#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/46/2014623.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2014623_Fobs loop_ _publ_author_name 'Dale, Sophie H.' 'Elsegood, Mark R. J.' 'Holmes, Kathryn E.' 'Kelly, Paul F.' _publ_section_title ; The effect of hydrogen-bonding anions on the structure of metal--sulfimide complexes ; _journal_issue 1 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first m34 _journal_page_last m39 _journal_volume 61 _journal_year 2005 _space_group_IT_number 205 _symmetry_space_group_name_Hall '-P 2ac 2ab 3' _symmetry_space_group_name_H-M 'P a -3' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 18.8566 _cell_length_b 18.8566 _cell_length_c 18.8566 _exptl_crystal_F_000 2852.00 _reflns_d_resolution_high 0.7698 _[local]_cod_data_source_file bm1594IIsup3.hkl _[local]_cod_data_source_block II #BEGIN Tags that were not found in dictionaries: _shelx_title ' keh01 in Pa-3' _shelx_refln_list_code 4 _shelx_f_calc_maximum 430.89 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' 'z, x, y' 'z+1/2, -x+1/2, -y' '-z+1/2, -x, y+1/2' '-z, x+1/2, -y+1/2' 'y, z, x' '-y, z+1/2, -x+1/2' 'y+1/2, -z+1/2, -x' '-y+1/2, -z, x+1/2' '-x, -y, -z' 'x-1/2, y, -z-1/2' 'x, -y-1/2, z-1/2' '-x-1/2, y-1/2, z' '-z, -x, -y' '-z-1/2, x-1/2, y' 'z-1/2, x, -y-1/2' 'z, -x-1/2, y-1/2' '-y, -z, -x' 'y, -z-1/2, x-1/2' '-y-1/2, z-1/2, x' 'y-1/2, z, -x-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 0 2 2 10965.01 10604.44 152.30 o 1 2 2 2159.18 2011.79 48.22 o 2 2 2 10307.99 9905.00 187.83 o 1 1 3 10.60 329.32 131.72 o 2 1 3 431.51 525.34 117.21 o 0 2 3 41266.54 37311.48 576.85 o 1 2 3 7005.66 6278.40 77.81 o 2 2 3 43712.32 43359.22 476.60 o 1 3 3 17818.25 16932.28 175.39 o 2 3 3 111.80 398.51 67.27 o 3 3 3 772.71 933.95 83.37 o 0 0 4 96025.34 96552.38 2545.54 o 1 0 4 46181.63 42549.80 664.78 o 2 0 4 168585.70 180980.19 2933.00 o 3 0 4 13108.83 11950.92 169.89 o 1 1 4 7012.54 6744.57 86.06 o 2 1 4 42315.39 42406.97 478.99 o 3 1 4 3228.72 3585.86 43.15 o 0 2 4 27.45 86.78 126.43 o 1 2 4 54.27 142.25 73.26 o 2 2 4 3014.80 2689.01 42.28 o 3 2 4 1036.21 1244.61 48.12 o 1 3 4 14369.67 14610.13 154.05 o 2 3 4 123.29 144.84 58.81 o 3 3 4 3518.28 3140.92 42.81 o 0 4 4 185664.61 190015.59 3168.70 o 1 4 4 504.75 596.73 58.47 o 2 4 4 37490.00 33104.18 354.42 o 3 4 4 10456.86 10556.60 119.50 o 4 4 4 2024.36 2467.04 76.26 o 1 1 5 62712.33 59731.33 681.80 o 2 1 5 4224.86 4324.78 45.11 o 3 1 5 15485.59 15040.30 163.94 o 4 1 5 1646.44 1797.97 42.65 o 0 2 5 17028.94 16648.70 284.47 o 1 2 5 20594.25 19481.00 219.01 o 2 2 5 2403.20 2622.17 42.77 o 3 2 5 2633.34 2230.81 43.21 o 4 2 5 19209.14 19581.60 207.35 o 1 3 5 36245.34 35928.15 416.53 o 2 3 5 2821.57 2679.23 43.07 o 3 3 5 2325.33 2253.81 41.72 o 4 3 5 7057.24 6653.45 84.52 o 0 4 5 4474.28 4531.56 69.35 o 1 4 5 6991.82 7154.14 81.38 o 2 4 5 5580.10 5319.43 57.51 o 3 4 5 0.16 55.55 60.53 o 4 4 5 257.38 