#------------------------------------------------------------------------------ #$Date: 2016-04-02 22:05:32 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180822 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/53/2015384.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2015384_Fobs loop_ _publ_author_name 'Banerjee, Rahul' 'Saha, Binoy K.' 'Desiraju, Gautam R.' _publ_section_title ; Solid-state architecture of saccharin salts of some diamines ; _journal_coeditor_code SF3006 _journal_issue 6 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first o346 _journal_page_last o349 _journal_volume 62 _journal_year 2006 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 109.196 _cell_angle_gamma 90.000 _cell_length_a 9.0016 _cell_length_b 11.2539 _cell_length_c 10.0269 _exptl_crystal_F_000 476.00 _reflns_d_resolution_high 0.8121 _cod_data_source_file sf3006IIIsup4.hkl _cod_data_source_block III #BEGIN Tags that were not found in dictionaries: _shelx_title ' grd85_m in P2(1)/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 167.30 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 0.21 -0.10 0.22 o 4 0 0 596.50 520.61 8.66 o 6 0 0 37.61 29.55 1.27 o 8 0 0 392.97 371.43 11.05 o 10 0 0 177.55 190.63 7.63 o 1 1 0 0.68 2.72 0.42 o 2 1 0 7.22 6.97 0.27 o 3 1 0 68.41 58.88 1.01 o 4 1 0 1000.32 1074.77 12.06 o 5 1 0 440.44 437.42 5.38 o 6 1 0 664.27 734.65 8.71 o 7 1 0 516.55 555.62 8.24 o 8 1 0 962.65 1016.59 17.91 o 9 1 0 3.20 3.45 1.03 o 10 1 0 32.19 37.48 2.25 o 0 2 0 5975.21 5299.13 117.48 o 1 2 0 2622.86 2683.47 50.70 o 2 2 0 1530.34 1361.17 24.72 o 3 2 0 11.40 8.48 0.32 o 4 2 0 100.09 141.71 3.94 o 5 2 0 1.22 2.41 0.27 o 6 2 0 1765.82 1818.67 23.78 o 7 2 0 1163.92 1241.53 20.39 o 8 2 0 994.89 1015.00 17.90 o 9 2 0 269.86 271.13 6.50 o 10 2 0 9.64 7.85 1.33 o 1 3 0 3935.73 3844.91 109.36 o 2 3 0 0.01 0.38 0.51 o 3 3 0 446.19 447.13 6.25 o 4 3 0 0.33 1.14 0.32 o 5 3 0 14.07 13.69 0.84 o 6 3 0 148.41 161.11 3.12 o 7 3 0 104.70 106.90 2.61 o 8 3 0 376.23 392.87 11.74 o 9 3 0 39.13 35.16 3.00 o 10 3 0 16.56 21.56 2.73 o 0 4 0 5450.09 4973.29 197.69 o 1 4 0 273.01 260.81 3.31 o 2 4 0 13.85 22.58 0.78 o 3 4 0 426.23 465.20 6.48 o 4 4 0 60.45 41.69 1.17 o 5 4 0 204.53 190.22 3.71 o 6 4 0 820.61 825.47 11.53 o 7 4 0 646.47 664.38 11.98 o 8 4 0 54.37 43.51 2.01 o 9 4 0 13.73 15.64 1.44 