#------------------------------------------------------------------------------ #$Date: 2016-04-02 22:03:46 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180818 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/49/2014925.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2014925_Fobs loop_ _publ_author_name 'D\'iaz, Jes\'us Garc\'ia' 'Ko\H-imidazole-\kN^3^)bis(N-nitrocyanamidato-\kN)copper(II) ; _journal_issue 4 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first m180 _journal_page_last m182 _journal_volume 61 _journal_year 2005 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 104.170 _cell_angle_beta 96.650 _cell_angle_gamma 96.860 _cell_length_a 9.8410 _cell_length_b 15.2490 _cell_length_c 15.2340 _exptl_crystal_F_000 1036.00 _reflns_d_resolution_high 0.8000 _cod_data_source_file sq1193Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' JK34 TRICLINIC' _shelx_refln_list_code 4 _shelx_f_calc_maximum 332.25 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 53604.66 52126.00 1002.58 o 3 0 0 4253.22 3860.95 36.86 o 4 0 0 4041.05 4010.86 21.86 o 5 0 0 13819.53 14005.78 96.74 o 6 0 0 147.51 150.33 9.75 o 7 0 0 742.06 714.61 35.70 o 8 0 0 131.60 131.16 15.48 o 9 0 0 1413.74 1453.55 72.45 o 10 0 0 579.60 611.64 30.76 o 11 0 0 495.09 485.92 30.93 o 12 0 0 141.17 201.36 31.59 o -12 1 0 265.45 207.26 25.31 o -11 1 0 1215.62 1338.14 35.18 o -10 1 0 291.91 272.42 17.45 o -9 1 0 1826.91 1817.85 107.70 o -8 1 0 13.97 13.39 7.11 o -7 1 0 0.71 11.03 6.15 o -6 1 0 770.47 796.55 17.15 o -5 1 0 798.99 740.26 14.30 o -4 1 0 11914.48 12227.64 415.34 o -3 1 0 5551.18 5166.69 91.50 o -2 1 0 339.78 336.17 7.25 o 2 1 0 34606.72 35227.09 555.50 o 3 1 0 5249.16 5445.42 67.15 o 4 1 0 5575.56 5972.21 88.59 o 5 1 0 4341.95 4477.85 190.58 o 6 1 0 637.82 614.32 14.24 o 7 1 0 204.05 178.08 10.84 o 8 1 0 112.89 92.11 11.54 o 9 1 0 549.08 530.26 23.47 o 10 1 0 203.72 188.44 21.46 o 11 1 0 161.81 154.75 27.55 o -12 2 0 105.12 50.21 19.36 o -11 2 0 190.21 201.88 20.75 o -10 2 0 1304.40 1330.33 24.65 o -9 2 0 271.76 293.32 35.33 o -8 2 0 3361.31 3333.78 39.52 o -7 2 0 1142.39 1279.63 65.26 o -6 2 0 496.58 392.01 36.51 o -5 2 0 3331.60 3345.72 136.54 o -4 2 0 7675.51 7679.46 213.62 o -3 2 0 7223.79 6728.95 307.40 o -2 2 0 10870.58 10464.21 386.04 o 2 2 0 8757.88 8818.79 343.89 o 3 2 0 2930.86 2948.85 60.26 o 4 2 0 