#------------------------------------------------------------------------------
#$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $
#$Revision: 26848 $
#$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/46/2014609.hkl $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2014609_Fobs
loop_
_publ_author_name
'Gustafsson, Joacim C. M.'
'Norberg, Stefan T.'
'Svensson, G\"oran'
'Albertsson, J\"orgen'
_publ_section_title
;
 Two new phosphate langbeinites, Rb~2~YbTi(PO~4~)~3~ and
 Rb~2~Yb~0.32~Ti~1.68~(PO~4~)~3~, investigated at 293 and 150K
;
_journal_issue                   2
_journal_name_full               'Acta Crystallographica Section C'
_journal_page_first              i9
_journal_page_last               i13
_journal_volume                  61
_journal_year                    2005
_space_group_IT_number           198
_symmetry_space_group_name_Hall  'P 2ac 2ab 3'
_symmetry_space_group_name_H-M   'P 21 3'
_[local]_cod_data_source_file    bc1051I_150_Ksup3.hkl
_[local]_cod_data_source_block   I_150_K
loop_
_refln_index_h
_refln_index_k
_refln_index_l
_refln_F_squared_calc
_refln_F_squared_meas
_refln_F_squared_sigma
_refln_observed_status
-1 1 1 2841.94 3699.46 95.76 o
0 1 1 798.45 1086.18 26.26 o
1 1 1 3536.09 4143.85 79.66 o
0 0 2 1349.92 1595.81 30.01 o
1 0 2 7.20 167.01 6.07 o
-1 1 2 17497.80 18709.10 149.47 o
0 1 2 15398.49 17422.81 119.70 o
1 1 2 13945.12 15045.36 136.24 o
-2 2 2 4622.12 4654.66 135.89 o
-1 2 2 3390.43 3816.94 39.65 o
0 2 2 12714.32 12740.41 108.41 o
1 2 2 2928.64 3484.12 46.77 o
2 2 2 4427.92 4332.48 105.30 o
1 0 3 119298.16 108452.14 660.59 o
2 0 3 7139.92 7519.87 72.53 o
-2 1 3 69912.74 66128.70 523.69 o
-1 1 3 25708.74 26027.97 184.91 o
0 1 3 75788.52 72887.22 417.85 o
1 1 3 25533.08 25003.24 186.31 o
2 1 3 72166.29 67557.52 439.92 o
-2 2 3 6405.29 6426.02 57.19 o
-1 2 3 30781.87 30673.14 237.08 o
0 2 3 8432.10 7629.57 72.72 o
1 2 3 33084.14 33391.55 343.45 o
2 2 3 6171.94 6080.03 74.72 o
-3 3 3 18033.82 19594.51 206.47 o
-2 3 3 6783.55 7000.23 71.81 o
-1 3 3 2581.86 2808.11 34.66 o
0 3 3 289.87 598.17 13.28 o
1 3 3 2746.07 3021.51 39.24 o
2 3 3 7158.22 7125.98 69.08 o
3 3 3 15691.13 16477.65 192.93 o
0 0 4 4892.49 5173.87 61.87 o
1 0 4 1328.55 1443.05 17.02 o
2 0 4 7449.77 7060.37 82.55 o
3 0 4 23362.36 24762.57 199.05 o
-3 1 4 15016.45 14953.51 130.47 o
-2 1 4 366.79 516.82 14.15 o
