#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2014392.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2014392_Fobs loop_ _publ_author_name 'Vasconcelos, Thatyana R. A.' 'de Souza, Marcus V. N.' 'Wardell, Solange M. S. V.' 'Wardell, James L.' 'Low, John N.' 'Glidewell, Christopher' _publ_section_title ; Simple chains in methyl 3,5-dinitrobenzoate, isolated molecules in isopropyl 3,5-dinitrobenzoate, and a three-dimensional framework containing double and sextuple helices in benzyl 3,5-dinitrobenzoate, all at 120 K ; _journal_coeditor_code SK1889 _journal_issue 1 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first o26 _journal_page_last o29 _journal_volume 62 _journal_year 2006 _space_group_IT_number 86 _symmetry_space_group_name_Hall '-P 4bc' _symmetry_space_group_name_H-M 'P 42/n :2' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 20.8531 _cell_length_b 20.8531 _cell_length_c 6.0377 _exptl_crystal_F_000 1248.00 _reflns_d_resolution_high 0.7695 _[local]_cod_data_source_file sk1889IIIsup4.hkl _[local]_cod_data_source_block III #BEGIN Tags that were not found in dictionaries: _shelx_title ' 1064' _shelx_refln_list_code 4 _shelx_f_calc_maximum 160.19 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-y, x+1/2, z+1/2' '-x+1/2, -y+1/2, z' 'y+1/2, -x, z+1/2' '-x, -y, -z' 'y, -x-1/2, -z-1/2' 'x-1/2, y-1/2, -z' '-y-1/2, x, -z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status -1 3 0 26.64 13.09 6.80 o 1 3 0 1553.43 653.17 82.15 o 3 3 0 1898.25 2122.77 39.99 o -2 4 0 3002.71 2873.83 48.75 o 0 4 0 59.33 52.85 3.61 o 4 4 0 19676.54 18903.52 339.02 o -3 5 0 25660.74 23791.09 386.57 o -1 5 0 11571.74 10907.53 222.74 o 1 5 0 4037.38 4009.53 82.12 o 3 5 0 13311.92 12785.91 165.87 o 5 5 0 3298.59 3447.71 49.87 o -4 6 0 2932.72 2647.29 40.75 o -2 6 0 6044.94 5638.71 101.43 o 0 6 0 4349.30 4244.09 89.71 o 2 6 0 12.76 30.02 3.04 o 4 6 0 538.79 530.22 9.75 o 6 6 0 10279.38 10253.45 135.85 o -5 7 0 1012.36 977.38 16.62 o -3 7 0 67.40 66.64 4.67 o -1 7 0 11139.33 11134.47 201.45 o 1 7 0 3210.57 3120.61 60.32 o 3 7 0 20600.37 21355.35 297.08 o 5 7 0 703.34 894.45 14.58 o 7 7 0 14125.76 14417.07 211.34 o -6 8 0 1026.45 1011.70 19.94 o -4 8 0 1761.27 1697.73 26.92 o -2 8 0 1190.79 1079.34 32.75 o 0 8 0 2936.29 2704.48 51.12 o 2 8 0 17372.88 16974.41 246.41 o 4 8 0 0.41 3.65 3.25 o 6 8 0 842.62 819.24 14.00 o 8 8 0 2218.42 2178.93 37.64 o -7 9 0 42.56 36.22 3.50 o -5 9 0 5282.91 5691.46 84.81 o -3 9 0 217.87 265.83 8.32 o -1 9 0 8367.62 8327.40 151.43 o 1 9 0 61.81 