3248.65 3047.40 102.78 o 5 2 0 153.98 132.73 7.75 o 6 2 0 7136.90 7274.79 148.04 o 7 2 0 1332.96 1212.73 48.44 o 8 2 0 5012.45 5257.86 51.58 o 9 2 0 676.90 593.79 26.23 o 10 2 0 115.99 88.41 20.04 o 11 2 0 240.69 291.44 37.75 o -12 3 0 345.52 364.53 35.11 o -11 3 0 115.23 108.60 22.26 o -10 3 0 472.21 475.21 19.57 o -9 3 0 579.29 530.83 17.36 o -8 3 0 613.72 658.17 18.74 o -7 3 0 228.85 231.23 42.56 o -6 3 0 97.47 134.94 18.95 o -5 3 0 3291.01 3087.62 78.02 o -4 3 0 1563.53 1628.20 76.95 o -3 3 0 6050.60 5931.27 116.24 o -2 3 0 2069.19 2062.81 26.78 o -1 3 0 1550.33 1454.58 40.68 o 0 3 0 628.73 627.78 9.95 o 1 3 0 5999.99 6179.97 218.28 o 2 3 0 2093.11 1850.82 46.37 o 3 3 0 8097.90 8416.04 117.25 o 4 3 0 1374.09 1259.49 19.37 o 5 3 0 1528.79 1584.58 16.28 o 6 3 0 49.81 54.89 7.77 o 7 3 0 290.50 266.17 20.47 o 8 3 0 19.96 16.11 12.45 o 9 3 0 695.71 675.46 29.29 o 10 3 0 415.07 387.25 24.43 o 11 3 0 437.46 451.93 34.03 o -12 4 0 317.64 316.46 23.64 o -11 4 0 125.92 97.66 15.88 o -10 4 0 123.65 119.91 18.20 o -9 4 0 3282.29 3298.71 59.14 o -8 4 0 402.99 397.81 15.58 o -7 4 0 4209.46 4285.89 79.99 o -6 4 0 4883.60 5245.24 189.40 o -5 4 0 6932.96 6613.95 170.16 o -4 4 0 1506.28 1408.68 63.85 o -3 4 0 4333.63 4347.52 63.75 o -2 4 0 3898.29 3605.57 74.19 o -1 4 0 21.17 71.55 13.01 o 0 4 0 4393.40 3923.17 132.96 o 1 4 0 1269.06 1398.59 50.94 o 2 4 0 9148.16 8756.70 417.78 o 3 4 0 3563.79 3860.78 259.64 o 4 4 0 699.75 696.79 17.51 o 5 4 0 4443.91 4570.56 40.80 o 6 4 0 255.51 253.17 21.90 o 7 4 0 6185.46 6355.12 54.03 o 8 4 0 296.72 297.33 25.53 o 9 4 0 1188.68 1293.76 36.65 o 10 4 0 948.21 840.61 32.83 o 11 4 0 319.24 301.95 32.86 o -12 5 0 140.82 132.51 25.46 o -11 5 0 217.38 227.56 43.62 o -10 5 0 865.95 888.82 22.11 o -9 5 0 196.87 200.68 35.03 o -8 5 0 449.64 449.49 17.75 o -7 5 0 25.47 53.58 13.77 o -6 5 0 212.60 169.31 12.32 o -5 5 0 1121.36 1052.65 23.70 o -4 5 0 4054.51 4078.66 93.31 o -3 5 0 4382.47 4461.33 245.86 o -2 5 0 1717.14 1681.58 47.43 o -1 5 0 305.72 341.37 13.71 o 0 5 0 810.40 944.82 20.24 o 1 5 0 3127.14 3071.95 44.82 o 2 5 0 7309.30 7598.25 237.65 o 3 5 0 504.33 443.26 29.67 o 4 5 0 4312.59 4577.64 41.17 o 5 5 0 1476.44 1553.48 52.38 o 6 5 0 393.61 428.75 24.51 o 7 5 0 19.44 23.78 12.91 o 8 5 0 91.15 129.86 20.29 o 9 5 0 87.33 72.31 16.06 o 10 5 0 760.18 839.40 31.81 o 11 5 0 212.82 224.72 32.83 o -12 6 0 145.57 125.44 28.18 o -11 6 0 85.79 60.86 14.73 o -10 6 0 913.55 928.75 23.10 o -9 6 0 768.63 782.47 78.86 o -8 6 0 3622.92 3708.46 31.79 o -7 6 0 1484.53 1634.14 33.21 o -6 6 0 2794.39 2594.86 106.54 o -5 6 0 2732.98 2731.75 37.09 o -4 6 0 2282.73 2194.09 57.94 o -3 6 0 1851.94 1726.35 73.78 o -2 6 0 2903.09 3240.97 116.86 o -1 6 0 3826.81 3336.76 32.48 o 0 6 0 388.83 467.22 14.46 o 1 6 0 2846.03 2576.48 12.99 o 2 6 0 2975.89 3123.13 68.97 o 3 6 0 1743.10 1658.02 79.77 o 4 6 0 1077.34 1047.30 75.96 o 5 6 0 657.11 725.57 32.99 o 6 6 0 2415.37 2415.53 39.25 o 7 6 0 186.39 156.66 18.24 o 8 6 0 996.64 1003.89 33.68 o 9 6 0 467.60 442.38 31.13 o 10 6 0 831.10 924.36 42.38 o -11 7 0 474.55 401.42 32.29 o -10 7 0 22.05 73.96 24.09 o -9 7 0 89.41 95.58 13.99 o -8 7 0 201.56 215.83 23.47 o -7 7 0 66.51 81.48 10.51 o -6 7 0 716.22 629.29 22.05 o -5 7 0 1581.41 1620.99 173.12 o -4 7 0 2714.78 2636.33 84.68 o -3 7 0 3872.74 3821.32 58.67 o -2 7 0 5283.26 5390.61 149.91 o -1 7 0 2.82 7.71 4.43 o 0 7 0 459.29 456.38 15.66 o 1 7 0 1190.81 1161.95 32.01 o 2 7 0 2504.25 2548.31 52.30 o 3 7 0 5349.13 5551.20 183.17 o 4 7 0 237.96 193.47 28.57 o 5 7 0 647.28 695.23 50.54 o 6 7 0 765.85 805.67 22.02 o 7 7 0 15.83 37.27 18.90 o 8 7 0 351.67 406.52 29.48 o 9 7 0 67.27 50.45 23.35 o 10 7 0 259.92 326.20 37.49 o -11 8 0 232.36 217.27 35.45 o -10 8 0 1175.13 1261.27 44.69 o -9 8 0 3162.56 3400.61 54.72 o -8 8 0 1162.06 1133.36 34.23 o -7 8 0 1131.66 1263.78 122.51 o -6 8 0 788.68 780.87 135.91 o -5 8 0 1193.61 1142.30 84.27 o -4 8 0 3740.90 3649.93 68.68 o -3 8 0 1217.82 1170.78 71.30 o -2 8 0 7524.17 7593.67 270.51 o -1 8 0 336.56 320.40 21.13 o 0 8 0 7750.46 7343.55 108.33 o 1 8 0 400.67 338.50 25.87 o 2 8 0 8899.71 9362.65 245.98 o 3 8 0 1626.46 1582.33 72.93 o 4 8 0 2098.28 2251.14 135.42 o 5 8 0 1510.81 1508.65 28.25 o 6 8 0 351.05 328.80 17.06 o 7 8 0 1756.49 2046.98 45.96 o 8 8 0 80.51 49.16 18.25 o 9 8 0 363.09 376.27 29.51 o 10 8 0 124.33 119.24 30.21 o -11 9 0 149.16 165.09 30.50 o -10 9 0 870.26 952.71 48.65 o -9 9 0 142.53 224.50 21.28 o -8 9 0 10.47 39.75 14.01 o -7 9 0 645.23 733.47 22.13 o -6 9 0 194.13 163.29 30.59 o -5 9 0 1595.60 1469.73 46.83 o -4 9 0 1246.20 1134.71 20.77 o -3 9 0 729.47 705.16 93.40 o -2 9 0 316.25 256.37 11.54 o -1 9 0 1592.86 1539.74 23.21 o 0 9 0 167.30 218.49 15.28 o 1 9 0 962.55 