#------------------------------------------------------------------------------
#$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $
#$Revision: 26848 $
#$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/43/2014375.hkl $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2014375_Fobs
loop_
_publ_author_name
'Matsushita, Nobuyuki'
_publ_section_title
;
 A one-dimensional iodine-bridged Pt^II^/Pt^IV^ mixed-valence complex,
 <i>catena</i>-poly[[[bis(ethylenediamine)platinum(II)]-\m-iodo-[bis(ethylenediamine)platinum(IV)]-\m-iodo]
 hydrogenphosphate dihydrogenphosphate iodide trihydrate]
;
_journal_coeditor_code           OB1246
_journal_issue                   2
_journal_name_full               'Acta Crystallographica Section C'
_journal_page_first              m33
_journal_page_last               m36
_journal_volume                  62
_journal_year                    2006
_space_group_IT_number           14
_symmetry_space_group_name_Hall  '-P 2yn'
_symmetry_space_group_name_H-M   'P 1 21/n 1'
_[local]_cod_data_source_file    ob1246Isup2.hkl
_[local]_cod_data_source_block   I
loop_
_refln_index_h
_refln_index_k
_refln_index_l
_refln_F_squared_calc
_refln_F_squared_meas
_refln_F_squared_sigma
_refln_observed_status
2 0 0 408345.13 414420.13 13962.70 o
4 0 0 1219070.50 1342612.38 3541.28 o
6 0 0 175370.95 177995.44 2782.82 o
8 0 0 686737.38 699712.75 15264.26 o
10 0 0 38480.45 38617.95 1277.90 o
12 0 0 202540.75 206335.73 1279.44 o
14 0 0 7332.12 6810.96 625.61 o
16 0 0 55393.20 57704.30 2958.42 o
18 0 0 6129.50 6012.57 307.33 o
2 1 0 3578.99 4045.94 79.46 o
3 1 0 917.34 1214.65 50.65 o
4 1 0 23172.75 24222.00 256.49 o
5 1 0 5541.03 6233.87 152.65 o
6 1 0 13708.45 13749.44 239.91 o
7 1 0 23151.70 25068.96 324.15 o
8 1 0 53053.80 54952.05 531.47 o
10 1 0 15298.89 16152.70 338.50 o
12 1 0 35330.47 37165.68 1053.74 o
14 1 0 8819.12 9693.67 364.37 o
15 1 0 918.30 1127.03 247.50 o
16 1 0 22021.99 24260.92 1089.82 o
18 1 0 7296.15 7495.62 630.06 o
1 2 0 18.83 228.03 51.13 o
2 2 0 814598.75 884140.81 4403.81 o
3 2 0 121.80 295.19 62.38 o
4 2 0 579369.25 616783.50 13966.53 o
5 2 0 35.84 32.72 120.66 o
6 2 0 399290.06 411515.09 2303.23 o
7 2 0 3956.11 3606.09 166.35 o
8 2 0 280027.97 292343.00 3548.78 o
10 2 0 180929.39 183409.55 2661.78 o
12 2 0 64602.15 68459.24 760.11 o
14 2 0 55467.91 55479.85 1581.65 o
15 2 0 1026.05 963.42 255.68 o
16 2 0 25350.64 25172.91 595.86 o
18 2 0 13529.35 14137.64 536.38 o
1 3 0 42.50 312.91 99.19 o
2 3 0 6511.10 6811.83 190.57 o
3 3 0 317.99 455.89 67.55 o
4 3 0 9450.40 10212.31 197.96 o
5 3 0 73988.34 77060.70 539.00 o
6 3 0 31068.08 32998.51 383.54 o
7 3 0 23385.93 24750.74 714.00 o
8 3 0 22591.63 24105.96 370.98 o
9 3 0 11872.89 11882.06 294.83 o
10 3 0 41347.89 43726.06 936.06 o
11 3 0 1955.11 2081.75 323.27 o
12 3 0 14535.54 16177.25 409.12 o
13 3 0 8623.64 9462.31 353.16 o
14 3 0 29450.60 30768.81 1038.73 o
15 3 0 4281.52 4292.51 381.69 o
16 3 0 11596.03 12942.10 592.65 o
