#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/46/2014604.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2014604_Fobs loop_ _publ_author_name '\'Slepokura, Katarzyna' 'Gaw\/lowska, Monika' _publ_section_title ; N-Amidino-4-hydroxy-L-proline monohydrate and N-amidino-L-methionine monohydrate ; _journal_issue 1 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first o25 _journal_page_last o28 _journal_volume 61 _journal_year 2005 _space_group_IT_number 19 _symmetry_space_group_name_Hall 'P 2ac 2ab' _symmetry_space_group_name_H-M 'P 21 21 21' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 4.6040 _cell_length_b 12.5140 _cell_length_c 14.4220 _exptl_crystal_F_000 408.00 _reflns_d_resolution_high 0.7829 _[local]_cod_data_source_file av1216Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' HER8DC in P2(1)2(1)2(1)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 87.67 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 611.07 564.68 25.05 o 4 0 0 33.56 31.96 9.29 o 1 1 0 1153.19 1056.63 7.70 o 2 1 0 552.70 592.71 12.04 o 3 1 0 1569.92 1600.92 11.28 o 4 1 0 176.48 160.97 7.20 o 5 1 0 6.18 13.88 8.00 o 0 2 0 69.84 65.95 3.11 o 1 2 0 3462.39 3459.09 85.64 o 2 2 0 1166.38 1155.12 12.54 o 3 2 0 326.58 340.86 7.22 o 4 2 0 88.60 94.47 8.91 o 5 2 0 9.09 21.91 7.01 o 1 3 0 45.54 50.53 3.22 o 2 3 0 1112.45 1130.50 22.29 o 3 3 0 7.38 16.06 6.21 o 4 3 0 23.07 26.07 5.58 o 5 3 0 41.86 41.81 10.24 o 0 4 0 351.39 381.76 13.64 o 1 4 0 59.01 57.89 2.21 o 2 4 0 504.97 531.80 8.07 o 3 4 0 33.66 37.16 5.29 o 4 4 0 75.96 75.44 8.65 o 5 4 0 150.37 140.44 10.07 o 1 5 0 544.91 518.79 21.18 o 2 5 0 969.72 1056.94 10.06 o 3 5 0 0.28 7.04 8.15 o 4 5 0 68.96 59.70 7.63 o 5 5 0 1.12 11.85 9.10 o 0 6 0 587.44 644.15 41.44 o 1 6 0 83.08 75.84 3.93 o 2 6 0 880.23 897.99 43.95 o 3 6 0 246.16 269.03 7.79 o 4 6 0 22.52 17.82 10.08 o 5 6 0 32.19 29.71 13.16 o 1 7 0 415.35 401.54 17.75 o 2 7 0 14.99 21.82 4.45 o 3 7 0 768.11 753.56 27.53 o 4 7 0 22.18 19.14 9.17 o 5 7 0 4.26 0.36 11.62 o 0 8 0 16.73 19.19 4.13 o 1 8 0 14.88 12.42 3.02 o 2 8 0 18.10 14.34 4.47 o 3 8 0 50.17 53.18 6.68 o 4 8 0 101.68 109.93 12.27 o 5 8 0 5.88 2.68 14.29 o 1 9 0 6.78 11.92 3.43 o 2 9 0 53.78 50.34 7.62 o 3 9 0 4.77 7.37 9.55 o 4 9 0 18.67 26.53 9.60 o 0 10 0 118.94 108.98 7.30 o 1 10 0 104.17 110.40 6.79 o 2 10 0 145.15 137.36 11.76 o 3 10 0 152.74 142.88 11.82 o 4 10 0 49.00 47.01 9.82 o 1 11 0 105.59 111.19 6.75 o 2 11 0 194.33 207.29 11.36 o 3 11 0 11.26 10.84 7.40 o 4 11 0 1.39 15.57 13.68 o 0 12 0 309.27 299.26 12.20 o 1 12 0 9.57 9.74 5.66 o 2 12 0 10.48 13.61 7.06 o 3 12 0 90.91 87.05 9.60 o 1 13 0 0.69 11.15 7.39 o 2 13 0 2.08 3.14 3.92 o 3 13 0 16.84 14.23 10.90 o 0 14 0 1.73 4.58 14.38 o 1 14 0 32.88 31.83 8.06 o 2 14 0 7.41 18.93 12.58 o 1 15 0 3.76 1.71 11.54 o 2 15 0 45.07 53.75 15.18 o 1 0 1 