#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2015267.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2015267_Fobs loop_ _publ_author_name 'Li, Wen-Ge' 'Zhang, You-Cai' 'Wang, Zuo-Wei' 'Li, Yi-Zhi' 'Zheng, He-Gen' _publ_section_title ; Bis(2,2'-bipyridine)iodo(oxo)tri-\m~3~-sulfido-tricopper(I)tungsten(VI) ; _journal_coeditor_code OB1248 _journal_issue 4 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first m159 _journal_page_last m160 _journal_volume 62 _journal_year 2006 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 79.660 _cell_angle_beta 85.900 _cell_angle_gamma 67.380 _cell_length_a 8.8950 _cell_length_b 9.8280 _cell_length_c 16.3310 _exptl_crystal_F_000 868.00 _reflns_d_resolution_high 0.8409 _[local]_cod_data_source_file ob1248Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 21025Bm in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 310.03 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 172.63 207.40 21.87 o 3 0 0 2967.01 3324.95 104.42 o 4 0 0 18095.38 19579.29 569.90 o 5 0 0 2313.72 2236.88 124.88 o 6 0 0 70.08 50.11 35.02 o 7 0 0 1135.00 1167.33 93.37 o 8 0 0 766.60 703.97 80.64 o 9 0 0 5.63 48.81 55.01 o -9 1 0 981.52 965.49 107.41 o -8 1 0 169.04 226.99 59.01 o -7 1 0 293.47 251.47 50.28 o -6 1 0 656.46 591.58 65.46 o -5 1 0 7253.51 7191.80 324.77 o -4 1 0 5960.94 6195.05 277.10 o -3 1 0 54127.27 55391.45 2199.83 o -2 1 0 53318.30 57683.75 2282.18 o -1 1 0 3454.27 3849.61 161.28 o 0 1 0 15756.57 17600.97 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