#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/46/2014691.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2014691_Fobs loop_ _publ_author_name 'Basok, Stepan S.' 'Croitoru, Lilia' 'Fonari, Marina S.' 'Ganin, Eduard V.' 'Gelmboldt, Vladimir O.' 'Lipkowski, Janusz' 'Simonov, Yurii A.' _publ_section_title ; A new phase of 7,16-dibenzyl-1,4,10,13-tetraoxa-7,16-diazacyclooctadecane, and 7,16-dibenzyl-1,4,10,13-tetraoxa-7,16-diazoniacyclooctadecane bis(tetrafluoroborate) monohydrate, both determined at 123K ; _journal_issue 3 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first o188 _journal_page_last o192 _journal_volume 61 _journal_year 2005 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 103.480 _cell_angle_gamma 90.000 _cell_length_a 16.9930 _cell_length_b 22.4550 _cell_length_c 13.3910 _exptl_crystal_F_000 1920.00 _reflns_d_resolution_high 0.8409 _[local]_cod_data_source_file gd1362Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' gb1.ins in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 401.66 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 5204.72 4848.50 170.43 o 4 0 0 26503.24 25870.77 342.94 o 6 0 0 16225.54 16522.82 212.77 o 8 0 0 733.74 612.07 28.28 o 10 0 0 432.54 475.18 39.84 o 12 0 0 6777.29 6741.34 144.02 o 14 0 0 1135.93 1098.32 42.42 o 16 0 0 192.50 279.36 166.32 o 18 0 0 901.90 1017.37 61.31 o 1 1 0 3.53 0.00 0.96 o 3 1 0 12.20 0.00 3.85 o 4 1 0 63.26 81.28 5.79 o 5 1 0 7.28 11.68 5.46 o 6 1 0 5.67 20.75 6.44 o 7 1 0 244.96 265.48 9.38 o 8 1 0 251.83 242.82 13.87 o 9 1 0 31.38 26.35 7.93 o 10 1 0 185.85 171.72 11.26 o 11 1 0 1.42 50.47 12.53 o 12 1 0 101.08 159.92 19.26 o 13 1 0 6.00 14.69 24.52 o 14 1 0 82.67 86.20 17.02 o 15 1 0 7.03 67.31 25.29 o 16 1 0 19.29 29.34 21.48 o 17 1 0 57.33 108.04 24.03 o 18 1 0 96.81 121.95 24.09 o 19 1 0 7.03 44.57 30.38 o 0 2 0 6.56 0.00 3.82 o 2 2 0 44.15 70.73 8.60 o 3 2 0 190.52 245.93 5.29 o 4 2 0 6.47 31.32 5.40 o 5 2 0 461.15 360.47 8.68 o 6 2 0 2.87 0.00 6.32 o 7 2 0 1235.18 1135.86 17.35 o 8 2 0 4.53 5.82 11.03 o 9 2 0 10606.21 10475.04 118.30 o 10 2 0 2.75 10.19 9.47 o 11 2 0 3098.02 2851.47 44.87 o 12 2 0 0.00 30.56 15.24 o 13 2 0 1959.68 1861.87 41.92 o 14 2 0 5.76 25.28 19.03 o 15 2 0 345.74 389.83 30.17 o 16 2 0 1.10 113.83 123.92 o 17 2 0 22.61 5.08 14.77 o 18 2 0 