11 0 2 13039.37 13923.49 247.04 o 12 0 2 2519.32 2365.14 75.06 o 13 0 2 3669.08 4005.50 159.22 o 14 0 2 121.70 -94.39 122.09 o 15 0 2 281.89 70.61 120.13 o 16 0 2 1046.86 1174.34 152.93 o 1 1 2 6609.31 6408.43 58.66 o 2 1 2 14899.29 14324.40 109.28 o 3 1 2 106902.02 103449.23 802.37 o 4 1 2 18623.39 18347.84 136.70 o 5 1 2 14714.12 14334.66 102.46 o 6 1 2 216.23 239.56 10.13 o 7 1 2 5898.76 5679.77 52.88 o 8 1 2 3156.48 3063.90 33.27 o 9 1 2 33431.89 34189.56 315.33 o 10 1 2 7174.29 7309.44 78.54 o 11 1 2 1566.75 1651.01 37.49 o 12 1 2 198.95 154.11 38.97 o 13 1 2 2102.43 2158.88 63.49 o 14 1 2 628.87 572.68 85.69 o 15 1 2 2753.06 2842.63 133.20 o 16 1 2 611.39 789.81 119.73 o 0 2 2 58280.69 58406.70 833.00 o 1 2 2 129064.02 123110.91 1270.41 o 2 2 2 20.57 38.23 5.46 o 3 2 2 28.24 40.74 6.70 o 4 2 2 1270.22 1201.83 18.31 o 5 2 2 32961.70 32875.62 269.38 o 6 2 2 2708.00 2499.65 28.87 o 7 2 2 16630.38 16557.53 158.29 o 8 2 2 410.43 327.17 17.06 o 9 2 2 9.71 31.55 17.11 o 10 2 2 1645.64 1647.30 33.36 o 11 2 2 3798.78 3829.87 61.27 o 12 2 2 2998.69 3366.50 75.10 o 13 2 2 2176.93 2282.22 66.27 o 14 2 2 7.51 58.99 77.98 o 15 2 2 0.06 -167.89 167.89 o 16 2 2 30.46 86.43 104.17 o 1 3 2 7168.80 7158.87 71.15 o 2 3 2 2035.42 2045.31 24.03 o 3 3 2 24077.82 24183.23 217.50 o 4 3 2 2674.24 2631.50 30.68 o 5 3 2 1296.49 1225.06 22.86 o 6 3 2 517.58 563.27 17.74 o 7 3 2 3611.19 3668.60 36.02 o 8 3 2 1319.09 1417.22 33.74 o 9 3 2 3513.91 3738.74 54.14 o 10 3 2 121.79 83.71 34.27 o 11 3 2 648.53 687.69 49.89 o 12 3 2 1383.57 1191.00 70.19 o 13 3 2 144.52 36.62 104.64 o 14 3 2 46.23 247.06 104.60 o 15 3 2 1119.17 948.79 149.93 o 16 3 2 25.87 189.81 132.91 o 0 4 2 794.01 845.62 26.15 o 1 4 2 979.64 1027.05 25.81 o 2 4 2 2248.33 2174.87 31.12 o 3 4 2 92.01 91.78 12.65 o 4 4 2 717.18 818.33 21.87 o 5 4 2 715.23 780.27 23.65 o 6 4 2 2866.66 3261.25 53.42 o 7 4 2 1237.17 1299.27 34.26 o 8 4 2 159.31 194.13 35.65 o 9 4 2 838.64 886.42 32.88 o 10 4 2 5.20 21.06 44.01 o 11 4 2 15.13 154.86 64.91 o 12 4 2 39.48 206.80 126.68 o 13 4 2 865.33 892.06 112.46 o 14 4 2 596.50 725.40 200.60 o 15 4 2 16.77 -137.61 137.61 o 1 5 2 14.94 60.77 18.20 o 2 5 2 194.47 329.04 19.05 o 3 5 2 1083.49 1263.07 27.11 o 4 5 2 597.01 649.53 22.05 o 5 5 2 59.51 88.89 18.92 o 6 5 2 0.74 21.21 26.20 