119.73 6.54 o 3 9 0 1481.49 1550.02 29.83 o 5 9 0 1671.48 1740.76 30.86 o 7 9 0 1347.21 1597.24 28.05 o 9 9 0 784.51 785.00 16.28 o -8 10 0 1313.96 1244.87 30.76 o -6 10 0 25.14 26.30 3.14 o -4 10 0 78.01 110.57 4.97 o -2 10 0 4994.86 5258.18 95.94 o 0 10 0 1175.68 1154.96 30.88 o 2 10 0 2054.75 2152.91 41.06 o 4 10 0 1802.15 1904.40 37.30 o 6 10 0 93.69 98.46 6.57 o 8 10 0 803.28 855.38 18.10 o 10 10 0 2479.18 2561.74 58.57 o -9 11 0 3543.69 3751.06 92.14 o -7 11 0 1256.31 1298.44 34.57 o -5 11 0 1546.15 1574.55 32.10 o -3 11 0 3927.10 4082.60 94.14 o -1 11 0 582.80 542.10 14.38 o 1 11 0 3635.18 3779.85 85.05 o 3 11 0 207.40 179.38 17.31 o 5 11 0 85.32 55.86 5.56 o 7 11 0 2016.88 1958.64 38.77 o 9 11 0 24.90 29.38 3.86 o 11 11 0 1029.02 1108.80 39.27 o -10 12 0 738.33 652.99 21.51 o -8 12 0 831.07 878.84 21.42 o -6 12 0 618.61 713.88 20.73 o -4 12 0 3347.37 3538.49 80.37 o -2 12 0 839.22 859.47 25.87 o 0 12 0 2449.39 2453.07 59.12 o 2 12 0 394.48 415.76 14.12 o 4 12 0 7.72 21.93 4.25 o 6 12 0 28.40 255.57 30.64 o 8 12 0 174.28 191.55 7.88 o 10 12 0 1208.75 1279.26 31.95 o 12 12 0 178.54 265.57 19.99 o -11 13 0 62.39 77.65 8.94 o -9 13 0 550.43 542.65 17.55 o -7 13 0 110.60 135.14 11.67 o -5 13 0 664.33 647.14 19.61 o -3 13 0 3186.88 3434.66 83.96 o -1 13 0 15.23 10.89 5.37 o 1 13 0 4106.21 4066.35 115.38 o 3 13 0 337.79 341.94 15.53 o 5 13 0 766.62 699.10 22.01 o 7 13 0 284.13 275.32 14.39 o 9 13 0 102.16 114.10 9.01 o 11 13 0 48.63 54.67 7.51 o 13 13 0 522.46 633.45 35.18 o -12 14 0 1147.92 1075.17 37.36 o -10 14 0 1058.69 1017.10 58.49 o -8 14 0 558.70 516.23 19.99 o -6 14 0 2839.19 3002.65 79.13 o -4 14 0 207.37 208.43 10.68 o -2 14 0 1.45 15.08 12.01 o 0 14 0 1237.16 1193.51 51.42 o 2 14 0 288.39 312.82 12.88 o 4 14 0 3096.75 3129.88 78.69 o 6 14 0 1900.06 1722.82 52.32 o 8 14 0 1732.72 1696.82 49.64 o 10 14 0 2525.93 2613.22 77.21 o 12 14 0 6.08 5.83 6.32 o 14 14 0 10.67 56.80 10.86 o -13 15 0 136.51 105.90 10.85 o -11 15 0 149.83 137.39 11.06 o -9 15 0 782.18 889.01 51.76 o -7 15 0 503.82 516.36 18.42 o -5 15 0 4283.64 4561.87 108.49 o -3 15 0 2271.10 2300.71 85.13 o -1 15 0 498.18 445.09 19.18 o 1 15 0 264.97 276.31 38.87 o 3 15 0 66.85 109.30 8.99 o 5 15 0 114.45 121.44 20.54 o 7 15 0 7262.33 7313.81 176.37 o 9 15 0 1045.05 1098.96 42.29 o 11 15 0 4388.48 4320.83 153.29 o 13 15 0 3529.47 3661.98 125.97 o 15 15 0 93.34 139.59 18.61 o -14 16 0 363.07 330.28 21.66 o -12 16 0 109.13 94.36 14.84 o -10 16 0 16.57 30.05 14.45 o -8 16 0 1.06 11.39 4.97 o -6 16 0 443.73 