-1 1 4 2644.56 3101.94 44.29 o
0 1 4 82.89 161.75 5.94 o
1 1 4 2399.05 2665.54 37.63 o
2 1 4 266.48 402.47 14.48 o
3 1 4 17005.09 16580.17 172.51 o
-3 2 4 20970.05 21194.65 206.14 o
-2 2 4 57264.34 55193.36 368.41 o
-1 2 4 6714.69 6880.17 67.74 o
0 2 4 4261.06 4842.11 60.76 o
1 2 4 5876.84 6127.07 74.99 o
2 2 4 57676.50 54462.36 374.64 o
3 2 4 18187.88 17917.21 130.51 o
-3 3 4 2299.85 2467.01 50.19 o
-2 3 4 2441.72 2682.79 27.69 o
-1 3 4 47093.87 46054.54 232.41 o
0 3 4 1048.98 1392.39 24.17 o
1 3 4 45588.29 44019.82 322.85 o
2 3 4 2973.04 3124.03 28.20 o
3 3 4 2584.14 2890.03 32.39 o
-4 4 4 58652.34 57806.63 759.69 o
-3 4 4 3354.67 3559.47 40.01 o
-2 4 4 9163.67 9364.22 74.48 o
-1 4 4 24039.40 24076.32 136.61 o
0 4 4 11686.33 12469.24 91.61 o
1 4 4 25471.54 24632.55 181.63 o
2 4 4 9350.31 9396.37 75.83 o
3 4 4 3935.54 4217.77 43.53 o
4 4 4 62448.52 57989.00 755.86 o
1 0 5 22600.64 22809.86 161.59 o
2 0 5 11428.16 11713.07 68.99 o
3 0 5 3578.82 4067.77 56.60 o
4 0 5 729.82 651.96 13.72 o
-4 1 5 13884.23 13970.64 121.26 o
-3 1 5 1199.53 1348.65 26.48 o
-2 1 5 1376.90 1514.45 25.17 o
-1 1 5 6730.14 7431.75 47.38 o
0 1 5 16761.80 16787.11 134.69 o
1 1 5 5499.03 5902.58 54.71 o
2 1 5 827.01 958.83 15.92 o
3 1 5 1195.70 1292.01 22.29 o
4 1 5 14451.97 14331.00 108.19 o
-4 2 5 21519.49 21382.53 164.86 o
-3 2 5 41684.54 41067.59 184.65 o
-2 2 5 1301.89 1630.53 25.20 o
-1 2 5 7110.18 7519.45 90.80 o
0 2 5 23816.44 24846.97 169.02 o
1 2 5 8848.03 9106.17 72.14 o
2 2 5 1571.64 2004.25 38.60 o
3 2 5 38771.08 36799.96 203.22 o
4 2 5 20010.47 19484.42 147.95 o
-4 3 5 10914.05 11170.61 114.32 o
-3 3 5 3800.56 3926.13 50.83 o
-2 3 5 37222.89 36002.92 359.82 o
-1 3 5 385.57 518.44 12.98 o
0 3 5 22710.69 22746.84 102.89 o
1 3 5 379.48 507.88 11.68 o
2 3 5 37808.58 36022.42 276.16 o
3 3 5 4577.79 4698.95 66.11 o
4 3 5 11523.75 11386.72 108.46 o
-4 4 5 6380.62 6526.31 70.69 o
-3 4 5 14471.13 14801.39 112.94 o
-2 4 5 4591.02 4768.20 45.94 o
-1 4 5 32670.82 31806.10 158.50 o
0 4 5 5110.20 5111.44 38.77 o
1 4 5 34744.32 33310.40 259.88 o
2 4 5 4879.44 4888.26 47.80 o
3 4 5 14181.80 14073.52 108.54 o
4 4 5 6971.04 7172.43 54.30 o
-5 5 5 24588.88 25046.56 186.41 o
-4 5 5 13217.18 13255.42 81.96 o
-3 5 5 5410.14 5599.76 78.96 o
-2 5 5 7664.18 7796.34 67.32 o
-1 5 5 5840.23 6088.99 67.56 o
0 5 5 13497.30 13044.26 96.62 o
