#------------------------------------------------------------------------------ #$Date: 2016-04-02 22:02:04 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180815 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/46/2014690.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2014690_Fobs loop_ _publ_author_name 'Bia\/lo\'nska, Agata' 'Ciunik, Zbigniew' _publ_section_title ; Similar environments for the ClO~4~^{-^}, HSO~4~^{-^} and H~2~PO~4~^{-^} anions offered by strychnine self-assemblies ; _journal_issue 3 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first o161 _journal_page_last o164 _journal_volume 61 _journal_year 2005 _space_group_IT_number 4 _symmetry_space_group_name_Hall 'P 2yb' _symmetry_space_group_name_H-M 'P 1 21 1' _cell_angle_alpha 90.000 _cell_angle_beta 91.203 _cell_angle_gamma 90.000 _cell_length_a 7.6407 _cell_length_b 7.6624 _cell_length_c 17.9922 _exptl_crystal_F_000 496.00 _reflns_d_resolution_high 0.7828 _cod_data_source_file gd1357IIIsup4.hkl _cod_data_source_block III #BEGIN Tags that were not found in dictionaries: _shelx_title ' S4 in P2(1)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 97.13 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 -9 0 256.97 244.11 24.79 o 2 -9 0 58.06 63.08 25.43 o 3 -9 0 16.67 22.46 23.11 o 0 -8 0 2.72 30.97 16.62 o 1 -8 0 61.18 56.17 14.11 o 2 -8 0 355.35 315.32 29.34 o 3 -8 0 124.25 123.24 21.87 o 4 -8 0 2.77 8.20 19.58 o 5 -8 0 47.79 70.21 23.91 o 1 -7 0 132.33 134.48 18.77 o 2 -7 0 84.99 75.50 16.60 o 3 -7 0 10.99 33.14 17.14 o 4 -7 0 17.87 20.76 20.81 o 5 -7 0 130.51 181.16 28.59 o 6 -7 0 22.86 32.75 16.47 o 0 -6 0 538.76 545.29 28.17 o 1 -6 0 73.96 73.67 10.50 o 2 -6 0 911.43 889.08 25.99 o 3 -6 0 57.41 73.47 11.35 o 4 -6 0 20.06 17.82 8.52 o 5 -6 0 21.58 41.62 13.76 o 6 -6 0 134.55 111.93 17.36 o 7 -6 0 45.43 69.71 18.23 o 1 -5 0 443.70 442.26 12.90 o 2 -5 0 430.62 432.59 14.82 o 3 -5 0 8.57 19.40 6.70 o 4 -5 0 30.75 51.53 18.47 o 5 -5 0 293.68 297.77 25.18 o 6 -5 0 31.39 32.20 13.88 o 7 -5 0 1.69 25.64 15.14 o 8 -5 0 62.54 59.58 24.66 o 0 -4 0 1605.66 1579.01 21.34 o 1 -4 0 37.61 47.23 8.50 o 2 -4 0 652.60 670.14 20.79 o 3 -4 0 716.45 737.09 18.26 o 4 -4 0 139.37 132.14 11.28 o 5 -4 0 102.71 112.45 16.07 o 6 -4 0 144.18 130.51 