7686.54 8132.50 66.91 o 2 0 1 16.55 22.36 3.82 o 3 0 1 796.35 797.55 9.53 o 4 0 1 148.92 160.83 9.52 o 5 0 1 235.85 219.89 9.45 o 1 1 1 1347.22 1303.08 16.41 o 2 1 1 233.86 222.11 2.14 o 3 1 1 15.91 21.29 2.65 o 4 1 1 99.75 91.61 5.85 o 5 1 1 78.82 84.83 6.59 o 0 2 1 2147.62 2009.55 75.11 o 1 2 1 1243.74 1158.00 33.82 o 2 2 1 420.49 419.31 5.19 o 3 2 1 165.27 175.90 5.40 o 4 2 1 331.59 336.22 8.06 o 5 2 1 119.73 115.33 7.28 o 0 3 1 284.44 257.61 5.00 o 1 3 1 1475.19 1281.92 50.37 o 2 3 1 1543.72 1651.77 15.58 o 3 3 1 82.47 82.81 4.29 o 4 3 1 124.98 140.21 6.37 o 5 3 1 162.42 175.23 7.55 o 0 4 1 1797.38 1784.32 62.79 o 1 4 1 1766.08 1574.10 47.38 o 2 4 1 170.88 177.23 5.05 o 3 4 1 59.13 64.68 4.00 o 4 4 1 270.66 280.04 6.98 o 5 4 1 11.31 13.44 5.19 o 0 5 1 312.66 282.33 11.14 o 1 5 1 1003.62 975.74 36.67 o 2 5 1 53.72 53.93 3.48 o 3 5 1 380.14 401.58 7.05 o 4 5 1 163.93 156.93 6.76 o 5 5 1 49.02 50.77 6.38 o 0 6 1 71.48 73.83 3.00 o 1 6 1 840.56 795.24 20.43 o 2 6 1 1092.94 1139.23 38.66 o 3 6 1 90.68 90.05 5.42 o 4 6 1 134.80 120.72 6.05 o 5 6 1 8.47 9.44 6.06 o 0 7 1 108.33 115.01 6.73 o 1 7 1 37.35 32.01 3.16 o 2 7 1 132.57 125.50 4.41 o 3 7 1 152.30 161.41 6.17 o 4 7 1 105.79 102.21 7.16 o 5 7 1 21.20 25.85 7.90 o 0 8 1 63.29 70.40 3.60 o 1 8 1 381.85 383.86 10.81 o 2 8 1 222.87 213.00 8.56 o 3 8 1 398.18 410.45 7.55 o 4 8 1 7.02 17.75 6.44 o 5 8 1 33.29 34.05 11.78 o 0 9 1 444.40 438.35 18.80 o 1 9 1 84.33 83.58 3.34 o 2 9 1 200.10 187.17 5.35 o 3 9 1 119.63 102.90 5.92 o 4 9 1 49.90 47.03 6.14 o 0 10 1 10.96 11.97 2.99 o 1 10 1 349.13 356.37 10.83 o 2 10 1 462.58 482.39 20.65 o 3 10 1 45.31 41.36 5.63 o 4 10 1 1.50 16.34 6.97 o 0 11 1 66.34 68.09 4.44 o 1 11 1 311.01 286.72 12.44 o 2 11 1 69.99 67.73 5.60 o 3 11 1 25.01 22.06 5.44 o 4 11 1 19.68 24.87 7.59 o 0 12 1 84.37 76.37 5.81 o 1 12 1 77.13 77.72 5.49 o 2 12 1 9.03 13.62 5.00 o 3 12 1 107.86 118.46 7.91 o 0 13 1 50.30 44.05 5.29 o 1 13 1 97.24 103.71 7.73 o 2 13 1 107.64 130.00 9.29 o 3 13 1 12.01 10.73 6.71 o 0 14 1 0.67 3.21 9.04 o 1 14 1 51.35 50.15 6.17 o 2 14 1 47.94 55.78 7.83 o 0 15 1 74.47 72.08 16.54 o 1 15 1 86.72 97.87 11.19 o 2 15 1 58.96 64.91 9.89 o 1 0 2 1857.36 1800.89 17.48 o 2 0 2 48.77 48.39 3.51 o 3 0 2 205.76 209.04 6.28 o 4 0 2 3.51 13.38 6.80 o 5 0 2 7.49 10.72 7.47 o 0 1 2 0.40 4.59 1.91 o 1 1 2 2955.62 2912.24 38.45 o 2 1 2 587.24 619.14 6.16 o 3 1 2 60.65 66.44 3.34 o 4 1 2 118.87 117.84 5.42 o 5 1 2 15.33 18.98 4.98 o 0 2 2 184.19 167.75 5.63 o 1 2 2 2467.14 2190.27 45.23 o 2 2 2 20.21 26.97 2.92 o 3 2 2 473.55 489.19 4.98 o 4 2 2 64.92 65.58 5.17 o 5 2 2 14.19 18.53 5.68 o 0 3 2 1428.52 1420.93 9.28 o 1 3 2 2078.88 1995.70 68.77 o 2 3 2 653.00 639.64 9.31 o 3 3 2 112.63 119.63 4.51 o 4 3 2 82.42 84.12 5.96 o 5 3 2 32.20 43.66 6.06 o 0 4 2 286.10 269.03 13.19 o 1 4 2 483.79 476.91 10.03 o 2 