8.53 34.50 24.78 o 19 2 0 217.37 214.09 44.73 o 1 3 0 5.34 13.57 7.64 o 2 3 0 991.71 832.35 18.86 o 3 3 0 43.72 47.38 4.87 o 4 3 0 814.23 775.60 11.51 o 5 3 0 273.31 279.56 8.10 o 6 3 0 256.79 252.45 7.96 o 7 3 0 0.75 7.10 7.49 o 8 3 0 0.33 21.70 11.53 o 9 3 0 93.39 91.57 12.47 o 10 3 0 90.74 111.73 16.55 o 11 3 0 9.33 42.82 14.93 o 12 3 0 11.41 22.46 13.33 o 13 3 0 82.71 78.09 18.15 o 14 3 0 15.49 17.35 14.95 o 15 3 0 28.63 20.05 24.30 o 16 3 0 68.41 125.56 29.73 o 17 3 0 16.62 105.54 38.94 o 18 3 0 37.41 69.58 48.62 o 19 3 0 1.53 23.11 31.25 o 0 4 0 10191.32 9256.20 175.58 o 1 4 0 5.71 2.10 6.32 o 2 4 0 105371.40 97201.83 1236.85 o 3 4 0 24.16 51.20 5.59 o 4 4 0 3804.13 4065.67 39.48 o 5 4 0 0.26 15.28 5.76 o 6 4 0 2779.78 3182.07 36.88 o 7 4 0 0.42 5.87 7.54 o 8 4 0 46.98 46.57 10.96 o 9 4 0 29.18 39.81 12.69 o 10 4 0 1005.46 986.10 21.62 o 11 4 0 0.67 32.13 18.15 o 12 4 0 1639.91 1551.63 37.62 o 13 4 0 0.63 21.90 20.68 o 14 4 0 110.52 92.64 18.91 o 15 4 0 7.19 45.36 49.44 o 16 4 0 17.26 34.17 20.82 o 17 4 0 4.63 7.65 23.79 o 18 4 0 93.06 114.67 39.05 o 19 4 0 4.57 84.57 35.19 o 1 5 0 139.92 135.78 4.79 o 2 5 0 99.87 126.02 6.37 o 3 5 0 82.56 93.98 11.89 o 4 5 0 18.29 20.32 6.45 o 5 5 0 2276.81 2163.08 23.45 o 6 5 0 145.11 122.25 8.72 o 7 5 0 1431.75 1464.43 20.96 o 8 5 0 247.12 259.60 11.40 o 9 5 0 1466.41 1421.70 25.54 o 10 5 0 336.78 328.82 16.20 o 11 5 0 420.95 431.17 19.81 o 12 5 0 358.39 372.47 19.25 o 13 5 0 78.07 94.12 33.15 o 14 5 0 61.62 50.93 17.61 o 15 5 0 873.17 846.88 45.89 o 16 5 0 59.58 93.13 35.11 o 17 5 0 60.57 44.28 22.38 o 18 5 0 8.42 31.63 47.60 o 19 5 0 5.08 25.30 31.08 o 0 6 0 17.93 34.25 12.51 o 1 6 0 1053.06 1134.34 20.52 o 2 6 0 20.84 29.30 5.48 o 3 6 0 511.57 533.42 10.43 o 4 6 0 3.09 5.37 5.94 o 5 6 0 964.42 1002.93 15.55 o 6 6 0 0.30 7.56 10.98 o 7 6 0 6570.12 6735.64 66.78 o 8 6 0 12.34 11.13 8.96 o 9 6 0 4641.94 4692.33 58.98 o 10 6 0 13.16 13.86 15.28 o 11 6 0 2245.89 2346.74 39.99 o 12 6 0 6.49 22.70 22.00 o 13 6 0 3434.43 3534.02 60.14 o 14 6 0 0.67 8.43 21.61 o 15 6 0 566.58 575.91 28.97 o 16 6 0 0.92 22.36 21.82 o 17 6 0 328.50 320.74 28.15 o 18 6 0 6.34 19.88 26.96 o 19 6 0 171.85 184.82 33.78 o 1 7 0 12.81 4.65 8.58 o 2 7 0 1940.40 1866.19 25.03 o 3 7 0 24.50 33.25 6.84 o 4 7 0 842.86 770.85 13.53 o 5 7 0 10875.56 10896.68 108.42 