#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/53/2015366.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2015366_Fobs loop_ _publ_author_name 'Nassimbeni, Luigi R.' 'Su, Hong' _publ_section_title ; Two salts of di-p-toluoyltartaric acid with aromatic amines ; _journal_coeditor_code GG1300 _journal_issue 6 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first o358 _journal_page_last o361 _journal_volume 62 _journal_year 2006 _space_group_IT_number 4 _symmetry_space_group_name_Hall 'P 2yb' _symmetry_space_group_name_H-M 'P 1 21 1' _cell_angle_alpha 90.000 _cell_angle_beta 103.324 _cell_angle_gamma 90.000 _cell_length_a 10.9366 _cell_length_b 8.0785 _cell_length_c 22.0995 _exptl_crystal_F_000 760.00 _reflns_d_resolution_high 0.7991 _[local]_cod_data_source_file gg1300Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' p21 in P2(1)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 107.45 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 3 0 0 2021.14 1887.28 20.90 o 4 0 0 250.51 209.53 2.37 o 5 0 0 80.03 89.13 1.24 o 6 0 0 106.55 118.06 1.72 o 7 0 0 52.15 51.50 1.05 o 8 0 0 146.01 140.44 2.35 o 9 0 0 0.41 2.33 0.88 o 10 0 0 1.75 0.62 1.19 o 11 0 0 150.55 139.96 2.85 o 12 0 0 6.57 -2.03 2.23 o 13 0 0 1.04 3.19 2.40 o 3 1 0 2958.71 3273.42 27.87 o 4 1 0 1168.27 1082.84 7.58 o 5 1 0 3566.63 3786.33 33.59 o 6 1 0 401.13 420.99 5.73 o 7 1 0 301.40 326.66 3.14 o 8 1 0 4.60 5.90 0.53 o 9 1 0 20.18 18.74 0.79 o 10 1 0 85.69 76.15 2.14 o 11 1 0 69.16 69.05 1.61 o 12 1 0 36.48 38.51 1.74 o 13 1 0 4.44 1.64 3.75 o 1 2 0 688.08 684.84 8.98 o 2 2 0 3272.78 3582.44 29.95 o 3 2 0 2654.42 2771.21 21.45 o 4 2 0 959.37 1038.44 7.73 o 5 2 0 161.20 158.25 1.36 o 6 2 0 7.68 17.51 0.63 o 7 2 0 141.28 153.78 2.23 o 8 2 0 109.93 107.23 1.38 o 9 2 0 149.97 155.10 2.06 o 10 2 0 86.99 89.21 1.87 o 11 2 0 64.06 62.23 1.95 o 12 2 0 33.05 44.12 2.05 o 13 2 0 13.55 9.45 3.62 o 1 3 0 3610.54 4055.18 55.48 o 2 3 0 69.92 101.15 0.94 o 3 3 0 163.48 228.04 2.03 o 4 3 0 299.14 322.82 2.51 o 5 3 0 928.32 963.97 8.37 o 6 3 0 395.21 398.01 3.36 o 7 3 0 206.50 203.81 2.04 o 8 3 0 269.31 256.74 2.86 o 9 3 0 283.62 288.96 3.60 o 10 3 0 105.50 108.17 2.60 o 11 3 0 39.50 38.66 1.59 o 12 3 0 62.91 60.67 2.17 o 0 4 0 857.90 956.08 11.78 o 1 4 0 1993.99 2200.06 24.51 o 2 4 0 564.04 585.02 5.21 o 3 4 0 367.26 