o 10 4 0 5.47 5.54 1.79 o 1 5 0 79.40 108.93 1.68 o 2 5 0 264.29 241.41 3.68 o 3 5 0 9.10 5.11 0.50 o 4 5 0 596.21 598.13 8.33 o 5 5 0 171.37 163.61 3.86 o 6 5 0 84.98 80.07 4.61 o 7 5 0 286.21 288.48 6.29 o 8 5 0 272.56 273.71 13.16 o 9 5 0 11.77 10.62 1.26 o 0 6 0 53.60 36.17 0.93 o 1 6 0 258.34 278.14 3.66 o 2 6 0 993.19 1013.03 13.09 o 3 6 0 62.56 75.30 2.16 o 4 6 0 166.86 152.22 3.62 o 5 6 0 4.98 5.50 0.81 o 6 6 0 2056.84 2096.23 33.67 o 7 6 0 24.07 24.49 3.05 o 8 6 0 127.60 123.38 6.19 o 9 6 0 226.24 251.18 6.23 o 1 7 0 610.92 623.01 7.57 o 2 7 0 14.04 16.85 0.73 o 3 7 0 301.47 284.50 7.43 o 4 7 0 1.05 1.43 0.59 o 5 7 0 385.62 395.74 8.18 o 6 7 0 1149.88 1147.07 19.48 o 7 7 0 0.14 1.14 0.67 o 8 7 0 64.46 55.84 2.52 o 9 7 0 16.96 17.03 1.60 o 0 8 0 1509.52 1599.07 33.97 o 1 8 0 1071.88 1114.89 47.70 o 2 8 0 209.34 211.80 4.36 o 3 8 0 52.61 48.13 2.01 o 4 8 0 367.70 355.28 13.92 o 5 8 0 136.47 133.85 4.48 o 6 8 0 316.20 308.43 6.75 o 7 8 0 77.94 77.81 3.22 o 8 8 0 228.08 245.50 6.13 o 1 9 0 810.33 775.09 16.28 o 2 9 0 55.80 43.07 2.53 o 3 9 0 2068.20 2084.66 46.22 o 4 9 0 130.25 130.87 3.55 o 5 9 0 20.08 16.43 1.34 o 6 9 0 28.01 29.07 1.77 o 7 9 0 484.81 525.61 10.53 o 0 10 0 278.37 277.72 6.14 o 1 10 0 137.14 115.93 3.39 o 2 10 0 16.72 18.93 1.89 o 3 10 0 177.77 172.22 6.08 o 4 10 0 15.67 15.60 1.89 o 5 10 0 453.95 433.35 12.38 o 6 10 0 57.54 52.35 2.40 o 7 10 0 84.79 85.13 3.23 o 1 11 0 285.15 274.76 5.42 o 2 11 0 17.61 14.08 1.67 o 3 11 0 429.55 425.06 11.86 o 4 11 0 66.15 59.40 3.52 o 5 11 0 278.66 278.27 9.13 o 6 11 0 5.49 3.29 1.33 o 0 12 0 0.53 -0.86 0.90 o 1 12 0 0.33 0.87 0.57 o 2 12 0 0.34 0.33 0.67 o 3 12 0 4.17 5.24 1.34 o 4 12 0 3.24 1.58 1.08 o 5 12 0 18.02 14.04 2.08 o 1 13 0 55.68 54.90 2.99 o 2 13 0 35.88 37.92 2.17 o 3 13 0 569.95 582.82 12.40 o -9 0 1 29.51 33.13 2.76 o -7 0 1 108.20 94.55 2.56 o -5 0 1 368.12 365.26 6.46 o -3 0 1 608.60 680.71 15.04 o -1 0 1 858.18 916.11 14.18 o 1 0 1 5271.44 5127.07 79.98 o 3 0 1 5551.25 5669.96 86.15 o 5 0 1 1122.16 1113.98 17.91 o 7 0 1 1111.30 1094.44 26.74 o 9 0 1 957.02 1011.94 25.90 o -10 1 1 132.23 135.78 4.99 o -9 1 1 10.06 11.69 1.34 o -8 1 1 49.09 45.51 2.14 o -7 1 1 2448.82 2463.30 31.86 o -6 1 1 1.23 0.85 0.39 o -5 1 1 4651.62 4911.36 52.99 o -4 1 1 225.40 246.87 3.17 o -3 1 1 443.85 408.06 4.78 o -2 1 1 361.87 399.80 4.57 