433.21 47.30 o 1 5 5 39898.47 37878.10 390.42 o 2 5 5 13706.50 13345.22 145.38 o 3 5 5 5295.81 5310.38 63.64 o 4 5 5 2702.53 2668.04 44.18 o 5 5 5 19228.23 18557.60 376.59 o 0 0 6 655.81 1129.29 131.56 o 1 0 6 121365.59 124469.58 2008.11 o 2 0 6 6138.51 5378.03 77.95 o 3 0 6 285.52 191.09 79.29 o 4 0 6 100500.32 98651.35 1423.60 o 5 0 6 528.26 450.53 70.21 o 1 1 6 1947.93 1968.18 45.84 o 2 1 6 1874.28 1836.96 43.89 o 3 1 6 407.90 411.88 52.49 o 4 1 6 275.79 304.58 52.48 o 5 1 6 837.17 907.34 47.21 o 0 2 6 8427.68 7359.88 128.67 o 1 2 6 9432.53 9597.22 105.71 o 2 2 6 2063.03 2835.04 43.89 o 3 2 6 13955.52 14166.80 157.36 o 4 2 6 21687.45 19371.94 198.08 o 5 2 6 2588.13 2577.98 42.59 o 1 3 6 68.36 145.85 61.92 o 2 3 6 5066.87 5209.35 52.60 o 3 3 6 708.01 1095.42 46.47 o 4 3 6 19597.33 20264.11 207.18 o 5 3 6 2684.73 2746.46 43.21 o 0 4 6 11953.38 9672.73 146.54 o 1 4 6 872.71 1015.05 47.32 o 2 4 6 28871.24 25365.01 274.26 o 3 4 6 6932.04 7100.27 80.41 o 4 4 6 10092.12 9756.07 113.62 o 5 4 6 2241.09 2151.33 46.45 o 1 5 6 0.60 0.00 57.38 o 2 5 6 63.84 87.69 53.69 o 3 5 6 1073.74 1193.79 45.78 o 4 5 6 1358.85 1690.54 43.33 o 5 5 6 10.21 -45.80 54.92 o 0 6 6 48162.20 43989.45 698.05 o 1 6 6 39.52 83.46 56.03 o 2 6 6 22855.79 20286.16 197.35 o 3 6 6 1520.57 1748.32 43.29 o 4 6 6 561.30 880.89 47.40 o 5 6 6 311.87 210.79 48.12 o 6 6 6 5445.09 5934.95 124.81 o 1 1 7 9380.44 9020.29 102.61 o 2 1 7 1796.06 1979.96 43.84 o 3 1 7 30.74 71.53 55.91 o 4 1 7 992.55 1202.10 44.43 o 5 1 7 3265.82 3467.29 43.12 o 6 1 7 22.54 109.59 53.72 o 0 2 7 9507.14 9677.60 183.84 o 1 2 7 3275.04 3249.78 48.46 o 2 2 7 1689.63 1969.28 43.29 o 3 2 7 58386.83 60140.81 644.57 o 4 2 7 6361.65 6974.15 81.75 o 5 2 7 328.01 384.68 46.42 o 6 2 7 1589.26 1182.89 43.73 o 1 3 7 6342.71 7138.01 81.56 o 2 3 7 3124.98 3073.21 42.76 o 3 3 7 2242.27 2410.96 42.79 o 4 3 7 67.19 168.67 52.66 o 5 3 7 1273.08 1351.01 45.51 o 6 3 7 356.72 371.06 51.36 o 0 4 7 885.45 1148.16 70.45 o 1 4 7 18.60 29.25 62.04 o 2 4 7 358.81 367.98 52.53 o 3 4 7 2232.65 2191.98 41.17 o 4 4 7 11297.88 10948.54 117.46 o 5 4 7 733.86 794.33 46.89 o 6 4 7 63.93 131.64 48.06 o 1 5 7 2731.65 3108.62 47.69 o 2 5 7 75.33 -11.53 54.90 o 3 5 7 4949.34 5104.06 60.12 o 4 5 7 1592.29 1807.50 43.97 o 5 5 7 5514.67 5948.71 75.56 o 6 5 7 373.55 278.56 44.53 o 0 6 7 318.30 486.35 73.07 o 1 6 7 586.13 495.61 47.24 o 2 6 7 749.23 879.69 45.65 o 3 6 7 900.17 792.77 45.79 o 4 6 7 1032.96 1424.19 43.69 o 5 6 7 3371.45 3186.67 49.40 o 6 6 7 117.33 181.02 46.57 o 1 7 7 10833.58 11863.18 133.67 o 2 7 7 7166.85 7424.55 88.28 o 3 7 7 897.91 938.74 45.11 o 4 7 7 938.64 1078.75 47.06 o 5 7 7 3183.51 3168.23 51.74 o 6 7 7 7347.58 7182.43 101.71 o 7 7 7 3786.23 3568.74 110.61 o 0 0 8 33630.98 27719.13 644.89 o 1 0 8 1164.69 1335.87 65.85 o 2 0 8 1091.49 525.53 72.88 o 3 0 8 1971.95 2013.00 67.61 o 4 0 8 2649.86 2302.36 60.37 o 5 0 8 29336.34 31697.78 510.48 o 