o 6 7 0 69.20 93.55 8.90 o 7 7 0 4617.63 4430.44 45.85 o 8 7 0 414.18 387.97 12.57 o 9 7 0 8.88 35.00 12.50 o 10 7 0 135.57 162.18 13.22 o 11 7 0 793.66 761.21 30.94 o 12 7 0 362.62 340.78 18.81 o 13 7 0 107.96 73.00 16.73 o 14 7 0 101.59 176.37 66.99 o 15 7 0 40.52 65.48 32.80 o 16 7 0 92.88 105.98 36.00 o 17 7 0 155.00 152.69 35.79 o 18 7 0 0.06 12.90 29.08 o 0 8 0 148.57 191.75 43.56 o 1 8 0 1.79 24.32 7.57 o 2 8 0 62.94 90.36 6.00 o 3 8 0 77.77 86.12 7.32 o 4 8 0 27103.63 28367.88 267.22 o 5 8 0 6.40 0.00 7.56 o 6 8 0 291.27 208.11 9.88 o 7 8 0 162.19 141.58 10.26 o 8 8 0 2498.95 2717.92 35.62 o 9 8 0 40.42 74.75 13.24 o 10 8 0 2913.67 2893.28 42.57 o 11 8 0 26.51 34.25 17.13 o 12 8 0 5729.94 5616.81 87.81 o 13 8 0 21.57 42.38 18.04 o 14 8 0 1729.26 1754.72 43.90 o 15 8 0 0.53 0.00 17.24 o 16 8 0 499.12 477.10 28.94 o 17 8 0 0.62 66.60 28.71 o 18 8 0 75.65 111.34 50.16 o 1 9 0 9.71 26.99 16.35 o 2 9 0 477.45 447.23 11.83 o 3 9 0 17.54 35.68 15.26 o 4 9 0 7532.01 7545.78 78.12 o 5 9 0 1456.42 1497.50 23.49 o 6 9 0 7769.65 8034.64 83.02 o 7 9 0 3447.72 3448.23 38.74 o 8 9 0 2.07 28.31 11.51 o 9 9 0 55.69 62.02 13.59 o 10 9 0 1228.12 1169.06 36.60 o 11 9 0 400.32 419.06 20.10 o 12 9 0 15.25 50.24 21.10 o 13 9 0 201.76 176.59 28.64 o 14 9 0 38.18 53.82 23.08 o 15 9 0 333.85 312.20 25.78 o 16 9 0 126.44 158.30 44.79 o 17 9 0 53.00 78.90 27.11 o 18 9 0 102.12 94.88 24.64 o 0 10 0 3.60 23.46 33.34 o 1 10 0 113.31 148.19 15.23 o 2 10 0 30.73 35.59 5.43 o 3 10 0 24511.37 25585.28 255.77 o 4 10 0 0.03 4.98 7.36 o 5 10 0 8147.53 8634.60 96.58 o 6 10 0 37.29 48.80 10.59 o 7 10 0 6079.22 6321.29 77.22 o 8 10 0 0.40 25.68 10.95 o 9 10 0 1.19 36.16 12.49 o 10 10 0 111.03 89.46 19.72 o 11 10 0 1637.57 1709.23 40.98 o 12 10 0 7.39 23.37 16.42 o 13 10 0 3069.28 3039.26 57.53 o 14 10 0 22.35 40.94 22.06 o 15 10 0 1527.70 1405.97 40.87 o 16 10 0 0.49 2.79 21.54 o 17 10 0 1.74 16.46 26.06 o 18 10 0 10.87 33.45 27.48 o 1 11 0 1897.41 1993.22 35.19 o 2 11 0 244.41 250.75 16.41 o 3 11 0 3822.20 3943.64 50.99 o 4 11 0 6090.61 6515.60 77.11 o 5 11 0 5892.66 5765.40 74.63 o 6 11 0 11.26 27.39 10.45 o 7 11 0 5443.49 5537.76 74.22 o 8 11 0 1732.95 1701.57 35.11 o 9 11 0 690.30 681.76 23.67 o 10 11 0 266.56 260.72 27.42 o 11 11 0 224.42 222.77 20.20 o 12 11 0 1.16 16.48 19.98 o 13 11 0 128.48 