#------------------------------------------------------------------------------ #$Date: 2016-04-02 22:04:37 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180820 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/51/2015137.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2015137_Fobs loop_ _publ_author_name 'Bond, Andrew D.' 'McKenzie, Christine J.' _publ_section_title ; One-dimensional zinc-based coordination polymers incorporating cyanate anions ; _journal_coeditor_code FG1873 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first m519 _journal_page_last m522 _journal_volume 61 _journal_year 2005 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 90.024 _cell_angle_gamma 90.000 _cell_length_a 14.3880 _cell_length_b 16.4830 _cell_length_c 26.4380 _exptl_crystal_F_000 3080.00 _reflns_d_resolution_high 0.7988 _cod_data_source_file fg1873IIsup3.hkl _cod_data_source_block II #BEGIN Tags that were not found in dictionaries: _shelx_title ' cm0541 in P2(1)/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 904.24 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 138123.30 148934.00 14363.82 o 6 0 0 21944.42 23887.32 2340.74 o 8 0 0 6841.73 6986.59 1004.26 o 10 0 0 14881.56 15488.17 2192.45 o 12 0 0 369.82 1184.35 462.02 o 14 0 0 2472.08 4105.99 1257.07 o 16 0 0 5609.05 6645.03 1781.84 o 3 1 0 29.17 -22.78 68.34 o 4 1 0 485.05 371.81 114.48 o 5 1 0 408.23 258.42 102.52 o 6 1 0 824.54 804.13 145.24 o 7 1 0 831.84 739.18 189.85 o 8 1 0 2306.48 2217.00 268.98 o 9 1 0 1677.77 1385.65 306.69 o 10 1 0 1753.93 1500.51 299.42 o 11 1 0 1288.18 1313.73 305.23 o 12 1 0 1047.96 1297.51 328.04 o 13 1 0 540.59 281.85 422.36 o 14 1 0 676.84 988.49 466.37 o 15 1 0 666.01 1300.66 750.63 o 16 1 0 935.79 1029.88 914.90 o 17 1 0 333.29 -870.57 870.57 o 2 2 0 1343.49 1316.97 179.55 o 3 2 0 1342.91 1175.01 151.67 o 4 2 0 3203.98 3581.46 307.09 o 5 2 0 141461.61 145020.64 11478.25 o 6 2 0 123.51 198.82 164.10 o 7 2 0 2523.99 3592.08 431.37 o 8 2 0 54.94 41.24 186.38 o 9 2 0 37663.29 30526.99 2965.06 o 10 2 0 493.56 807.28 279.98 o 11 2 0 76488.55 76910.85 7272.72 o 12 2 0 327.99 852.41 549.49 o 13 2 0 26050.01 30123.11 3283.81 o 14 2 0 477.66 179.74 483.84 o 15 2 0 13853.69 15259.47 1822.73 o 16 2 0 200.65 1397.65 821.70 o 17 2 0 3472.98 3054.98 1020.86 o 1 3 0 163.23 142.92 62.18 o 2 3 0 0.94 -55.05 92.39 o 3 3 0 4.95 -68.02 124.00 o 4 3 0 313.18 269.51 107.93 o 5 3 0 1101.47 1031.60 199.01 o 6 3 0 582.41 321.01 198.35 o 7 3 0 2702.57 2324.12 302.31 o 8 3 0 991.61 971.98 281.08 o 9 3 0 2577.71 3235.23 475.01 o 10 3 0 699.98 476.75 334.04 o 11 3 0 533.35 272.70 365.19 o 12 3 0 86.74 322.97 586.54 o 13 3 0 15.61 253.28 448.36 o 14 3 0 2.61 -2.57 484.21 o 15 3 0 111.35 947.49 560.42 o 16 3 0 138.77 1222.38 844.03 o 17 3 0 534.13 691.16 879.78 o 