6 0 8 1029.87 782.08 70.26 o 7 0 8 5665.52 5559.39 100.70 o 1 1 8 11155.28 11595.74 136.38 o 2 1 8 14021.19 14356.25 168.56 o 3 1 8 1810.07 2210.40 43.28 o 4 1 8 1744.69 1690.97 43.14 o 5 1 8 234.92 234.56 49.59 o 6 1 8 4298.15 4316.10 55.00 o 7 1 8 532.74 483.66 47.24 o 0 2 8 10800.97 9179.62 165.90 o 1 2 8 168.98 179.97 60.38 o 2 2 8 4361.68 3502.55 46.82 o 3 2 8 450.77 463.68 51.65 o 4 2 8 454.06 932.65 45.10 o 5 2 8 1665.26 1811.33 41.86 o 6 2 8 12260.93 11570.72 133.65 o 7 2 8 630.04 861.62 44.67 o 1 3 8 175.72 240.28 54.76 o 2 3 8 27109.03 28808.43 313.41 o 3 3 8 1125.95 1206.70 52.19 o 4 3 8 2367.30 2643.57 43.27 o 5 3 8 66.90 105.13 47.98 o 6 3 8 6562.80 6663.29 84.47 o 7 3 8 2281.59 2453.45 45.69 o 0 4 8 5948.72 7368.75 115.96 o 1 4 8 1464.11 1469.84 44.56 o 2 4 8 12751.19 12288.12 138.49 o 3 4 8 4.51 47.39 53.22 o 4 4 8 55733.26 55288.24 589.64 o 5 4 8 227.41 203.96 47.24 o 6 4 8 13904.70 13528.50 166.02 o 7 4 8 289.21 320.43 50.42 o 1 5 8 710.37 684.96 49.54 o 2 5 8 2130.54 2218.94 42.76 o 3 5 8 856.80 930.14 47.83 o 4 5 8 654.37 737.53 47.80 o 5 5 8 687.76 578.86 47.27 o 6 5 8 6122.35 6411.04 85.01 o 7 5 8 461.58 441.51 45.16 o 0 6 8 9469.67 9454.74 168.21 o 1 6 8 8218.10 8672.99 97.67 o 2 6 8 7766.96 7165.18 89.15 o 3 6 8 434.60 341.07 50.60 o 4 6 8 5169.42 4291.28 54.89 o 5 6 8 4585.39 4942.85 69.05 o 6 6 8 19250.15 19612.23 238.82 o 7 6 8 5005.45 5301.86 88.76 o 1 7 8 329.26 422.17 51.39 o 2 7 8 2900.20 2592.90 55.79 o 3 7 8 1713.29 1733.64 42.72 o 4 7 8 510.35 477.56 46.31 o 5 7 8 8.38 66.91 48.61 o 6 7 8 2823.42 2838.89 51.99 o 7 7 8 11.24 31.96 45.81 o 0 8 8 5856.55 4681.00 96.07 o 1 8 8 373.24 365.09 47.28 o 2 8 8 13262.70 12996.21 153.76 o 3 8 8 734.04 808.56 45.28 o 4 8 8 1268.23 1188.08 46.13 o 5 8 8 843.57 840.42 45.87 o 6 8 8 4807.06 4834.14 78.91 o 7 8 8 90.68 70.73 45.65 o 8 8 8 6800.53 7223.25 215.83 o 1 1 9 37456.11 39318.46 444.96 o 2 1 9 8933.15 8696.20 108.88 o 3 1 9 1048.35 938.47 45.11 o 4 1 9 1103.90 1382.07 44.47 o 5 1 9 685.89 409.28 50.59 o 6 1 9 7326.46 7577.17 92.55 o 7 1 9 799.68 820.57 47.09 o 8 1 9 1216.64 1204.82 42.69 o 0 2 9 20302.72 21319.66 358.10 o 1 2 9 6.04 12.05 56.13 o 2 2 9 2932.22 2978.66 48.05 o 3 2 9 3168.03 3243.97 46.28 o 4 2 9 261.55 481.68 47.95 o 5 2 9 10856.65 11824.12 135.68 o 6 2 9 152.26 181.77 50.37 o 7 2 9 12319.97 13307.90 164.21 o 8 2 9 1374.40 1358.86 42.14 o 1 3 9 1777.04 1724.37 45.78 o 2 3 9 16841.71 16979.75 187.93 o 3 3 9 6799.63 7150.34 75.77 o 4 3 9 1569.74 1530.32 43.89 o 5 3 9 8809.39 9079.49 101.05 o 6 3 9 10781.45 11673.73 140.47 o 7 3 9 213.56 204.36 50.08 o 8 3 9 1455.76 1525.10 42.73 o 0 4 9 958.45 943.84 68.05 o 1 4 9 453.24 443.25 48.91 o 2 4 9 22.76 11.44 54.84 o 3 4 9 745.02 870.59 47.80 o 4 4 9 3705.03 3814.88 50.76 o 5 4 9 2152.66 2425.33 42.64 o 6 4 9 418.96 577.80 45.77 o 7 4 9 185.93 198.45 47.85 o 8 4 9 38.38 16.96 47.22 o 1 5 9 19824.30 19433.09 229.74 o 2 5 9 