#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/43/2014357.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2014357_Fobs loop_ _publ_author_name 'Bourne, Susan A.' 'De Villiers, Katherine' 'Egan, Timothy J.' _publ_section_title ; Three 4-aminoquinolines of antimalarial interest ; _journal_coeditor_code HJ1079 _journal_issue 2 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first o53 _journal_page_last o57 _journal_volume 62 _journal_year 2006 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 79.552 _cell_angle_beta 88.019 _cell_angle_gamma 72.336 _cell_length_a 11.0960 _cell_length_b 14.6481 _cell_length_c 15.1797 _exptl_crystal_F_000 1192.00 _reflns_d_resolution_high 0.7877 _[local]_cod_data_source_file hj1079IIIsup4.hkl _[local]_cod_data_source_block III #BEGIN Tags that were not found in dictionaries: _shelx_title ' kat_qclp in P-1 (Sue's attempt)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 309.33 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 47465.83 33494.41 1627.04 o 3 0 0 2435.42 1939.66 99.50 o 4 0 0 1653.58 1635.24 104.72 o 5 0 0 60.20 63.35 10.43 o 6 0 0 2252.39 2519.65 191.89 o 7 0 0 2260.82 2279.80 115.14 o 8 0 0 38.35 38.96 15.35 o 9 0 0 181.77 167.21 27.65 o 10 0 0 1048.90 1079.60 84.66 o 11 0 0 18.40 33.63 28.07 o 12 0 0 0.36 -46.11 82.94 o 13 0 0 139.61 56.85 91.51 o -13 1 0 1420.58 1605.91 521.11 o -12 1 0 23.78 90.14 48.32 o -11 1 0 332.97 282.42 50.27 o -10 1 0 79.73 85.88 27.74 o -9 1 0 353.45 328.15 36.18 o -8 1 0 367.18 382.07 28.96 o -7 1 0 529.96 500.51 29.38 o -6 1 0 4716.22 4972.95 384.86 o -5 1 0 1110.18 1224.03 81.55 o -4 1 0 133.52 125.69 10.84 o -3 1 0 5543.89 4252.23 246.61 o -2 1 0 285.62 223.64 17.12 o -1 1 0 8.25 0.13 5.84 o 0 1 0 30.48 4.79 6.04 o 1 1 0 42.37 0.29 8.56 o 2 1 0 906.07 809.81 43.98 o 3 1 0 34.58 58.87 6.04 o 4 1 0 142.00 136.00 11.28 o 5 1 0 143.96 135.95 10.68 o 6 1 0 15.35 19.50 9.47 o 7 1 0 324.37 312.14 19.67 o 8 1 0 295.83 294.44 22.01 o 9 1 0 611.43 632.00 39.79 o 10 1 0 218.97 206.16 25.23 o 11 1 0 966.87 1017.37 91.70 o 12 1 0 0.03 -22.92 35.37 o -12 2 0 329.34 487.06 161.14 o -11 2 0 119.34 115.95 34.44 o -10 2 0 4387.08 4622.81 254.35 o -9 2 0 3086.78 3151.83 167.41 o -8 2 0 3753.50 3794.41 179.94 o -7 2 0 1055.58 1192.90 80.30 o -6 2 0 2.62 12.85 16.79 o -5 2 0 3503.65 4291.43 288.63 