4 2 235.87 230.40 6.49 o 3 4 2 372.22 387.29 5.87 o 4 4 2 130.55 129.48 5.96 o 5 4 2 137.21 150.35 7.10 o 0 5 2 6798.06 7085.95 324.90 o 1 5 2 255.92 262.85 10.86 o 2 5 2 321.09 328.87 9.58 o 3 5 2 17.38 22.05 4.14 o 4 5 2 26.57 29.54 4.68 o 5 5 2 93.20 92.72 7.49 o 0 6 2 46.83 48.09 3.09 o 1 6 2 930.65 987.52 21.68 o 2 6 2 336.47 349.03 12.17 o 3 6 2 924.84 994.85 10.18 o 4 6 2 285.28 266.13 7.60 o 5 6 2 9.33 12.58 6.75 o 0 7 2 368.05 361.60 15.06 o 1 7 2 567.63 551.00 23.37 o 2 7 2 29.72 30.34 4.09 o 3 7 2 87.00 89.16 5.44 o 4 7 2 171.00 183.01 8.37 o 5 7 2 5.87 13.99 9.53 o 0 8 2 333.89 343.38 14.97 o 1 8 2 93.33 88.33 3.33 o 2 8 2 540.71 554.51 22.24 o 3 8 2 2.65 7.11 4.28 o 4 8 2 73.18 67.49 6.79 o 5 8 2 68.72 51.10 11.49 o 0 9 2 111.12 118.14 4.40 o 1 9 2 123.90 124.87 3.99 o 2 9 2 266.82 241.74 9.11 o 3 9 2 14.20 12.04 4.87 o 4 9 2 14.50 11.52 5.96 o 0 10 2 12.88 16.55 3.62 o 1 10 2 74.42 72.55 3.89 o 2 10 2 588.66 616.04 26.69 o 3 10 2 103.97 109.65 7.32 o 4 10 2 14.28 7.60 6.91 o 0 11 2 30.71 30.39 4.69 o 1 11 2 223.47 214.60 6.25 o 2 11 2 15.99 13.78 4.58 o 3 11 2 4.58 11.56 5.51 o 4 11 2 20.58 20.31 7.77 o 0 12 2 6.41 11.06 4.22 o 1 12 2 51.12 57.83 5.74 o 2 12 2 97.73 89.01 7.55 o 3 12 2 74.94 80.14 9.03 o 0 13 2 468.50 456.81 27.86 o 1 13 2 7.18 10.87 5.96 o 2 13 2 31.37 30.28 6.75 o 3 13 2 31.63 38.14 8.30 o 0 14 2 13.84 12.98 6.13 o 1 14 2 37.95 24.72 8.68 o 2 14 2 15.44 16.76 8.63 o 0 15 2 6.56 20.66 17.58 o 1 15 2 32.40 21.46 12.83 o 1 0 3 92.76 101.58 4.03 o 2 0 3 180.71 175.83 3.41 o 3 0 3 837.75 889.10 10.59 o 4 0 3 658.89 694.86 10.47 o 5 0 3 143.17 132.00 8.97 o 0 1 3 955.29 890.23 52.18 o 1 1 3 3339.71 3215.38 33.98 o 2 1 3 553.00 567.72 4.22 o 3 1 3 238.03 248.92 4.08 o 4 1 3 18.86 24.89 4.08 o 5 1 3 7.49 13.04 5.22 o 0 2 3 176.33 165.15 5.23 o 1 2 3 689.52 654.84 11.26 o 2 2 3 268.45 265.21 4.01 o 3 2 3 119.73 116.62 3.74 o 4 2 3 311.24 287.69 6.57 o 5 2 3 167.36 162.16 7.14 o 0 3 3 787.28 814.24 12.83 o 1 3 3 4996.83 4970.63 120.70 o 2 3 3 178.15 167.37 4.45 o 3 3 3 104.89 118.95 4.24 o 4 3 3 107.16 97.01 6.08 o 5 3 3 247.21 242.39 7.49 o 0 4 3 120.41 123.18 6.08 o 1 4 3 220.16 202.58 5.85 o 2 4 3 299.57 300.54 11.14 o 3 4 3 458.95 455.86 13.60 o 4 4 3 12.72 16.15 4.97 o 5 4 3 147.73 141.62 7.40 o 0 5 3 1099.02 1222.52 7.81 o 1 5 3 11.78 12.75 2.08 o 2 5 3 237.77 230.32 8.40 o 3 5 3 24.12 31.70 4.40 o 4 5 3 82.43 84.47 5.38 o 5 5 3 88.66 90.15 8.54 o 0 6 3 0.01 5.67 3.17 o 1 6 3 366.84 371.26 14.37 o 2 6 3 159.69 167.68 6.06 o 3 6 3 85.18 82.59 5.43 o 4 6 3 72.14 66.14 6.37 o 5 6 3 13.16 21.77 9.00 o 0 7 3 230.51 236.75 12.33 o 1 7 3 271.73 261.13 8.33 o 2 7 3 285.78 294.04 6.52 o 3 7 3 85.62 85.43 5.51 o 4 7 3 96.33 101.95 7.63 o 5 7 3 31.58 25.34 10.70 o 0 8 3 1.40 5.78 2.83 o 1 8 3 820.31 824.35 30.85 o 2 8 3 351.43 376.46 11.67 o 3 8 3 135.27 