12177.72 12180.58 147.33 o 3 5 9 6213.77 6569.01 78.10 o 4 5 9 25.94 -37.54 50.13 o 5 5 9 32416.08 32947.98 379.44 o 6 5 9 6257.72 6609.77 95.88 o 7 5 9 2725.45 2460.42 47.10 o 8 5 9 44.43 155.66 47.07 o 0 6 9 922.67 854.89 63.87 o 1 6 9 1432.54 1517.87 44.88 o 2 6 9 1860.39 1929.13 46.98 o 3 6 9 8709.70 9309.34 113.84 o 4 6 9 288.67 343.85 47.68 o 5 6 9 1397.16 1275.77 46.36 o 6 6 9 26.65 54.23 45.12 o 7 6 9 1290.26 1382.47 49.28 o 8 6 9 302.31 279.66 46.56 o 1 7 9 4025.06 4309.51 55.44 o 2 7 9 2249.73 2261.69 46.21 o 3 7 9 3742.46 3710.33 54.67 o 4 7 9 340.70 374.65 45.78 o 5 7 9 1699.07 1608.65 51.46 o 6 7 9 1066.27 1086.43 46.33 o 7 7 9 2387.66 2137.99 50.91 o 8 7 9 844.34 843.34 47.09 o 0 8 9 1886.49 1726.27 61.15 o 1 8 9 13.60 -9.40 49.73 o 2 8 9 272.11 202.34 51.64 o 3 8 9 540.42 477.99 45.12 o 4 8 9 0.18 18.20 48.82 o 5 8 9 7.78 13.27 48.46 o 6 8 9 303.68 318.53 47.84 o 7 8 9 1389.02 1413.78 45.84 o 8 8 9 810.72 788.97 46.17 o 1 9 9 7851.21 8177.00 103.83 o 2 9 9 5233.58 5246.01 82.02 o 3 9 9 2914.69 2884.16 47.59 o 4 9 9 571.15 476.89 48.92 o 5 9 9 1200.27 1168.11 44.35 o 6 9 9 7201.78 7612.22 127.82 o 7 9 9 31.02 23.88 45.83 o 8 9 9 1502.12 1507.02 51.51 o 9 9 9 3042.28 2914.06 119.52 o 0 0 10 100809.54 106119.71 2380.66 o 1 0 10 34200.44 36312.98 554.19 o 2 0 10 44452.82 44994.07 702.20 o 3 0 10 252.00 150.02 70.16 o 4 0 10 2789.62 3674.26 74.24 o 5 0 10 3071.86 3127.38 66.52 o 6 0 10 205.17 142.30 75.65 o 7 0 10 621.64 526.12 63.75 o 8 0 10 9312.95 9746.90 174.64 o 9 0 10 3684.10 3740.40 92.79 o 1 1 10 954.18 943.12 45.82 o 2 1 10 1773.85 1655.84 48.50 o 3 1 10 532.18 389.51 50.59 o 4 1 10 1731.75 1946.55 45.90 o 5 1 10 323.51 309.23 49.59 o 6 1 10 1783.70 1960.21 42.11 o 7 1 10 3446.37 3405.43 49.35 o 8 1 10 241.60 217.91 48.86 o 9 1 10 1337.68 1415.68 42.94 o 0 2 10 11341.05 9697.09 164.81 o 1 2 10 1579.55 1711.53 44.57 o 2 2 10 21486.81 21073.41 243.48 o 3 2 10 29.16 67.31 54.67 o 4 2 10 8.01 9.74 50.62 o 5 2 10 1564.25 1581.06 41.94 o 6 2 10 12287.01 12405.65 164.56 o 7 2 10 1263.25 1260.74 42.15 o 8 2 10 7435.94 7095.56 104.84 o 9 2 10 2462.38 2369.85 45.78 o 1 3 10 15244.85 16084.01 186.83 o 2 3 10 9966.73 10901.42 128.56 o 3 3 10 804.92 765.89 44.99 o 4 3 10 2382.23 2371.85 44.51 o 5 3 10 151.81 121.97 49.67 o 6 3 10 101.31 80.90 48.77 o 7 3 10 2562.18 2461.67 42.87 o 8 3 10 1681.61 1651.07 42.55 o 9 3 10 2987.89 2990.80 54.67 o 0 4 10 3969.88 4727.69 85.38 o 1 4 10 10846.60 11042.69 140.42 o 2 4 10 4025.86 3745.71 51.52 o 3 4 10 5605.28 5248.51 83.12 o 4 4 10 30282.06 29210.34 343.31 o 5 4 10 20.77 49.24 46.48 o 6 4 10 34139.22 34732.57 460.90 o 7 4 10 3104.10 2793.89 53.16 o 8 4 10 7452.48 7802.11 116.45 o 9 4 10 163.23 124.25 48.76 o 1 5 10 2066.61 1863.61 43.73 o 2 5 10 11031.29 12133.35 141.90 o 3 5 10 1336.57 1200.73 43.88 o 4 5 10 14.69 36.26 48.81 o 5 5 10 84.99 131.54 48.03 o 6 5 10 482.76 362.45 47.07 o 7 5 10 1425.77 1348.21 