1 4 0 6252.63 7282.71 789.99 o 2 4 0 2701.76 3575.30 371.96 o 3 4 0 163.22 545.83 151.20 o 4 4 0 148201.00 159406.19 15382.59 o 5 4 0 14683.82 15935.34 1587.27 o 6 4 0 28862.89 31115.79 3518.94 o 7 4 0 1537.81 1641.83 256.79 o 8 4 0 567.49 1148.78 251.61 o 9 4 0 3.42 335.45 292.52 o 10 4 0 23073.43 25217.62 2853.33 o 11 4 0 463.18 182.89 373.72 o 12 4 0 5698.50 7630.70 973.16 o 13 4 0 214.03 362.38 460.35 o 14 4 0 1418.12 2261.44 576.50 o 15 4 0 123.00 -493.74 548.84 o 16 4 0 1487.50 2527.25 708.94 o 17 4 0 148.77 406.86 1357.60 o 1 5 0 279.69 359.09 285.91 o 2 5 0 7.48 -100.69 100.69 o 3 5 0 76.80 86.74 133.65 o 4 5 0 65.28 -177.65 177.65 o 5 5 0 91.02 -255.01 255.01 o 6 5 0 545.40 551.17 315.09 o 7 5 0 55.33 154.50 445.53 o 8 5 0 2488.12 2588.85 372.47 o 9 5 0 55.00 -44.75 293.07 o 10 5 0 1288.37 1005.24 463.89 o 11 5 0 7.17 -320.48 374.92 o 12 5 0 202.27 131.56 429.07 o 13 5 0 34.27 -196.77 470.07 o 14 5 0 8.12 32.09 511.61 o 15 5 0 4.11 -348.07 567.88 o 16 5 0 238.15 80.07 635.65 o 17 5 0 47.32 -82.63 696.67 o 1 6 0 322098.94 361456.84 49492.98 o 2 6 0 543.34 791.85 127.25 o 3 6 0 936.65 1990.74 248.47 o 4 6 0 3571.61 3389.08 520.17 o 5 6 0 373.94 915.79 297.37 o 6 6 0 5037.08 4206.04 660.29 o 7 6 0 37813.77 43435.48 4921.14 o 8 6 0 3821.72 4723.17 513.51 o 9 6 0 19699.44 19688.67 1922.90 o 10 6 0 5357.73 5506.22 739.07 o 11 6 0 12342.53 14274.94 1662.56 o 12 6 0 627.32 1359.61 650.15 o 13 6 0 1860.38 3182.06 693.93 o 14 6 0 352.24 1165.78 549.13 o 15 6 0 4281.48 6699.84 975.24 o 16 6 0 220.52 462.36 649.53 o 17 6 0 2014.60 2274.08 1272.28 o 1 7 0 126.52 9.64 208.90 o 2 7 0 171.06 -10.66 290.52 o 3 7 0 333.16 241.48 137.26 o 4 7 0 23.45 103.98 257.78 o 5 7 0 605.29 1196.93 319.75 o 6 7 0 4.44 -573.18 618.39 o 7 7 0 1130.98 682.90 285.94 o 8 7 0 30.85 629.73 257.06 o 9 7 0 1484.36 1815.19 318.10 o 10 7 0 18.15 -33.68 340.41 o 11 7 0 1030.92 1130.37 414.93 o 12 7 0 41.27 149.40 429.76 o 13 7 0 316.92 252.57 493.65 o 14 7 0 98.15 199.79 532.07 o 15 7 0 701.69 751.41 611.00 o 16 7 0 84.75 688.64 662.27 o 0 8 0 445828.75 501386.16 68671.09 o 1 8 0 83171.49 91880.19 12609.98 o 2 8 0 45495.61 53549.66 7343.54 o 3 8 0 14592.18 16991.75 1934.08 o 4 8 0 43992.87 45837.64 5089.77 o 5 8 0 19021.90 20170.60 2826.72 o 6 8 0 5052.89 6416.16 956.22 o 7 8 0 2.11 -211.62 318.21 o 8 8 0 2893.70 2996.09 515.15 o 9 8 0 3166.25 3198.00 488.15 o 10 8 0 24307.77 24780.14 2790.49 o 11 8 0 6662.89 7336.90 1096.74 o 12 8 0 14269.12 16507.40 1939.70 o 13 8 0 5067.84 5223.45 788.66 o 14 8 0 6755.50 8017.62 1575.00 o 15 8 0 2183.19 2706.06 713.03 o 16 8 0 2496.90 2808.72 785.88 o 1 9 0 366.54 330.28 204.25 o 2 9 0 7.47 -317.02 369.83 o 3 9 0 76.34 -349.54 349.54 o 4 9 0 341.00 450.51 226.84 o 5 9 0 11.36 -191.28 274.56 o 6 9 0 798.30 883.09 349.32 o 7 9 0 95.87 392.97 