119.58 18.98 o 14 11 0 77.99 123.62 31.00 o 15 11 0 10.77 35.71 21.91 o 16 11 0 97.89 115.85 25.26 o 17 11 0 0.85 34.65 25.43 o 0 12 0 1369.19 1592.91 61.65 o 1 12 0 58.92 90.23 36.26 o 2 12 0 1.52 30.40 6.92 o 3 12 0 4.38 0.00 8.00 o 4 12 0 698.04 790.31 18.60 o 5 12 0 13.69 16.43 10.79 o 6 12 0 11579.85 12665.29 161.52 o 7 12 0 59.01 68.61 14.00 o 8 12 0 132.50 161.66 13.37 o 9 12 0 0.16 33.05 30.53 o 10 12 0 1.72 27.46 13.96 o 11 12 0 0.16 12.96 19.56 o 12 12 0 1067.24 1092.91 33.75 o 13 12 0 48.17 49.71 18.56 o 14 12 0 70.27 87.89 23.93 o 15 12 0 45.81 53.78 19.60 o 16 12 0 294.41 268.79 41.41 o 17 12 0 2.03 68.70 28.26 o 1 13 0 17.71 20.90 28.66 o 2 13 0 355.87 318.80 70.31 o 3 13 0 225.67 252.34 12.22 o 4 13 0 452.64 399.34 15.37 o 5 13 0 14.57 30.60 11.18 o 6 13 0 123.14 146.77 12.06 o 7 13 0 1.49 20.50 19.90 o 8 13 0 666.70 653.42 20.81 o 9 13 0 811.85 804.17 27.58 o 10 13 0 156.75 151.68 38.61 o 11 13 0 670.83 633.11 28.33 o 12 13 0 154.36 127.45 23.00 o 13 13 0 0.00 25.14 21.38 o 14 13 0 42.48 95.54 24.67 o 15 13 0 83.47 99.58 24.37 o 16 13 0 33.95 105.75 28.03 o 17 13 0 3.73 28.66 23.83 o 0 14 0 38.62 23.12 34.39 o 1 14 0 368.26 382.71 41.17 o 2 14 0 3.02 1.37 10.51 o 3 14 0 78.54 64.01 11.62 o 4 14 0 0.29 22.73 10.50 o 5 14 0 102.27 182.28 18.28 o 6 14 0 25.64 27.74 11.60 o 7 14 0 207.94 185.76 16.53 o 8 14 0 37.46 48.52 14.41 o 9 14 0 44.25 130.42 44.54 o 10 14 0 7.31 38.42 32.46 o 11 14 0 745.68 801.87 45.05 o 12 14 0 1.36 0.00 19.59 o 13 14 0 4.10 2.73 18.62 o 14 14 0 0.81 50.27 33.34 o 15 14 0 926.14 868.67 44.09 o 16 14 0 9.95 81.72 39.39 o 1 15 0 1145.31 1150.97 77.54 o 2 15 0 481.22 536.31 23.01 o 3 15 0 72.24 60.74 7.89 o 4 15 0 370.97 384.91 21.37 o 5 15 0 1703.93 1665.31 36.07 o 6 15 0 48.97 44.20 13.40 o 7 15 0 1617.55 1544.64 37.25 o 8 15 0 299.75 288.02 24.82 o 9 15 0 635.49 588.63 32.98 o 10 15 0 3.18 17.58 20.19 o 11 15 0 24.41 20.24 18.97 o 12 15 0 4.65 0.00 20.94 o 13 15 0 110.25 106.41 21.34 o 14 15 0 621.07 645.11 36.73 o 15 15 0 14.12 80.81 32.50 o 16 15 0 86.42 108.95 25.61 o 0 16 0 590.63 694.72 92.09 o 1 16 0 2.15 85.92 47.79 o 2 16 0 7.78 54.48 30.76 o 3 16 0 1.16 7.64 6.61 o 4 16 0 103.05 116.77 15.41 o 5 16 0 1.00 32.44 23.90 o 6 16 0 431.47 390.14 21.71 o 7 16 0 0.01 11.39 15.36 o 8 16 0 1.88 110.97 40.90 o 9 16 0 2.70 34.89 