#------------------------------------------------------------------------------
#$Date: 2016-04-02 22:05:32 +0300 (Sat, 02 Apr 2016) $
#$Revision: 180822 $
#$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/53/2015320.hkl $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2015320_Fobs
loop_
_publ_author_name
'Kato, Masako'
'Okada, Yoshiko'
'Shishido, Yasuko'
'Kishi, Shinobu'
_publ_section_title
;
 Dichloro(4,4'-dialkyl-2,2'-bipyridine-\k^2^<i>N</i>,<i>N</i>')platinum(II),
 where alkyl is pentyl and heptyl
;
_journal_coeditor_code           OB1249
_journal_issue                   5
_journal_name_full               'Acta Crystallographica Section C'
_journal_page_first              m171
_journal_page_last               m173
_journal_volume                  62
_journal_year                    2006
_space_group_IT_number           14
_symmetry_space_group_name_Hall  '-P 2ybc'
_symmetry_space_group_name_H-M   'P 1 21/c 1'
_cod_data_source_file            ob1249IIsup3.hkl
_cod_data_source_block           II
loop_
_refln_index_h
_refln_index_k
_refln_index_l
_refln_F_squared_meas
_refln_F_squared_sigma
_refln_F_squared_calc
_refln_observed_status
3 0 0 28706.52 5.90 27194.46 o
4 0 0 9541.38 9.24 9967.80 o
5 0 0 796.37 49.28 1587.78 o
6 0 0 36588.04 14.14 37759.95 o
7 0 0 159656.18 32.49 166774.68 o
8 0 0 365746.75 30.47 351828.11 o
9 0 0 476900.74 89.68 490903.43 o
10 0 0 391062.62 74.13 372287.20 o
11 0 0 236040.51 26.01 221756.99 o
12 0 0 207316.30 68.89 192368.33 o
13 0 0 5973.74 74.48 5335.71 o
14 0 0 5835.43 135.96 4658.26 o
15 0 0 9964.03 73.79 9064.09 o
16 0 0 44116.80 76.21 44707.93 o
17 0 0 62665.11 87.80 57294.91 o
18 0 0 56753.53 90.82 52334.45 o
2 1 0 489300.25 9.55 529283.19 o
3 1 0 471666.77 10.63 441352.45 o
4 1 0 341324.69 11.49 331483.08 o
5 1 0 354120.21 15.52 352545.42 o
6 1 0 504199.40 16.24 522155.27 o
7 1 0 338665.80 27.77 336045.25 o
8 1 0 128199.80 26.52 127802.06 o
9 1 0 1600.80 29.81 980.03 o
10 1 0 43201.62 27.77 41743.05 o
11 1 0 82162.49 47.33 79427.77 o
12 1 0 89042.56 48.86 79950.95 o
13 1 0 163409.98 82.63 147150.60 o
14 1 0 125040.03 74.65 114730.53 o
15 1 0 86583.06 65.93 74334.30 o
16 1 0 42911.12 99.60 39855.13 o
17 1 0 10312.40 132.71 11554.96 o
0 2 0 577980.06 11.70 607043.79 o
1 2 0 300610.96 9.36 307707.88 o
2 2 0 112566.96 10.11 120198.39 o
3 2 0 90288.23 11.36 94924.67 o
4 2 0 54512.91 12.82 58516.49 o
5 2 0 3876.31 19.80 206.89 o
6 2 0 27004.35 14.44 15339.27 o
7 2 0 3689.35 28.30 3785.08 o
8 2 0 120041.46 29.05 136768.99 o
9 2 0 121319.86 46.10 121627.39 o