45.81 o 8 5 10 2127.30 2135.07 49.40 o 9 5 10 11.92 -37.57 47.05 o 0 6 10 353.91 495.27 63.85 o 1 6 10 3744.37 4067.72 54.36 o 2 6 10 3555.11 3458.22 51.95 o 3 6 10 42.43 97.65 51.50 o 4 6 10 29448.50 30693.09 385.18 o 5 6 10 0.02 44.82 47.14 o 6 6 10 20450.11 20916.25 280.19 o 7 6 10 779.07 722.20 46.35 o 8 6 10 2405.96 2412.92 50.29 o 9 6 10 146.21 167.80 48.41 o 1 7 10 2727.36 2794.55 46.36 o 2 7 10 7258.70 7388.23 106.55 o 3 7 10 823.52 705.06 45.09 o 4 7 10 1169.51 1174.39 44.25 o 5 7 10 3831.70 3614.54 57.47 o 6 7 10 16.04 -12.89 47.84 o 7 7 10 1640.24 1593.60 46.55 o 8 7 10 3932.22 4071.51 94.83 o 9 7 10 683.27 643.89 49.54 o 0 8 10 18869.37 19536.32 371.55 o 1 8 10 3605.94 3620.58 55.76 o 2 8 10 5532.62 5573.15 82.27 o 3 8 10 10554.10 11099.49 160.22 o 4 8 10 176.58 116.58 47.84 o 5 8 10 9073.25 9723.10 164.10 o 6 8 10 220.15 178.32 47.21 o 7 8 10 5725.94 5524.36 116.08 o 8 8 10 1819.55 1857.05 50.22 o 9 8 10 6.24 24.66 46.50 o 1 9 10 8130.76 8748.17 132.49 o 2 9 10 2717.21 2821.38 48.15 o 3 9 10 44.30 39.20 48.40 o 4 9 10 5.36 37.13 47.81 o 5 9 10 8951.80 9084.54 165.65 o 6 9 10 5058.82 5367.49 102.56 o 7 9 10 176.02 242.20 47.65 o 8 9 10 997.22 1018.04 48.48 o 9 9 10 993.88 1034.56 54.58 o 0 10 10 36598.76 38999.13 793.75 o 1 10 10 1064.01 1037.87 42.49 o 2 10 10 5022.63 4890.06 87.78 o 3 10 10 3022.23 3180.82 55.49 o 4 10 10 474.24 431.75 46.25 o 5 10 10 6.60 23.79 45.73 o 6 10 10 461.59 313.71 48.37 o 7 10 10 4579.40 4559.78 115.54 o 8 10 10 2411.29 2682.85 79.72 o 9 10 10 1062.29 900.74 54.43 o 10 10 10 5852.92 6205.45 291.76 o 1 1 11 2791.56 2625.50 57.97 o 2 1 11 54.27 51.22 50.50 o 3 1 11 65.19 126.32 52.63 o 4 1 11 80.43 133.89 50.41 o 5 1 11 103.93 197.78 49.68 o 6 1 11 204.18 195.09 50.64 o 7 1 11 6.02 62.20 50.49 o 8 1 11 957.04 916.99 45.44 o 9 1 11 9170.00 9113.94 147.20 o 10 1 11 202.76 207.10 45.74 o 0 2 11 22491.78 23805.84 387.39 o 1 2 11 615.09 564.61 46.56 o 2 2 11 1818.35 1879.22 45.84 o 3 2 11 3919.51 3622.73 57.15 o 4 2 11 7422.69 7653.99 102.04 o 5 2 11 2823.10 2715.52 59.85 o 6 2 11 6572.49 6716.69 94.18 o 7 2 11 10068.20 10466.31 157.48 o 8 2 11 156.45 122.96 48.53 o 9 2 11 238.47 125.31 47.85 o 10 2 11 4499.90 4501.10 85.31 o 1 3 11 5799.18 6323.11 89.85 o 2 3 11 3555.48 3441.65 59.96 o 3 3 11 5879.96 6458.87 95.14 o 4 3 11 223.76 162.00 47.25 o 5 3 11 26.18 23.79 45.77 o 6 3 11 415.97 383.08 47.44 o 7 3 11 1308.30 1307.15 43.32 o 8 3 11 1154.17 1184.98 44.43 o 9 3 11 181.43 135.86 47.30 o 10 3 11 113.73 75.66 47.34 o 0 4 11 689.28 572.06 63.45 o 1 4 11 9.78 68.47 50.73 o 2 4 11 9781.25 10488.15 128.42 o 3 4 11 8743.74 9093.03 110.70 o 4 4 11 639.57 611.47 46.18 o 5 4 11 3135.82 3396.22 51.36 o 6 4 11 1745.03 1711.90 42.69 o 7 4 11 153.61 90.37 46.47 o 8 4 11 30.95 39.83 45.76 o 9 4 11 180.95 194.24 47.79 o 10 4 11 232.84 193.38 45.12 o 1 5 11 3276.34 3161.94 50.13 o 2 5 11 1570.66 1480.09 43.93 o 3 5 11 1548.28 1724.44 