o -4 2 0 0.66 19.97 10.85 o -3 2 0 8019.10 7314.22 525.52 o -2 2 0 39264.95 29203.16 2386.50 o -1 2 0 3269.85 2346.16 186.24 o 0 2 0 1073.02 958.43 76.29 o 1 2 0 12282.44 9086.08 709.11 o 2 2 0 9021.81 7518.33 427.59 o 3 2 0 7811.41 6196.21 409.52 o 4 2 0 26264.47 22699.28 1175.52 o 5 2 0 7.92 16.54 11.82 o 6 2 0 10635.24 10325.59 597.02 o 7 2 0 3.18 3.91 11.64 o 8 2 0 3145.49 3082.29 147.08 o 9 2 0 3.87 -20.34 20.34 o 10 2 0 13.11 -21.85 24.06 o 11 2 0 1.20 -12.07 27.91 o 12 2 0 130.94 147.06 42.88 o 13 2 0 547.47 448.46 99.84 o -12 3 0 693.25 832.75 178.38 o -11 3 0 237.53 228.74 43.94 o -10 3 0 1.43 -23.51 24.48 o -9 3 0 755.64 706.70 48.37 o -8 3 0 1752.47 1729.54 86.48 o -7 3 0 59.35 46.22 21.45 o -6 3 0 253.78 257.21 21.56 o -5 3 0 7972.67 8521.96 976.77 o -4 3 0 669.79 660.62 45.06 o -3 3 0 243.14 285.31 41.42 o -2 3 0 19.27 17.05 9.43 o -1 3 0 1092.68 959.31 80.29 o 0 3 0 325.40 354.29 44.06 o 1 3 0 64.54 67.23 9.02 o 2 3 0 107.35 107.36 7.56 o 3 3 0 81.04 98.89 14.27 o 4 3 0 249.24 249.05 17.83 o 5 3 0 837.03 786.20 39.59 o 6 3 0 1001.62 949.55 45.93 o 7 3 0 119.69 150.56 33.70 o 8 3 0 145.40 137.94 18.49 o 9 3 0 1109.11 1030.96 55.07 o 10 3 0 78.83 71.79 26.89 o 11 3 0 9.33 -6.22 27.59 o 12 3 0 2.70 -35.54 39.69 o 13 3 0 10.93 106.41 122.83 o -12 4 0 30.42 162.05 157.19 o -11 4 0 246.30 281.54 59.87 o -10 4 0 68.49 35.07 28.96 o -9 4 0 1050.47 1066.65 69.34 o -8 4 0 752.55 712.86 46.34 o -7 4 0 429.06 384.89 30.77 o -6 4 0 148.12 143.88 23.67 o -5 4 0 333.10 277.88 21.81 o -4 4 0 132.27 137.63 19.91 o -3 4 0 27.88 20.51 11.94 o -2 4 0 661.05 404.61 37.34 o -1 4 0 6881.43 6260.27 487.54 o 0 4 0 55030.25 46953.90 3838.39 o 1 4 0 61276.35 54164.00 5551.23 o 2 4 0 62125.30 50108.14 3752.47 o 3 4 0 29743.90 25633.71 1457.22 o 4 4 0 8233.02 6499.81 418.36 o 5 4 0 274.31 156.14 19.06 o 6 4 0 502.39 524.41 30.70 o 7 4 0 3497.61 3232.67 160.95 o 8 4 0 3302.89 3307.20 182.39 o 9 4 0 694.52 690.70 50.10 o 10 4 0 148.97 98.70 28.75 o 11 4 0 1088.16 1144.58 90.40 o 12 4 0 9.16 -24.91 47.03 o 13 4 0 4.10 -12.12 65.47 o -11 5 0 464.61 551.97 135.93 o -10 5 0 838.18 845.48 78.04 o -9 5 0 80.22 126.99 27.40 o -8 5 0 17.38 8.33 22.35 o -7 5 0 64.92 75.65 21.54 o -6 5 0 2436.62 2363.20 111.54 o -5 5 0 1642.14 1726.90 120.52 o -4 5 0 198.98 190.65 23.00 o -3 5 0 2155.83 2119.23 191.28 