o -1 1 1 5720.86 5299.57 58.53 o 0 1 1 35.18 17.61 0.41 o 1 1 1 495.91 487.56 5.49 o 2 1 1 9735.00 9293.16 101.43 o 3 1 1 241.31 318.01 3.87 o 4 1 1 229.57 229.26 3.06 o 5 1 1 16.63 26.23 0.79 o 6 1 1 3.75 3.30 1.00 o 7 1 1 623.65 617.52 9.09 o 8 1 1 34.60 35.34 2.10 o 9 1 1 526.29 557.03 11.19 o 10 1 1 3.67 3.26 1.10 o -10 2 1 129.19 132.12 8.71 o -9 2 1 135.08 129.88 5.34 o -8 2 1 16.71 18.46 1.10 o -7 2 1 140.96 155.90 3.12 o -6 2 1 818.55 848.10 11.68 o -5 2 1 30.69 34.43 0.83 o -4 2 1 175.48 158.16 2.18 o -3 2 1 153.85 108.95 1.77 o -2 2 1 165.35 170.32 2.43 o -1 2 1 92.04 99.40 1.29 o 0 2 1 2.53 0.44 0.19 o 1 2 1 27990.40 22671.84 514.92 o 2 2 1 243.71 243.49 2.97 o 3 2 1 35.00 46.58 1.03 o 4 2 1 114.62 126.11 1.88 o 5 2 1 1760.24 1788.54 23.29 o 6 2 1 27.34 30.33 1.20 o 7 2 1 0.20 0.65 0.47 o 8 2 1 454.85 470.33 11.07 o 9 2 1 257.35 266.57 6.48 o 10 2 1 91.67 89.38 3.52 o -10 3 1 6.08 3.43 1.46 o -9 3 1 119.25 108.27 5.28 o -8 3 1 62.47 65.33 2.36 o -7 3 1 1381.91 1419.01 19.02 o -6 3 1 1696.87 1838.74 25.42 o -5 3 1 11.93 15.81 0.79 o -4 3 1 205.24 206.44 2.71 o -3 3 1 242.52 200.68 2.56 o -2 3 1 29.65 44.22 0.76 o -1 3 1 35.15 25.16 0.59 o 0 3 1 3116.35 3207.18 53.01 o 1 3 1 10118.61 9362.42 226.15 o 2 3 1 3566.93 3723.43 40.52 o 3 3 1 374.55 480.85 6.72 o 4 3 1 436.56 453.16 10.66 o 5 3 1 1.98 1.03 0.40 o 6 3 1 400.86 370.40 13.35 o 7 3 1 919.46 920.19 16.15 o 8 3 1 222.88 236.91 4.52 o 9 3 1 108.44 108.58 5.37 o -10 4 1 47.04 53.49 3.95 o -9 4 1 3.07 4.22 1.89 o -8 4 1 32.92 32.73 1.91 o -7 4 1 81.95 74.14 3.26 o -6 4 1 617.59 634.87 13.37 o -5 4 1 27.93 29.58 1.07 o -4 4 1 213.92 218.03 2.84 o -3 4 1 66.59 51.86 1.17 o -2 4 1 396.13 459.06 5.31 o -1 4 1 972.77 863.46 9.98 o 0 4 1 285.32 341.61 4.17 o 1 4 1 1036.97 1236.21 12.53 o 2 4 1 685.23 737.11 8.33 o 3 4 1 139.21 122.37 2.23 o 4 4 1 192.42 205.81 3.46 o 5 4 1 62.66 52.03 1.51 o 6 4 1 206.20 207.79 6.71 o 7 4 1 2213.67 2248.59 36.01 o 8 4 1 82.50 79.07 3.70 o 9 4 1 110.58 93.26 5.08 o -10 5 1 2.95 4.08 1.67 o -9 5 1 200.91 199.09 9.95 o -8 5 1 6.29 5.85 0.96 o -7 5 1 2040.32 2113.48 33.98 o -6 5 1 1.43 1.87 0.86 o -5 5 1 176.77 149.96 6.81 o -4 5 1 67.96 70.45 1.54 o -3 5 1 277.43 323.21 3.92 o -2 5 1 280.69 310.60 4.42 o -1 5 1 1008.70 1022.65 11.83 o 0 5 1 8.99 2.02 0.20 o 1 5 1 1996.76 2211.03 22.19 o 2 5 1 596.94 690.56 