359.12 3.08 o 4 4 0 91.83 103.26 1.22 o 5 4 0 94.51 78.07 1.83 o 6 4 0 707.12 706.38 6.82 o 7 4 0 1454.40 1430.60 14.50 o 8 4 0 384.47 389.10 4.46 o 9 4 0 34.25 41.99 1.38 o 10 4 0 105.63 108.40 2.33 o 11 4 0 25.75 27.30 1.88 o 12 4 0 8.87 13.31 1.98 o 1 5 0 1023.20 1025.27 13.91 o 2 5 0 371.95 347.20 3.40 o 3 5 0 317.42 311.31 3.16 o 4 5 0 41.14 45.57 1.07 o 5 5 0 650.04 627.65 6.57 o 6 5 0 392.95 379.96 4.46 o 7 5 0 133.75 128.24 2.02 o 8 5 0 228.18 209.47 7.10 o 9 5 0 54.06 49.56 1.90 o 10 5 0 73.33 76.41 2.28 o 11 5 0 10.90 10.96 1.91 o 0 6 0 1596.80 1614.84 24.11 o 1 6 0 685.66 717.85 6.87 o 2 6 0 23.24 22.12 0.75 o 3 6 0 118.12 120.78 1.69 o 4 6 0 165.95 142.31 2.00 o 5 6 0 54.25 45.24 2.38 o 6 6 0 511.35 481.92 5.97 o 7 6 0 5.70 6.10 0.94 o 8 6 0 42.59 38.67 2.55 o 9 6 0 21.27 20.63 1.98 o 10 6 0 32.89 26.47 2.71 o 1 7 0 322.66 327.75 3.62 o 2 7 0 9.20 8.18 0.78 o 3 7 0 377.17 378.55 4.34 o 4 7 0 495.13 438.69 5.63 o 5 7 0 153.51 148.28 2.49 o 6 7 0 58.06 58.76 3.93 o 7 7 0 43.45 40.51 2.83 o 8 7 0 66.73 60.85 2.29 o 9 7 0 45.37 38.25 2.69 o 0 8 0 156.24 165.40 4.00 o 1 8 0 47.48 45.12 1.63 o 2 8 0 63.53 68.64 1.77 o 3 8 0 38.34 40.44 2.92 o 4 8 0 342.77 346.07 4.21 o 5 8 0 71.77 81.81 2.20 o 6 8 0 88.42 90.98 2.60 o 7 8 0 84.51 81.82 3.61 o 8 8 0 44.83 42.76 2.94 o 1 9 0 78.90 86.66 3.20 o 2 9 0 85.74 93.76 3.36 o 3 9 0 150.00 160.75 3.33 o 4 9 0 12.84 9.03 1.86 o 5 9 0 8.37 13.21 6.85 o 6 9 0 106.25 123.65 4.20 o 0 10 0 122.47 122.52 10.99 o 1 10 0 120.66 127.84 4.48 o -13 0 1 12.43 12.57 2.42 o -12 0 1 82.65 63.87 2.72 o -11 0 1 19.43 17.31 1.52 o -10 0 1 1.26 2.82 1.19 o -9 0 1 252.35 227.60 3.37 o -8 0 1 109.69 116.08 2.09 o -7 0 1 526.28 561.05 7.67 o -6 0 1 123.44 137.75 2.22 o -5 0 1 6144.21 6499.73 98.73 o -4 0 1 13.23 11.92 0.49 o -3 0 1 5359.98 5738.25 105.20 o 2 0 1 875.78 759.05 11.41 o 3 0 1 2150.53 2612.60 28.82 o 4 0 1 1013.33 941.97 9.23 o 5 0 1 8441.56 10047.69 187.34 o 6 0 1 1061.40 925.15 11.59 o 7 0 1 400.02 427.96 5.33 o 8 0 1 134.89 103.50 1.74 o 9 0 1 9.25 12.78 0.99 o 10 0 1 52.26 54.64 1.67 o 11 0 1 0.46 2.23 1.54 o 12 0 1 37.06 39.17 2.61 o 13 0 1 8.57 8.56 2.37 o -13 1 1 59.76 48.89 2.98 o -12 1 1 36.66 32.62 1.54 o -11 1 1 41.71 32.57 1.28 o -10 1 1 13.47 11.79 1.75 o -9 1 1 83.09 86.51 1.75 o -8 1 1 39.54 35.54 0.76 o -7 1 1 227.64 190.98 2.03 o -6 1 1 165.25 