21.45 o 10 16 0 77.30 49.10 36.61 o 11 16 0 0.87 39.21 30.90 o 12 16 0 3.30 25.00 14.43 o 13 16 0 11.81 67.11 25.98 o 14 16 0 0.18 12.26 26.96 o 15 16 0 0.99 0.00 27.41 o 1 17 0 143.42 183.13 47.90 o 2 17 0 673.45 616.36 43.82 o 3 17 0 1746.56 1761.86 134.70 o 4 17 0 41.98 49.45 9.96 o 5 17 0 3791.43 3728.01 69.97 o 6 17 0 78.56 87.35 26.08 o 7 17 0 966.42 917.98 49.10 o 8 17 0 21.60 10.89 24.54 o 9 17 0 2.18 6.19 20.78 o 10 17 0 63.92 41.64 20.69 o 11 17 0 37.26 78.54 26.47 o 12 17 0 11.74 73.55 64.94 o 13 17 0 65.19 81.59 26.14 o 14 17 0 10.45 91.55 40.85 o 15 17 0 0.90 53.37 35.33 o 0 18 0 135.95 200.62 74.32 o 1 18 0 7492.98 7290.19 213.34 o 2 18 0 6.15 0.00 48.53 o 3 18 0 173.20 281.90 35.31 o 4 18 0 47.09 43.49 8.41 o 5 18 0 296.18 287.07 40.22 o 6 18 0 2.32 65.35 24.90 o 7 18 0 806.09 850.47 59.42 o 8 18 0 5.53 50.82 30.33 o 9 18 0 38.47 78.70 31.61 o 10 18 0 5.19 54.37 24.86 o 11 18 0 130.01 125.88 49.80 o 12 18 0 9.08 84.25 34.18 o 13 18 0 19.85 59.93 53.62 o 14 18 0 4.18 0.00 47.55 o 1 19 0 6423.99 5930.10 180.67 o 2 19 0 2644.87 2792.18 95.65 o 3 19 0 1109.87 1254.13 60.84 o 4 19 0 3165.84 3007.05 94.82 o 5 19 0 1759.97 1693.79 58.49 o 6 19 0 570.73 544.01 37.35 o 7 19 0 5.86 52.49 26.72 o 8 19 0 216.34 262.17 62.10 o 9 19 0 311.55 272.89 30.47 o 10 19 0 34.28 32.20 26.75 o 11 19 0 164.62 234.93 40.15 o 12 19 0 5.31 56.49 37.14 o 13 19 0 110.24 44.72 85.98 o 0 20 0 1250.62 1338.61 121.52 o 1 20 0 9.56 234.09 270.74 o 2 20 0 0.74 113.03 228.32 o 3 20 0 63.99 32.67 46.81 o 4 20 0 608.46 633.56 56.08 o 5 20 0 78.13 102.21 71.55 o 6 20 0 508.82 329.69 45.29 o 7 20 0 14.83 90.36 67.92 o 8 20 0 88.41 360.32 575.87 o 9 20 0 0.49 52.65 44.06 o 10 20 0 22.66 70.45 76.62 o 11 20 0 0.40 1.50 32.43 o 12 20 0 4.01 34.41 57.17 o 13 20 0 7.16 132.43 67.83 o 1 21 0 122.60 96.43 51.94 o 2 21 0 1234.90 1109.04 67.09 o 3 21 0 750.24 706.22 65.35 o 4 21 0 5.42 18.99 38.89 o 5 21 0 59.80 147.29 60.38 o 6 21 0 185.29 190.33 48.58 o 7 21 0 95.82 318.58 154.67 o 8 21 0 43.11 132.62 81.59 o 9 21 0 104.58 157.49 77.86 o 10 21 0 299.59 418.47 151.71 o 11 21 0 122.90 339.68 90.95 o 12 21 0 164.35 186.07 52.48 o 0 22 0 90.30 111.01 63.63 o 1 22 0 1593.13 1630.72 81.43 o 2 22 0 15.11 0.00 38.06 o 3 22 0 939.60 781.96 75.85 o 4 22 0 10.95 31.52 51.74 o 5 22 0 1170.75 1013.63 152.66 o 6 22 