433.73 19.84 o -4 16 0 71.54 59.13 10.67 o -2 16 0 233.71 223.92 14.20 o 0 16 0 0.48 6.17 4.54 o 2 16 0 2110.55 2073.35 68.99 o 4 16 0 1802.98 1723.55 59.35 o 6 16 0 4667.87 4681.87 168.61 o 8 16 0 708.97 761.26 30.85 o 10 16 0 893.06 1059.34 83.10 o 12 16 0 977.67 1011.02 44.09 o 14 16 0 76.29 65.23 11.47 o 16 16 0 102.22 145.68 13.29 o -15 17 0 249.79 243.02 23.66 o -13 17 0 82.77 65.69 17.52 o -11 17 0 80.52 112.19 18.67 o -9 17 0 1159.32 1202.65 44.70 o -7 17 0 540.22 519.71 33.04 o -5 17 0 560.63 577.65 22.21 o -3 17 0 45.75 50.05 7.07 o -1 17 0 0.07 4.79 4.62 o 1 17 0 391.48 412.20 29.28 o 3 17 0 343.53 309.80 18.37 o 5 17 0 64.91 58.53 12.19 o 7 17 0 991.96 890.72 62.08 o 9 17 0 7458.34 7582.83 269.23 o 11 17 0 1281.13 1273.80 64.72 o 13 17 0 1989.15 2275.43 85.06 o 15 17 0 70.09 62.98 10.75 o 17 17 0 84.51 94.56 12.99 o -16 18 0 6.12 23.65 11.68 o -14 18 0 760.57 785.00 51.93 o -12 18 0 34.13 32.46 12.41 o -10 18 0 115.04 121.29 15.03 o -8 18 0 358.21 346.92 28.37 o -6 18 0 1052.37 1048.97 59.45 o -4 18 0 1663.36 1742.54 54.27 o -2 18 0 285.41 246.06 15.72 o 0 18 0 525.36 528.17 26.59 o 2 18 0 519.85 478.19 25.69 o 4 18 0 17.48 14.73 9.71 o 6 18 0 173.39 189.41 15.10 o 8 18 0 514.01 547.81 30.18 o 10 18 0 466.88 499.53 29.84 o 12 18 0 609.69 586.72 36.98 o 14 18 0 156.65 173.24 31.88 o 16 18 0 1414.37 1457.35 55.38 o 18 18 0 8.23 20.86 17.80 o -17 19 0 138.26 111.99 16.96 o -15 19 0 285.81 289.86 36.45 o -13 19 0 474.22 468.15 35.20 o -11 19 0 921.97 993.58 55.80 o -9 19 0 8.67 6.59 7.89 o -7 19 0 61.97 68.85 11.74 o -5 19 0 1129.87 1212.36 49.22 o -3 19 0 46.81 65.75 8.96 o -1 19 0 0.22 -1.27 5.57 o 1 19 0 282.04 285.51 14.99 o 3 19 0 997.05 1058.80 56.49 o 5 19 0 1379.34 1354.55 65.01 o 7 19 0 2369.72 2345.89 106.32 o 9 19 0 704.74 618.52 36.36 o 11 19 0 6.04 -1.74 7.78 o 13 19 0 31.48 41.51 10.08 o 15 19 0 3.52 -7.10 13.79 o 17 19 0 93.99 93.24 31.05 o 19 19 0 503.15 451.72 83.85 o -18 20 0 150.21 183.68 51.51 o -16 20 0 91.05 51.56 16.22 o -14 20 0 369.16 395.80 54.99 o -12 20 0 877.96 884.68 56.04 o -10 20 0 1087.94 1069.02 61.25 o -8 20 0 283.91 272.74 20.25 o -6 20 0 297.37 273.54 31.65 o -4 20 0 633.94 706.19 45.93 o -2 20 0 555.58 559.72 32.24 o 0 20 0 103.80 130.24 16.29 o 2 20 0 301.99 289.74 22.93 o 4 20 0 14.64 16.46 6.64 o 6 20 0 3154.68 3320.25 143.80 o 8 20 0 205.41 155.31 17.36 o 10 20 0 22.13 -0.64 10.80 o 12 20 0 58.47 132.76 25.27 o 14 20 0 0.05 -9.18 14.28 o 16 20 0 173.08 162.62 33.32 o 18 20 0 1.31 22.38 25.81 o -17 21 0 1.93 -3.51 33.00 o -15 