1 5 5 6841.06 7139.00 76.91 o
2 5 5 7840.85 8042.76 84.40 o
3 5 5 4124.58 4078.81 48.96 o
4 5 5 11737.68 11603.58 98.26 o
5 5 5 22613.77 21574.98 185.77 o
0 0 6 27438.57 27109.11 247.92 o
1 0 6 26797.99 25413.00 172.06 o
2 0 6 23873.92 23817.27 232.45 o
3 0 6 10745.20 10175.63 72.36 o
4 0 6 5548.10 5686.52 58.28 o
5 0 6 44.16 198.72 9.15 o
-5 1 6 5506.04 5744.62 69.72 o
-4 1 6 530.42 693.39 14.83 o
-3 1 6 55084.67 53900.19 253.36 o
-2 1 6 11161.37 11305.30 111.59 o
-1 1 6 28617.29 28246.91 159.75 o
0 1 6 15476.28 15079.59 123.85 o
1 1 6 29564.50 29596.21 173.30 o
2 1 6 10730.44 11085.19 71.84 o
3 1 6 58979.49 56839.33 465.12 o
4 1 6 627.99 764.81 18.95 o
5 1 6 6045.64 6134.12 60.26 o
-5 2 6 2019.00 2160.31 26.28 o
-4 2 6 11780.08 11471.62 90.67 o
-3 2 6 5352.37 5767.63 44.81 o
-2 2 6 10817.19 11073.96 101.23 o
-1 2 6 12547.12 12306.42 110.72 o
0 2 6 21782.00 21340.83 155.05 o
1 2 6 12197.09 11899.18 83.63 o
2 2 6 10037.60 10022.02 90.34 o
3 2 6 4602.19 4805.80 46.05 o
4 2 6 10180.17 9899.67 117.27 o
5 2 6 2317.84 2406.99 36.62 o
-5 3 6 8940.87 9131.25 90.40 o
-4 3 6 1981.34 2293.37 29.31 o
-3 3 6 4292.92 4565.86 52.82 o
-2 3 6 12750.26 12644.77 112.92 o
-1 3 6 1710.96 2068.71 32.00 o
0 3 6 27121.42 26685.92 202.04 o
1 3 6 1971.70 2267.69 24.46 o
2 3 6 12571.73 12451.45 101.80 o
3 3 6 4644.09 4650.62 38.88 o
4 3 6 1769.00 1911.81 28.62 o
5 3 6 7823.95 7495.96 53.93 o
-5 4 6 6268.78 6728.16 53.96 o
-4 4 6 1099.92 1215.22 34.17 o
-3 4 6 1747.97 1941.84 31.93 o
-2 4 6 4757.41 4807.40 41.84 o
-1 4 6 5293.63 5685.76 47.97 o
0 4 6 25.40 138.80 8.68 o
1 4 6 4377.54 4673.42 39.11 o
2 4 6 4954.68 4968.13 51.53 o
3 4 6 1093.26 1160.96 29.10 o
4 4 6 1300.24 1477.80 30.34 o
5 4 6 6223.92 6431.45 56.96 o
-5 5 6 6644.05 7015.94 51.11 o
-4 5 6 1184.18 1555.82 40.82 o
-3 5 6 15738.73 16278.56 138.82 o
-2 5 6 6100.09 6225.57 48.74 o
-1 5 6 16991.33 16842.00 127.73 o
0 5 6 388.05 489.20 12.67 o
1 5 6 15352.63 14517.98 100.90 o
2 5 6 4195.70 4145.47 40.92 o
3 5 6 16441.49 15963.85 87.20 o
4 5 6 679.39 795.30 18.29 o
5 5 6 6343.75 6490.66 43.71 o
-6 6 6 18467.96 19519.69 372.68 o
-5 6 6 2059.81 2314.67 45.88 o
-4 6 6 18099.16 18346.88 147.96 o
-3 6 6 2297.85 2435.09 27.52 o
-2 6 6 7833.80 8178.14 80.75 o
-1 6 6 1112.10 1277.18 24.38 o
0 6 6 44350.69 43062.66 445.15 o
1 6 6 1451.14 1577.62 28.59 o
2 6 6 7639.03 7964.55 71.53 o
3 6 6 2428.05 2644.74 29.76 o