55.81 o 4 5 11 3243.60 3238.14 52.03 o 5 5 11 10923.99 11258.07 165.63 o 6 5 11 35.97 57.37 46.50 o 7 5 11 4298.61 4197.77 68.13 o 8 5 11 79.67 85.08 46.33 o 9 5 11 939.62 970.87 48.38 o 10 5 11 16.30 4.03 46.65 o 0 6 11 233.60 319.74 70.34 o 1 6 11 3802.60 3749.99 54.45 o 2 6 11 904.10 836.09 47.13 o 3 6 11 5986.82 6135.97 92.48 o 4 6 11 366.50 361.77 50.18 o 5 6 11 13.34 41.13 46.53 o 6 6 11 3813.39 3807.66 64.84 o 7 6 11 7209.73 7513.57 117.59 o 8 6 11 2977.03 2944.99 59.06 o 9 6 11 127.79 65.81 46.49 o 10 6 11 10.38 72.89 46.31 o 1 7 11 142.34 125.16 48.24 o 2 7 11 3157.68 3123.96 51.28 o 3 7 11 5034.18 5338.14 84.87 o 4 7 11 28.92 9.43 50.40 o 5 7 11 4843.64 4849.01 80.54 o 6 7 11 2124.15 1989.51 48.35 o 7 7 11 162.74 100.50 45.13 o 8 7 11 738.40 659.05 47.27 o 9 7 11 340.63 401.47 47.62 o 10 7 11 760.80 763.27 50.21 o 0 8 11 11955.20 12471.66 252.79 o 1 8 11 873.27 787.45 43.53 o 2 8 11 1306.95 1018.69 41.58 o 3 8 11 3892.97 3819.80 77.48 o 4 8 11 6740.54 6994.36 114.48 o 5 8 11 42.83 40.20 48.65 o 6 8 11 15237.40 16013.01 302.63 o 7 8 11 81.81 76.54 47.28 o 8 8 11 1254.15 1225.52 55.83 o 9 8 11 191.17 313.41 50.86 o 10 8 11 2393.17 2405.02 79.67 o 1 9 11 8047.05 8246.20 138.89 o 2 9 11 13579.35 14408.13 235.56 o 3 9 11 1165.33 1117.62 45.43 o 4 9 11 399.85 423.08 47.13 o 5 9 11 1046.24 1033.58 47.83 o 6 9 11 3843.49 3738.27 85.55 o 7 9 11 1061.37 1073.30 52.62 o 8 9 11 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0 8 13 813.19 690.10 67.84 o 1 8 13 506.98 616.83 44.59 o 2 8 13 314.33 171.54 44.89 o 3 8 13 112.27 118.19 48.81 o 4 8 13 24.91 -39.58 47.06 o 5 8 13 6888.20 7203.48 145.78 o 6 8 13 22.37 -17.89 48.63 o 7 8 13 2648.42 2542.82 74.13 o 8 8 13 461.31 362.25 52.94 o 9 8 13 71.87 87.80 53.99 o 10 8 13 1477.34 1400.53 66.60 o 11 8 13 1891.48 1886.18 90.89 o 12 8 13 1074.82 1075.46 72.23 o 1 9 13 1127.92 1182.64 44.76 o 2 9 13 2578.54 2377.46 66.78 o 3 9 13 199.79 186.25 47.21 o 4 9 13 1094.52 957.36 53.76 o 5 9 13 637.17 607.20 70.59 o 6 9 13 3684.05 3544.77 91.41 o 7 9 13 2634.31 2526.36 82.48 o 8 9 13 18.64 66.97 49.91 o 9 9 13 4250.82 3989.95 133.54 o 10 9 13 1968.60 1838.79 89.17 o 11 9 13 743.67 760.45 71.46 o 12 9 13 761.85 720.30 73.98 o 0 10 13 364.46 368.96 67.34 o 1 10 13 297.33 266.58 45.19 o 2 10 13 867.14 843.75 47.84 o 3 10 13 816.29 759.39 52.26 o 4 10 13 32.42 57.11 49.29 o 5 10 13 98.64 119.38 48.24 o 6 10 13 145.41 96.53 65.73 o 7 10 13 682.13 681.64 89.11 o 8 10 13 16.04 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57.43 o 5 13 13 4323.52 4248.24 150.24 o 6 13 13 978.08 983.00 66.43 o 7 13 13 114.84 93.37 57.29 o 8 13 13 1047.93 1006.06 79.06 o 9 13 13 51.86 37.90 76.44 o 10 13 13 2.48 -8.85 77.34 o 11 13 13 6.09 -90.15 90.15 o 12 13 13 105.22 172.13 100.95 o 13 13 13 507.61 584.20 343.99 o 0 0 14 225.50 296.64 93.15 o 1 0 14 11565.79 11710.38 250.69 o 2 0 14 6103.20 6328.62 147.90 o 3 0 14 4860.65 4806.07 