1019.68 22.46 o 2 9 0 2018.87 2169.98 24.08 o 3 9 0 353.73 353.18 15.33 o 4 9 0 4101.24 4393.95 150.87 o 5 9 0 1378.96 1386.32 27.72 o 6 9 0 608.60 618.95 64.44 o 7 9 0 91.80 79.57 21.13 o 8 9 0 109.19 107.00 24.73 o 9 9 0 141.13 111.78 26.08 o -11 10 0 178.50 243.78 28.10 o -10 10 0 1349.01 1508.83 100.50 o -9 10 0 27.31 50.55 17.56 o -8 10 0 2846.04 3093.34 45.98 o -7 10 0 73.17 110.09 24.52 o -6 10 0 1959.58 1874.94 74.05 o -5 10 0 1168.90 1014.50 21.44 o -4 10 0 776.41 749.53 158.29 o -3 10 0 2569.40 2497.02 155.55 o -2 10 0 139.13 123.55 10.03 o -1 10 0 2019.72 2083.24 45.59 o 0 10 0 1617.01 1511.12 45.93 o 1 10 0 4909.60 5045.74 51.30 o 2 10 0 1200.40 1271.05 23.22 o 3 10 0 1260.34 1321.92 37.31 o 4 10 0 251.36 250.64 26.40 o 5 10 0 354.12 339.94 18.70 o 6 10 0 1432.34 1530.05 29.57 o 7 10 0 168.71 216.68 21.84 o 8 10 0 343.87 336.68 33.12 o 9 10 0 41.16 62.59 24.59 o -10 11 0 117.79 129.28 30.26 o -9 11 0 313.74 380.53 43.68 o -8 11 0 141.20 208.66 55.83 o -7 11 0 379.28 497.57 71.87 o -6 11 0 900.27 800.90 21.98 o -5 11 0 505.95 468.58 70.68 o -4 11 0 2677.39 2676.18 132.22 o -3 11 0 1821.72 1829.52 108.05 o -2 11 0 1563.27 1515.34 66.59 o -1 11 0 1383.17 1317.27 18.92 o 0 11 0 6.51 7.16 9.00 o 1 11 0 673.54 736.70 30.92 o 2 11 0 1590.73 1715.42 25.91 o 3 11 0 361.97 364.26 17.86 o 4 11 0 22.50 22.38 9.82 o 5 11 0 169.96 129.70 36.30 o 6 11 0 319.12 305.56 23.52 o 7 11 0 173.97 164.77 24.15 o 8 11 0 19.28 10.48 16.32 o -10 12 0 27.60 32.01 13.89 o -9 12 0 737.78 876.61 43.29 o -8 12 0 118.55 103.17 16.80 o -7 12 0 2647.16 2843.14 69.74 o -6 12 0 38.09 51.69 11.05 o -5 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707.12 806.41 27.86 o -4 14 0 682.07 763.70 75.26 o -3 14 0 1310.88 1259.36 24.35 o -2 14 0 752.74 722.89 31.62 o -1 14 0 1749.57 1950.38 44.39 o 0 14 0 86.79 61.98 21.35 o 1 14 0 1766.78 1836.62 43.07 o 2 14 0 1067.04 990.75 23.20 o 3 14 0 476.51 421.66 64.32 o 4 14 0 369.98 315.32 23.13 o 5 14 0 10.98 29.84 13.28 o 6 14 0 783.70 712.91 30.54 o -8 15 0 319.68 368.31 28.37 o -7 15 0 100.48 136.33 26.96 o -6 15 0 210.41 263.59 38.95 o -5 15 0 626.68 660.10 67.30 o -4 15 0 305.50 293.77 45.93 o -3 15 0 274.61 324.34 34.45 o -2 15 0 278.40 291.31 33.64 o -1 15 0 79.35 70.53 19.95 o 0 15 0 318.67 308.03 31.47 o 1 15 0 360.26 390.42 33.98 o 2 15 0 242.55 315.30 38.79 o 3 15 0 85.91 62.25 24.06 