o -2 5 0 1157.22 997.71 72.15 o -1 5 0 299.22 304.87 21.30 o 0 5 0 131.57 155.62 23.11 o 1 5 0 63.34 77.99 12.44 o 2 5 0 4617.84 4274.25 239.89 o 3 5 0 1844.25 1607.26 84.06 o 4 5 0 851.48 781.94 49.85 o 5 5 0 0.26 14.49 9.25 o 6 5 0 418.06 378.57 32.83 o 7 5 0 54.70 31.23 15.17 o 8 5 0 4.74 -15.29 18.16 o 9 5 0 2745.68 2923.62 172.48 o 10 5 0 85.65 140.40 24.16 o 11 5 0 280.63 278.65 34.83 o 12 5 0 55.73 123.70 34.91 o 13 5 0 253.40 272.72 124.35 o 14 5 0 2.97 -0.61 97.59 o -11 6 0 209.92 296.88 120.97 o -10 6 0 590.97 566.88 83.97 o -9 6 0 0.02 -8.15 47.58 o -8 6 0 352.91 317.14 33.12 o -7 6 0 667.74 655.04 47.78 o -6 6 0 3646.14 3713.31 203.60 o -5 6 0 68.29 73.41 28.27 o -4 6 0 1963.42 1809.02 108.98 o -3 6 0 1036.13 1066.90 80.06 o -2 6 0 451.49 461.14 29.41 o -1 6 0 933.73 980.68 77.46 o 0 6 0 352.21 387.68 35.22 o 1 6 0 6229.14 5758.62 324.32 o 2 6 0 433.25 481.21 36.64 o 3 6 0 0.90 2.25 7.30 o 4 6 0 2632.70 2013.38 115.54 o 5 6 0 22.03 25.41 10.45 o 6 6 0 24496.49 22242.54 1403.63 o 7 6 0 169.22 144.08 25.48 o 8 6 0 148.52 127.27 26.48 o 9 6 0 300.13 351.20 33.36 o 10 6 0 0.26 8.76 28.20 o 11 6 0 1865.12 1822.98 114.71 o 12 6 0 1.58 -13.92 36.57 o 13 6 0 610.60 613.04 104.84 o -10 7 0 4.28 113.50 69.00 o -9 7 0 155.39 122.16 51.51 o -8 7 0 176.91 152.32 36.78 o -7 7 0 573.89 571.82 52.18 o -6 7 0 53.36 45.74 23.62 o -5 7 0 865.54 890.75 63.73 o -4 7 0 89.35 76.48 20.20 o -3 7 0 2.04 -21.71 24.27 o -2 7 0 915.12 930.35 78.39 o -1 7 0 107.54 90.65 17.39 o 0 7 0 21.20 28.35 16.12 o 1 7 0 173.65 225.31 20.49 o 2 7 0 1109.89 1040.95 61.74 o 3 7 0 261.07 299.09 21.74 o 4 7 0 417.96 390.96 39.04 o 5 7 0 41.82 56.54 14.27 o 6 7 0 607.98 651.62 49.99 o 7 7 0 447.61 357.83 36.76 o 8 7 0 78.70 37.43 23.01 o 9 7 0 419.85 466.70 48.42 o 10 7 0 41.25 42.79 25.30 o 11 7 0 41.87 31.25 45.26 o 12 7 0 115.32 127.93 63.44 o 13 7 0 58.53 -6.38 84.22 o 14 7 0 51.03 -79.96 106.72 o -10 8 0 1001.97 1276.08 254.62 o -9 8 0 19.34 87.37 49.01 o -8 8 0 37.41 59.76 64.06 o -7 8 0 8.54 -7.97 38.08 o -6 8 0 383.04 338.99 33.71 o -5 8 0 434.86 365.50 38.32 o -4 8 0 4829.28 4709.79 238.45 o -3 8 0 4690.55 4434.72 278.35 o -2 8 0 4547.98 4651.84 282.12 o -1 8 0 21.60 32.54 19.35 o 0 8 0 964.27 967.77 50.94 o 1 8 0 35.66 38.64 16.60 o 2 8 0 2984.80 2590.27 147.24 o 3 8 0 2870.48 2635.57 142.67 o 4 8 0 