10 2 0 61727.40 33.18 62017.52 o
11 2 0 6226.79 62.41 6663.09 o
12 2 0 4288.94 63.20 7357.80 o
17 2 0 8469.52 82.08 9272.41 o
1 3 0 2804.76 25.30 4334.12 o
2 3 0 110084.60 13.25 122021.15 o
3 3 0 64241.97 14.14 48890.57 o
4 3 0 4529.29 29.38 3140.88 o
5 3 0 34043.94 21.34 32580.14 o
6 3 0 4416.93 30.47 6040.34 o
8 3 0 2645.04 26.83 4774.47 o
9 3 0 5904.39 19.71 6065.42 o
10 3 0 5925.92 59.75 8557.38 o
13 3 0 5722.92 137.59 8254.49 o
0 4 0 301390.02 17.31 300995.35 o
1 4 0 425064.88 19.27 423181.63 o
2 4 0 50886.34 23.62 44998.05 o
3 4 0 52011.36 25.91 59122.32 o
5 4 0 2335.79 40.96 4021.67 o
6 4 0 29697.63 25.10 29791.74 o
7 4 0 101799.28 31.02 101232.78 o
8 4 0 45808.84 27.77 44810.22 o
9 4 0 94341.12 37.58 98204.82 o
10 4 0 104723.43 49.70 105376.47 o
11 4 0 127777.65 93.12 132452.73 o
12 4 0 16078.24 82.45 18986.68 o
13 4 0 3254.70 117.51 4006.35 o
1 5 0 56116.87 27.77 49534.10 o
2 5 0 262379.57 54.61 262192.14 o
3 5 0 395980.73 36.97 391204.80 o
4 5 0 329992.80 40.58 322589.56 o
5 5 0 520331.40 55.06 507470.21 o
6 5 0 384970.61 47.20 377764.66 o
7 5 0 236147.40 37.58 232314.92 o
8 5 0 76120.81 39.82 80201.78 o
9 5 0 10720.53 45.02 12672.13 o
10 5 0 7826.94 42.38 9609.06 o
11 5 0 48880.79 49.98 48233.55 o
12 5 0 76729.00 129.28 71268.85 o
13 5 0 71363.78 67.73 74092.83 o
14 5 0 80072.02 81.54 71397.98 o
15 5 0 54597.00 87.05 50525.38 o
16 5 0 44825.36 106.09 43708.33 o
0 6 0 659457.68 56.10 658570.22 o
1 6 0 546017.54 46.92 521340.41 o
2 6 0 320389.96 32.95 322589.56 o
3 6 0 299504.45 42.51 290131.41 o
4 6 0 8407.06 43.30 11667.84 o
5 6 0 6988.96 52.56 8342.57 o
6 6 0 34406.54 40.32 33164.52 o
7 6 0 196249.00 34.11 184533.09 o
8 6 0 374752.11 48.72 340356.49 o
9 6 0 456759.71 87.80 413902.41 o
10 6 0 215528.06 31.81 187382.45 o
11 6 0 85556.25 46.24 86576.40 o
12 6 0 27669.00 70.39 29791.74 o
13 6 0 4723.81 98.41 5236.12 o
16 6 0 14268.30 137.83 13482.95 o
1 7 0 53749.79 48.30 51691.25 o
2 7 0 113656.64 50.69 116704.12 o
3 7 0 120825.76 53.00 125165.56 o
4 7 0 157767.84 40.07 151729.56 o
5 7 0 214924.96 61.78 204463.05 o
6 7 0 245530.16 43.82 234807.26 o
7 7 0 132306.79 51.27 122810.56 o
8 7 0 17635.84 49.98 21911.66 o
10 7 0 21939.53 60.68 23724.96 o
11 7 0 33668.58 66.42 35508.44 o
12 7 0 22894.72 79.39 25417.28 o
13 7 0 17405.52 73.27 20399.96 o
14 7 0 21626.64 132.02 23774.63 o
15 7 0 34154.74 105.06 31042.44 o
0 8 0 150637.13 65.61 137694.36 o
1 8 0 105027.85 55.95 98356.39 o
2 8 0 19312.66 56.85 22900.66 o
3 8 0 6955.56 61.94 7050.05 o
4 8 0 3543.82 68.23 3328.76 o
7 8 0 4193.86 75.52 5359.28 o
8 8 0 12084.60 70.56 14338.20 o