17 3 0 2904.34 2856.33 240.88 o
18 3 0 12711.32 13109.46 542.95 o
0 4 0 252337.50 299669.72 2187.01 o
1 4 0 241.50 413.55 105.53 o
2 4 0 588702.25 637177.31 7915.75 o
3 4 0 11.83 60.33 155.43 o
4 4 0 318138.09 339498.88 254.96 o
5 4 0 4055.17 4412.83 249.39 o
6 4 0 492658.50 513768.81 3010.79 o
8 4 0 182127.30 186843.06 1027.66 o
9 4 0 3533.70 3994.54 159.58 o
10 4 0 176473.19 182245.94 1095.65 o
12 4 0 49332.43 50828.29 664.46 o
13 4 0 5317.15 5312.55 276.88 o
14 4 0 61508.79 63485.03 850.69 o
16 4 0 15719.30 14062.02 525.43 o
17 4 0 2024.57 2052.72 237.60 o
18 4 0 11984.26 11815.33 542.12 o
1 5 0 69048.62 76915.62 3251.95 o
2 5 0 2853.38 2905.31 134.97 o
3 5 0 12816.49 13430.00 636.07 o
4 5 0 15595.26 16557.67 306.29 o
5 5 0 122430.92 129748.18 837.36 o
6 5 0 19952.39 22211.86 641.17 o
8 5 0 29220.29 31341.12 459.03 o
9 5 0 69961.97 72567.43 696.77 o
10 5 0 23837.26 24759.28 469.95 o
11 5 0 4405.61 4447.32 190.86 o
12 5 0 27636.90 28204.44 768.50 o
13 5 0 45114.83 46984.00 1080.01 o
14 5 0 16251.47 16504.84 577.33 o
15 5 0 3511.20 3872.96 230.73 o
16 5 0 13053.95 14367.03 816.65 o
17 5 0 11447.81 13019.57 666.83 o
18 5 0 6391.51 6527.22 848.99 o
0 6 0 562525.44 651741.19 3578.58 o
1 6 0 136.58 337.32 192.76 o
2 6 0 174066.83 185153.20 9523.25 o
3 6 0 1426.71 1581.52 171.37 o
4 6 0 504439.59 529852.56 5813.11 o
5 6 0 267.82 458.84 97.93 o
6 6 0 84112.73 87084.02 1078.17 o
8 6 0 202753.88 207051.75 1988.94 o
9 6 0 2061.54 2161.42 151.99 o
10 6 0 43223.49 45736.30 625.17 o
12 6 0 87318.64 92384.95 986.09 o
13 6 0 3989.63 5005.74 444.11 o
14 6 0 12538.41 13792.54 515.96 o
15 6 0 841.78 920.43 285.33 o
16 6 0 19648.28 19340.42 597.94 o
17 6 0 2591.42 3072.47 331.95 o
18 6 0 2858.66 2906.04 288.57 o
1 7 0 6868.64 7823.94 314.23 o
2 7 0 3602.28 3963.19 199.66 o
3 7 0 223.26 318.04 164.64 o
4 7 0 14782.52 15666.73 408.43 o
5 7 0 12890.19 14305.18 386.50 o
6 7 0 10623.81 11302.63 354.35 o
7 7 0 18602.35 18211.21 590.31 o
8 7 0 22901.37 22781.78 440.91 o
9 7 0 15559.61 16342.43 483.83 o
10 7 0 15541.38 16470.94 1594.27 o
11 7 0 29408.67 30433.16 695.79 o
12 7 0 24999.83 26733.09 588.15 o
13 7 0 16729.64 18032.29 495.21 o
14 7 0 10067.45 10466.63 538.26 o
15 7 0 14657.03 15356.19 536.62 o
16 7 0 11664.15 11918.30 688.90 o
17 7 0 7322.24 8147.30 341.22 o
18 7 0 6601.14 6534.96 395.07 o
0 8 0 106779.66 124645.20 1701.64 o
1 8 0 2592.22 3146.86 208.24 o
2 8 0 186904.50 197813.67 9969.71 o
3 8 0 705.63 580.98 148.65 o
4 8 0 55552.48 59643.03 1942.99 o
5 8 0 1472.88 1607.37 146.25 o
6 8 0 129173.12 133118.20 2886.38 o
7 8 0 825.75 1024.42 135.23 o
8 8 0 22941.39 24444.92 1322.98 o
10 8 0 52422.11 54177.82 1131.60 o
11 8 0 3962.23 4148.94 214.17 o
12 8 0 15559.69 17071.71 489.79 o
14 8 0 23110.60 24786.09 603.95 o
15 8 0 3960.41 4053.51 270.95 o
16 8 0 4197.08 4591.51 295.06 o
1 9 0 2839.93 2924.59 221.42 o
2 9 0 1699.89 1653.87 199.60 o
3 9 0 38458.07 40392.00 879.65 o
4 9 0 3779.17 4040.92 208.70 o