119.53 o 4 0 14 12269.74 12153.87 293.91 o 5 0 14 139.13 52.76 72.64 o 6 0 14 13637.67 13959.13 361.38 o 7 0 14 2052.68 1681.97 69.10 o 8 0 14 3405.17 3141.35 95.71 o 9 0 14 15.54 49.82 61.61 o 10 0 14 16.15 87.61 66.29 o 11 0 14 97.31 142.16 72.23 o 12 0 14 383.31 452.55 73.91 o 13 0 14 14.74 69.84 73.44 o 1 1 14 500.23 436.32 44.38 o 2 1 14 153.83 131.67 45.13 o 3 1 14 1278.35 1335.92 45.82 o 4 1 14 460.15 430.54 45.81 o 5 1 14 1253.76 1165.56 46.66 o 6 1 14 39.30 56.06 47.83 o 7 1 14 798.80 774.91 42.68 o 8 1 14 848.68 959.69 53.34 o 9 1 14 170.85 217.46 46.36 o 10 1 14 370.05 326.72 43.80 o 11 1 14 1377.43 1420.09 51.21 o 12 1 14 546.66 562.58 49.64 o 13 1 14 230.05 168.01 56.85 o 0 2 14 643.05 566.42 63.49 o 1 2 14 962.99 1100.56 46.02 o 2 2 14 6135.37 6324.00 102.75 o 3 2 14 564.23 430.12 45.12 o 4 2 14 16103.53 17097.48 297.79 o 5 2 14 363.60 345.51 45.69 o 6 2 14 5464.36 5624.88 101.50 o 7 2 14 791.92 675.52 44.17 o 8 2 14 780.88 652.29 43.73 o 9 2 14 190.19 159.05 47.21 o 10 2 14 719.58 814.41 46.87 o 11 2 14 20.51 29.44 44.95 o 12 2 14 1508.42 1587.26 61.42 o 13 2 14 265.94 311.80 52.71 o 1 3 14 540.50 506.64 44.27 o 2 3 14 1866.82 1897.32 46.22 o 3 3 14 0.02 49.33 46.51 o 4 3 14 447.41 384.35 47.04 o 5 3 14 457.61 499.06 45.64 o 6 3 14 1.14 47.84 45.80 o 7 3 14 784.20 745.97 74.46 o 8 3 14 167.37 112.78 47.44 o 9 3 14 24.78 32.99 49.56 o 10 3 14 2812.40 2971.79 81.67 o 11 3 14 1848.73 1671.01 64.52 o 12 3 14 460.65 431.19 56.73 o 13 3 14 466.09 435.51 53.32 o 0 4 14 17069.78 18101.27 380.14 o 1 4 14 7425.70 7250.16 117.55 o 2 4 14 13854.02 14350.65 237.07 o 3 4 14 12638.39 13018.03 217.93 o 4 4 14 499.10 519.08 47.21 o 5 4 14 1000.35 1075.41 43.84 o 6 4 14 374.61 399.00 45.56 o 7 4 14 5152.60 5595.59 102.37 o 8 4 14 4847.89 5089.85 106.50 o 9 4 14 37.32 55.24 48.04 o 10 4 14 2748.30 2781.66 88.64 o 11 4 14 1667.70 1598.46 60.96 o 12 4 14 6977.94 7381.80 205.80 o 13 4 14 507.09 454.88 67.13 o 1 5 14 0.09 45.97 47.51 o 2 5 14 4546.13 4450.35 95.09 o 3 5 14 929.90 944.83 45.55 o 4 5 14 108.98 35.64 48.60 o 5 5 14 88.50 80.08 44.94 o 6 5 14 613.76 630.92 44.29 o 7 5 14 208.80 243.37 45.41 o 8 5 14 72.99 -17.28 50.18 o 9 5 14 7.33 96.06 47.45 o 10 5 14 0.81 -31.33 50.95 o 11 5 14 2183.26 2242.93 77.11 o 12 5 14 6.14 127.38 59.16 o 13 5 14 1203.52 1092.16 60.25 o 0 6 14 7202.05 7452.08 196.84 o 1 6 14 843.01 719.99 46.28 o 2 6 14 12514.36 13382.48 250.21 o 3 6 14 1128.71 1080.99 48.93 o 4 6 14 214.75 142.59 44.38 o 5 6 14 2970.58 3067.49 66.03 o 6 6 14 1217.24 1048.59 45.43 o 7 6 14 290.45 222.26 51.18 o 8 6 14 3814.04 4112.60 92.34 o 9 6 14 250.61 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16 3434.88 3546.74 181.65 o 1 0 16 32.58 86.22 89.50 o 2 0 16 2037.69 1859.96 75.43 o 3 0 16 1895.15 1951.80 81.23 o 4 0 16 44.52 87.67 67.20 o 5 0 16 4.23 37.58 70.30 o 6 0 16 4332.36 4493.17 158.42 o 7 0 16 97.30 180.80 65.66 o 8 0 16 3825.93 4072.05 