9 8 0 45543.83 54.02 49983.46 o
10 8 0 9727.88 70.90 12195.93 o
11 8 0 5692.70 82.63 7899.65 o
1 9 0 2928.97 84.09 3046.76 o
3 9 0 2655.34 106.71 3676.80 o
4 9 0 4365.24 83.17 4140.06 o
5 9 0 21187.71 60.06 22186.86 o
6 9 0 15883.56 69.72 18677.06 o
7 9 0 3685.70 82.45 4570.68 o
0 10 0 108609.79 51.27 112179.23 o
1 10 0 98828.50 57.15 96570.30 o
2 10 0 117772.51 55.06 100005.89 o
3 10 0 37601.09 62.09 39118.57 o
5 10 0 3210.36 103.02 4376.66 o
6 10 0 27476.38 74.65 27420.83 o
7 10 0 43209.94 67.90 43758.89 o
8 10 0 31765.93 72.08 34753.29 o
9 10 0 35652.99 74.48 36348.49 o
10 10 0 31085.22 78.50 35402.23 o
11 10 0 24351.60 111.72 29251.78 o
12 10 0 11310.32 108.37 17688.38 o
1 11 0 6554.52 95.06 7735.78 o
2 11 0 54887.12 68.72 47968.46 o
3 11 0 94944.10 81.18 90945.35 o
4 11 0 146084.48 66.59 126595.04 o
5 11 0 123116.77 66.59 109896.91 o
6 11 0 62095.66 67.73 60046.78 o
7 11 0 31162.84 84.82 32376.83 o
8 11 0 15225.09 93.12 18600.06 o
11 11 0 12694.53 154.26 15771.41 o
0 12 0 109091.48 72.25 91944.41 o
1 12 0 78809.33 84.64 79609.55 o
2 12 0 82869.14 71.74 73698.55 o
3 12 0 17929.21 95.65 19987.74 o
6 12 0 9830.72 114.06 12329.78 o
7 12 0 19262.66 89.87 21154.92 o
8 12 0 15430.61 99.20 20851.29 o
9 12 0 35377.85 108.37 38768.73 o
2 13 0 11785.27 104.24 15041.33 o
3 13 0 28981.66 116.21 27970.64 o
4 13 0 29818.38 100.20 33223.25 o
5 13 0 16837.66 134.56 19919.44 o
6 13 0 19558.02 121.66 22791.05 o
0 14 0 3543.82 183.33 3305.56 o
-15 1 1 5049.52 51.70 5706.89 o
-14 1 1 30370.03 70.73 28376.40 o
-13 1 1 115464.04 32.49 108273.46 o
-12 1 1 58791.70 78.50 54739.47 o
-11 1 1 38056.21 35.76 39630.23 o
-10 1 1 16892.20 27.25 20607.65 o
-9 1 1 14368.82 21.90 15041.33 o
-8 1 1 36656.93 20.25 37151.75 o
-7 1 1 37655.40 19.01 36011.29 o
-6 1 1 4529.29 19.27 5934.34 o
-5 1 1 7506.49 16.32 12491.36 o
-4 1 1 72889.20 11.02 83172.60 o
-3 1 1 304869.62 10.05 322132.05 o
-2 1 1 429798.25 9.67 441727.26 o
2 1 1 1452.37 10.89 834.52 o
3 1 1 127870.61 8.76 137335.79 o
4 1 1 115967.49 12.67 113668.53 o
5 1 1 78685.86 24.50 91822.28 o
6 1 1 90498.69 26.52 86789.92 o
7 1 1 120304.92 32.04 120505.89 o
8 1 1 129225.87 32.60 137604.68 o
9 1 1 98941.70 37.58 107268.24 o
10 1 1 46083.21 26.11 51179.55 o
11 1 1 11214.81 26.63 14203.43 o
13 1 1 21918.80 68.89 21911.66 o
14 1 1 27885.66 76.91 31113.47 o
15 1 1 34849.42 79.39 33828.17 o
16 1 1 12818.77 83.72 14357.50 o
17 1 1 4694.99 264.71 6841.87 o
-18 2 1 35133.75 138.77 37712.99 o
-17 2 1 65469.46 83.17 58887.43 o
-16 2 1 89072.40 71.06 82361.22 o
-15 2 1 86942.42 67.73 78838.41 o