17.88 o 7 -4 0 66.91 71.70 19.07 o 8 -4 0 11.25 24.00 22.71 o 1 -3 0 920.14 961.02 14.65 o 2 -3 0 323.76 320.87 12.13 o 3 -3 0 149.82 173.17 10.63 o 4 -3 0 172.74 181.40 11.48 o 5 -3 0 121.42 136.12 15.14 o 6 -3 0 80.14 47.73 13.21 o 7 -3 0 112.69 122.58 23.07 o 8 -3 0 218.28 274.76 31.88 o 9 -3 0 10.31 6.86 16.78 o 0 -2 0 2613.40 2434.53 26.21 o 1 -2 0 632.16 609.08 17.82 o 2 -2 0 616.50 622.74 12.24 o 3 -2 0 210.25 199.23 10.33 o 4 -2 0 496.71 492.71 17.07 o 5 -2 0 8.88 25.96 9.31 o 6 -2 0 111.13 99.01 18.62 o 7 -2 0 180.02 158.71 21.08 o 8 -2 0 54.73 62.96 22.63 o 9 -2 0 56.73 39.93 22.24 o 1 -1 0 276.30 267.50 8.37 o 2 -1 0 976.81 962.57 15.99 o 3 -1 0 180.87 190.83 21.03 o 4 -1 0 1309.09 1359.49 28.68 o 5 -1 0 51.82 45.60 13.26 o 6 -1 0 16.69 27.52 14.30 o 7 -1 0 208.46 215.03 22.05 o 8 -1 0 37.87 52.27 18.79 o 9 -1 0 28.13 45.00 15.33 o 2 0 0 1263.69 1199.43 20.44 o 3 0 0 706.13 677.32 30.95 o 4 0 0 4.93 17.24 11.92 o 5 0 0 369.75 327.77 18.43 o 6 0 0 15.15 11.37 11.52 o 7 0 0 215.77 196.55 23.91 o 8 0 0 8.36 32.44 17.66 o 9 0 0 15.77 43.17 25.16 o 2 1 0 979.27 873.01 22.79 o 3 1 0 180.38 191.74 19.55 o 4 1 0 1316.90 1386.02 41.20 o 5 1 0 49.25 69.21 16.04 o 6 1 0 16.64 19.80 12.38 o 7 1 0 204.84 199.72 21.24 o 8 1 0 37.96 41.44 17.25 o 9 1 0 27.98 49.17 21.51 o 3 2 0 203.33 191.38 17.62 o 4 2 0 502.76 517.62 26.13 o 5 2 0 8.38 26.06 17.26 o 6 2 0 112.12 96.75 26.32 o 7 2 0 178.26 167.80 24.35 o 8 2 0 55.21 68.18 20.20 o 9 2 0 57.50 37.57 36.20 o 4 3 0 174.51 156.66 20.63 o 5 3 0 124.49 152.18 22.20 o 6 3 0 79.93 89.17 23.18 o 8 3 0 221.77 235.04 40.68 o 9 3 0 10.35 10.17 25.15 o -3 -9 1 14.02 11.48 23.11 o -2 -9 1 150.30 158.96 31.87 o -1 -9 1 54.64 28.90 22.11 o 0 -9 1 15.62 8.71 14.51 o 1 -9 1 78.31 69.14 19.87 o 2 -9 1 8.22 19.00 21.00 o 3 -9 1 38.95 34.56 24.33 o -5 -8 1 59.69 59.40 46.60 o -4 -8 1 19.49 33.51 18.51 o -3 -8 1 118.20 102.65 27.21 o -2 -8 1 118.81 154.69 26.31 o -1 -8 1 55.87 71.48 15.45 o 0 -8 1 85.67 76.93 14.47 o 1 -8 1 19.19 25.69 14.03 o 2 -8 1 11.35 25.80 16.65 o 3 -8 1 53.75 74.75 24.20 o 4 -8 1 91.05 99.19 27.44 o 5 -8 1 16.97 35.05 20.35 o -6 -7 1 12.27 20.88 20.35 o -5 -7 1 14.36 18.75 18.32 o -4 -7 1 18.13 24.27 16.94 o -3 -7 1 126.63 141.18 23.66 o -2 -7 1 219.10 209.89 19.95 o -1 -7 