182.75 1.91 o -5 1 1 120.38 118.75 1.27 o -4 1 1 1437.46 1425.49 10.96 o -3 1 1 1396.06 1239.26 10.23 o 3 1 1 645.07 644.08 5.37 o 4 1 1 152.82 193.47 1.39 o 5 1 1 405.08 398.16 3.10 o 6 1 1 243.10 295.54 2.56 o 7 1 1 130.55 124.49 1.44 o 8 1 1 82.36 72.27 1.05 o 9 1 1 14.31 11.04 1.88 o 10 1 1 68.09 56.41 1.78 o 11 1 1 76.44 67.22 1.59 o 12 1 1 21.21 15.65 1.50 o 13 1 1 26.97 33.07 2.59 o -13 2 1 2.20 1.46 1.98 o -12 2 1 20.95 14.67 2.53 o -11 2 1 48.59 43.54 1.40 o -10 2 1 103.25 110.27 1.74 o -9 2 1 240.81 221.13 4.93 o -8 2 1 2.87 3.95 0.55 o -7 2 1 206.62 200.78 2.79 o -6 2 1 26.96 40.68 0.63 o -5 2 1 142.25 132.43 1.28 o -4 2 1 1072.30 1066.23 7.93 o -3 2 1 136.56 132.51 1.10 o -2 2 1 725.96 761.82 5.91 o -1 2 1 6701.14 6648.32 210.97 o 0 2 1 5266.90 3681.50 171.99 o 1 2 1 4445.28 4382.79 48.59 o 2 2 1 2152.30 2174.32 17.04 o 3 2 1 854.32 871.89 5.97 o 4 2 1 75.54 107.22 1.79 o 5 2 1 1082.65 1082.13 8.70 o 6 2 1 295.98 310.40 2.61 o 7 2 1 482.59 455.07 3.84 o 8 2 1 114.74 111.12 1.70 o 9 2 1 41.36 40.25 1.06 o 10 2 1 133.44 139.51 2.10 o 11 2 1 192.47 174.26 2.77 o 12 2 1 3.49 4.98 1.84 o -12 3 1 6.95 11.00 3.84 o -11 3 1 288.39 281.04 3.86 o -10 3 1 32.58 25.62 1.59 o -9 3 1 37.42 40.23 1.17 o -8 3 1 452.89 446.81 4.56 o -7 3 1 528.48 493.82 4.42 o -6 3 1 610.65 567.99 4.91 o -5 3 1 147.72 150.61 1.47 o -4 3 1 428.74 418.63 3.27 o -3 3 1 2285.13 2465.46 21.94 o -2 3 1 360.06 353.19 2.62 o -1 3 1 313.62 362.46 2.88 o 0 3 1 2377.08 2485.98 27.86 o 1 3 1 166.70 150.54 1.09 o 2 3 1 578.29 590.61 6.39 o 3 3 1 878.55 911.12 14.12 o 4 3 1 109.87 131.23 1.21 o 5 3 1 46.74 45.15 1.45 o 6 3 1 840.31 892.08 7.31 o 7 3 1 477.86 466.86 4.44 o 8 3 1 677.16 680.48 6.70 o 9 3 1 49.82 52.66 1.33 o 10 3 1 102.77 111.46 2.05 o 11 3 1 54.21 61.58 1.94 o 12 3 1 42.82 40.31 2.15 o -12 4 1 30.75 31.82 2.10 o -11 4 1 12.37 16.14 1.49 o -10 4 1 59.72 60.54 1.71 o -9 4 1 146.91 151.92 2.42 o -8 4 1 767.69 723.88 7.81 o -7 4 1 393.53 412.88 4.55 o -6 4 1 249.37 267.77 3.90 o -5 4 1 214.36 213.01 2.17 o -4 4 1 237.80 252.62 3.16 o -3 4 1 29.38 42.51 0.54 o -2 4 1 1186.27 1350.46 11.97 o -1 4 1 1766.24 2008.44 18.14 o 0 4 1 903.69 938.16 11.19 o 1 4 1 2168.19 2323.37 20.43 o 2 4 1 296.37 326.15 2.70 o 3 4 1 1692.44 1705.69 12.98 o 4 4 1 824.90 784.19 6.81 o 5 4 1 4.84 7.27 0.35 o 6 4 1 535.47 512.75 5.21 o 