21 0 4.86 93.58 46.40 o -13 21 0 38.18 29.37 15.96 o -11 21 0 719.71 709.55 44.12 o -9 21 0 139.12 158.18 20.59 o -7 21 0 1098.78 1031.36 55.94 o -5 21 0 625.49 600.70 32.66 o -3 21 0 536.97 621.46 38.44 o -1 21 0 410.43 428.51 29.56 o 1 21 0 173.64 192.27 15.43 o 3 21 0 429.57 441.52 32.12 o 5 21 0 28.23 37.16 17.08 o 7 21 0 71.66 104.71 32.57 o 9 21 0 46.86 103.32 19.36 o 11 21 0 161.72 122.19 22.43 o 13 21 0 317.51 247.13 39.20 o 15 21 0 786.79 758.86 73.47 o 17 21 0 306.18 353.19 63.87 o -14 22 0 112.28 105.10 25.60 o -12 22 0 782.14 827.33 68.17 o -10 22 0 334.71 311.95 36.04 o -8 22 0 62.34 45.31 13.75 o -6 22 0 280.87 266.85 24.38 o -4 22 0 44.32 44.88 12.36 o -2 22 0 371.72 425.72 57.34 o 0 22 0 49.84 76.42 14.09 o 2 22 0 4.19 11.07 17.96 o 4 22 0 314.30 310.69 39.79 o 6 22 0 89.17 50.84 15.72 o 8 22 0 154.73 150.60 22.25 o 10 22 0 141.09 163.65 28.08 o 12 22 0 406.05 393.67 44.32 o 14 22 0 381.22 292.82 55.11 o -13 23 0 31.97 22.96 24.05 o -11 23 0 91.85 82.49 18.68 o -9 23 0 541.15 449.85 86.45 o -7 23 0 9.98 1.99 17.65 o -5 23 0 6.01 6.55 14.22 o -3 23 0 27.12 43.16 13.26 o -1 23 0 141.99 176.53 19.44 o 1 23 0 0.81 -3.47 12.78 o 3 23 0 79.50 58.58 18.03 o 5 23 0 153.70 133.52 22.97 o 7 23 0 1.55 -10.62 10.62 o 9 23 0 27.05 -2.21 20.53 o 11 23 0 182.15 194.40 44.71 o 13 23 0 473.49 444.53 52.79 o -12 24 0 5.84 4.55 34.39 o -10 24 0 1075.54 1166.73 98.94 o -8 24 0 65.60 79.17 19.03 o -6 24 0 50.95 69.21 49.48 o -4 24 0 0.04 -16.50 26.99 o -2 24 0 221.72 168.69 23.65 o 0 24 0 163.23 208.61 30.05 o 2 24 0 216.02 273.23 27.87 o 4 24 0 548.18 667.57 49.84 o 6 24 0 6.62 52.57 19.00 o 8 24 0 69.43 27.86 21.85 o 10 24 0 27.53 72.90 23.49 o 12 24 0 26.08 2.39 16.91 o -9 25 0 5.27 -3.25 18.37 o -7 25 0 1010.64 1097.95 133.27 o -5 25 0 420.49 407.01 40.64 o -3 25 0 73.52 106.32 22.45 o -1 25 0 0.03 -1.66 16.05 o 1 25 0 3.73 11.68 16.50 o 3 25 0 401.74 444.08 38.60 o 5 25 0 1220.35 1417.15 94.99 o 7 25 0 36.62 21.50 21.41 o 9 25 0 22.58 -0.19 20.02 o -6 26 0 50.06 41.75 19.93 o -4 26 0 2251.27 2323.73 209.30 o -2 26 0 311.41 332.58 34.47 o 0 26 0 19.00 12.61 17.40 o 2 26 0 452.11 555.31 45.90 o 4 26 0 0.32 9.59 18.72 o 6 26 0 15.36 18.83 43.05 o -1 27 0 81.37 58.49 26.68 o 1 27 0 141.71 235.43 40.58 o 0 1 1 4.97 5.62 1.38 o 1 1 1 3852.32 3535.63 62.19 o -1 2 1 422.17 390.46 10.92 o 0 2 1 4954.40 4631.68 68.11 o 1 2 1 2010.23 1910.36 27.46 o 2 2 1 6543.18 6234.37 79.34 o -2 3 1 1598.53 1484.20 17.62 o -1 3 1 5731.83 5575.82 72.29 o 0 3 1 754.11 800.08 10.55 o 1 3 1 9560.43 