7.86 o 3 5 1 64.71 83.34 2.50 o 4 5 1 24.15 23.67 0.94 o 5 5 1 141.54 124.95 3.32 o 6 5 1 1.41 2.11 0.72 o 7 5 1 0.57 -0.19 0.61 o 8 5 1 42.74 46.10 2.18 o 9 5 1 4.52 5.85 1.04 o -9 6 1 7.51 6.35 1.09 o -8 6 1 28.84 28.12 2.53 o -7 6 1 19.40 20.51 1.47 o -6 6 1 679.50 682.32 16.91 o -5 6 1 69.24 61.28 2.16 o -4 6 1 130.18 124.93 5.22 o -3 6 1 320.10 304.00 4.46 o -2 6 1 13.61 6.43 0.45 o -1 6 1 974.58 988.88 11.54 o 0 6 1 887.36 929.91 9.64 o 1 6 1 521.57 542.46 5.83 o 2 6 1 6.36 12.10 0.73 o 3 6 1 28.41 26.39 1.80 o 4 6 1 781.17 782.69 14.20 o 5 6 1 1522.56 1529.10 24.94 o 6 6 1 60.47 57.51 2.28 o 7 6 1 582.54 565.09 10.81 o 8 6 1 63.82 62.90 4.35 o 9 6 1 101.62 106.89 5.00 o -9 7 1 512.30 526.26 10.70 o -8 7 1 30.35 29.46 1.86 o -7 7 1 935.00 930.42 16.43 o -6 7 1 44.29 42.24 2.18 o -5 7 1 11.13 9.56 1.03 o -4 7 1 3.65 3.89 0.70 o -3 7 1 409.01 407.86 7.48 o -2 7 1 247.20 232.81 3.62 o -1 7 1 743.46 790.65 9.43 o 0 7 1 34.52 26.10 0.60 o 1 7 1 1919.04 2058.51 23.38 o 2 7 1 502.68 467.51 8.30 o 3 7 1 1.91 0.78 0.53 o 4 7 1 323.78 310.64 11.71 o 5 7 1 28.80 34.71 1.75 o 6 7 1 0.60 0.45 0.57 o 7 7 1 3.10 2.69 0.86 o 8 7 1 845.85 896.63 16.33 o -8 8 1 430.36 455.57 9.50 o -7 8 1 0.20 0.42 0.65 o -6 8 1 305.00 293.47 10.85 o -5 8 1 617.69 620.53 11.29 o -4 8 1 2009.70 1859.21 109.06 o -3 8 1 5.82 7.23 1.58 o -2 8 1 253.25 220.34 3.54 o -1 8 1 751.53 749.49 10.63 o 0 8 1 310.99 326.28 4.69 o 1 8 1 69.34 67.85 1.93 o 2 8 1 1.92 2.68 0.98 o 3 8 1 214.01 202.76 4.51 o 4 8 1 23.82 19.51 1.36 o 5 8 1 1067.81 1064.90 18.20 o 6 8 1 14.68 12.53 1.43 o 7 8 1 331.92 308.82 17.06 o 8 8 1 1.01 2.75 1.08 o -8 9 1 59.16 67.80 2.90 o -7 9 1 209.91 199.25 5.25 o -6 9 1 0.15 0.24 0.64 o -5 9 1 237.43 230.29 5.33 o -4 9 1 255.69 246.90 5.38 o -3 9 1 4.24 5.54 1.21 o -2 9 1 240.25 218.95 6.62 o -1 9 1 835.50 861.72 12.23 o 0 9 1 1309.94 1306.22 16.09 o 1 9 1 6.63 6.19 0.76 o 2 9 1 927.57 961.31 22.63 o 3 9 1 1.00 2.48 1.11 o 4 9 1 446.40 452.87 8.75 o 5 9 1 6.36 5.61 0.97 o 6 9 1 207.74 220.99 5.88 o 7 9 1 0.93 0.50 0.65 o -7 10 1 102.36 114.77 7.30 o -6 10 1 52.81 54.19 8.51 o -5 10 1 38.93 36.30 2.69 o -4 10 1 1050.00 1009.75 24.21 o -3 10 1 211.71 197.97 6.58 o -2 10 1 714.61 696.09 17.04 o -1 10 1 8.58 10.19 1.15 o 0 10 1 295.58 304.49 4.66 o 1 10 1 0.12 0.19 0.48 o 2 10 1 4.79 5.14 1.19 o 3 10 1 14.87 9.23 1.53 o 