121.79 6.83 o 4 8 3 8.52 15.24 5.86 o 5 8 3 73.33 79.37 16.34 o 0 9 3 3.26 10.23 3.58 o 1 9 3 241.90 232.31 4.36 o 2 9 3 194.88 219.97 11.07 o 3 9 3 29.20 34.37 6.22 o 4 9 3 1.04 13.03 6.04 o 0 10 3 258.55 258.75 17.10 o 1 10 3 649.32 619.84 31.19 o 2 10 3 215.83 210.60 6.98 o 3 10 3 124.98 134.42 7.47 o 4 10 3 127.68 120.50 8.47 o 0 11 3 123.21 105.79 10.29 o 1 11 3 10.63 15.14 5.81 o 2 11 3 156.13 171.41 8.12 o 3 11 3 7.46 10.18 8.76 o 4 11 3 74.77 76.47 8.41 o 0 12 3 135.52 130.64 8.76 o 1 12 3 131.83 129.31 14.98 o 2 12 3 3.67 9.97 6.06 o 3 12 3 159.30 180.23 10.02 o 0 13 3 32.24 31.35 7.46 o 1 13 3 107.45 106.05 8.74 o 2 13 3 3.42 8.87 8.00 o 3 13 3 43.03 49.46 9.50 o 0 14 3 119.23 124.30 9.75 o 1 14 3 9.82 14.84 7.68 o 2 14 3 25.15 25.21 8.42 o 0 15 3 66.56 87.09 15.47 o 1 15 3 38.05 34.52 8.19 o 0 0 4 4550.50 4235.59 131.41 o 1 0 4 704.77 747.13 6.56 o 2 0 4 241.46 236.56 4.15 o 3 0 4 27.44 43.57 11.09 o 4 0 4 30.43 38.98 6.14 o 5 0 4 182.42 187.13 10.79 o 0 1 4 842.22 762.45 10.50 o 1 1 4 1343.72 1280.87 32.24 o 2 1 4 134.30 134.84 2.53 o 3 1 4 183.96 193.32 4.87 o 4 1 4 220.32 233.71 5.77 o 5 1 4 46.06 54.02 5.95 o 0 2 4 41.16 50.96 3.67 o 1 2 4 170.37 170.12 3.87 o 2 2 4 550.97 581.27 5.28 o 3 2 4 59.83 62.22 3.75 o 4 2 4 108.20 98.26 5.70 o 5 2 4 34.25 33.81 5.87 o 0 3 4 28.24 23.59 4.47 o 1 3 4 121.22 118.39 4.73 o 2 3 4 2060.51 1990.86 37.40 o 3 3 4 354.40 346.88 6.10 o 4 3 4 336.55 356.14 7.42 o 5 3 4 112.90 113.36 6.20 o 0 4 4 2291.52 2553.14 20.83 o 1 4 4 389.69 406.08 14.61 o 2 4 4 179.65 179.68 5.42 o 3 4 4 67.18 71.86 4.22 o 4 4 4 209.73 198.68 7.16 o 5 4 4 76.17 88.22 8.01 o 0 5 4 241.78 254.02 3.51 o 1 5 4 869.92 906.83 28.81 o 2 5 4 209.84 227.38 10.27 o 3 5 4 205.16 207.19 11.74 o 4 5 4 77.01 77.53 5.93 o 5 5 4 125.25 129.15 11.68 o 0 6 4 4.40 5.73 2.19 o 1 6 4 26.98 27.28 2.73 o 2 6 4 172.82 171.44 8.50 o 3 6 4 156.45 154.09 6.78 o 4 6 4 5.44 7.48 4.93 o 5 6 4 107.39 98.28 11.61 o 0 7 4 1365.12 1419.69 64.62 o 1 7 4 37.81 39.91 3.47 o 2 7 4 252.07 244.20 5.90 o 3 7 4 385.80 374.73 10.71 o 4 7 4 24.26 21.66 5.92 o 5 7 4 10.50 5.44 7.91 o 0 8 4 1381.75 1413.40 53.51 o 1 8 4 251.84 253.27 8.17 o 2 8 4 49.34 48.69 4.79 o 3 8 4 77.99 72.25 5.56 o 4 8 4 44.22 32.82 6.09 o 0 9 4 142.08 143.02 10.48 o 1 9 4 161.26 164.61 5.28 o 2 9 4 210.13 216.53 7.93 o 3 9 4 9.91 18.51 5.20 o 4 9 4 34.42 31.30 6.41 o 0 10 4 69.02 76.81 6.98 o 1 10 4 24.32 26.13 4.53 o 2 10 4 56.39 54.05 5.46 o 3 10 4 1.61 7.08 6.17 o 4 10 4 71.18 65.26 9.70 o 0 11 4 26.32 36.85 8.15 o 1 11 4 239.19 253.23 11.00 o 2 11 4 48.93 38.87 7.95 o 3 11 4 213.37 222.13 9.42 o 4 11 4 43.22 38.74 7.50 o 0 12 4 31.67 28.76 6.00 o 1 12 4 84.20 67.83 9.26 o 2 12 4 265.66 265.37 12.14 o 3 12 4 119.79 126.07 12.67 o 0 13 4 28.90 31.45 7.24 o 1 13 4 124.55 124.73 12.15 o 2 13 4 247.61 246.72 11.00 o 3 13 4 6.35 