5 9 0 778.82 714.72 156.19 o
6 9 0 15622.72 15612.04 620.50 o
7 9 0 61311.21 63896.08 2115.99 o
8 9 0 6207.28 6351.29 258.55 o
9 9 0 10449.20 10866.94 395.81 o
10 9 0 15114.43 15369.66 464.24 o
11 9 0 37521.78 39218.72 691.08 o
12 9 0 8512.09 9140.89 416.19 o
13 9 0 8795.75 9089.96 349.11 o
14 9 0 15709.72 15623.36 539.26 o
15 9 0 20189.97 20614.06 636.64 o
16 9 0 4833.04 4562.24 313.65 o
17 9 0 3587.32 3987.49 345.80 o
0 10 0 8027.31 8940.32 595.41 o
1 10 0 4017.04 4493.67 257.26 o
2 10 0 71133.88 74362.91 1070.74 o
3 10 0 3763.00 4053.64 686.29 o
4 10 0 23309.21 24503.41 1051.15 o
5 10 0 1792.70 1473.26 178.31 o
6 10 0 52999.97 55993.18 893.15 o
8 10 0 4677.60 4890.00 226.76 o
10 10 0 23181.40 24206.60 577.25 o
12 10 0 6338.28 6338.92 278.98 o
13 10 0 1764.50 1624.38 227.83 o
14 10 0 13893.45 14960.45 548.95 o
15 10 0 1430.16 1286.65 339.56 o
16 10 0 2753.43 3083.73 266.90 o
17 10 0 1329.65 1902.20 257.80 o
1 11 0 24401.51 28244.26 683.75 o
2 11 0 593.82 826.34 283.29 o
3 11 0 712.08 1060.91 218.35 o
4 11 0 2475.00 2546.61 223.55 o
5 11 0 40338.49 42569.78 2641.35 o
6 11 0 2918.35 3075.54 282.40 o
7 11 0 8244.87 8350.57 412.28 o
8 11 0 7162.69 7269.74 652.80 o
9 11 0 36844.13 36578.03 1312.31 o
10 11 0 6709.49 6228.53 269.98 o
11 11 0 6810.29 7107.93 355.76 o
12 11 0 6791.64 6754.31 311.60 o
13 11 0 23085.46 23937.13 906.24 o
14 11 0 5534.24 4961.12 296.49 o
15 11 0 4687.40 4832.04 538.75 o
16 11 0 5288.75 5226.10 333.93 o
0 12 0 23563.00 26457.84 984.91 o
1 12 0 7564.18 9262.17 740.08 o
3 12 0 5385.75 5748.79 305.45 o
4 12 0 33284.46 34993.63 2026.87 o
5 12 0 1472.46 1413.59 299.19 o
6 12 0 2244.12 2339.38 316.11 o
7 12 0 2729.34 2897.21 472.16 o
8 12 0 23304.90 25149.92 641.14 o
12 12 0 9739.88 10222.90 355.89 o
13 12 0 1369.69 1791.90 346.72 o
3 13 0 3406.26 4240.55 296.25 o
4 13 0 1473.77 1670.24 256.31 o
5 13 0 8666.56 8440.60 406.65 o
7 13 0 5098.45 5335.81 301.36 o
8 13 0 3861.80 3518.95 477.35 o
9 13 0 11579.08 12208.60 1144.49 o
10 13 0 962.72 1060.56 327.27 o
11 13 0 14535.04 15498.77 572.19 o
12 13 0 4635.33 4475.22 303.43 o
13 13 0 4557.07 3916.32 331.54 o
14 13 0 819.48 833.63 324.70 o
15 13 0 3507.04 2961.98 324.38 o
1 14 0 6831.71 7261.43 347.27 o
2 14 0 1240.74 1468.91 257.03 o
3 14 0 5410.19 5673.28 335.42 o
5 14 0 4208.70 4794.15 644.72 o
12 14 0 1484.35 1836.92 382.52 o
1 15 0 1116.35 724.12 360.01 o
3 15 0 5163.36 6095.44 360.28 o
7 15 0 12150.20 13198.18 573.11 o
9 15 0 1827.85 2461.55 271.53 o
11 15 0 7473.80 6496.30 383.92 o
13 15 0 1461.38 1936.10 425.47 o
0 16 0 9091.51 10287.13 563.31 o
1 16 0 5701.30 6232.19 858.28 o
2 16 0 923.39 1138.29 389.66 o
3 16 0 4179.40 4445.08 320.86 o
4 16 0 6880.63 7577.69 384.70 o
5 16 0 1993.28 1688.58 412.74 o
8 16 0 1615.17 2078.92 287.47 o
1 17 0 5856.22 6377.03 580.87 o
3 17 0 1633.53 1609.94 410.16 o
5 17 0 9368.93 9727.01 433.12 o
9 17 0 7547.54 7489.66 532.84 o
0 18 0 5934.96 5387.87 531.21 o
1 18 0 1722.47 2064.86 392.26 o