344.13 o 8 9 0 2402.70 2396.98 380.81 o 9 9 0 13.14 73.96 333.14 o 10 9 0 1848.11 1718.63 542.05 o 11 9 0 0.11 0.84 397.81 o 12 9 0 1119.35 1631.06 494.14 o 13 9 0 14.33 -484.11 484.11 o 14 9 0 561.64 279.63 573.04 o 15 9 0 4.76 570.73 614.75 o 16 9 0 1089.53 1513.11 713.59 o 0 10 0 288451.75 323272.28 44336.76 o 1 10 0 233747.30 262514.59 36015.32 o 2 10 0 59647.90 70535.02 13713.38 o 3 10 0 43226.44 49310.61 9607.39 o 4 10 0 41576.48 41789.68 4719.15 o 5 10 0 23398.08 21308.11 2853.07 o 6 10 0 3557.76 4767.75 764.84 o 7 10 0 210.77 500.89 476.82 o 8 10 0 154.42 435.71 418.89 o 9 10 0 7071.45 7717.15 1201.09 o 10 10 0 4453.74 4853.68 854.56 o 11 10 0 8421.81 9133.80 1142.98 o 12 10 0 2263.64 3012.89 599.92 o 13 10 0 1805.14 2015.45 571.73 o 14 10 0 1477.08 1951.48 722.13 o 15 10 0 2699.53 3330.71 749.34 o 1 11 0 22.73 422.99 168.99 o 2 11 0 348.03 52.57 351.39 o 3 11 0 461.19 175.23 444.54 o 4 11 0 28.60 -209.36 497.11 o 5 11 0 537.72 299.81 203.97 o 6 11 0 69.30 264.42 318.51 o 7 11 0 1286.31 2118.55 493.84 o 8 11 0 107.52 -404.53 404.53 o 9 11 0 1942.41 1313.19 683.41 o 10 11 0 0.68 -309.95 384.22 o 11 11 0 1408.67 1771.34 622.41 o 12 11 0 0.46 -175.12 578.41 o 13 11 0 194.44 24.81 669.73 o 14 11 0 0.10 960.72 768.96 o 15 11 0 181.65 1051.99 847.11 o 0 12 0 46911.76 48093.69 6595.85 o 1 12 0 46511.32 48286.35 4692.20 o 2 12 0 12841.42 15610.51 3111.77 o 3 12 0 8232.75 12169.48 2456.95 o 4 12 0 13267.44 14151.46 2842.47 o 5 12 0 10470.20 10122.02 2098.19 o 6 12 0 2758.63 3801.38 643.62 o 7 12 0 12.81 166.28 363.92 o 8 12 0 4616.25 4556.49 800.97 o 9 12 0 4039.24 4620.25 835.59 o 10 12 0 16947.88 18680.16 2673.06 o 11 12 0 5863.07 6792.96 1297.65 o 12 12 0 8795.80 9339.55 1459.48 o 13 12 0 3640.44 5339.99 1058.44 o 14 12 0 2127.34 1925.57 834.34 o 1 13 0 196.81 606.45 211.71 o 2 13 0 13.75 508.18 481.43 o 3 13 0 77.01 524.78 575.50 o 4 13 0 501.51 139.26 581.96 o 5 13 0 89.40 54.41 583.80 o 6 13 0 566.16 -147.56 617.01 o 7 13 0 439.99 287.75 677.88 o 8 13 0 818.26 910.29 779.33 o 9 13 0 247.07 313.02 482.05 o 10 13 0 302.64 1088.54 584.16 o 11 13 0 17.20 -579.99 579.99 o 12 13 0 32.83 -16.87 630.96 o 13 13 0 26.44 -667.73 984.99 o 0 14 0 59836.66 68976.38 13417.33 o 1 14 0 40173.12 45357.35 6214.65 o 2 14 0 13693.20 17660.55 2449.35 o 3 14 0 3890.21 4100.46 1037.56 o 4 14 0 16911.08 18798.83 3765.67 o 5 14 0 392.81 750.74 718.46 o 6 14 0 7881.56 10509.38 2241.14 o 7 14 0 246.84 -110.67 715.69 o 8 14 0 842.26 1574.33 925.05 o 9 14 0 799.32 -84.85 835.59 o 10 14 0 316.82 -647.44 857.72 o 11 14 0 799.74 1963.53 1112.27 o 12 14 0 997.58 1559.57 1079.99 o 13 14 0 258.40 -218.58 1044.02 o 1 15 0 105.88 78.78 356.69 o 2 15 0 107.69 305.37 336.57 o 3 15 0 0.92 -244.40 632.68 o 4 15 0 2.45 250.86 684.33 o 5 15 0 36.65 -67.33 743.36 o 6 15 0 62.07 