2.16 12.18 o 0 14 4 21.89 22.21 7.83 o 1 14 4 61.16 65.64 9.97 o 2 14 4 5.93 9.21 7.91 o 0 15 4 2.59 14.25 13.49 o 1 15 4 36.60 42.53 8.77 o 1 0 5 25.83 22.84 2.98 o 2 0 5 563.95 568.86 6.43 o 3 0 5 131.62 133.22 11.76 o 4 0 5 0.06 6.81 7.65 o 5 0 5 32.17 46.44 9.37 o 0 1 5 564.41 568.91 9.87 o 1 1 5 20.55 21.97 1.86 o 2 1 5 281.85 296.81 3.15 o 3 1 5 4.50 9.19 2.79 o 4 1 5 6.92 16.37 4.15 o 5 1 5 38.66 40.22 5.99 o 0 2 5 169.38 172.92 6.33 o 1 2 5 2696.45 2686.74 56.84 o 2 2 5 313.64 311.61 4.09 o 3 2 5 56.79 58.04 3.78 o 4 2 5 9.76 13.81 4.61 o 5 2 5 218.77 217.51 8.23 o 0 3 5 834.84 843.75 21.52 o 1 3 5 338.39 309.33 9.29 o 2 3 5 1078.11 1069.88 17.64 o 3 3 5 255.79 267.87 6.66 o 4 3 5 748.43 805.41 9.49 o 5 3 5 139.43 135.24 8.99 o 0 4 5 365.44 363.45 27.31 o 1 4 5 1706.61 1559.89 60.91 o 2 4 5 394.24 390.77 11.03 o 3 4 5 5.25 8.85 3.25 o 4 4 5 64.24 56.91 7.49 o 5 4 5 43.38 52.78 9.13 o 0 5 5 330.66 359.19 5.03 o 1 5 5 44.78 44.16 2.60 o 2 5 5 555.79 560.18 14.47 o 3 5 5 248.27 229.50 6.03 o 4 5 5 53.80 56.54 6.11 o 5 5 5 21.11 17.62 9.71 o 0 6 5 7.69 11.11 2.98 o 1 6 5 97.92 95.54 3.52 o 2 6 5 65.97 62.26 3.50 o 3 6 5 281.28 279.12 7.41 o 4 6 5 214.39 201.87 7.21 o 5 6 5 16.50 27.23 11.37 o 0 7 5 165.54 194.60 13.78 o 1 7 5 163.25 167.71 3.90 o 2 7 5 136.49 127.10 4.90 o 3 7 5 479.02 505.56 12.47 o 4 7 5 52.60 37.42 5.88 o 5 7 5 38.28 36.01 9.10 o 0 8 5 86.04 91.90 7.66 o 1 8 5 44.89 40.35 3.95 o 2 8 5 120.96 127.69 9.01 o 3 8 5 28.57 30.97 6.19 o 4 8 5 90.78 91.59 7.64 o 0 9 5 0.45 11.33 6.06 o 1 9 5 56.34 50.70 4.70 o 2 9 5 143.38 134.32 9.03 o 3 9 5 417.30 402.29 10.67 o 4 9 5 47.24 37.63 7.56 o 0 10 5 6.69 6.27 5.20 o 1 10 5 402.22 379.93 6.67 o 2 10 5 23.45 12.81 6.10 o 3 10 5 23.14 26.45 8.57 o 4 10 5 1.30 9.26 7.35 o 0 11 5 161.77 172.65 8.15 o 1 11 5 50.18 37.55 7.17 o 2 11 5 76.83 77.43 9.16 o 3 11 5 5.15 6.10 7.51 o 0 12 5 8.94 9.74 6.10 o 1 12 5 25.27 15.06 6.67 o 2 12 5 87.83 87.59 11.71 o 3 12 5 28.98 25.60 8.77 o 0 13 5 101.16 104.95 10.17 o 1 13 5 97.74 112.27 9.83 o 2 13 5 85.84 71.84 9.06 o 3 13 5 150.34 160.61 14.70 o 0 14 5 13.62 16.19 7.80 o 1 14 5 46.42 39.54 12.78 o 2 14 5 122.29 137.43 12.00 o 0 15 5 21.91 26.85 11.27 o 1 15 5 10.66 0.00 9.32 o 0 0 6 874.19 924.92 26.86 o 1 0 6 69.52 74.91 4.69 o 2 0 6 228.02 220.96 4.81 o 3 0 6 81.62 88.08 9.10 o 4 0 6 29.65 34.70 7.15 o 5 0 6 59.65 42.61 8.29 o 0 1 6 0.81 4.32 2.87 o 1 1 6 207.91 216.43 2.68 o 2 1 6 48.93 52.88 2.77 o 3 1 6 288.63 288.65 5.61 o 4 1 6 189.46 201.00 6.60 o 5 1 6 107.56 109.32 7.20 o 0 2 6 3303.15 3264.28 179.79 o 1 2 6 2.58 5.49 1.44 o 2 2 6 499.88 462.99 7.13 o 3 2 6 48.79 59.96 3.58 o 4 2 6 271.56 280.46 6.46 o 5 2 6 3.10 5.86 6.38 o 0 3 6 748.36 753.73 22.15 o 1 3 6 142.94 141.95 4.05 o 2 3 6 337.68 353.32 9.53 o 3 3 6 40.93 38.79 4.01 o 4 3 6 102.69 104.77 7.57 o 5 3 6 436.23 