7 4 1 58.62 55.95 1.18 o 8 4 1 260.22 252.27 3.10 o 9 4 1 175.55 175.87 2.67 o 10 4 1 7.43 11.03 1.51 o 11 4 1 50.76 54.77 2.13 o 12 4 1 2.32 4.70 2.14 o -11 5 1 6.35 4.76 1.72 o -10 5 1 32.25 36.16 1.89 o -9 5 1 102.12 91.99 2.10 o -8 5 1 139.46 143.67 2.16 o -7 5 1 182.27 171.49 2.36 o -6 5 1 353.50 337.86 3.92 o -5 5 1 125.47 112.56 2.39 o -4 5 1 319.03 339.18 6.15 o -3 5 1 163.31 168.31 1.78 o -2 5 1 353.98 383.64 3.45 o -1 5 1 189.22 177.08 1.79 o 0 5 1 720.94 722.75 9.12 o 1 5 1 830.45 787.30 9.83 o 2 5 1 565.39 557.26 5.32 o 3 5 1 118.97 120.78 1.21 o 4 5 1 183.43 184.92 2.17 o 5 5 1 290.59 287.04 3.52 o 6 5 1 6.81 11.95 0.85 o 7 5 1 23.57 22.32 1.08 o 8 5 1 194.15 195.55 3.07 o 9 5 1 42.33 36.39 1.77 o 10 5 1 26.89 19.56 1.82 o 11 5 1 15.99 13.59 2.01 o -10 6 1 81.45 94.18 3.28 o -9 6 1 61.86 62.19 2.37 o -8 6 1 49.77 48.27 1.91 o -7 6 1 25.59 24.57 1.40 o -6 6 1 74.11 67.23 1.61 o -5 6 1 386.33 379.81 4.75 o -4 6 1 255.94 227.85 2.94 o -3 6 1 452.68 450.16 7.96 o -2 6 1 230.79 221.18 2.39 o -1 6 1 943.88 915.88 8.63 o 0 6 1 89.60 92.10 1.22 o 1 6 1 299.61 282.81 2.91 o 2 6 1 239.32 243.68 3.00 o 3 6 1 64.12 76.11 2.89 o 4 6 1 479.38 493.11 5.61 o 5 6 1 94.61 96.69 1.69 o 6 6 1 243.87 241.02 3.30 o 7 6 1 22.05 18.09 1.26 o 8 6 1 41.46 49.89 1.76 o 9 6 1 6.65 7.78 2.12 o 10 6 1 12.79 11.58 2.40 o -9 7 1 57.65 52.97 2.80 o -8 7 1 12.74 14.25 2.02 o -7 7 1 39.18 42.37 2.99 o -6 7 1 98.16 95.89 2.09 o -5 7 1 5.68 5.68 2.59 o -4 7 1 31.19 29.90 1.14 o -3 7 1 182.39 164.59 2.25 o -2 7 1 17.42 19.41 0.87 o -1 7 1 429.01 449.06 4.83 o 0 7 1 969.82 936.00 9.87 o 1 7 1 641.44 646.05 7.03 o 2 7 1 59.56 57.66 1.24 o 3 7 1 7.27 6.22 0.80 o 4 7 1 44.91 47.62 1.34 o 5 7 1 100.67 93.22 2.62 o 6 7 1 87.90 77.95 2.21 o 7 7 1 89.27 82.13 2.25 o 8 7 1 0.35 4.84 1.95 o 9 7 1 2.13 -0.54 1.98 o -8 8 1 27.01 26.23 2.95 o -7 8 1 5.29 5.60 1.95 o -6 8 1 49.91 48.18 2.33 o -5 8 1 247.34 238.43 3.76 o -4 8 1 415.54 431.42 5.35 o -3 8 1 137.24 136.18 2.22 o -2 8 1 128.85 120.14 2.20 o -1 8 1 234.06 243.78 3.67 o 0 8 1 19.45 23.62 1.91 o 1 8 1 127.77 120.18 2.28 o 2 8 1 69.53 71.40 1.72 o 3 8 1 18.16 15.14 1.02 o 4 8 1 55.13 60.92 1.66 o 5 8 1 58.21 53.74 2.09 o 6 8 1 77.43 80.13 2.53 o 7 8 1 31.65 23.99 1.91 o 8 8 1 42.84 36.12 4.20 o -6 9 1 140.08 153.77 4.52 o -5 9 1 103.72 132.70 3.69 o -4 9 1 32.13 25.91 