146.60 o 9 0 16 10.69 59.34 69.67 o 10 0 16 11.80 43.82 69.09 o 11 0 16 1.07 65.82 81.08 o 12 0 16 30.50 38.91 73.54 o 13 0 16 554.84 644.70 83.05 o 14 0 16 1012.51 935.75 103.31 o 15 0 16 862.57 1087.78 139.61 o 1 1 16 2964.91 3023.25 68.95 o 2 1 16 716.04 784.04 46.53 o 3 1 16 377.54 352.25 45.50 o 4 1 16 36.79 15.63 47.71 o 5 1 16 426.16 465.56 49.01 o 6 1 16 1523.89 1365.42 49.99 o 7 1 16 1161.98 1207.87 49.30 o 8 1 16 181.62 207.82 57.28 o 9 1 16 760.81 716.79 90.33 o 10 1 16 1749.42 1724.89 67.47 o 11 1 16 2073.32 2047.78 74.53 o 12 1 16 442.74 425.11 53.30 o 13 1 16 1411.90 1321.10 65.50 o 14 1 16 465.05 627.18 75.32 o 15 1 16 871.12 776.11 89.57 o 0 2 16 1526.48 1393.96 64.28 o 1 2 16 5394.81 5390.68 103.34 o 2 2 16 3872.30 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73.51 o 5 4 16 125.28 130.59 49.48 o 6 4 16 4.73 0.13 47.30 o 7 4 16 44.72 79.57 51.04 o 8 4 16 1576.65 1582.11 60.84 o 9 4 16 2734.38 2756.44 99.27 o 10 4 16 5564.02 5989.33 197.79 o 11 4 16 86.17 144.78 55.07 o 12 4 16 5425.39 5694.72 215.12 o 13 4 16 670.39 694.93 68.05 o 14 4 16 810.30 849.73 100.96 o 15 4 16 1385.19 1363.61 134.88 o 1 5 16 53.84 7.57 44.77 o 2 5 16 1404.05 1278.42 47.11 o 3 5 16 759.20 865.54 48.03 o 4 5 16 39.10 78.71 47.76 o 5 5 16 386.28 373.63 45.41 o 6 5 16 1281.90 1294.56 48.44 o 7 5 16 293.87 258.36 49.66 o 8 5 16 1686.85 1602.49 64.17 o 9 5 16 95.25 220.69 57.52 o 10 5 16 103.69 74.10 58.21 o 11 5 16 146.34 81.70 57.68 o 12 5 16 152.37 156.32 71.72 o 13 5 16 121.12 237.81 73.26 o 14 5 16 53.27 167.12 78.09 o 15 5 16 21.78 -96.17 99.00 o 0 6 16 12935.30 14356.20 432.50 o 1 6 16 24.26 96.65 45.24 o 2 6 16 7194.44 8243.60 181.49 o 3 6 16 59.81 -7.51 44.69 o 4 6 16 699.37 761.20 49.02 o 5 6 16 18.58 127.59 47.53 o 6 6 16 11.18 9.26 46.02 o 7 6 16 733.14 594.69 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1174.16 81.07 o 10 8 16 5.45 38.72 67.90 o 11 8 16 0.48 -36.19 74.86 o 12 8 16 764.22 808.66 98.24 o 13 8 16 673.70 900.11 119.19 o 14 8 16 2339.33 2644.34 193.00 o 15 8 16 11.27 26.28 106.92 o 1 9 16 1784.60 1715.87 74.15 o 2 9 16 837.54 848.69 52.10 o 3 9 16 85.06 65.66 52.38 o 4 9 16 356.86 320.83 59.14 o 5 9 16 2951.40 2875.93 92.25 o 6 9 16 2.46 160.19 61.79 o 7 9 16 969.07 983.64 65.39 o 8 9 16 1.96 -72.95 72.95 o 9 9 16 762.86 748.31 74.29 o 10 9 16 385.58 457.21 78.99 o 11 9 16 714.98 590.40 99.73 o 12 9 16 4.91 -58.81 93.41 o 13 9 16 1424.05 1488.42 141.34 o 14 9 16 724.55 705.96 121.86 o 15 9 16 4.67 -129.09 129.09 o 0 10 16 98.08 73.42 78.24 o 1 10 16 758.27 672.14 61.30 o 2 10 16 1170.64 1125.99 53.28 o 3 10 16 8.24 30.95 57.85 o 4 10 16 5376.21 6073.89 193.11 o 5 10 16 270.27 197.50 62.65 o 6 10 16 1094.18 1119.50 66.38 o 7 10 16 569.18 474.99 63.40 o 8 10 16 519.52 654.01 85.57 o 9 10 16 2749.53 2781.36 143.21 o 10 10 16 377.41 555.13 87.56 o 11 10 16 87.05 119.74 83.14 o 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