423.87 9.99 o 0 4 6 5.42 10.70 3.62 o 1 4 6 290.76 307.28 10.10 o 2 4 6 707.47 720.41 15.65 o 3 4 6 10.19 9.63 3.95 o 4 4 6 65.73 42.96 7.84 o 5 4 6 37.71 27.14 10.87 o 0 5 6 13.12 10.11 3.31 o 1 5 6 71.85 77.60 3.45 o 2 5 6 251.11 249.30 8.86 o 3 5 6 421.14 423.79 8.91 o 4 5 6 40.84 33.28 6.96 o 5 5 6 88.25 77.03 10.12 o 0 6 6 349.20 398.44 15.52 o 1 6 6 184.98 181.74 8.59 o 2 6 6 45.95 45.13 3.64 o 3 6 6 17.77 20.13 4.42 o 4 6 6 214.77 214.30 7.86 o 5 6 6 28.73 25.93 8.51 o 0 7 6 369.91 366.83 19.16 o 1 7 6 229.02 241.35 7.10 o 2 7 6 263.82 240.30 12.36 o 3 7 6 60.72 61.09 6.08 o 4 7 6 31.70 32.20 6.14 o 0 8 6 279.58 269.33 9.17 o 1 8 6 66.40 63.64 5.27 o 2 8 6 230.62 225.45 8.49 o 3 8 6 46.37 44.73 6.66 o 4 8 6 17.32 13.36 7.63 o 0 9 6 277.52 289.41 14.98 o 1 9 6 80.09 78.97 5.77 o 2 9 6 450.79 422.65 27.47 o 3 9 6 27.77 33.47 7.64 o 4 9 6 4.64 13.67 9.78 o 0 10 6 307.00 282.26 20.67 o 1 10 6 16.13 14.70 4.59 o 2 10 6 267.09 235.19 9.77 o 3 10 6 18.75 30.72 8.42 o 4 10 6 22.48 28.94 9.37 o 0 11 6 17.03 14.81 5.87 o 1 11 6 253.77 281.61 8.76 o 2 11 6 44.80 48.81 8.72 o 3 11 6 60.42 52.28 8.99 o 0 12 6 422.92 480.04 17.34 o 1 12 6 12.25 12.10 8.80 o 2 12 6 39.02 38.86 7.85 o 3 12 6 41.77 45.46 10.38 o 0 13 6 375.80 385.98 13.33 o 1 13 6 53.41 44.36 8.27 o 2 13 6 34.67 35.70 12.71 o 0 14 6 0.76 9.74 7.58 o 1 14 6 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0 8 1082.65 1137.03 84.62 o 1 0 8 10.53 14.85 3.16 o 2 0 8 306.41 340.99 7.61 o 3 0 8 1000.08 1105.14 19.53 o 4 0 8 65.68 67.09 8.78 o 5 0 8 8.07 15.73 11.26 o 0 1 8 1777.38 1804.33 55.00 o 1 1 8 342.14 354.56 8.29 o 2 1 8 238.22 253.77 7.45 o 3 1 8 7.24 14.38 5.98 o 4 1 8 332.44 359.65 16.49 o 5 1 8 64.97 71.00 9.27 o 0 2 8 74.03 82.72 5.25 o 1 2 8 219.47 217.14 5.91 o 2 2 8 320.32 333.75 7.88 o 3 2 8 422.10 419.64 12.34 o 4 2 8 59.21 69.04 9.74 o 5 2 8 106.55 111.90 11.30 o 0 3 8 396.25 381.44 10.18 o 1 3 8 342.39 338.35 14.47 o 2 3 8 406.08 384.83 13.00 o 3 3 8 77.99 81.69 4.84 o 4 3 8 161.47 155.28 8.38 o 5 3 8 84.99 80.77 10.11 o 0 4 8 119.38 102.22 5.84 o 1 4 8 257.68 257.48 7.27 o 2 4 8 321.81 307.41 10.57 o 3 4 8 442.05 453.17 9.36 o 4 4 8 5.68 5.82 6.27 o 5 4 8 120.30 117.48 11.67 o 0 5 8 183.19 181.31 7.01 o 1 5 8 148.98 163.68 5.57 o 2 5 8 79.33 76.96 5.32 o 3 5 8 9.65 12.95 5.76 o 4 5 8 14.17 28.60 10.94 o 0 6 8 76.09 71.38 5.34 o 1 6 8 273.21 255.25 13.29 o 2 6 8 158.69 179.34 6.66 o 3 6 8 60.26 54.49 7.72 o 4 6 8 280.57 274.33 10.09 o 0 7 8 753.05 735.42 55.15 o 1 7 8 183.59 204.22 5.94 o 2 7 8 30.60 33.11 6.93 o 3 7 8 84.02 74.92 9.23 o 4 7 8 111.82 101.18 8.89 o 0 8 8 1.28 7.30 5.10 o 1 8 8 345.91 340.98 13.46 o 2 8 8 72.41 74.12 8.27 o 3 8 8 138.96 145.59 9.72 o 4 8 8 68.86 58.07 10.21 o 0 9 8 76.07 65.53 8.50 o 1 9 8 305.42 272.30 15.94 o 2 9 8 27.17 20.54 6.64 o 3 9 8 3.06 16.68 7.92 o 4 9 8 12.80 