17620.22 16594.35 1278.44 o 5 8 0 9.48 22.01 16.99 o 6 8 0 121.79 147.96 19.22 o 7 8 0 2918.03 2651.19 172.32 o 8 8 0 1634.52 1694.29 111.18 o 9 8 0 13208.84 13246.56 741.05 o 10 8 0 50.62 44.23 31.63 o 11 8 0 267.58 235.62 44.05 o 12 8 0 4.47 79.64 74.58 o 13 8 0 19.52 -13.03 58.32 o -9 9 0 960.80 933.27 214.66 o -8 9 0 2.06 63.92 69.54 o -7 9 0 3.29 3.14 32.09 o -6 9 0 305.78 300.11 35.73 o -5 9 0 660.88 622.19 48.22 o -4 9 0 1004.60 945.01 58.81 o -3 9 0 1163.12 1077.62 61.72 o -2 9 0 219.84 181.08 24.99 o -1 9 0 110.52 131.06 23.72 o 0 9 0 615.04 545.36 37.64 o 1 9 0 320.78 279.50 25.38 o 2 9 0 24.03 25.66 15.82 o 3 9 0 292.82 324.58 25.70 o 4 9 0 198.63 182.17 25.52 o 5 9 0 405.93 392.75 32.73 o 6 9 0 190.00 215.71 24.03 o 7 9 0 110.34 81.14 27.52 o 8 9 0 106.85 104.41 36.51 o 9 9 0 473.61 425.13 49.90 o 10 9 0 0.02 63.65 37.87 o 11 9 0 443.13 363.39 130.05 o 12 9 0 11.51 -52.34 57.44 o 13 9 0 704.54 731.88 180.80 o -8 10 0 89.04 24.48 68.22 o -7 10 0 2.18 44.94 49.25 o -6 10 0 246.06 181.86 38.41 o -5 10 0 757.01 658.22 69.18 o -4 10 0 557.17 537.83 54.80 o -3 10 0 50.02 53.73 27.50 o -2 10 0 27.83 0.42 26.43 o -1 10 0 785.41 727.88 45.53 o 0 10 0 2616.39 2734.30 158.01 o 1 10 0 1394.11 1389.58 82.01 o 2 10 0 2057.02 1975.13 103.77 o 3 10 0 165.56 147.49 22.58 o 4 10 0 1309.87 1222.08 72.59 o 5 10 0 81.66 71.97 20.91 o 6 10 0 1706.44 1634.03 91.50 o 7 10 0 1780.19 1716.84 104.60 o 8 10 0 1019.76 1049.66 80.10 o 9 10 0 957.78 1017.22 94.56 o 10 10 0 1200.16 1397.02 125.91 o 11 10 0 500.59 501.87 75.60 o 12 10 0 855.71 955.01 162.11 o 13 10 0 349.25 379.74 141.38 o -8 11 0 203.77 155.36 88.48 o -7 11 0 601.90 488.64 96.68 o -6 11 0 56.36 40.86 50.74 o -5 11 0 489.29 446.69 56.30 o -4 11 0 0.62 16.92 39.81 o -3 11 0 91.83 101.07 31.97 o -2 11 0 340.09 364.61 47.04 o -1 11 0 670.00 595.86 47.01 o 0 11 0 63.78 67.57 27.09 o 1 11 0 6027.01 5878.42 293.12 o 2 11 0 32.90 28.53 22.51 o 3 11 0 657.87 692.38 45.21 o 4 11 0 684.41 662.57 40.94 o 5 11 0 186.08 167.28 29.01 o 6 11 0 897.02 905.43 60.18 o 7 11 0 83.79 99.03 24.88 o 8 11 0 22.99 -14.11 33.12 o 9 11 0 15.95 81.73 81.49 o 10 11 0 175.13 161.06 67.99 o 11 11 0 0.14 -45.22 57.09 o 12 11 0 0.03 58.33 54.89 o 13 11 0 19.76 20.32 84.49 o -7 12 0 280.87 262.66 92.74 o -6 12 0 468.62 443.90 88.80 o -5 12 0 238.51 191.97 62.76 o -4 