4 6 6 18652.16 18089.94 152.24 o
5 6 6 1670.82 1755.89 26.54 o
6 6 6 18927.66 17912.86 306.84 o
1 0 7 6357.72 6383.56 56.84 o
2 0 7 2791.51 2866.69 28.63 o
3 0 7 42.27 135.65 8.09 o
4 0 7 24919.55 24097.33 189.19 o
5 0 7 516.17 527.92 14.38 o
6 0 7 4568.70 4439.34 46.77 o
-6 1 7 1074.81 1242.07 20.28 o
-5 1 7 4259.23 4449.46 58.39 o
-4 1 7 11949.11 12545.04 120.73 o
-3 1 7 17861.35 17099.40 205.59 o
-2 1 7 12028.35 11729.75 104.22 o
-1 1 7 3741.35 4163.79 42.77 o
0 1 7 9091.53 9317.91 105.00 o
1 1 7 3346.69 3758.51 35.57 o
2 1 7 13636.68 13026.67 106.91 o
3 1 7 16267.95 15459.46 182.22 o
4 1 7 13398.34 13378.28 131.83 o
5 1 7 4778.06 4968.69 53.55 o
6 1 7 1257.05 1416.19 35.03 o
-6 2 7 3046.59 3335.52 50.94 o
-5 2 7 24280.80 24380.27 161.69 o
-4 2 7 6964.67 7211.51 66.91 o
-3 2 7 11300.71 11344.11 93.99 o
-2 2 7 7017.76 7035.40 71.49 o
-1 2 7 1412.44 1501.77 19.36 o
0 2 7 14340.59 14196.37 142.62 o
1 2 7 875.53 945.89 20.15 o
2 2 7 7901.53 7896.10 63.35 o
3 2 7 10866.73 10634.42 96.17 o
4 2 7 7967.21 7859.46 75.10 o
5 2 7 25193.42 24235.71 134.68 o
6 2 7 3696.47 3929.86 37.23 o
-6 3 7 15351.23 15530.92 196.99 o
-5 3 7 1878.95 1885.82 32.83 o
-4 3 7 3378.41 3673.47 51.38 o
-3 3 7 16507.48 16375.45 179.71 o
-2 3 7 309.90 567.16 15.39 o
-1 3 7 4316.78 4398.26 48.15 o
0 3 7 69259.06 65780.10 482.71 o
1 3 7 4992.44 5098.58 76.80 o
2 3 7 439.79 633.02 16.16 o
3 3 7 17402.08 17274.48 182.10 o
4 3 7 3619.03 3748.09 39.33 o
5 3 7 2881.82 2876.63 33.64 o
6 3 7 16711.99 16175.97 131.29 o
-6 4 7 6673.04 7080.76 70.29 o
-5 4 7 4738.95 5078.96 65.60 o
-4 4 7 1189.95 1400.35 26.25 o
-3 4 7 45111.16 43965.02 288.01 o
-2 4 7 426.34 605.59 14.52 o
-1 4 7 2215.29 2495.27 41.40 o
0 4 7 7853.71 7774.49 46.83 o
1 4 7 2377.39 2649.79 45.30 o
2 4 7 570.93 668.83 15.97 o
3 4 7 48298.86 45319.77 275.83 o
4 4 7 1106.17 1341.66 20.63 o
5 4 7 4757.66 4808.39 38.49 o
6 4 7 6651.47 6749.58 62.12 o
-6 5 7 19525.28 20023.01 163.67 o
-5 5 7 9843.42 10308.41 87.47 o
-4 5 7 2083.93 2403.40 36.81 o
-3 5 7 3168.58 3468.80 52.51 o
-2 5 7 16949.68 17064.76 114.42 o
-1 5 7 3278.18 3623.86 43.93 o
0 5 7 103.63 302.25 13.48 o
1 5 7 3234.69 3493.58 48.01 o
2 5 7 17145.67 16034.16 112.79 o
3 5 7 2792.07 2998.37 43.22 o
4 5 7 1783.00 2124.49 25.66 o
5 5 7 10512.46 10527.86 75.60 o
6 5 7 20391.74 19775.52 138.52 o
-6 6 7 2226.20 2534.89 37.62 o