10.60 8.67 o 0 10 8 1.10 2.35 5.83 o 1 10 8 14.98 13.86 4.99 o 2 10 8 219.87 216.86 13.62 o 3 10 8 2.31 5.17 8.17 o 0 11 8 12.36 15.04 7.12 o 1 11 8 57.88 71.73 7.22 o 2 11 8 5.75 15.45 6.89 o 3 11 8 11.30 13.36 8.75 o 0 12 8 0.00 10.58 7.18 o 1 12 8 88.76 80.40 8.97 o 2 12 8 55.82 54.37 10.96 o 0 13 8 18.79 17.14 9.61 o 1 13 8 14.01 16.11 8.04 o 2 13 8 30.87 35.34 9.90 o 0 14 8 0.16 9.09 9.15 o 1 14 8 53.70 45.33 9.55 o 1 0 9 448.03 458.46 21.82 o 2 0 9 40.74 44.85 5.38 o 4 0 9 122.21 122.91 12.61 o 5 0 9 0.04 6.61 10.98 o 0 1 9 182.45 189.39 5.93 o 1 1 9 158.74 169.51 6.76 o 2 1 9 144.88 154.97 5.18 o 3 1 9 125.76 133.08 10.41 o 4 1 9 61.66 63.31 9.75 o 5 1 9 43.06 59.32 11.82 o 0 2 9 34.80 30.23 6.02 o 1 2 9 619.46 639.33 12.56 o 2 2 9 204.08 208.16 6.50 o 3 2 9 11.29 18.72 4.07 o 4 2 9 75.99 71.87 12.22 o 5 2 9 107.95 128.01 10.04 o 0 3 9 89.26 103.25 6.16 o 1 3 9 6.84 13.83 3.70 o 2 3 9 151.66 151.95 4.12 o 3 3 9 200.25 199.13 6.44 o 4 3 9 116.15 117.05 8.40 o 5 3 9 6.08 9.81 11.04 o 0 4 9 166.21 169.54 16.23 o 1 4 9 120.82 115.01 4.58 o 2 4 9 171.86 163.22 6.65 o 3 4 9 18.72 20.32 5.37 o 4 4 9 24.72 13.76 7.25 o 0 5 9 38.73 49.01 5.67 o 1 5 9 434.66 431.53 14.23 o 2 5 9 82.84 76.78 5.00 o 3 5 9 138.93 136.86 8.66 o 4 5 9 37.98 29.41 10.10 o 0 6 9 46.04 46.01 5.96 o 1 6 9 911.94 899.87 38.47 o 2 6 9 44.79 42.08 5.04 o 3 6 9 120.11 115.39 8.78 o 4 6 9 44.72 42.45 13.76 o 0 7 9 53.02 54.14 6.44 o 1 7 9 291.21 277.90 14.66 o 2 7 9 25.95 30.50 5.03 o 3 7 9 76.52 65.23 9.68 o 4 7 9 43.71 36.20 12.38 o 0 8 9 199.40 201.06 7.77 o 1 8 9 392.20 359.50 8.99 o 2 8 9 96.71 87.67 8.88 o 3 8 9 73.89 74.54 9.84 o 4 8 9 128.91 126.36 11.92 o 0 9 9 138.74 148.91 8.06 o 1 9 9 15.05 16.29 4.71 o 2 9 9 186.29 173.38 12.03 o 3 9 9 101.66 109.23 10.32 o 0 10 9 0.22 9.61 5.97 o 1 10 9 322.25 340.81 9.06 o 2 10 9 11.75 16.53 7.14 o 3 10 9 10.46 2.37 7.70 o 0 11 9 48.83 44.19 9.53 o 1 11 9 34.95 35.09 5.78 o 2 11 9 37.56 36.36 8.01 o 3 11 9 27.55 28.85 9.17 o 0 12 9 112.46 109.86 9.96 o 1 12 9 44.42 40.30 8.40 o 2 12 9 22.62 26.41 9.07 o 0 13 9 30.69 42.02 9.51 o 1 13 9 7.71 5.30 11.93 o 0 0 10 22.35 21.12 6.53 o 1 0 10 354.12 340.41 21.14 o 2 0 10 1039.01 995.63 64.32 o 4 0 10 0.21 8.28 14.55 o 0 1 10 13.30 7.25 5.81 o 1 1 10 298.95 281.35 6.78 o 2 1 10 71.25 77.40 5.78 o 3 1 10 95.56 94.42 12.92 o 4 1 10 15.29 17.06 9.35 o 0 2 10 250.52 243.25 24.73 o 1 2 10 175.05 177.54 5.73 o 2 2 10 82.95 85.56 4.94 o 3 2 10 9.73 11.98 3.93 o 4 2 10 125.03 107.63 11.44 o 0 3 10 145.31 161.28 10.64 o 1 3 10 190.73 192.01 6.31 o 2 3 10 186.83 188.84 5.57 o 3 3 10 35.03 39.18 5.92 o 4 3 10 29.99 31.37 12.25 o 0 4 10 356.24 408.20 15.65 o 1 4 10 5.03 9.15 3.30 o 2 4 10 47.53 46.27 5.46 o 3 4 10 433.88 422.80 12.92 o 4 4 10 4.13 12.76 15.85 o 0 5 10 8.96 9.61 5.14 o 1 5 10 149.64 145.63 7.45 o 2 5 10 307.86 313.65 