4 10 1 168.42 150.39 5.79 o 5 10 1 59.51 58.38 3.56 o 6 10 1 0.96 1.98 0.81 o -6 11 1 146.39 153.87 6.38 o -5 11 1 99.83 81.33 4.26 o -4 11 1 64.98 58.19 3.39 o -3 11 1 10.65 8.54 1.50 o -2 11 1 461.68 462.57 12.32 o -1 11 1 75.48 81.35 2.44 o 0 11 1 40.36 30.98 1.47 o 1 11 1 87.33 90.49 2.64 o 2 11 1 859.04 851.56 17.05 o 3 11 1 13.33 12.31 1.71 o 4 11 1 459.90 465.85 13.14 o 5 11 1 0.37 1.21 1.15 o -5 12 1 109.11 96.69 4.85 o -4 12 1 388.61 384.40 11.43 o -3 12 1 3.91 3.28 1.18 o -2 12 1 535.53 533.19 11.09 o -1 12 1 85.39 78.93 3.46 o 0 12 1 85.66 82.32 3.53 o 1 12 1 61.17 58.45 2.16 o 2 12 1 20.24 13.96 1.48 o 3 12 1 14.30 11.09 1.83 o 4 12 1 233.51 237.36 8.31 o -3 13 1 4.95 4.53 1.34 o -2 13 1 6.65 10.60 1.36 o -1 13 1 196.44 194.44 8.84 o 0 13 1 83.63 84.95 3.89 o 1 13 1 16.94 18.42 1.91 o 2 13 1 5.14 2.38 0.91 o 3 13 1 157.03 151.89 10.64 o -10 0 2 72.02 74.33 4.33 o -8 0 2 513.05 493.90 13.61 o -6 0 2 4664.29 4929.52 75.42 o -4 0 2 690.20 782.43 12.63 o -2 0 2 1.19 1.48 0.40 o 0 0 2 4.15 -0.05 0.22 o 2 0 2 3580.19 3974.32 88.44 o 4 0 2 2581.71 2815.73 43.43 o 6 0 2 979.60 1057.41 20.56 o 8 0 2 289.10 263.99 8.89 o -10 1 2 120.44 121.27 4.00 o -9 1 2 1.78 0.90 0.79 o -8 1 2 405.78 380.54 15.61 o -7 1 2 315.53 317.34 5.16 o -6 1 2 403.00 333.74 4.37 o -5 1 2 1355.85 1446.21 16.13 o -4 1 2 3154.33 3261.80 35.31 o -3 1 2 67.16 75.14 1.61 o -2 1 2 11228.45 10393.22 141.61 o -1 1 2 405.65 369.96 4.29 o 0 1 2 4592.28 4563.24 41.09 o 1 1 2 1715.72 1735.06 26.18 o 2 1 2 462.34 361.96 4.37 o 3 1 2 5.12 4.82 0.40 o 4 1 2 85.16 64.49 1.26 o 5 1 2 409.35 403.74 9.69 o 6 1 2 468.80 436.58 7.39 o 7 1 2 461.18 457.99 9.65 o 8 1 2 1246.43 1239.29 21.63 o 9 1 2 18.11 17.41 2.78 o -10 2 2 55.60 62.55 2.80 o -9 2 2 291.41 291.26 6.68 o -8 2 2 382.15 383.59 6.22 o -7 2 2 43.51 43.34 1.81 o -6 2 2 813.68 811.49 16.53 o -5 2 2 356.24 331.40 4.22 o -4 2 2 248.21 282.01 3.57 o -3 2 2 3429.49 3615.10 34.71 o -2 2 2 619.07 727.75 8.17 o -1 2 2 10.99 8.58 0.34 o 0 2 2 2859.72 3355.86 37.45 o 1 2 2 1229.19 1287.45 13.99 o 2 2 2 112.95 120.45 1.85 o 3 2 2 5.95 6.57 0.42 o 4 2 2 2186.15 2333.38 25.58 o 5 2 2 33.67 38.55 1.29 o 6 2 2 0.11 1.77 1.14 o 7 2 2 16.68 18.93 1.09 o 8 2 2 409.40 411.22 8.69 o 9 2 2 0.03 -0.69 0.69 o -10 3 2 9.13 11.60 2.13 o -9 3 2 342.86 324.08 6.99 o -8 3 2 90.31 90.12 2.89 o -7 3 2 87.17 