-5 6 7 2201.30 2575.07 47.32 o
-4 6 7 2188.72 2298.92 29.60 o
-3 6 7 1129.05 1285.08 39.00 o
-2 6 7 8785.40 8881.71 78.80 o
-1 6 7 13526.12 13226.93 98.91 o
0 6 7 1658.74 1744.28 54.22 o
1 6 7 12404.30 11986.07 144.91 o
2 6 7 9413.64 9650.80 55.86 o
3 6 7 1007.31 1178.14 22.57 o
4 6 7 2416.24 2541.26 31.58 o
5 6 7 2620.50 2697.91 45.69 o
6 6 7 1840.96 1960.37 32.24 o
-7 7 7 11949.63 12888.51 175.03 o
-6 7 7 3288.01 3424.98 47.17 o
-5 7 7 123.85 180.64 15.43 o
-4 7 7 662.44 759.42 21.90 o
-3 7 7 1477.43 1681.55 42.16 o
-2 7 7 2702.03 2871.79 32.63 o
-1 7 7 200.08 254.17 14.20 o
0 7 7 6141.70 6227.92 58.00 o
1 7 7 298.99 375.38 16.94 o
2 7 7 3166.62 3350.37 63.43 o
3 7 7 1168.01 1283.56 28.83 o
4 7 7 728.32 811.22 21.87 o
5 7 7 284.28 394.27 18.17 o
6 7 7 3500.28 3624.74 40.11 o
7 7 7 10713.07 10924.90 137.08 o
0 0 8 8073.68 7720.34 184.27 o
1 0 8 11473.26 11801.92 81.01 o
2 0 8 383.97 479.35 16.58 o
3 0 8 4318.19 4732.84 36.04 o
4 0 8 756.70 821.30 18.98 o
5 0 8 1045.05 1139.28 33.28 o
6 0 8 18093.18 17472.44 141.33 o
7 0 8 88.24 169.07 15.94 o
-7 1 8 19039.28 18916.92 154.06 o
-6 1 8 12691.60 12816.31 113.81 o
-5 1 8 2499.75 2568.87 37.38 o
-4 1 8 2997.78 3050.50 49.18 o
-3 1 8 16586.47 16370.85 124.75 o
-2 1 8 5197.16 5383.89 64.61 o
-1 1 8 3283.67 3458.49 49.21 o
0 1 8 68.60 91.50 9.64 o
1 1 8 3107.59 3175.56 53.36 o
2 1 8 4762.15 5069.21 66.32 o
3 1 8 15158.48 14939.00 144.66 o
4 1 8 2150.72 2124.79 45.00 o
5 1 8 2847.83 2778.94 33.28 o
6 1 8 10959.79 10887.01 119.61 o
7 1 8 18175.66 17607.61 146.08 o
-7 2 8 282.32 377.79 19.99 o
-6 2 8 7285.48 7721.79 130.72 o
-5 2 8 1894.49 2065.38 28.67 o
-4 2 8 9126.79 9242.86 86.43 o
-3 2 8 3495.94 3821.25 47.72 o
-2 2 8 32631.11 32628.60 230.77 o
-1 2 8 2196.82 2230.83 26.12 o
0 2 8 8732.92 8678.47 79.21 o
1 2 8 2078.70 2012.47 23.68 o
2 2 8 32429.01 31506.65 227.52 o
3 2 8 3723.13 3917.66 31.74 o
4 2 8 7254.75 7264.45 75.15 o
5 2 8 2219.50 2415.11 54.53 o
6 2 8 7781.76 7664.97 65.00 o
7 2 8 708.68 825.96 30.65 o
-7 3 8 6885.57 7047.33 80.94 o
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0 3 8 5041.53 5384.00 73.66 o
1 3 8 12685.38 12911.25 102.06 o
2 3 8 2034.07 2223.23 43.09 o
3 3 8 3418.41 3467.24 58.56 o
4 3 8 2183.87 2403.00 30.42 o
5 3 8 14062.10 13665.53 136.56 o
6 3 8 5151.37 5213.70 51.38 o
7 3 8 7017.70 7109.43 70.99 o
-7 4 8 215.81 238.98 18.02 o