7.97 o 3 5 10 292.79 290.75 9.57 o 4 5 10 63.73 36.91 12.69 o 0 6 10 1973.99 2025.38 43.51 o 1 6 10 26.77 28.70 4.78 o 2 6 10 126.19 124.43 6.19 o 3 6 10 17.50 10.50 6.54 o 4 6 10 80.43 83.23 13.66 o 0 7 10 8.12 11.51 5.47 o 1 7 10 2.20 10.95 4.43 o 2 7 10 271.72 249.46 8.55 o 3 7 10 79.12 72.43 15.66 o 4 7 10 110.37 106.42 10.08 o 0 8 10 175.58 165.36 9.24 o 1 8 10 95.73 104.59 8.03 o 2 8 10 74.16 61.04 7.30 o 3 8 10 2.93 2.06 7.28 o 0 9 10 18.52 26.49 7.18 o 1 9 10 82.81 78.75 6.72 o 2 9 10 64.18 51.11 7.97 o 3 9 10 53.72 53.43 9.09 o 0 10 10 98.93 88.58 8.29 o 1 10 10 20.38 18.47 5.86 o 2 10 10 2.16 13.45 8.18 o 3 10 10 4.00 6.10 7.64 o 0 11 10 7.07 10.13 7.01 o 1 11 10 9.55 16.77 6.15 o 2 11 10 100.94 110.67 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225.96 204.08 6.81 o 2 7 11 59.29 58.53 5.90 o 3 7 11 30.50 26.63 8.79 o 0 8 11 18.99 22.28 6.98 o 1 8 11 76.01 62.06 6.27 o 2 8 11 28.97 28.24 6.23 o 3 8 11 29.00 16.85 8.41 o 0 9 11 16.92 19.56 7.18 o 1 9 11 72.91 78.13 6.22 o 2 9 11 116.95 114.31 12.64 o 3 9 11 7.50 17.51 8.58 o 0 10 11 2.61 15.30 6.81 o 1 10 11 60.79 63.71 7.72 o 2 10 11 27.00 20.68 8.03 o 0 11 11 31.75 18.98 11.58 o 1 11 11 56.75 55.25 7.31 o 2 11 11 10.89 8.72 9.15 o 0 12 11 30.97 34.21 9.23 o 1 12 11 32.05 43.84 9.27 o 0 0 12 31.38 17.41 7.27 o 1 0 12 15.79 13.63 5.09 o 2 0 12 368.46 346.12 22.95 o 3 0 12 315.90 284.06 17.62 o 0 1 12 357.64 325.44 9.69 o 1 1 12 420.40 379.50 17.15 o 2 1 12 9.27 18.59 4.37 o 3 1 12 49.68 67.18 12.09 o 0 2 12 614.82 588.07 17.93 o 1 2 12 107.85 108.32 6.38 o 2 2 12 367.23 381.78 18.97 o 3 2 12 4.27 9.79 10.23 o 0 3 12 453.23 460.03 9.88 o 1 3 12 18.49 21.85 4.45 o 2 3 12 14.57 24.48 6.28 o 3 3 12 1.21 4.25 7.61 o 0 4 12 26.70 57.86 14.42 o 1 4 12 73.46 65.96 5.45 o 2 4 12 283.29 289.26 11.27 o 3 4 12 200.87 205.95 11.04 o 0 5 12 97.16 92.60 9.92 o 1 5 12 522.50 523.60 6.50 o 2 5 12 8.39 9.74 5.87 o 3 5 12 6.93 9.37 9.52 o 0 6 12 193.72 221.80 15.24 o 1 6 12 90.08 85.53 5.93 o 2 6 12 238.31 226.44 12.25 o 3 6 12 11.06 16.27 8.20 o 0 7 12 275.30 293.36 12.99 o 1 7 12 11.48 7.88 5.76 o 2 7 12 23.69 28.27 5.95 o 3 7 12 10.06 8.94 7.36 o 0 8 12 3.49 4.10 7.02 o 1 8 12 78.44 72.57 6.82 o 2 8 12 58.68 57.23 7.74 o 3 8 12 121.67 115.51 11.15 o 0 9 12 268.38 295.36 18.17 o 1 9 12 41.80 37.70 6.10 o 2 9 12 50.35 40.31 10.78 o 0 10 12 282.39 293.96 16.24 o 1 10 12 21.55 23.97 6.08 o 2 10 12 34.18 24.66 9.16 o 0 11 12 21.25 27.93 11.71 o 1 11 12 5.86 10.44 6.40 o 0 12 12 0.11 12.42 12.66 o 1 0 13 385.33 343.48 15.30 o 2 0 13 18.33 24.38 6.84 o 3 0 13 1.51 21.81 14.89 o 0 1 13 31.51 23.61 5.79 o 1 1 13 111.91 117.81 5.65 o 2 1 13 108.84 103.81 6.29 o 3 1 13 38.99 29.50 9.23 o 0 2 13 61.05 53.26 6.61 o 1 2 13 179.03 168.47 5.98 o 2 2 13 303.39 309.22 8.94 o 3 2 13 60.86 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