1 148.43 128.59 16.05 o 0 -7 1 12.06 24.41 10.52 o 1 -7 1 27.82 16.83 8.83 o 2 -7 1 538.28 560.01 25.71 o 3 -7 1 382.18 338.97 26.25 o 4 -7 1 36.16 16.00 17.05 o 5 -7 1 73.03 56.50 18.70 o 6 -7 1 37.76 43.43 16.99 o -7 -6 1 13.31 14.11 14.52 o -6 -6 1 49.98 40.26 14.41 o -5 -6 1 143.22 144.10 20.65 o -4 -6 1 37.81 34.22 12.15 o -3 -6 1 13.71 44.63 16.66 o -2 -6 1 1102.45 1084.92 28.65 o -1 -6 1 195.52 205.01 17.68 o 0 -6 1 498.19 494.37 19.30 o 1 -6 1 301.74 271.59 22.74 o 2 -6 1 432.07 435.43 17.69 o 3 -6 1 281.42 266.81 14.83 o 4 -6 1 124.72 108.37 15.76 o 5 -6 1 9.05 29.58 13.40 o 6 -6 1 17.70 11.22 13.30 o 7 -6 1 72.54 78.90 20.01 o -8 -5 1 55.48 72.16 23.50 o -7 -5 1 12.54 26.56 14.62 o -6 -5 1 27.73 27.40 14.14 o -5 -5 1 562.27 565.49 26.11 o -4 -5 1 411.47 423.88 21.13 o -3 -5 1 44.70 45.25 9.82 o -2 -5 1 45.08 61.25 10.37 o -1 -5 1 15.35 22.73 6.43 o 0 -5 1 57.46 63.65 8.14 o 1 -5 1 852.48 874.34 19.97 o 2 -5 1 563.31 547.21 16.61 o 3 -5 1 39.10 47.29 9.61 o 4 -5 1 93.35 101.35 14.77 o 5 -5 1 275.20 289.29 21.47 o 6 -5 1 109.10 135.39 19.76 o 7 -5 1 144.93 126.18 19.15 o 8 -5 1 78.50 71.60 22.92 o -8 -4 1 69.03 101.52 24.63 o -7 -4 1 133.11 149.33 20.82 o -6 -4 1 354.96 375.95 23.49 o -5 -4 1 273.35 276.12 17.94 o -4 -4 1 42.25 38.08 10.92 o -3 -4 1 145.91 171.87 11.53 o -2 -4 1 475.68 495.57 17.25 o -1 -4 1 389.77 374.09 11.05 o 0 -4 1 255.32 251.69 8.16 o 1 -4 1 210.64 211.57 10.11 o 2 -4 1 148.34 138.60 12.09 o 3 -4 1 131.82 144.96 11.51 o 4 -4 1 91.02 93.84 11.97 o 5 -4 1 185.31 197.62 17.86 o 6 -4 1 206.10 181.84 17.88 o 7 -4 1 62.07 68.89 19.59 o 8 -4 1 12.74 40.32 28.33 o -9 -3 1 28.39 57.57 25.48 o -8 -3 1 134.38 131.06 46.73 o -7 -3 1 0.65 21.74 15.29 o -6 -3 1 407.46 431.93 22.55 o -5 -3 1 68.88 61.05 11.40 o -4 -3 1 556.81 563.19 24.36 o -3 -3 1 157.98 191.66 11.10 o -2 -3 1 1798.08 1876.76 26.40 o -1 -3 1 1164.02 1126.41 28.37 o 0 -3 1 247.00 246.76 9.24 o 1 -3 1 247.50 224.73 8.66 o 2 -3 1 687.78 702.31 11.61 o 3 -3 1 342.30 376.71 13.52 o 4 -3 1 249.66 250.88 12.15 o 5 -3 1 5.27 17.37 10.37 o 6 -3 1 185.88 167.44 22.74 o 7 -3 1 216.38 236.36 27.58 o 8 -3 1 9.11 5.15 28.94 o 9 -3 1 27.19 41.66 19.11 o -9 -2 1 35.16 11.70 19.08 o -8 -2 1 89.23 85.64 30.39 o -7 -2 1 110.47 93.78 20.53 o -6 -2 1 106.31 