-6 4 8 7495.17 7927.20 90.54 o
-5 4 8 4125.91 4456.46 79.30 o
-4 4 8 6237.01 6730.56 73.68 o
-3 4 8 14730.34 14881.78 143.82 o
-2 4 8 10607.67 10431.50 81.29 o
-1 4 8 3304.49 3456.00 51.55 o
0 4 8 1047.23 1228.80 31.33 o
1 4 8 2726.87 2758.88 41.88 o
2 4 8 10794.58 10193.89 74.43 o
3 4 8 13862.20 13290.52 162.56 o
4 4 8 7059.35 7096.48 60.32 o
5 4 8 3498.23 3536.20 46.87 o
6 4 8 6785.67 6989.77 97.12 o
7 4 8 342.55 372.26 20.63 o
-7 5 8 391.94 454.72 21.65 o
-6 5 8 6901.36 7009.78 66.30 o
-5 5 8 4899.97 4965.58 56.32 o
-4 5 8 1068.96 1058.53 24.02 o
-3 5 8 8982.00 9150.91 62.06 o
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-1 5 8 14897.17 14512.92 140.29 o
0 5 8 18335.19 17525.37 157.12 o
1 5 8 16258.37 15876.24 182.16 o
2 5 8 2140.97 2116.86 28.82 o
3 5 8 9374.44 9356.76 101.52 o
4 5 8 1017.41 934.02 23.86 o
5 5 8 3640.23 3825.83 42.64 o
6 5 8 7149.43 6972.37 66.91 o
7 5 8 185.99 241.89 19.37 o
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2 7 8 2759.53 3027.00 53.75 o
3 7 8 10017.86 9969.33 124.08 o
4 7 8 10881.40 10731.17 89.77 o
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6 7 8 117.61 159.76 18.84 o
7 7 8 200.24 298.48 35.30 o
-8 8 8 6560.69 6935.10 213.80 o
-7 8 8 322.98 374.72 29.93 o
-6 8 8 2104.56 2416.02 66.50 o
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-4 8 8 13893.35 13711.89 218.12 o
-3 8 8 236.56 335.69 22.05 o
-2 8 8 1368.31 1457.93 32.65 o
-1 8 8 2106.86 2220.88 59.20 o
0 8 8 6379.98 6373.63 93.17 o
1 8 8 2259.44 2386.17 51.71 o
2 8 8 1239.28 1292.70 32.10 o
3 8 8 220.36 257.17 20.63 o
4 8 8 14324.74 13750.33 141.63 o
5 8 8 3125.57 3073.19 57.91 o
6 8 8 1488.63 1582.15 38.37 o
7 8 8 468.73 466.51 29.37 o
8 8 8 6436.90 5841.76 169.36 o
1 0 9 22567.35 22430.86 151.78 o
2 0 9 96.26 167.23 13.14 o
3 0 9 3043.45 3163.16 60.37 o
4 0 9 4556.12 4638.65 45.63 o
5 0 9 31182.93 29844.47 158.94 o
6 0 9 371.49 426.85 19.77 o
7 0 9 2391.62 2436.57 37.26 o
8 0 9 813.85 900.48 30.38 o
-8 1 9 15052.08 14417.39 170.72 o
-7 1 9 2537.21 2564.55 37.44 o
-6 1 9 2915.90 3140.31 79.39 o
-5 1 9 2374.87 2498.46 30.64 o
-4 1 9 22751.01 22327.71 179.48 o
-3 1 9 3736.83 3916.78 33.82 o
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0 1 9 5146.99 5060.90 72.93 o
1 1 9 9604.67 9549.46 83.67 o
2 1 9 9889.77 9787.28 79.64 o
3 1 9 3002.44 3136.33 62.31 o
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