o 4 15 0 154.30 103.79 36.20 o 5 15 0 246.17 254.81 23.31 o -7 16 0 606.00 724.71 70.82 o -6 16 0 214.40 264.44 68.63 o -5 16 0 473.37 610.93 105.35 o -4 16 0 377.35 318.13 31.05 o -3 16 0 284.18 258.60 32.53 o -2 16 0 2154.64 2392.94 54.78 o -1 16 0 312.22 241.83 30.58 o 0 16 0 2444.90 2656.37 54.13 o 1 16 0 461.34 382.00 33.02 o 2 16 0 854.36 903.54 43.76 o 3 16 0 365.28 356.34 41.64 o 4 16 0 201.87 225.58 39.98 o -6 17 0 176.23 204.03 25.46 o -5 17 0 137.60 104.57 30.60 o -4 17 0 21.68 23.51 19.47 o -3 17 0 8.25 6.92 15.61 o -2 17 0 85.65 93.54 25.80 o -1 17 0 71.98 76.01 21.74 o 0 17 0 71.86 28.69 17.20 o 1 17 0 114.25 74.31 24.96 o 2 17 0 42.24 10.15 14.73 o 3 17 0 458.81 351.52 40.83 o -4 18 0 269.31 242.84 38.71 o -3 18 0 705.00 592.50 46.00 o -2 18 0 155.72 95.51 25.87 o -1 18 0 943.12 1010.43 52.24 o 0 18 0 218.41 207.73 38.42 o -1 -18 1 148.57 74.66 23.43 o 0 -18 1 327.06 220.86 34.47 o 1 -18 1 87.43 104.89 29.69 o 2 -18 1 35.21 22.16 19.17 o 3 -18 1 138.09 65.02 22.21 o 4 -18 1 128.31 125.30 33.21 o 5 -18 1 369.51 347.46 37.85 o -3 -17 1 300.75 260.75 38.13 o -2 -17 1 11.00 21.59 16.77 o -1 -17 1 514.29 573.59 42.91 o 0 -17 1 111.29 59.81 24.05 o 1 -17 1 668.78 680.49 42.76 o 2 -17 1 96.63 36.54 22.23 o 3 -17 1 690.67 795.03 44.37 o 4 -17 1 73.64 55.90 27.85 o 5 -17 1 608.09 674.66 47.40 o 6 -17 1 402.50 448.53 56.02 o -4 -16 1 11.98 54.44 27.15 o -3 -16 1 184.68 169.84 33.78 o -2 -16 1 365.22 412.66 39.71 o -1 -16 1 535.71 492.57 34.70 o 0 -16 1 92.63 88.66 25.85 o 1 -16 1 514.05 539.45 37.67 o 2 -16 1 148.94 139.57 25.71 o 3 -16 1 388.11 430.55 37.40 o 4 -16 1 1107.42 1049.97 40.61 o 5 -16 1 89.66 99.92 26.35 o 6 -16 1 772.88 871.26 57.21 o 7 -16 1 225.44 256.85 25.40 o -5 -15 1 339.49 284.71 24.64 o -4 -15 1 257.40 206.99 31.76 o -3 -15 1 923.04 931.82 44.80 o -2 -15 1 439.94 430.30 33.82 o -1 -15 1 468.80 405.42 32.72 o 0 -15 1 2222.25 2445.94 46.37 o 1 -15 1 68.28 39.35 20.26 o 2 -15 1 1468.90 1587.38 43.35 o 3 -15 1 557.03 463.04 27.32 o 4 -15 1 1654.68 1646.68 91.47 o 5 -15 1 1327.46 1268.31 48.84 o 6 -15 1 87.58 84.25 16.58 o 7 -15 1 352.35 430.64 25.95 o 8 -15 1 18.65 46.37 16.96 o -6 -14 1 96.27 90.09 17.91 o -5 -14 1 3.27 10.42 11.62 o -4 -14 1 29.16 24.44 10.25 o -3 -14 1 89.47 54.73 13.79 o -2 -14 1 137.65 85.79 20.40 o -1 -14 1 93.05 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