o 7 5 2 777.48 791.60 38.87 o 8 5 2 116.58 297.33 64.70 o 9 5 2 266.98 154.09 52.68 o 10 5 2 248.49 195.22 87.86 o 11 5 2 1226.38 1135.04 124.83 o 12 5 2 712.96 643.74 144.54 o 14 5 2 26.70 -114.22 237.66 o 0 6 2 2680.82 2897.10 83.47 o 1 6 2 4045.14 4386.68 72.05 o 2 6 2 457.96 505.39 37.61 o 3 6 2 13.50 9.15 25.94 o 4 6 2 167.45 149.62 35.76 o 5 6 2 2835.81 2870.03 52.77 o 6 6 2 1846.82 1744.83 62.95 o 7 6 2 2821.33 2736.52 204.21 o 8 6 2 192.70 134.38 96.89 o 9 6 2 71.64 83.90 96.68 o 10 6 2 105.33 70.04 268.23 o 11 6 2 518.20 827.03 330.81 o 12 6 2 794.50 652.73 271.95 o 13 6 2 209.18 34.67 235.42 o 1 7 2 1219.98 1144.00 53.83 o 2 7 2 242.45 309.67 74.75 o 3 7 2 7175.63 6912.62 272.64 o 4 7 2 327.76 363.16 102.55 o 5 7 2 542.25 499.01 66.08 o 6 7 2 196.20 136.37 92.73 o 8 7 2 583.81 527.51 306.97 o 9 7 2 3481.61 3178.60 278.55 o 10 7 2 620.95 579.95 259.69 o 11 7 2 414.27 744.77 263.01 o 12 7 2 2.12 852.37 399.36 o 0 8 2 595.52 669.08 219.05 o 4 8 2 193.04 168.90 117.20 o 5 8 2 4304.97 4005.52 208.35 o 6 8 2 1562.30 1171.26 204.15 o 3 9 2 8386.72 7502.27 349.04 o 4 9 2 782.02 633.55 166.90 o 5 9 2 614.44 286.11 178.82 o 7 9 2 1138.06 907.50 311.44 o 1 10 2 3508.58 2462.09 255.94 o 2 10 2 283.50 -4.54 158.26 o 1 1 3 1134.04 1071.96 13.26 o 2 1 3 58460.79 56315.83 496.25 o 3 1 3 41.51 67.93 5.74 o 4 1 3 126.69 113.42 6.63 o 5 1 3 2085.15 2139.22 19.83 o 6 1 3 2632.00 2955.15 29.94 o 7 1 3 118.15 165.65 11.96 o 8 1 3 3738.52 3584.17 34.48 o 9 1 3 3607.37 3607.91 41.08 o 10 1 3 2949.84 2941.65 37.50 o 11 1 3 2426.82 2456.27 41.65 o 12 1 3 1.69 -36.71 36.71 o 13 1 3 28.35 98.87 54.75 o 14 1 3 180.22 170.24 46.12 o 15 1 3 55.07 3.92 86.50 o 16 1 3 29.09 146.48 144.59 o 0 2 3 98890.84 94772.23 1372.13 o 1 2 3 18794.04 18595.51 186.19 o 2 2 3 11263.23 11142.50 101.61 o 3 2 3 1063.76 993.66 18.39 o 4 2 3 15144.30 15436.32 138.04 o 5 2 3 306.23 381.72 11.33 o 6 2 3 24257.89 24037.02 205.29 o 7 2 3 407.97 343.47 16.58 o 8 2 3 179.57 163.71 17.08 o 9 2 3 580.62 545.52 22.02 o 10 2 3 2555.52 2576.05 41.02 o 11 2 3 1616.52 1717.31 40.30 o 12 2 3 5024.87 5011.00 85.88 o 13 2 3 74.43 -25.25 47.14 o 14 2 3 767.39 747.78 125.70 o 15 2 3 619.46 705.74 116.93 o 16 2 3 69.20 36.69 115.18 o 1 3 3 83.38 91.62 9.48 o 2 3 3 33841.88 33340.80 298.50 o 3 3 3 4823.20 