2 18 0 9062.34 10220.52 621.08 o
3 18 0 2201.51 2065.76 321.50 o
4 18 0 4150.42 5054.55 359.86 o
6 18 0 3713.50 4129.13 378.51 o
10 18 0 1401.82 1692.66 438.76 o
6 19 0 1256.20 1850.14 450.01 o
0 20 0 12465.66 16560.05 990.63 o
2 20 0 5397.51 5334.10 436.47 o
4 20 0 5383.38 7274.15 1038.70 o
6 20 0 4339.88 4399.83 400.10 o
1 21 0 1759.15 1586.73 335.43 o
-19 0 1 1541.99 1693.72 355.93 o
-17 0 1 17672.93 16986.81 767.98 o
-15 0 1 7531.93 7318.63 374.74 o
-13 0 1 31754.27 31524.14 773.67 o
-11 0 1 25140.84 23964.05 628.31 o
-9 0 1 64217.49 63423.70 876.88 o
-7 0 1 3331.87 3752.97 228.29 o
-5 0 1 44411.24 46649.00 499.93 o
-3 0 1 228.26 663.75 65.45 o
3 0 1 7503.06 7537.61 175.82 o
5 0 1 35496.89 36573.42 441.73 o
7 0 1 7837.54 8374.55 291.18 o
9 0 1 26302.51 27997.89 581.83 o
11 0 1 17049.71 18786.25 556.34 o
13 0 1 5049.17 6030.77 294.78 o
15 0 1 4699.41 4686.03 341.81 o
17 0 1 4645.49 5238.20 383.73 o
19 0 1 3326.58 3502.88 388.75 o
-19 1 1 2860.43 2721.10 371.34 o
-17 1 1 750.78 1269.14 302.71 o
-14 1 1 4176.96 4490.37 292.67 o
-13 1 1 661.94 1847.99 236.24 o
-12 1 1 2939.49 2784.07 229.19 o
-11 1 1 178.83 1039.98 186.11 o
-10 1 1 14107.84 14076.79 446.34 o
-9 1 1 5714.61 7113.60 342.06 o
-7 1 1 106.54 998.05 118.62 o
-6 1 1 7974.76 7048.96 242.08 o
-5 1 1 17627.34 19263.94 361.84 o
-4 1 1 1950.83 1915.31 100.32 o
-3 1 1 4204.34 3864.57 144.61 o
-2 1 1 33244.60 33267.68 329.02 o
2 1 1 31464.54 30321.86 311.54 o
3 1 1 1546.71 1801.67 123.86 o
4 1 1 548.02 622.93 78.76 o
5 1 1 59089.70 59016.37 568.05 o
6 1 1 5103.45 4621.93 235.66 o
7 1 1 16649.79 16110.48 404.12 o
8 1 1 1269.68 1066.93 142.19 o
9 1 1 45167.73 46225.37 750.29 o
10 1 1 9481.50 8595.98 403.82 o
11 1 1 18465.03 18035.21 586.29 o
13 1 1 23700.59 24104.63 726.24 o
14 1 1 2894.56 2977.19 286.47 o
15 1 1 8660.55 9734.75 579.62 o
17 1 1 9645.19 10476.25 664.62 o
19 1 1 1874.26 1807.33 367.19 o
-19 2 1 6043.70 5725.05 472.82 o
-17 2 1 2919.41 3162.14 331.46 o
-16 2 1 1782.79 1755.21 296.63 o
-15 2 1 22357.97 22868.96 754.43 o
-14 2 1 956.36 1455.35 235.23 o
-13 2 1 9556.21 9885.74 522.46 o
-12 2 1 4279.73 4260.65 265.08 o
-11 2 1 37762.79 36571.21 783.64 o
-10 2 1 43.01 457.09 156.45 o
-9 2 1 6870.90 6643.38 332.94 o
-8 2 1 2426.81 2279.89 152.47 o
-7 2 1 47640.81 48873.41 649.15 o
-6 2 1 748.42 837.71 109.44 o
-5 2 1 25.73 73.62 129.87 o
-4 2 1 2067.91 2147.67 110.56 o
-3 2 1 13628.22 14125.41 254.80 o
-2 2 1 2995.71 3509.75 154.78 o
-1 2 1 9335.67 9568.14 224.99 o
0 2 1 10903.00 11264.60 360.07 o
1 2 1 92.10 87.95 92.04 o
2 2 1 5665.14 5286.05 163.33 o
3 2 1 28442.12 28001.77 356.07 o
4 2 1 4563.89 4026.25 187.58 o
5 2 1 5142.85 4563.77 196.78 o
6 2 1 3924.94 3618.06 209.94 o
7 2 1 32417.41 34493.42 542.58 o
8 2 1 3133.14 2973.26 175.02 o
9 2 1 9254.83 9292.17 392.60 o
10 2 1 6303.03 6145.68 342.05 o
11 2 1 12213.26 14371.91 490.10 o
12 2 1 6935.57 6536.26 401.41 o
13 2 1 8697.86 9126.13 504.96 o
14 2 1 1350.41 987.01 258.77 o