275.76 795.93 o 7 15 0 126.31 -61.79 776.56 o 8 15 0 322.99 393.81 898.30 o 9 15 0 161.92 218.58 898.30 o 10 15 0 330.46 -719.38 931.50 o 11 15 0 74.83 592.10 1101.20 o 12 15 0 235.88 -831.90 1072.61 o 0 16 0 9126.55 11222.30 2303.85 o 1 16 0 31502.96 36293.04 4981.42 o 2 16 0 1782.73 2764.99 878.01 o 3 16 0 1304.17 1180.52 762.73 o 4 16 0 483.14 330.18 771.03 o 5 16 0 499.67 684.33 832.82 o 6 16 0 808.92 587.49 895.53 o 7 16 0 8910.30 10124.79 2262.35 o 8 16 0 1623.25 1833.49 1085.52 o 9 16 0 11167.90 10440.21 2378.56 o 10 16 0 1302.01 1799.37 1099.36 o 11 16 0 6514.94 5455.28 1607.53 o 1 17 0 132.67 1041.25 741.51 o 2 17 0 6.79 644.67 786.70 o 3 17 0 221.35 783.02 796.85 o 4 17 0 62.21 265.62 836.51 o 5 17 0 253.41 -290.52 885.39 o 6 17 0 2.20 -412.26 941.65 o 7 17 0 416.02 912.13 984.99 o 8 17 0 126.55 642.83 1007.13 o 9 17 0 210.05 367.99 1129.79 o 10 17 0 446.76 283.14 1192.51 o 0 18 0 53106.75 57115.86 11159.58 o 1 18 0 915.10 419.64 776.56 o 2 18 0 25949.92 31829.72 6313.00 o 3 18 0 1859.92 1787.38 1006.21 o 4 18 0 17175.63 18464.96 3782.27 o 5 18 0 3427.69 2836.93 1173.14 o 6 18 0 5318.22 5421.16 1558.65 o 7 18 0 406.55 -313.58 1014.51 o 8 18 0 208.59 246.25 1185.13 o 1 19 0 54.79 -431.63 865.10 o 2 19 0 273.27 1050.48 898.30 o 3 19 0 3.06 -37.81 936.11 o 4 19 0 335.52 245.33 1005.28 o 5 19 0 14.54 -228.73 1066.16 o 6 19 0 396.53 671.42 1158.38 o 2 20 0 2038.88 2108.33 1101.20 o 3 20 0 6130.64 4806.92 1447.06 o 4 20 0 165.43 -68.25 1099.36 o -17 0 1 278.91 1256.15 1373.27 o -15 0 1 2564.08 3924.30 1325.32 o -13 0 1 3672.63 2307.51 565.27 o -11 0 1 7807.00 5941.36 1160.23 o -9 0 1 7042.10 5447.91 1238.62 o -7 0 1 6038.84 4237.58 649.60 o -5 0 1 1750.63 1372.51 202.31 o -3 0 1 393.30 309.43 101.57 o 3 0 1 395.37 173.88 101.92 o 5 0 1 1752.11 1579.31 227.24 o 7 0 1 6105.48 4969.75 752.53 o 9 0 1 7119.94 6028.55 905.84 o 11 0 1 7887.09 7410.52 1564.19 o 13 0 1 3710.67 2755.85 624.35 o 15 0 1 2586.31 2338.90 1142.70 o 17 0 1 275.84 914.90 1283.81 o -17 1 1 57.01 848.21 898.12 o -16 1 1 101.50 -310.55 793.64 o -15 1 1 490.65 290.53 762.60 o -14 1 1 606.18 274.84 461.57 o -13 1 1 1890.40 1477.07 576.40 o -12 1 1 2375.15 2131.03 388.31 o -11 1 1 5600.12 5106.57 588.44 o -10 1 1 4204.12 4099.84 484.85 o -9 1 1 6043.29 4959.65 540.67 o -8 1 1 4673.61 4266.91 415.22 o -7 1 1 7049.61 7140.38 652.56 o -6 1 1 2519.49 2187.91 211.57 o -5 1 1 1090.68 877.67 190.32 o -4 1 1 345.45 239.78 81.34 o -3 1 1 525.31 358.88 64.61 o 3 1 1 521.17 441.47 86.06 o 4 1 1 343.05 273.09 101.83 o 5 1 1 1078.84 938.06 146.62 o 6 1 1 2493.74 2275.67 231.61 o 7 1 1 6974.60 7250.29 647.11 o 8 1 1 4625.32 5178.99 541.76 o 9 1 1 5978.74 4605.71 572.95 o 10 1 1 4159.40 3361.02 418.82 o 11 1 1 5542.69 5578.39 705.36 o 12 1 1 2348.59 1852.12 601.62 o 13 1 1 1870.07 1400.91 357.05 