4931.44 48.81 o 4 3 3 35725.97 35673.47 319.71 o 5 3 3 1736.07 1780.25 29.12 o 6 3 3 422.48 440.31 19.87 o 7 3 3 24.38 26.61 18.54 o 8 3 3 12938.30 13532.94 129.05 o 9 3 3 534.61 546.29 27.51 o 10 3 3 3158.34 3041.47 55.91 o 11 3 3 66.34 83.03 38.99 o 12 3 3 3.41 12.63 68.05 o 13 3 3 361.15 232.35 98.02 o 14 3 3 4596.50 4866.59 211.64 o 15 3 3 43.32 219.95 127.50 o 16 3 3 1560.80 1533.61 148.08 o 0 4 3 55835.25 55239.11 773.02 o 1 4 3 1418.95 1416.93 22.17 o 2 4 3 8668.46 8797.68 91.70 o 3 4 3 1272.10 1381.59 25.40 o 4 4 3 13108.85 13411.37 128.41 o 5 4 3 1266.31 1277.35 28.55 o 6 4 3 33749.84 34341.52 412.66 o 7 4 3 83.33 65.20 20.50 o 8 4 3 6468.38 6659.10 93.71 o 9 4 3 822.14 815.40 36.71 o 10 4 3 1460.59 1521.01 60.34 o 11 4 3 864.80 780.97 62.94 o 12 4 3 7623.07 8345.32 223.32 o 13 4 3 453.33 446.09 123.80 o 14 4 3 342.33 250.56 156.37 o 15 4 3 60.85 170.09 137.85 o 1 5 3 7.04 -16.42 18.81 o 2 5 3 31607.93 33344.61 339.21 o 3 5 3 629.91 591.06 20.06 o 4 5 3 21108.17 21643.16 264.69 o 5 5 3 263.80 324.47 24.22 o 6 5 3 31.30 47.53 25.40 o 7 5 3 651.76 662.26 29.52 o 8 5 3 19333.15 20269.00 416.17 o 9 5 3 386.45 286.98 63.77 o 10 5 3 9996.13 10852.00 256.91 o 11 5 3 64.39 94.81 104.48 o 12 5 3 49.28 -72.73 104.09 o 13 5 3 103.71 299.45 195.62 o 14 5 3 1761.63 1540.22 200.85 o 0 6 3 19586.51 20930.53 367.90 o 1 6 3 88.34 100.81 25.14 o 2 6 3 7778.27 8185.84 115.86 o 3 6 3 293.66 260.37 34.67 o 4 6 3 3358.34 3487.22 66.72 o 5 6 3 618.26 587.14 39.97 o 6 6 3 15040.17 15443.20 369.89 o 7 6 3 222.68 155.15 70.95 o 8 6 3 2101.09 2139.55 190.50 o 9 6 3 110.25 225.15 196.91 o 10 6 3 4462.24 4120.25 314.47 o 11 6 3 94.42 359.74 167.10 o 12 6 3 3852.15 5110.52 641.51 o 13 6 3 429.10 594.35 148.51 o 1 7 3 355.69 395.48 70.27 o 2 7 3 6747.84 6565.06 213.31 o 3 7 3 578.54 568.11 88.97 o 4 7 3 9579.29 9278.43 451.06 o 5 7 3 183.58 64.93 105.06 o 6 7 3 124.21 7.67 65.28 o 7 7 3 9.58 177.33 146.03 o 8 7 3 3668.07 3742.30 299.83 o 9 7 3 35.26 208.70 227.59 o 10 7 3 2645.45 3136.09 575.86 o 11 7 3 53.83 589.82 229.45 o 12 7 3 5.24 143.77 227.60 o 0 8 3 1155.90 1074.40 174.35 o 4 8 3 384.42 373.20 96.11 o 5 8 3 7.59 0.80 109.99 o 6 8 3 1383.14 1217.45 196.70 o 8 8 3 882.76 597.42 199.92 o 9 8 3 129.26 -63.65 315.91 o 10 8 3 87.83 -15.73 243.56 o 3 9 3 29.70 572.71 