15 2 1 6796.18 7600.20 409.49 o
16 2 1 2512.88 2579.93 314.05 o
17 2 1 3305.85 3693.30 360.12 o
19 2 1 2433.41 2553.17 393.82 o
-19 3 1 717.07 1264.01 339.52 o
-17 3 1 4327.46 4509.38 377.57 o
-15 3 1 105.19 1536.93 278.14 o
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-10 3 1 16990.72 17880.63 510.26 o
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-8 3 1 6709.63 7168.61 323.75 o
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-6 3 1 40517.54 42141.71 617.32 o
-5 3 1 11396.11 11391.89 322.61 o
-4 3 1 29544.60 29817.56 430.41 o
-3 3 1 51065.23 52118.86 521.80 o
-2 3 1 66014.13 69235.97 660.50 o
-1 3 1 53047.93 56754.68 608.25 o
0 3 1 10801.20 10842.51 461.05 o
1 3 1 31863.83 30160.78 491.13 o
2 3 1 64699.92 62320.64 612.91 o
3 3 1 106521.48 105966.44 750.34 o
4 3 1 29277.65 27113.33 406.47 o
5 3 1 3744.49 4402.79 218.14 o
6 3 1 45784.59 45274.59 635.05 o
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8 3 1 12236.68 12288.98 390.96 o
9 3 1 121.92 705.59 148.28 o
10 3 1 22584.15 23749.20 588.02 o
11 3 1 58393.73 59466.73 936.11 o
12 3 1 10043.51 10575.27 484.65 o
13 3 1 724.18 1157.69 220.90 o
14 3 1 8968.01 8789.58 525.41 o
15 3 1 26768.51 28452.19 850.48 o
16 3 1 3276.31 2852.38 332.50 o
18 3 1 3772.40 3447.91 404.13 o
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-13 4 1 3716.78 3950.83 298.79 o
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-11 4 1 21223.72 22281.16 621.46 o
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1 4 1 8384.71 7458.61 334.03 o
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10 4 1 577.89 809.97 184.08 o
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15 4 1 2805.35 4235.36 309.98 o
17 4 1 3256.26 3341.31 363.19 o
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-10 5 1 5455.06 6470.50 412.60 o
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-8 5 1 55707.27 57530.67 885.07 o
-7 5 1 217.79 670.84 136.01 o
-6 5 1 46234.51 48498.41 696.26 o
-5 5 1 6545.72 6265.44 307.48 o
-4 5 1 113949.55 115410.80 1053.74 o
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-1 5 1 13075.29 14536.83 515.68 o
0 5 1 176298.02 185618.55 1851.30 o
1 5 1 20676.42 18877.37 559.99 o
2 5 1 85523.49 80060.65 888.92 o
3 5 1 9.14 21.47 190.20 o
4 5 1 100969.77 94620.32 942.38 o
5 5 1 17427.06 15927.76 406.40 o
6 5 1 66610.82 63526.79 795.64 o
7 5 1 7058.97 6795.48 353.50 o
8 5 1 64993.04 65962.72 944.35 o
9 5 1 27899.93 26022.15 633.13 o
10 5 1 27934.78 26576.07 686.32 o
11 5 1 1226.22 1528.09 210.70 o
12 5 1 21146.79 19622.72 672.54 o
13 5 1 19924.69 19752.05 717.38 o
14 5 1 11917.37 11443.50 609.68 o
15 5 1 1645.92 1844.17 297.64 o
16 5 1 9036.99 8407.07 442.37 o
17 5 1 4820.05 5030.51 427.74 o
18 5 1 6457.65 5527.95 449.32 o
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-17 6 1 4436.89 4558.49 388.83 o
-16 6 1 6640.81 6853.06 427.87 o
-14 6 1 13454.01 13057.29 659.01 o
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