12 0 127.35 99.04 46.53 o -3 12 0 1278.28 1141.09 84.86 o -2 12 0 722.62 701.36 57.26 o -1 12 0 50.48 18.92 32.17 o 0 12 0 894.13 924.11 58.20 o 1 12 0 1817.73 1773.19 96.03 o 2 12 0 489.35 534.79 41.08 o 3 12 0 707.26 714.32 46.68 o 4 12 0 877.76 903.40 54.43 o 5 12 0 0.05 28.88 26.16 o 6 12 0 439.52 434.51 42.77 o 7 12 0 1350.94 1412.63 91.65 o 8 12 0 13.13 65.40 35.63 o 9 12 0 2350.16 2511.28 257.42 o 10 12 0 2526.49 2903.93 385.69 o 11 12 0 312.76 457.27 183.64 o 12 12 0 981.16 1130.36 199.88 o -6 13 0 54.57 79.35 108.26 o -5 13 0 5.95 -12.54 73.40 o -4 13 0 381.65 375.55 77.91 o -3 13 0 1604.40 1734.33 186.42 o -2 13 0 468.86 482.26 67.83 o -1 13 0 2100.63 2146.30 135.77 o 0 13 0 119.14 158.18 41.77 o 1 13 0 208.54 179.28 34.73 o 2 13 0 404.84 375.25 37.60 o 3 13 0 833.39 843.05 59.74 o 4 13 0 885.12 827.80 52.87 o 5 13 0 963.05 933.14 62.62 o 6 13 0 206.26 172.97 35.88 o 7 13 0 460.88 498.35 65.33 o 8 13 0 167.01 162.56 43.93 o 9 13 0 64.38 58.32 38.45 o 10 13 0 29.56 1.35 60.06 o 11 13 0 0.42 23.31 89.33 o 12 13 0 4.94 -33.28 124.94 o -5 14 0 129.94 88.98 90.13 o -4 14 0 90.17 21.62 97.16 o -3 14 0 417.40 474.81 95.96 o -2 14 0 12.69 -10.25 48.24 o -1 14 0 564.50 617.76 78.60 o 0 14 0 338.46 375.46 53.00 o 1 14 0 6.03 -18.17 36.89 o 2 14 0 363.58 397.50 45.97 o 3 14 0 142.65 110.53 33.46 o 4 14 0 32.64 18.92 27.70 o 5 14 0 275.65 284.19 43.18 o 6 14 0 380.78 319.83 44.72 o 7 14 0 32.28 -8.92 33.36 o 8 14 0 256.00 250.31 60.94 o 9 14 0 284.60 346.41 68.59 o 10 14 0 404.30 352.48 112.61 o 11 14 0 85.53 94.25 89.52 o -4 15 0 27.27 -10.14 88.44 o -3 15 0 138.94 137.23 100.50 o -2 15 0 13.16 2.19 66.90 o -1 15 0 159.89 211.71 60.28 o 0 15 0 19.24 112.24 54.29 o 1 15 0 624.63 716.37 80.90 o 2 15 0 1579.85 1484.99 135.00 o 3 15 0 580.64 638.31 72.67 o 4 15 0 293.90 374.34 65.30 o 5 15 0 1021.32 937.79 96.05 o 6 15 0 43.06 73.75 50.78 o 7 15 0 52.92 49.29 47.83 o 8 15 0 1.18 -43.62 46.12 o 9 15 0 169.17 101.53 101.16 o 10 15 0 50.79 17.64 94.24 o 11 15 0 69.04 93.90 81.15 o -2 16 0 1215.31 1036.21 275.96 o -1 16 0 375.03 371.54 83.00 o 0 16 0 87.15 78.85 60.46 o 1 16 0 297.88 249.00 77.65 o 2 16 0 159.63 176.18 57.70 o 3 16 0 378.19 423.99 74.39 o 4 16 0 262.55 216.78 70.94 o 5 16 0 549.64 522.37 109.91 o 6 16 0 434.89 569.44 96.92 o 7 16 0 761.01 714.16 119.42 o 8 16 0 122.74 65.76 