1.99 o -3 9 1 29.51 31.77 2.12 o -2 9 1 74.77 71.20 2.66 o -1 9 1 133.42 136.15 3.25 o 0 9 1 6.40 9.32 2.88 o 1 9 1 151.11 138.22 2.84 o 2 9 1 186.47 193.44 4.08 o 3 9 1 105.08 119.52 3.24 o 4 9 1 57.91 48.73 2.43 o 5 9 1 64.22 73.48 3.39 o -2 10 1 165.56 194.84 10.35 o -1 10 1 115.00 115.61 4.22 o 0 10 1 24.38 24.48 4.11 o 1 10 1 5.62 4.27 2.49 o -13 0 2 1.60 0.91 2.34 o -12 0 2 0.00 0.38 1.89 o -11 0 2 18.13 24.34 1.64 o -10 0 2 3.32 3.06 1.13 o -9 0 2 0.69 7.85 0.99 o -8 0 2 85.21 98.87 2.10 o -7 0 2 147.51 155.70 2.87 o -6 0 2 7.76 7.27 1.03 o -5 0 2 6886.46 7971.38 181.78 o -4 0 2 5790.42 5769.77 90.74 o -3 0 2 2352.93 2505.03 31.38 o 2 0 2 893.65 1094.57 13.22 o 3 0 2 38.38 40.19 1.17 o 4 0 2 212.44 171.69 1.79 o 5 0 2 13.43 28.20 0.77 o 6 0 2 218.36 261.51 3.44 o 7 0 2 146.50 136.70 2.03 o 8 0 2 42.00 47.82 1.31 o 9 0 2 66.95 64.72 1.77 o 10 0 2 526.39 486.71 6.90 o 11 0 2 135.59 152.06 3.31 o 12 0 2 61.40 60.77 2.64 o 13 0 2 59.80 56.95 4.06 o -13 1 2 12.19 14.01 1.80 o -12 1 2 5.35 6.82 1.20 o -11 1 2 71.68 57.82 1.53 o -10 1 2 58.45 67.98 3.59 o -9 1 2 28.11 24.03 0.91 o -8 1 2 291.81 268.52 3.09 o -7 1 2 12.95 18.43 0.66 o -6 1 2 2459.29 2489.51 22.51 o -5 1 2 1538.09 1693.07 14.81 o -4 1 2 2055.17 2175.06 17.43 o -3 1 2 4772.68 4638.68 42.20 o 2 1 2 1147.57 1055.27 13.20 o 3 1 2 1319.69 1171.80 7.98 o 4 1 2 1206.54 1184.95 7.91 o 5 1 2 298.83 307.63 2.64 o 6 1 2 1161.77 1157.84 8.90 o 7 1 2 154.96 169.42 1.62 o 8 1 2 12.94 13.82 0.63 o 9 1 2 501.76 459.71 4.42 o 10 1 2 153.97 168.01 2.25 o 11 1 2 82.41 75.13 3.40 o 12 1 2 29.24 23.04 1.61 o -13 2 2 10.28 10.22 2.19 o -12 2 2 21.14 22.43 1.60 o -11 2 2 23.15 18.87 1.20 o -10 2 2 376.08 372.50 4.16 o -9 2 2 471.80 486.93 4.98 o -8 2 2 180.88 182.01 2.04 o -7 2 2 491.44 497.67 4.51 o -6 2 2 512.51 490.97 4.20 o -5 2 2 93.59 85.64 0.83 o -4 2 2 484.00 531.75 4.09 o -3 2 2 5659.24 6104.21 65.34 o -2 2 2 533.85 620.89 9.89 o 0 2 2 558.66 507.07 9.91 o 1 2 2 5893.59 6285.42 141.24 o 2 2 2 434.64 476.22 3.22 o 3 2 2 358.64 368.05 3.06 o 4 2 2 237.11 277.50 2.06 o 5 2 2 23.97 24.23 0.41 o 6 2 2 64.30 86.57 0.93 o 7 2 2 564.37 551.25 4.65 o 8 2 2 289.00 297.33 2.91 o 9 2 2 21.45 22.59 0.98 o 10 2 2 186.56 178.34 2.53 o 11 2 2 23.12 20.11 1.83 o 12 2 2 62.80 59.83 2.08 o -12 3 2 45.74 46.30 2.73 o -11 3 2 29.19 20.36 1.38 o -10 3 2 61.59 