270.92 o 4 9 3 3.75 152.13 146.85 o 5 9 3 16.61 -105.77 154.53 o 6 9 3 38.14 193.72 378.50 o 7 9 3 57.74 290.58 384.46 o 1 10 3 0.56 368.56 493.98 o 2 10 3 38.86 219.25 210.86 o 1 0 4 18543.00 16823.71 286.28 o 2 0 4 7765.34 7591.83 99.86 o 3 0 4 2922.91 2908.18 39.32 o 4 0 4 31746.43 32363.82 370.52 o 5 0 4 19533.11 17981.22 184.34 o 6 0 4 42962.37 44303.00 463.66 o 7 0 4 24818.08 24179.78 246.50 o 8 0 4 4765.37 4763.98 59.05 o 9 0 4 9.03 47.94 18.69 o 10 0 4 40.98 81.71 29.20 o 11 0 4 8826.96 9021.00 140.53 o 12 0 4 955.30 957.07 61.30 o 13 0 4 5469.17 5950.38 150.99 o 14 0 4 1201.49 1465.36 145.56 o 15 0 4 258.68 275.67 113.25 o 16 0 4 656.68 950.33 200.56 o 1 1 4 664.30 640.53 8.98 o 2 1 4 61393.92 58992.49 528.54 o 3 1 4 84878.84 81021.06 648.98 o 4 1 4 25460.81 24584.99 204.20 o 5 1 4 7827.19 7471.19 57.54 o 6 1 4 126.98 163.86 10.05 o 7 1 4 2629.44 2355.00 24.15 o 8 1 4 10560.18 10314.78 91.07 o 9 1 4 22536.54 22742.00 204.27 o 10 1 4 6250.50 6174.92 65.06 o 11 1 4 895.15 878.43 31.68 o 12 1 4 260.10 263.20 40.17 o 13 1 4 908.36 808.67 54.83 o 14 1 4 2089.08 2070.90 79.00 o 15 1 4 2917.94 3281.13 174.36 o 16 1 4 1075.26 1187.73 188.66 o 0 2 4 130861.45 129150.28 1896.93 o 1 2 4 20334.75 19170.63 188.85 o 2 2 4 26177.86 25535.96 231.10 o 3 2 4 0.87 1.48 9.28 o 4 2 4 3518.59 3247.86 30.61 o 5 2 4 16764.69 16595.16 150.74 o 6 2 4 8185.31 7744.20 74.78 o 7 2 4 11217.25 11027.14 84.82 o 8 2 4 2843.57 2772.04 39.99 o 9 2 4 1132.23 1102.09 27.78 o 10 2 4 6124.21 6244.49 67.04 o 11 2 4 5990.72 5998.76 83.89 o 12 2 4 5275.39 5519.71 105.13 o 13 2 4 3189.71 3185.25 98.13 o 14 2 4 6.65 85.62 158.30 o 15 2 4 5.86 77.15 83.27 o 16 2 4 123.38 -66.62 137.29 o 1 3 4 10241.58 10248.40 92.88 o 2 3 4 7550.16 7409.08 72.35 o 3 3 4 18191.38 18131.64 183.49 o 4 3 4 10256.12 10494.76 99.64 o 5 3 4 1039.77 885.85 18.91 o 6 3 4 69.51 43.78 16.27 o 7 3 4 1273.39 1238.69 29.95 o 8 3 4 6047.28 6214.85 71.14 o 9 3 4 4182.82 4456.34 56.16 o 10 3 4 993.74 981.83 42.98 o 11 3 4 1653.87 1736.81 66.56 o 12 3 4 785.58 720.23 46.65 o 13 3 4 89.72 102.53 79.92 o 14 3 4 718.01 684.07 141.77 o 15 3 4 481.57 598.01 178.05 o 16 3 4 6.34 6.75 178.81 o 0 4 4 193.27 298.21 17.50 o 1 4 4 3324.15 3325.40 37.56 o 2 4 4 750.90 805.13 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