o 14 1 1 600.15 132.28 796.62 o 15 1 1 485.23 693.20 714.10 o 16 1 1 101.17 30.73 791.05 o 17 1 1 57.65 -618.76 918.29 o -17 2 1 10.41 208.15 923.65 o -16 2 1 341.77 646.70 812.11 o -15 2 1 15.95 433.94 532.68 o -14 2 1 950.69 761.08 476.04 o -13 2 1 36.44 -408.98 435.03 o -12 2 1 1426.13 1220.07 430.67 o -11 2 1 94.76 -166.50 352.37 o -10 2 1 5021.04 3144.64 490.81 o -9 2 1 158.94 -134.30 247.23 o -8 2 1 7212.07 6565.55 981.41 o -7 2 1 254.70 693.15 138.43 o -6 2 1 4030.19 3747.62 493.59 o -5 2 1 141.48 68.54 125.40 o -4 2 1 1054.47 1071.97 138.19 o -3 2 1 30.02 -122.12 122.12 o -2 2 1 560.12 362.38 113.70 o 2 2 1 563.82 266.22 138.35 o 3 2 1 29.84 36.28 106.21 o 4 2 1 1062.08 543.26 163.30 o 5 2 1 142.20 1849.95 598.52 o 6 2 1 4072.03 3564.58 467.14 o 7 2 1 257.51 369.56 210.12 o 8 2 1 7289.08 6617.52 974.25 o 9 2 1 160.03 523.85 197.61 o 10 2 1 5076.76 4141.62 490.23 o 11 2 1 95.80 829.32 246.76 o 12 2 1 1439.46 2124.41 368.86 o 13 2 1 36.81 714.88 462.03 o 14 2 1 960.62 859.24 497.18 o 15 2 1 16.09 817.06 563.51 o 16 2 1 345.25 1068.20 834.50 o 17 2 1 10.34 -247.52 883.44 o -17 3 1 80.32 -381.54 1145.93 o -16 3 1 65.46 430.91 785.50 o -15 3 1 13.25 32.51 544.83 o -14 3 1 76.60 -311.57 736.75 o -13 3 1 101.37 261.61 453.49 o -12 3 1 1125.64 424.22 474.11 o -11 3 1 1634.95 1581.30 444.43 o -10 3 1 4121.57 4565.28 847.36 o -9 3 1 2194.43 2243.56 400.83 o -8 3 1 7586.63 6849.21 820.17 o -7 3 1 3074.18 2664.74 337.54 o -6 3 1 6042.78 5239.06 550.69 o -5 3 1 544.58 389.21 136.05 o -4 3 1 667.31 365.14 156.57 o -3 3 1 76.47 251.05 132.68 o -2 3 1 39.51 98.79 108.56 o -1 3 1 65.41 -167.34 179.98 o 0 3 1 14.38 -32.39 77.93 o 1 3 1 66.10 -109.10 154.36 o 2 3 1 39.09 175.78 94.28 o 3 3 1 75.85 220.30 126.70 o 4 3 1 661.29 472.08 114.71 o 5 3 1 543.61 271.11 169.01 o 6 3 1 5975.26 5832.74 596.33 o 7 3 1 3041.35 3050.83 361.74 o 8 3 1 7503.11 7579.90 906.95 o 9 3 1 2174.21 2015.28 398.44 o 10 3 1 4084.03 3570.06 538.76 o 11 3 1 1624.92 1519.33 500.99 o 12 3 1 1119.34 1238.17 443.64 o 13 3 1 101.55 -444.22 444.22 o 14 3 1 75.98 -158.17 473.09 o 15 3 1 13.25 -183.00 529.66 o 16 3 1 65.78 196.53 739.56 o 17 3 1 81.20 772.95 917.99 o -17 4 1 75.04 -826.63 850.16 o -16 4 1 1.18 -317.14 619.53 o -15 4 1 68.51 203.51 574.57 o -14 4 1 3.13 107.82 840.64 o -13 4 1 250.60 1062.98 485.73 o -12 4 1 94.52 180.20 402.82 o -11 4 1 993.26 1015.67 390.85 o -10 4 1 186.52 653.18 351.81 o -9 4 1 3450.91 3914.30 540.34 o -8 4 1 718.23 678.38 232.24 o -7 4 1 4835.64 4426.97 484.17 o -6 4 1 325.05 568.65 308.72 o -5 4 1 1333.91 1138.17 307.39 o -4 4 1 295.27 -79.63 161.87 o -3 4 1 235.42 441.98 149.83 o -2 4 1 22.27 14.57 154.07 o -1 4 1 86.53 18.86 76.27 o 0 4 1 880.63 828.76 135.88 o 1 4 1 85.73 -205.86 290.98 o 2 4 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