114.69 19.69 o -5 -2 1 16.49 12.36 6.88 o -4 -2 1 416.71 454.05 17.09 o -3 -2 1 1082.05 1148.84 25.65 o -2 -2 1 412.91 449.30 10.85 o -1 -2 1 247.44 235.24 7.43 o 0 -2 1 1069.78 1104.11 21.05 o 1 -2 1 4189.48 4039.77 41.94 o 2 -2 1 648.67 637.24 14.35 o 3 -2 1 53.45 58.10 8.53 o 4 -2 1 164.98 171.29 13.71 o 5 -2 1 52.09 55.66 17.43 o 6 -2 1 81.05 64.32 16.19 o 7 -2 1 514.08 516.19 30.21 o 8 -2 1 41.90 42.54 20.13 o 9 -2 1 76.48 82.39 25.40 o -9 -1 1 1.67 59.61 25.84 o -8 -1 1 16.28 8.10 16.54 o -7 -1 1 329.85 326.11 28.74 o -6 -1 1 585.55 605.94 28.21 o -5 -1 1 180.78 191.62 17.66 o -4 -1 1 235.40 240.91 12.32 o -3 -1 1 2150.26 2267.15 54.49 o -2 -1 1 1493.22 1449.65 39.82 o -1 -1 1 1507.11 1435.99 18.31 o 1 -1 1 6243.05 5698.52 95.24 o 2 -1 1 228.95 212.55 10.76 o 3 -1 1 794.11 884.02 33.21 o 4 -1 1 420.51 416.88 32.08 o 5 -1 1 325.19 333.20 32.53 o 6 -1 1 234.60 240.05 21.13 o 7 -1 1 2.76 30.44 17.74 o 8 -1 1 90.56 102.26 22.92 o 9 -1 1 10.38 49.86 22.63 o -9 0 1 70.25 29.07 25.95 o -8 0 1 4.36 28.00 25.49 o -7 0 1 279.00 271.30 23.80 o -6 0 1 622.34 638.75 30.09 o -5 0 1 129.73 126.92 22.04 o -4 0 1 0.33 15.60 11.47 o -3 0 1 414.04 386.88 17.32 o -2 0 1 2129.97 2061.93 33.63 o 2 0 1 56.43 54.35 9.96 o 3 0 1 486.79 487.30 17.12 o 4 0 1 0.04 9.93 7.57 o 5 0 1 708.93 742.10 25.43 o 6 0 1 682.50 708.52 29.08 o 7 0 1 498.48 447.93 27.37 o 8 0 1 0.54 1.90 19.36 o 9 0 1 21.06 9.01 19.30 o -9 1 1 1.67 28.40 18.09 o -8 1 1 15.74 23.31 26.98 o -7 1 1 333.83 330.41 26.75 o -6 1 1 585.51 526.53 26.86 o -5 1 1 185.77 193.19 17.95 o -4 1 1 243.10 246.84 22.69 o -3 1 1 2149.93 2286.73 42.80 o 2 1 1 223.53 183.93 15.37 o 3 1 1 792.95 818.18 28.28 o 4 1 1 418.38 413.50 24.69 o 5 1 1 331.66 348.21 25.08 o 6 1 1 235.49 210.86 18.81 o 7 1 1 2.41 7.45 14.18 o 8 1 1 92.68 63.63 18.30 o 9 1 1 10.38 30.10 17.65 o -9 2 1 36.38 36.90 17.27 o -8 2 1 90.29 94.96 22.46 o -7 2 1 110.01 96.09 19.50 o -6 2 1 107.45 110.52 24.23 o -5 2 1 16.41 34.86 22.46 o -4 2 1 421.17 462.39 25.77 o 2 2 1 645.78 612.83 17.23 o 3 2 1 54.28 41.07 11.31 o 4 2 1 163.69 143.58 19.55 o 5 2 1 53.07 69.35 19.06 o 6 2 1 83.95 75.44 24.92 o 7 2 1 518.51 530.49 39.47 o 8 2 1 41.69 24.51 15.73 o 9 2 1 74.91 89.23 32.73 o -9 3 1 28.39 37.83 32.37 o -8 3 1 132.57 127.10 36.52 o -6 3 1 407.57 411.25 31.55 o -5 3 1 68.49 65.07 20.53 o -4 3 1 548.68 542.83 28.12 o 3 3 1 342.85 332.22 16.02 o 4 3 1 244.75 223.85 18.02 o 5 3 1 4.47 15.27 13.90 o 8 3 1 8.61 19.65 24.88 o -3 -9 2 13.28 70.43 26.06 o -2 -9 2 58.53 446.76 262.11 o -1 -9 2 109.10 179.42 34.16 o 0 -9 2 5.88 18.02 18.83 o 1 -9 2 7.14 31.57 13.67 o 2 -9 2 36.12 63.14 25.23 o 3 -9 2 74.69 52.24 24.75 o -5 -8 2 2.42 35.84 23.01 o -4 -8 2 76.19 71.15 26.54 o -3 -8 2 34.77 40.59 19.43 o -2 -8 2 15.40 39.66 20.16 o -1 -8 2 321.86 345.45 27.16 o 0 -8 2 65.35 62.34 14.82 o 1 -8 2 11.33 28.58 14.83 o 2 -8 2 330.24 314.26 24.07 o 3 -8 2 4.62 14.24 19.18 o 4 -8 2 73.89 103.72 24.52 o 5 -8 2 107.66 136.43 27.91 o -6 -7 2 1.05 1.66 24.93 o -5 -7 2 62.76 53.36 22.65 o -4 -7 2 370.17 414.29 32.00 o -3 -7 2 9.83 17.00 16.56 o -2 -7 2 115.36 91.80 22.02 o -1 -7 2 196.35 192.59 18.60 o 0 -7 2 125.15 124.77 14.75 o 1 -7 2 407.05 394.89 19.16 o 2 -7 2 201.65 193.35 19.39 o 3 -7 2 233.49 226.57 22.11 o 4 -7 2 10.02 24.42 17.19 o 5 -7 2 82.70 76.68 19.60 o 6 -7 2 10.52 14.99 17.39 o -7 -6 2 2.94 29.98 14.09 o -6 -6 2 2.88 14.61 15.51 o -5 -6 2 31.32 25.07 14.50 o -4 -6 2 36.71 33.79 12.70 o -3 -6 2 323.32 309.12 25.55 o -2 -6 2 303.48 271.73 17.92 o -1 -6 2 129.08 118.85 15.62 o 0 -6 2 153.94 160.42 14.25 o 1 -6 2 251.18 246.24 15.49 o 2 -6 2 352.03 360.59 16.69 o 3 -6 2 518.12 513.94 20.88 o 4 -6 2 99.91 103.97 17.60 o 5 -6 2 222.94 190.03 20.26 o 6 -6 2 33.18 31.21 12.90 o 7 -6 2 142.01 155.40 20.90 o -8 -5 2 87.04 84.38 26.96 o -7 -5 2 75.90 67.45 27.15 o -6 -5 2 4.47 9.73 14.72 o -5 -5 2 335.24 316.44 20.52 o -4 -5 2 19.12 30.37 10.82 o -3 -5 2 58.85 67.26 12.66 o -2 -5 2 186.16 191.05 12.73 o -1 -5 2 1624.86 1735.50 39.87 o 0 -5 2 165.96 164.80 10.21 o 1 -5 2 619.30 639.46 15.58 o 2 -5 2 138.13 175.74 13.69 o 3 -5 2 522.13 519.10 18.02 o 4 -5 2 250.61 242.35 15.44 o 5 -5 2 14.13 14.70 9.31 o 6 -5 2 168.39 138.94 18.91 o 7 -5 2 58.15 62.07 21.00 o 8 -5 2 21.30 18.65 22.58 o -8 -4 2 0.86 20.25 19.00 o -7 -4 2 18.28 19.69 11.20 o -6 -4 2 92.32 86.87 14.90 o -5 -4 2 118.26 127.44 16.06 o -4 -4 2 177.16 183.33 15.76 o -3 -4 2 58.94 66.37 9.11 o -2 -4 2 39.08 37.91 7.60 o -1 -4 2 1224.98 1316.96 17.87 o 0 -4 2 1512.35 1493.11 21.10 o 1 -4 2 928.32 903.94 18.16 o 