8753.36 119.78 o 2 3 1 1193.91 1245.31 14.82 o 3 3 1 2.78 -1.06 1.06 o -3 4 1 7632.38 7202.48 82.30 o -2 4 1 1578.61 1595.83 20.29 o -1 4 1 518.12 518.64 7.70 o 0 4 1 9262.65 8653.94 115.77 o 2 4 1 829.39 826.39 9.24 o 3 4 1 2302.17 2427.15 24.62 o 4 4 1 4797.94 4887.53 48.14 o -4 5 1 4296.74 4138.12 47.19 o -3 5 1 5025.41 4898.43 54.49 o -2 5 1 205.91 175.46 3.80 o -1 5 1 7645.52 7319.18 101.40 o 0 5 1 526.48 403.88 6.32 o 2 5 1 17113.75 16657.61 182.07 o 3 5 1 3315.93 3164.21 31.75 o 4 5 1 2185.60 2087.47 21.19 o 5 5 1 426.80 424.50 6.07 o -5 6 1 1176.73 1103.12 12.41 o -4 6 1 47.61 50.99 2.26 o -3 6 1 756.67 706.37 9.58 o -2 6 1 2539.49 2385.47 30.86 o -1 6 1 10869.66 10521.51 136.11 o 0 6 1 543.14 584.51 9.28 o 2 6 1 11202.61 10802.18 125.48 o 3 6 1 2282.21 2245.84 22.94 o 4 6 1 585.84 611.53 9.67 o 5 6 1 3391.98 3281.02 35.46 o 6 6 1 1607.35 1487.03 16.69 o -6 7 1 3.91 2.82 2.22 o -5 7 1 3402.33 3464.21 38.87 o -4 7 1 190.78 169.40 4.66 o -3 7 1 1855.18 1934.70 23.48 o -2 7 1 5004.88 5023.41 63.27 o -1 7 1 3816.87 3825.96 54.52 o 0 7 1 2377.54 2359.72 29.59 o 1 7 1 1124.51 1184.06 16.63 o 2 7 1 7256.33 7231.55 78.64 o 3 7 1 3855.45 3854.58 39.91 o 4 7 1 2.49 1.40 2.35 o 5 7 1 522.79 470.55 7.10 o 6 7 1 7.15 15.95 2.12 o 7 7 1 139.87 132.46 4.10 o -7 8 1 71.18 97.06 3.45 o -6 8 1 383.39 397.95 7.09 o -5 8 1 1202.99 1155.33 15.00 o -4 8 1 1508.88 1606.00 18.67 o -3 8 1 267.24 262.75 4.98 o -2 8 1 326.84 361.14 6.84 o -1 8 1 3511.16 3709.86 50.74 o 0 8 1 923.52 985.31 18.80 o 1 8 1 1.26 -2.06 2.06 o 2 8 1 79.80 77.27 4.52 o 3 8 1 913.57 937.68 12.46 o 4 8 1 287.97 299.30 6.83 o 5 8 1 784.76 851.73 10.75 o 6 8 1 13.40 21.42 2.19 o 7 8 1 1314.48 1423.44 18.26 o 8 8 1 173.16 178.35 4.55 o -8 9 1 1321.09 1254.59 18.14 o -7 9 1 5564.94 6000.76 76.38 o -6 9 1 4571.29 4905.63 61.85 o -5 9 1 12.98 4.96 2.05 o -4 9 1 117.14 135.85 3.78 o -3 9 1 3015.83 2984.72 37.17 o -2 9 1 322.72 383.11 8.15 o -1 9 1 1.12 -0.66 1.69 o 0 9 1 335.39 338.46 8.11 o 1 9 1 551.53 605.29 10.76 o 2 9 1 962.86 1050.82 15.43 o 3 9 1 12412.05 12940.13 148.20 o 4 9 1 405.80 373.08 7.47 o 5 9 1 4405.19 4600.86 53.32 o 6 9 1 843.19 831.33 12.49 o 7 9 1 78.67 61.89 2.89 o 8 9 1 14.87 14.36 2.14 o 9 9 1 18.50 21.92 2.73 o -9 10 1 928.90 936.13 16.02 o -8 10 1 634.62 622.72 12.63 o -7 10 1 83.54 102.38 4.26 o -6 10 1 3964.26 4061.45 50.38 o -5 10 1 474.02 472.09 7.98 o -4 10 1 289.11 312.22 6.42 o -3 10 1 129.26 160.65 4.34 o -2 10 1 183.84 156.93 5.15 o -1 10 1 2.94 9.92 1.97 o 0 10 1 7165.22 7609.96 104.85 o 1 10 