-14 2 1 33551.25 77.79 36164.37 o
-13 2 1 24105.67 61.31 28308.57 o
-11 2 1 106106.55 52.27 104124.64 o
-10 2 1 94623.91 40.07 93145.56 o
-9 2 1 136663.30 42.25 136798.79 o
-8 2 1 261918.77 46.65 253801.88 o
-7 2 1 469444.23 37.45 476167.23 o
-6 2 1 1012599.44 29.81 905412.25 o
-5 2 1 557710.24 19.98 608677.23 o
-4 2 1 130740.10 11.76 141184.73 o
-3 2 1 41152.18 12.32 29224.22 o
-2 2 1 245242.85 10.43 235471.53 o
-1 2 1 57926.86 8.76 79746.02 o
0 2 1 1179743.55 18.06 1184520.40 o
1 2 1 1097046.76 17.56 1098528.12 o
2 2 1 601757.03 12.74 637553.38 o
3 2 1 711424.77 14.67 700479.37 o
4 2 1 513200.30 13.62 508848.82 o
5 2 1 104930.64 25.81 140006.37 o
6 2 1 95548.99 16.56 93342.41 o
8 2 1 10140.49 32.49 9585.38 o
9 2 1 82087.98 39.06 86339.46 o
10 2 1 195417.04 34.22 187208.08 o
11 2 1 256076.48 121.00 240424.14 o
12 2 1 305267.30 168.22 265586.44 o
13 2 1 190218.10 69.06 170114.88 o
14 2 1 60816.49 65.93 54720.61 o
15 2 1 6656.93 86.12 7385.48 o
-18 3 1 4066.61 222.31 4281.23 o
-16 3 1 3283.29 201.36 3145.40 o
-15 3 1 18371.09 90.82 17517.32 o
-14 3 1 88768.24 64.64 77598.92 o
-13 3 1 189390.34 58.68 173555.34 o
-12 3 1 278467.29 98.60 256978.19 o
-11 3 1 252204.84 29.81 238688.80 o
-10 3 1 215110.44 55.50 196561.32 o
-9 3 1 94648.52 35.88 97071.77 o
-8 3 1 18314.21 26.32 19086.75 o
-7 3 1 6796.35 34.81 11108.93 o
-6 3 1 103323.67 30.69 92998.07 o
-5 3 1 430401.60 28.20 432828.73 o
-4 3 1 878737.51 26.94 958143.84 o
-3 3 1 1034777.22 21.81 1047036.31 o
-2 3 1 720104.99 17.64 781394.14 o
-1 3 1 279809.26 12.53 290913.20 o
0 3 1 291157.37 12.11 302544.64 o
1 3 1 344416.40 12.89 357587.03 o
2 3 1 2726.93 27.56 2007.27 o
3 3 1 118267.21 27.98 114130.85 o
4 3 1 530406.32 20.52 551854.42 o
5 3 1 842173.29 25.60 791613.24 o
6 3 1 681631.87 44.62 669338.29 o
7 3 1 382245.43 40.83 357731.60 o
8 3 1 237919.57 39.31 248752.83 o
9 3 1 146803.92 52.42 144657.48 o
10 3 1 90799.77 58.37 95446.74 o
11 3 1 20474.75 46.38 18315.42 o
12 3 1 6385.61 65.61 7461.85 o
13 3 1 60925.05 66.26 60165.31 o
14 3 1 125741.16 69.89 109603.26 o
15 3 1 58913.00 77.09 56334.57 o
16 3 1 38990.45 81.00 36981.10 o
17 3 1 25837.35 192.38 24969.63 o
-17 4 1 29169.22 128.82 31056.64 o
-16 4 1 59087.89 89.87 52759.30 o
-15 4 1 64353.54 73.96 62964.26 o
-14 4 1 61558.57 78.32 57836.24 o
-13 4 1 41314.63 53.29 43372.05 o
-12 4 1 6112.11 70.73 6643.37 o
-11 4 1 25901.68 29.38 29458.87 o
-10 4 1 61971.12 46.51 66240.98 o
-9 4 1 137040.64 47.89 135490.58 o
-8 4 1 455800.52 51.70 464836.57 o
-7 4 1 317915.55 28.41 289654.17 o
-6 4 1 398489.19 36.48 410849.41 o