2 -4 2 76.66 62.41 7.43 o 3 -4 2 166.11 159.19 11.86 o 4 -4 2 253.62 241.73 15.52 o 5 -4 2 150.73 152.22 15.87 o 6 -4 2 110.77 95.45 15.11 o 7 -4 2 114.14 95.69 21.45 o 8 -4 2 102.96 117.96 27.22 o -9 -3 2 27.64 50.55 26.24 o -8 -3 2 43.51 37.61 22.21 o -7 -3 2 86.17 96.07 20.12 o -6 -3 2 74.41 62.28 14.49 o -5 -3 2 391.00 397.36 19.59 o -4 -3 2 224.83 239.59 15.68 o -3 -3 2 382.82 416.13 12.02 o -2 -3 2 808.70 857.57 16.53 o -1 -3 2 551.94 564.99 12.52 o 0 -3 2 2068.00 2171.17 34.73 o 1 -3 2 314.60 331.87 9.34 o 2 -3 2 655.39 685.83 12.30 o 3 -3 2 241.93 242.94 8.88 o 4 -3 2 46.49 46.95 9.83 o 5 -3 2 95.55 83.26 10.30 o 6 -3 2 288.62 255.11 21.77 o 7 -3 2 16.23 22.42 21.74 o 8 -3 2 146.11 143.58 28.10 o 9 -3 2 23.30 54.33 22.94 o -9 -2 2 30.67 23.07 23.04 o -8 -2 2 29.64 24.60 21.67 o -7 -2 2 181.84 170.49 22.91 o -6 -2 2 454.47 470.58 20.83 o -5 -2 2 754.29 753.12 27.69 o -4 -2 2 629.35 610.13 16.13 o -3 -2 2 1230.81 1320.16 28.23 o -2 -2 2 691.49 677.21 19.57 o -1 -2 2 163.65 152.81 6.63 o 0 -2 2 6700.27 6396.47 34.43 o 1 -2 2 376.16 371.73 7.86 o 2 -2 2 201.11 178.90 10.36 o 3 -2 2 535.59 562.28 19.04 o 4 -2 2 277.24 288.50 16.16 o 5 -2 2 480.30 497.45 28.19 o 6 -2 2 214.90 198.14 18.85 o 7 -2 2 257.07 227.03 29.48 o 8 -2 2 30.05 35.89 19.44 o 9 -2 2 15.26 42.28 27.24 o -9 -1 2 13.34 15.17 23.77 o -8 -1 2 4.85 23.00 20.08 o -7 -1 2 66.24 56.74 19.88 o -6 -1 2 12.30 20.48 14.91 o -5 -1 2 549.51 553.00 24.47 o -4 -1 2 198.39 203.82 12.95 o -3 -1 2 2714.16 2835.98 51.51 o -2 -1 2 526.05 518.16 12.34 o -1 -1 2 533.25 486.91 11.56 o 0 -1 2 448.76 451.17 15.89 o 1 -1 2 9433.31 8646.12 194.29 o 2 -1 2 3806.34 3599.43 141.65 o 3 -1 2 1928.01 1881.39 19.46 o 4 -1 2 167.53 189.02 10.37 o 5 -1 2 129.94 123.15 14.73 o 6 -1 2 115.71 90.91 16.55 o 7 -1 2 35.94 41.95 16.09 o 8 -1 2 5.07 20.90 15.78 o 9 -1 2 65.56 30.47 24.00 o -9 0 2 38.06 34.96 18.19 o -8 0 2 41.92 28.12 23.82 o -7 0 2 129.55 90.59 20.40 o -6 0 2 47.38 30.48 11.98 o -5 0 2 15.79 22.60 12.37 o -4 0 2 504.00 509.29 22.08 o -3 0 2 172.14 168.66 15.40 o -2 0 2 7519.52 6856.60 218.62 o 2 0 2 21.49 28.42 7.16 o 3 0 2 397.06 439.75 28.51 o 4 0 2 603.58 562.83 26.68 o 5 0 2 170.70 192.49 16.35 o 6 0 2 147.65 169.47 21.97 o 7 0 2 539.90 557.84 28.47 o 8 0 2 24.98 21.65 