0 0.49 28.82 41.95 o 7 22 0 4.70 25.13 56.97 o 8 22 0 3.25 42.62 109.10 o 9 22 0 12.49 91.64 201.38 o 10 22 0 10.30 64.66 82.34 o 11 22 0 20.84 124.61 139.77 o 1 23 0 314.69 227.20 45.63 o 2 23 0 49.54 80.60 46.36 o 3 23 0 327.65 401.53 68.11 o 4 23 0 488.84 557.52 122.66 o 5 23 0 12.91 129.61 62.43 o 6 23 0 61.86 174.94 61.64 o 7 23 0 268.55 232.89 49.37 o 8 23 0 0.38 224.16 99.46 o 9 23 0 419.32 288.66 77.51 o 0 24 0 125.54 101.07 99.35 o 1 24 0 4.56 5.25 84.26 o 2 24 0 5.95 49.17 42.24 o 3 24 0 0.02 65.37 45.43 o 4 24 0 16.61 54.07 44.60 o 5 24 0 39.03 59.85 98.49 o 6 24 0 593.21 678.99 205.01 o 7 24 0 17.20 309.45 96.49 o 8 24 0 11.17 0.00 72.65 o 1 25 0 3.50 0.00 55.46 o 2 25 0 222.36 344.32 129.59 o 3 25 0 36.47 38.01 80.03 o 4 25 0 816.20 776.98 177.79 o 5 25 0 10.31 19.12 61.70 o 6 25 0 11.57 104.93 87.09 o 0 26 0 0.01 32.29 102.79 o 1 26 0 51.97 11.48 64.10 o 2 26 0 5.00 90.25 95.82 o 3 26 0 12.09 165.17 107.47 o 4 26 0 0.07 139.54 59.89 o -19 1 1 38.32 11.06 32.82 o -18 1 1 1.72 5.46 22.26 o -17 1 1 53.80 68.70 24.05 o -16 1 1 308.50 225.72 20.72 o -15 1 1 67.98 92.45 15.65 o -14 1 1 0.00 46.16 20.93 o -13 1 1 18.28 46.58 15.69 o -12 1 1 156.00 154.36 12.37 o -11 1 1 16.11 31.83 11.19 o -10 1 1 36.44 45.57 8.85 o -9 1 1 37.44 51.35 9.51 o -8 1 1 457.89 517.08 11.51 o -7 1 1 353.34 314.60 9.23 o -6 1 1 248.84 249.17 7.90 o -5 1 1 245.98 254.60 7.06 o -4 1 1 550.69 568.23 9.10 o -3 1 1 0.29 0.00 3.24 o -2 1 1 221.00 290.61 25.41 o 2 1 1 262.64 236.76 10.47 o 3 1 1 231.72 209.24 6.49 o 4 1 1 171.54 173.83 7.24 o 5 1 1 1.01 0.00 6.57 o 6 1 1 230.74 220.40 13.49 o 7 1 1 421.31 410.63 11.58 o 8 1 1 48.42 65.51 8.64 o 9 1 1 41.95 69.74 22.45 o 10 1 1 391.15 414.32 15.79 o 11 1 1 52.11 54.31 14.57 o 12 1 1 30.02 48.81 15.01 o 13 1 1 0.04 23.53 15.94 o 14 1 1 37.62 80.88 22.64 o 15 1 1 12.07 32.65 41.06 o 16 1 1 0.04 0.00 18.20 o 17 1 1 14.09 55.75 25.98 o 18 1 1 209.08 246.03 39.46 o 19 1 1 0.74 22.18 32.50 o -19 2 1 7.74 6.88 29.69 o -18 2 1 190.19 205.04 35.89 o -17 2 1 1.33 3.76 21.79 o -16 2 1 64.92 43.61 49.39 o -15 2 1 0.46 47.23 16.37 o -14 2 1 235.19 225.65 18.12 o -13 2 1 7.60 26.72 16.23 o -12 2 1 647.99 534.87 18.85 o -11 2 1 6.65 18.93 11.34 o -10 2 1 1097.69 1085.99 21.54 o -9 2 1 3.57 14.95 9.60 o -8 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