1 2066.26 2172.59 30.72 o 2 10 1 2217.45 2254.95 28.66 o 3 10 1 1327.73 1428.34 19.83 o 4 10 1 737.10 720.77 11.65 o 5 10 1 3081.89 3084.02 39.24 o 6 10 1 99.95 98.97 3.53 o 7 10 1 831.74 772.25 13.09 o 8 10 1 198.57 183.39 5.49 o 9 10 1 1781.86 1726.81 30.15 o 10 10 1 46.35 52.61 3.19 o -10 11 1 597.36 550.18 12.86 o -9 11 1 9.81 14.43 3.20 o -8 11 1 218.64 221.22 6.15 o -7 11 1 7.16 19.71 3.23 o -6 11 1 2367.96 2586.72 33.05 o -5 11 1 2744.66 2700.14 38.33 o -4 11 1 1862.08 1805.36 25.76 o -3 11 1 113.79 129.93 5.32 o -2 11 1 187.51 235.36 6.67 o -1 11 1 64.66 94.68 3.76 o 0 11 1 1166.39 1174.93 20.38 o 1 11 1 2370.91 2351.55 31.86 o 2 11 1 3295.58 3494.72 46.24 o 3 11 1 244.68 238.56 6.87 o 4 11 1 2798.31 2768.82 41.79 o 5 11 1 952.81 982.07 17.53 o 6 11 1 129.81 152.60 5.82 o 7 11 1 927.99 924.63 17.01 o 8 11 1 1267.01 1190.87 22.05 o 9 11 1 38.33 48.81 3.34 o 10 11 1 0.51 2.46 2.86 o 11 11 1 4.67 5.80 2.72 o -11 12 1 9.39 4.80 2.86 o -10 12 1 330.28 340.81 9.89 o -9 12 1 380.99 395.31 11.05 o -8 12 1 356.04 347.88 10.39 o -7 12 1 417.71 426.85 9.43 o -6 12 1 2817.92 2784.56 46.86 o -5 12 1 34.28 44.22 2.98 o -4 12 1 31.14 25.22 3.51 o -3 12 1 121.68 113.36 4.48 o -2 12 1 81.20 79.24 4.95 o -1 12 1 3073.46 3022.51 52.81 o 0 12 1 788.92 842.62 15.90 o 1 12 1 1849.96 1913.29 27.34 o 2 12 1 1156.94 1146.87 18.68 o 3 12 1 521.22 519.91 10.70 o 4 12 1 181.07 143.26 6.58 o 5 12 1 17.07 18.14 2.98 o 6 12 1 1479.37 1489.22 23.68 o 7 12 1 67.36 68.54 4.26 o 8 12 1 278.57 300.02 8.24 o 9 12 1 681.56 639.36 15.27 o 10 12 1 61.77 65.81 4.31 o 11 12 1 106.02 108.52 5.54 o 12 12 1 521.76 558.73 16.65 o -12 13 1 301.70 304.41 13.74 o -11 13 1 362.19 379.51 12.66 o -10 13 1 316.24 308.24 10.97 o -9 13 1 560.67 565.59 14.75 o -8 13 1 655.40 670.15 16.16 o -7 13 1 64.59 51.88 3.49 o -6 13 1 2086.95 2039.80 32.65 o -5 13 1 96.25 103.57 5.00 o -4 13 1 3.04 4.18 2.20 o -3 13 1 209.61 212.92 7.98 o -2 13 1 210.11 201.22 6.99 o -1 13 1 2965.73 3056.54 57.36 o 0 13 1 239.31 241.28 8.25 o 1 13 1 65.36 73.58 7.11 o 2 13 1 404.44 396.93 11.68 o 3 13 1 0.31 0.75 2.31 o 4 13 1 7179.11 7351.72 140.98 o 5 13 1 607.07 586.49 20.41 o 6 13 1 252.94 266.24 9.09 o 7 13 1 403.25 421.21 12.58 o 8 13 1 1356.84 1365.96 31.65 o 9 13 1 2.40 -3.02 3.86 o 10 13 1 274.05 283.44 9.45 o 11 13 1 2.23 0.33 3.13 o 12 13 1 1890.78 1968.91 39.52 o 13 13 1 1074.61 1108.05 29.16 o -13 14 1 184.55 196.60 10.57 o -12 14 1 56.74 76.94 7.00 o -11 14 1 233.98 236.45 11.82 o 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