-5 4 1 248183.31 52.71 253720.70 o
-4 4 1 142129.00 36.72 116869.34 o
-3 4 1 10786.90 25.20 7594.69 o
-2 4 1 183312.42 39.82 164577.17 o
-1 4 1 94968.75 27.56 93934.20 o
0 4 1 56468.02 22.18 54194.10 o
1 4 1 447708.19 19.62 472947.64 o
2 4 1 425704.05 20.16 420251.23 o
3 4 1 1104622.02 76.04 1123327.88 o
4 4 1 1024832.28 24.50 971917.38 o
5 4 1 73072.90 26.32 103371.95 o
6 4 1 5301.30 28.84 3930.21 o
7 4 1 45220.02 28.41 48890.57 o
8 4 1 57667.22 30.69 61038.13 o
9 4 1 67044.74 51.98 67156.64 o
10 4 1 118845.67 50.41 116952.00 o
11 4 1 83289.96 37.82 80498.71 o
12 4 1 127063.73 53.44 118472.55 o
13 4 1 113683.61 80.46 105507.30 o
14 4 1 34362.04 139.95 36934.62 o
15 4 1 19689.70 91.39 21166.64 o
-14 5 1 2572.52 145.44 4016.56 o
-13 5 1 21963.24 66.26 25097.12 o
-12 5 1 49782.53 51.84 51563.08 o
-11 5 1 45560.90 33.41 42670.09 o
-10 5 1 29577.12 36.12 29833.48 o
-9 5 1 13453.68 45.83 12249.38 o
-8 5 1 13310.24 40.70 18173.93 o
-7 5 1 2591.83 43.69 1782.87 o
-6 5 1 9696.34 35.16 8722.15 o
-5 5 1 154653.43 40.70 146718.17 o
-4 5 1 118914.63 37.70 123121.38 o
-3 5 1 84844.04 32.83 100465.10 o
-2 5 1 17768.89 30.14 14405.82 o
-1 5 1 22882.61 25.10 28173.15 o
0 5 1 56088.45 31.58 50942.84 o
1 5 1 81367.56 35.88 73043.74 o
2 5 1 94206.02 27.67 93071.80 o
3 5 1 4148.65 52.27 2264.11 o
4 5 1 58883.88 74.65 51471.63 o
5 5 1 202509.00 44.62 199897.83 o
6 5 1 117731.33 43.43 121458.84 o
7 5 1 56316.04 34.34 61416.97 o
8 5 1 7712.35 37.58 7002.77 o
9 5 1 17479.48 59.44 23899.04 o
10 5 1 14522.66 54.76 13850.33 o
11 5 1 3600.00 59.75 3254.79 o
13 5 1 4774.81 59.91 5780.17 o
14 5 1 5291.11 134.79 8130.50 o
15 5 1 6400.00 143.04 6922.09 o
-10 6 1 9120.25 51.98 11348.01 o
-9 6 1 23076.65 43.30 21768.75 o
-8 6 1 28173.62 55.50 30196.45 o
-7 6 1 23648.29 44.09 27621.34 o
-6 6 1 5060.90 52.85 7131.48 o
-5 6 1 3059.20 51.70 3899.96 o
-4 6 1 31930.12 39.44 30196.45 o
-3 6 1 15321.49 64.48 17464.04 o
-2 6 1 12086.80 53.44 13604.86 o
0 6 1 4653.97 64.80 3218.12 o
1 6 1 6609.69 58.98 11159.95 o
2 6 1 17617.25 39.44 15630.05 o
3 6 1 26419.25 38.56 26350.66 o
4 6 1 3523.61 54.32 4286.51 o
5 6 1 5321.70 43.96 4999.78 o
6 6 1 8951.05 49.00 10080.75 o
8 6 1 4142.21 49.98 5780.17 o
9 6 1 2145.54 51.27 3324.12 o
-15 7 1 6355.28 122.54 6669.67 o
-14 7 1 6121.50 94.28 9233.66 o
-13 7 1 13481.53 82.26 17040.68 o
-12 7 1 25081.06 74.82 30308.57 o
-11 7 1 59340.96 75.69 63328.74 o
-10 7 1 94925.61 41.09 95995.22 o
-9 7 1 25692.88 70.73 29045.42 o
-8 7 1 6160.68 64.80 8609.64 o
-7 7 1 4188.68 67.90 6577.86 o
-6 7 1 42004.50 56.85 44012.10 o