84.44 o 9 16 0 125.15 -73.99 97.45 o 10 16 0 17.70 -5.55 135.75 o 0 17 0 235.77 166.35 99.66 o 1 17 0 44.59 27.03 87.01 o 2 17 0 6.51 -79.36 79.36 o 3 17 0 52.63 104.75 87.78 o 4 17 0 208.77 118.03 83.66 o 5 17 0 609.85 688.18 128.55 o 6 17 0 11.59 4.10 83.09 o 7 17 0 346.72 352.45 106.55 o 8 17 0 38.71 5.32 119.79 o 2 18 0 460.80 109.76 163.27 o 3 18 0 91.31 89.98 96.65 o 4 18 0 111.75 30.05 89.80 o 5 18 0 12.00 -30.93 89.60 o 6 18 0 217.89 281.73 106.23 o -4 -18 1 54.64 71.68 71.44 o -8 -17 1 109.36 100.26 102.09 o -7 -17 1 73.94 42.75 75.28 o -6 -17 1 42.06 -29.13 76.05 o -5 -17 1 20.25 -52.47 77.50 o -4 -17 1 83.52 7.05 68.44 o -3 -17 1 202.24 90.00 83.34 o -2 -17 1 72.78 -7.82 120.01 o -1 -17 1 256.93 170.48 116.42 o 0 -17 1 384.40 375.99 118.62 o -9 -16 1 16.40 103.31 100.65 o -8 -16 1 36.42 109.27 70.48 o -7 -16 1 28.35 99.03 56.61 o -6 -16 1 92.55 63.61 65.60 o -5 -16 1 477.67 595.95 101.49 o -4 -16 1 550.28 565.88 91.46 o -3 -16 1 736.94 1088.59 144.51 o -2 -16 1 119.90 59.10 51.34 o -1 -16 1 372.70 431.08 93.65 o 0 -16 1 469.18 446.28 86.55 o 1 -16 1 2152.22 2083.05 271.57 o 2 -16 1 780.73 634.53 158.45 o -10 -15 1 121.01 247.95 115.70 o -9 -15 1 1.15 -80.13 80.13 o -8 -15 1 300.95 394.08 93.93 o -7 -15 1 9.36 37.83 50.03 o -6 -15 1 126.25 95.73 57.23 o -5 -15 1 97.50 110.99 50.45 o -4 -15 1 358.97 307.27 51.03 o -3 -15 1 385.01 340.63 65.02 o -2 -15 1 399.59 389.66 63.62 o -1 -15 1 888.35 1006.51 112.55 o 0 -15 1 210.10 249.12 60.65 o 1 -15 1 96.42 44.49 53.78 o 2 -15 1 154.36 99.60 57.47 o 3 -15 1 144.35 156.58 95.74 o -11 -14 1 210.51 238.71 92.34 o -10 -14 1 0.58 -14.23 79.34 o -9 -14 1 216.74 266.47 69.74 o -8 -14 1 213.63 224.19 58.91 o -7 -14 1 445.60 536.18 67.66 o -6 -14 1 373.38 398.96 53.71 o -5 -14 1 515.56 601.72 60.72 o -4 -14 1 265.58 268.86 48.33 o -3 -14 1 526.70 462.32 49.91 o -2 -14 1 147.15 165.49 40.43 o -1 -14 1 998.55 987.78 88.93 o 0 -14 1 827.56 775.17 82.92 o 1 -14 1 17.98 43.72 46.68 o 2 -14 1 1479.35 1617.81 177.93 o 3 -14 1 1612.73 1670.29 235.66 o 4 -14 1 27.50 90.03 80.10 o 5 -14 1 180.69 77.93 138.03 o -12 -13 1 126.20 111.54 63.21 o -11 -13 1 2.02 -68.85 101.24 o -10 -13 1 26.75 -14.04 75.93 o -9 -13 1 0.02 -5.19 42.13 o -8 -13 1 225.49 242.37 54.48 o -7 -13 1 24.90 -22.53 33.81 o 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