18.00 o 9 0 2 0.28 5.85 32.08 o -9 1 2 13.15 0.00 20.70 o -8 1 2 4.41 22.59 22.81 o -7 1 2 68.39 71.01 19.22 o -6 1 2 12.44 28.77 13.88 o -5 1 2 556.95 556.18 23.70 o -4 1 2 192.22 209.89 24.43 o 2 1 2 3831.93 3589.14 38.58 o 3 1 2 1935.88 1916.94 37.01 o 4 1 2 163.36 165.55 20.47 o 5 1 2 128.88 137.17 15.07 o 6 1 2 116.44 97.71 16.79 o 7 1 2 36.49 49.51 15.42 o 8 1 2 4.82 17.67 13.92 o 9 1 2 65.30 77.23 35.61 o -9 2 2 31.27 27.56 19.89 o -8 2 2 30.20 46.36 16.61 o -7 2 2 182.76 164.43 24.49 o -6 2 2 448.36 457.58 37.77 o -5 2 2 755.96 819.39 36.33 o 2 2 2 202.13 179.02 12.16 o 3 2 2 533.56 594.56 21.88 o 4 2 2 278.46 268.81 23.12 o 5 2 2 479.27 459.61 32.57 o 6 2 2 218.53 253.87 28.15 o 7 2 2 255.03 235.60 23.58 o 8 2 2 29.92 46.24 24.98 o -9 3 2 27.77 72.56 33.12 o -8 3 2 43.72 100.29 36.52 o -7 3 2 86.95 118.27 31.46 o -6 3 2 75.08 69.52 21.52 o -5 3 2 385.98 434.50 30.44 o 2 3 2 643.55 662.83 14.26 o 3 3 2 240.55 261.69 16.35 o 4 3 2 47.86 56.90 14.71 o 8 3 2 145.41 160.75 36.36 o -3 -9 3 234.06 188.74 61.52 o -2 -9 3 15.91 30.79 23.15 o -1 -9 3 222.90 271.74 31.88 o 0 -9 3 12.41 25.80 18.11 o 1 -9 3 15.04 29.15 15.69 o 2 -9 3 26.94 27.44 17.07 o 3 -9 3 5.98 27.28 22.02 o -5 -8 3 27.41 30.71 25.31 o -4 -8 3 40.59 45.70 20.23 o -3 -8 3 44.62 51.50 21.15 o -2 -8 3 285.81 257.77 32.27 o -1 -8 3 100.69 106.68 25.92 o 0 -8 3 53.40 48.25 14.19 o 1 -8 3 75.34 88.42 19.73 o 2 -8 3 43.48 47.48 14.75 o 3 -8 3 69.39 59.60 24.11 o 4 -8 3 40.04 33.35 24.81 o 5 -8 3 6.98 12.42 17.10 o -6 -7 3 31.57 16.85 22.58 o -5 -7 3 57.32 71.85 30.87 o -4 -7 3 81.57 64.20 18.98 o -3 -7 3 79.36 107.50 26.08 o -2 -7 3 3.68 17.64 12.58 o -1 -7 3 46.07 56.92 13.76 o 0 -7 3 125.15 120.98 14.45 o 1 -7 3 559.25 578.92 26.28 o 2 -7 3 129.17 119.95 17.38 o 3 -7 3 472.84 443.06 24.24 o 4 -7 3 17.65 45.50 14.79 o 5 -7 3 30.15 35.61 16.06 o 6 -7 3 57.26 50.77 18.14 o -7 -6 3 51.72 66.01 20.30 o -6 -6 3 201.24 202.66 24.05 o -5 -6 3 19.63 109.79 63.74 o -4 -6 3 37.00 45.32 22.82 o -3 -6 3 369.20 343.11 26.92 o -2 -6 3 553.62 547.08 30.13 o -1 -6 3 171.57 158.63 15.01 o 0 -6 3 56.02 43.66 9.22 o 1 -6 3 90.89 93.27 11.02 o 2 -6 3 208.76 196.25 15.78 o 3 -6 3 380.64 381.97 18.26 o 4 -6 3 56.02 60.22 11.82 o 5 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