-5 7 1 88780.16 50.98 92164.45 o
-4 7 1 59107.33 50.13 56124.38 o
-3 7 1 70097.86 46.79 69367.15 o
-2 7 1 87805.54 47.75 87957.03 o
-1 7 1 134014.57 54.91 128928.00 o
0 7 1 101098.56 49.00 106399.09 o
1 7 1 28267.70 42.51 32784.08 o
3 7 1 55088.78 46.10 49426.55 o
4 7 1 35359.04 40.20 35054.38 o
5 7 1 123692.89 54.76 127370.33 o
6 7 1 164689.87 40.07 155360.64 o
7 7 1 159352.66 52.56 159549.24 o
8 7 1 79445.06 42.38 80201.78 o
9 7 1 12108.80 57.76 15239.63 o
14 7 1 6889.00 127.69 8050.77 o
15 7 1 10096.23 184.96 14002.47 o
-15 8 1 28187.05 113.64 36133.73 o
-14 8 1 9494.55 127.24 12249.38 o
-11 8 1 7670.26 84.46 11159.95 o
-10 8 1 19257.11 65.12 26024.66 o
-9 8 1 192589.32 61.47 159131.09 o
-8 8 1 267547.56 39.82 240661.26 o
-7 8 1 381886.92 111.30 342663.90 o
-6 8 1 299362.18 74.48 269044.37 o
-5 8 1 93177.56 62.73 89613.73 o
-4 8 1 8956.73 74.30 10316.74 o
-2 8 1 23599.10 52.27 26823.66 o
-1 8 1 55752.65 47.61 49247.57 o
0 8 1 105086.19 61.31 113207.15 o
1 8 1 211646.00 64.64 187696.51 o
2 8 1 279576.56 75.52 256651.51 o
3 8 1 440272.06 56.55 456142.35 o
4 8 1 187922.25 44.89 159227.53 o
5 8 1 149830.93 48.16 141275.58 o
6 8 1 32446.82 45.97 35584.41 o
8 8 1 43701.90 47.75 43087.23 o
9 8 1 53319.43 50.98 53502.24 o
10 8 1 73565.71 70.39 72110.29 o
11 8 1 66213.58 61.78 62278.67 o
12 8 1 50153.60 73.79 58380.12 o
13 8 1 43655.92 79.57 47212.58 o
14 8 1 27702.27 133.40 29100.38 o
-14 9 1 25382.86 102.82 31184.58 o
-13 9 1 59355.58 87.80 60600.94 o
-12 9 1 76579.49 73.79 73283.50 o
-11 9 1 72484.79 76.21 71699.74 o
-10 9 1 64110.24 60.37 62097.81 o
-9 9 1 27201.90 69.39 29293.14 o
-8 9 1 16788.38 75.00 16674.51 o
-7 9 1 3282.14 78.85 3555.66 o
-6 9 1 5721.41 73.96 7601.71 o
-5 9 1 40064.03 54.32 42437.37 o
-4 9 1 113333.22 45.16 102492.96 o
-3 9 1 193116.30 64.48 180128.96 o
-2 9 1 339073.29 82.99 300597.60 o
-1 9 1 252777.67 79.57 233871.08 o
0 9 1 111375.71 58.06 106267.71 o
1 9 1 25667.24 56.40 26757.71 o
3 9 1 20641.07 57.30 22512.11 o
4 9 1 107518.41 41.99 94577.41 o
5 9 1 166635.40 42.64 151541.29 o
6 9 1 196001.00 63.68 178150.84 o
7 9 1 172889.64 71.57 149384.59 o
8 9 1 118411.69 69.22 110057.24 o
9 9 1 74425.30 59.44 71678.16 o
10 9 1 32428.81 87.05 37385.09 o
11 9 1 3245.58 112.15 5177.97 o
13 9 1 3999.30 146.17 7413.20 o
-10 10 1 8693.70 117.29 11219.62 o
-9 10 1 27370.39 73.27 30070.55 o
-8 10 1 36119.00 74.48 36872.70 o
-7 10 1 57845.06 61.94 60086.28 o
-6 10 1 104684.60 72.93 94899.84 o
-5 10 1 131681.89 70.22 118722.30 o
-4 10 1 34905.45 61.15 33326.14 o
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