84.95 5.01 o -6 3 2 564.74 509.96 7.47 o -5 3 2 190.20 179.33 2.21 o -4 3 2 768.64 772.31 7.83 o -3 3 2 25.81 20.44 0.57 o -2 3 2 771.33 734.60 8.26 o -1 3 2 0.19 -0.17 0.17 o 0 3 2 499.73 461.72 4.93 o 1 3 2 1896.18 2168.23 21.74 o 2 3 2 96.75 80.31 1.28 o 3 3 2 2887.06 3292.78 35.73 o 4 3 2 319.90 281.34 4.48 o 5 3 2 166.72 163.15 3.11 o 6 3 2 1214.99 1198.29 16.33 o 7 3 2 260.93 262.12 6.78 o 8 3 2 277.74 254.70 14.86 o 9 3 2 124.18 115.33 5.71 o -10 4 2 68.77 59.79 4.10 o -9 4 2 213.92 211.14 5.26 o -8 4 2 1.73 2.51 0.90 o -7 4 2 97.26 95.44 4.25 o -6 4 2 741.96 747.69 10.47 o -5 4 2 374.97 345.79 5.26 o -4 4 2 10.68 10.59 0.46 o -3 4 2 389.93 440.45 5.21 o -2 4 2 90.87 103.46 1.53 o -1 4 2 243.80 210.13 2.84 o 0 4 2 2596.91 2892.85 28.88 o 1 4 2 117.54 127.21 1.69 o 2 4 2 1140.05 1176.11 11.61 o 3 4 2 775.40 764.35 11.00 o 4 4 2 0.04 0.29 0.33 o 5 4 2 278.28 280.92 5.19 o 6 4 2 114.73 113.82 2.63 o 7 4 2 22.13 17.75 1.36 o 8 4 2 87.75 76.81 2.81 o 9 4 2 142.19 144.76 6.64 o -10 5 2 36.70 40.09 2.18 o -9 5 2 15.57 15.82 1.42 o -8 5 2 680.56 676.53 13.32 o -7 5 2 7.14 6.89 0.98 o -6 5 2 269.36 239.86 5.25 o -5 5 2 453.24 466.41 26.54 o -4 5 2 109.25 125.24 2.70 o -3 5 2 1281.90 1348.41 14.95 o -2 5 2 793.45 774.89 10.17 o -1 5 2 18.85 23.12 0.56 o 0 5 2 213.29 182.46 2.25 o 1 5 2 1700.99 1888.30 19.07 o 2 5 2 5740.53 6247.93 67.27 o 3 5 2 85.07 87.15 1.86 o 4 5 2 25.75 19.61 0.91 o 5 5 2 91.94 90.07 2.80 o 6 5 2 901.97 864.40 15.13 o 7 5 2 0.35 0.97 0.64 o 8 5 2 1.12 2.19 0.79 o 9 5 2 159.05 173.33 7.43 o -9 6 2 2.74 2.43 0.82 o -8 6 2 140.09 142.22 5.81 o -7 6 2 12.27 11.99 1.82 o -6 6 2 266.99 263.65 5.75 o -5 6 2 900.07 905.23 15.34 o -4 6 2 518.40 543.54 9.63 o -3 6 2 725.29 709.73 12.19 o -2 6 2 207.22 225.27 3.51 o -1 6 2 231.72 265.63 3.12 o 0 6 2 103.75 120.48 1.67 o 1 6 2 0.18 1.96 0.35 o 2 6 2 29.83 22.18 0.79 o 3 6 2 663.70 703.66 12.14 o 4 6 2 682.92 676.48 11.94 o 5 6 2 110.12 101.00 3.07 o 6 6 2 177.39 165.52 4.35 o 7 6 2 160.54 156.80 4.36 o 8 6 2 317.16 305.79 7.07 o -9 7 2 147.93 161.19 4.71 o -8 7 2 182.56 186.88 4.97 o -7 7 2 2.96 2.97 0.84 o -6 7 2 2042.21 2112.01 33.95 o -5 7 2 257.04 240.96 5.27 o -4 7 2 7.44 4.52 0.71 o -3 7 2 149.56 150.82 2.67 o -2 7 2 1044.49 1043.05 13.63 o -1 7 2 26.77 32.21 0.90 o 0 7 2 2370.14 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