59.10 1.53 o -9 3 2 723.75 707.88 7.51 o -8 3 2 98.47 105.05 1.46 o -7 3 2 8.02 9.56 0.81 o -6 3 2 603.78 593.51 5.01 o -5 3 2 2131.49 2276.85 19.64 o -4 3 2 1368.48 1467.08 12.23 o -3 3 2 2278.66 2353.27 22.24 o -2 3 2 1931.33 2115.57 14.32 o -1 3 2 3784.17 4016.17 36.63 o 0 3 2 62.48 65.97 0.66 o 1 3 2 936.69 910.34 9.64 o 2 3 2 1567.90 1522.23 14.62 o 3 3 2 1275.10 1246.39 9.35 o 4 3 2 959.81 960.27 7.68 o 5 3 2 1281.19 1208.34 9.36 o 6 3 2 75.62 74.02 0.87 o 7 3 2 721.32 710.83 6.50 o 8 3 2 182.23 183.93 2.16 o 9 3 2 190.63 192.74 2.70 o 10 3 2 81.15 79.53 1.90 o 11 3 2 45.98 32.80 1.74 o 12 3 2 41.41 47.55 3.55 o -12 4 2 13.75 12.09 2.00 o -11 4 2 145.52 125.97 2.54 o -10 4 2 167.85 157.28 2.81 o -9 4 2 9.91 9.35 1.13 o -8 4 2 300.51 299.16 3.52 o -7 4 2 353.22 342.94 3.99 o -6 4 2 118.53 114.44 1.72 o -5 4 2 48.06 38.51 0.79 o -4 4 2 726.11 694.99 6.57 o -3 4 2 1771.15 1840.81 15.34 o -2 4 2 667.83 692.95 6.31 o -1 4 2 1340.95 1436.16 11.67 o 0 4 2 359.98 318.15 3.42 o 1 4 2 535.01 532.73 3.82 o 2 4 2 317.74 312.69 3.50 o 3 4 2 36.17 43.16 0.50 o 4 4 2 1075.50 1133.06 9.86 o 5 4 2 74.33 71.26 1.42 o 6 4 2 318.05 314.43 5.38 o 7 4 2 222.67 213.96 2.62 o 8 4 2 259.14 253.34 3.29 o 9 4 2 125.58 123.46 2.54 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50.78 48.27 4.68 o -6 1 23 14.90 13.21 1.30 o -5 1 23 32.04 34.34 1.56 o -4 1 23 40.19 42.84 1.55 o -3 1 23 57.03 49.74 1.74 o -2 1 23 55.70 46.78 2.24 o -1 1 23 9.82 10.13 1.32 o 0 1 23 49.06 42.49 1.71 o 1 1 23 75.81 75.34 3.77 o 2 1 23 34.33 30.57 1.97 o 3 1 23 94.87 86.12 4.99 o 4 1 23 72.08 81.83 3.53 o -9 2 23 41.55 39.24 3.42 o -8 2 23 34.78 31.50 1.89 o -7 2 23 21.67 20.40 2.52 o -6 2 23 64.91 72.62 1.93 o -5 2 23 47.51 45.93 1.57 o -4 2 23 167.42 166.88 3.74 o -3 2 23 256.61 243.20 4.51 o -2 2 23 163.12 162.33 4.29 o -1 2 23 64.72 61.56 2.62 o 0 2 23 40.50 42.15 1.87 o 1 2 23 102.42 101.62 2.38 o 2 2 23 33.20 33.63 2.25 o 3 2 23 14.34 11.81 1.69 o 4 2 23 1.21 2.46 2.13 o -8 3 23 12.25 8.42 1.77 o -7 3 23 18.15 19.55 1.74 o -6 3 23 23.16 24.09 1.66 o -5 3 23 0.63 2.11 1.61 o -4 3 23 85.46 81.81 3.37 o -3 3 23 214.96 233.82 6.18 o -2 3 23 297.48 320.95 4.45 o -1 3 23 7.10 12.62 2.15 o 0 3 23 29.66 31.46 4.02 o 1 3 23 4.84 1.17 1.53 o 2 3 23 1.33 2.45 1.58 o 3 3 23 29.34 40.09 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