#------------------------------------------------------------------------------ #$Date: 2016-04-02 22:12:13 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180830 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/61/2016140.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2016140_Fobs loop_ _publ_author_name 'Ojala, Charles R.' 'Ojala, William H.' 'Britton, Doyle' 'Cramer, Christopher J.' _publ_section_title ; Three polymorphs of 4-4'-diiodobenzalazine, and 4-chloro-4'-iodobenzalazine ; _journal_coeditor_code GA3056 _journal_issue 9 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first o518 _journal_page_last o523 _journal_volume 63 _journal_year 2007 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 92.407 _cell_angle_gamma 90.000 _cell_length_a 11.8545 _cell_length_b 7.7308 _cell_length_c 7.6827 _exptl_crystal_F_000 452.00 _reflns_d_resolution_high 0.7698 _cod_data_source_file ga3056I,I-Asup2.hkl _cod_data_source_block I,I-A #BEGIN Tags that were not found in dictionaries: _shelx_title 'polymorph A in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 226.62 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 9050.39 6698.74 213.54 o 2 0 0 410.26 389.60 26.59 o 3 0 0 10502.13 9593.98 221.07 o 4 0 0 30362.92 28278.42 558.05 o 5 0 0 13625.78 12868.97 300.41 o 6 0 0 290.62 191.53 9.81 o 7 0 0 127.09 110.04 8.24 o 8 0 0 7130.26 7125.70 144.20 o 9 0 0 7177.34 7352.69 171.81 o 10 0 0 2722.33 2878.13 88.28 o 11 0 0 148.68 135.31 16.89 o 12 0 0 1918.46 1981.70 65.09 o 13 0 0 990.53 1059.64 40.48 o 14 0 0 877.67 981.15 39.05 o 15 0 0 20.69 38.07 38.39 o 1 1 0 2619.51 2686.07 37.97 o 2 1 0 3766.17 3714.90 52.44 o 3 1 0 4716.64 4588.66 70.40 o 4 1 0 991.87 938.04 15.01 o 5 1 0 797.55 728.65 20.22 o 6 1 0 3548.21 3410.86 57.44 o 7 1 0 1971.30 1802.32 43.40 o 8 1 0 578.17 551.57 11.01 o 9 1 0 58.85 64.16 5.85 o 10 1 0 661.05 682.49 20.22 o 11 1 0 901.86 900.65 24.66 o 12 1 0 307.12 294.41 13.56 o 13 1 0 1.16 15.78 9.90 o 14 1 0 110.45 113.20 12.94 o 15 1 0 237.32 256.65 15.66 o 0 2 0 44055.93 49159.61 967.41 o 1 2 0 1700.50 1802.31 25.96 o 2 2 0 2.67 8.71 2.13 o 3 2 0 3416.69 3455.86 49.20 o 4 2 0 7621.31 7659.77 107.78 o 5 2 0 4036.45 3885.18 55.80 o 6 2 0 43.18 37.44 4.02 o 7 2 0 14.58 11.94 3.47 o 8 2 0 2231.56 2059.56 45.37 o 9 2 0 2004.48 1804.25 44.25 o 10 2 0 925.88 899.07 21.49 o 11 2 0 52.80 37.10 9.30 o 12 2 0 596.12 609.73 20.31 o 13 2 0 287.16 297.10 24.54 o 14 2 0 301.56 332.90 16.30 o 15 2 0 0.74 16.85 21.52 o 1 3 0 8055.72 8707.96 122.11 o 2 3 0 14952.01 15730.05 219.68 o 3 3 0 13291.97 13555.78 189.52 o 4 3 0 2065.59 2107.17 31.02 o 5 3 0 2265.17 2240.21 33.18 o 6 3 0 10765.87 10845.71 152.80 o 7 3 0 7073.12 6831.37 104.16 o 8 3 0 2249.77 2101.56 41.04 o 9 3 0 194.56 176.15 7.36 o 10 3 0 2243.98 2115.13 81.01 o 11 3 0 3457.32 3053.52 214.92 o 12 3 0 1198.22 1251.23 46.96 o 13 3 0 1.19 13.30 14.35 o 14 3 0 435.81 506.25 20.44 o 0 4 0 1232.99 1324.16 32.85 o 1 4 0 1730.81 1902.18 30.12 o 2 4 0 27.02 32.73 2.60 o 3 4 0 172.27 201.90 5.42 o 4 4 0 1633.91 1649.02 25.03 o 5 4 0 669.12 694.12 12.18 o 6 4 0 287.87 304.45 7.13 o 7 4 0 190.95 208.80 6.80 o 8 4 0 397.11 378.22 9.66 o 9 4 0 448.33 441.19 10.90 o 10 4 0 65.89 71.45 8.56 o 11 4 0 3.05 15.53 9.03 o 12 4 0 101.77 87.41 12.91 o 13 4 0 68.91 91.95 35.02 o 14 4 0 24.16 15.13 20.34 o 1 5 0 2066.48 2144.21 34.22 o 2 5 0 5294.03 5637.77 86.11 o 3 5 0 2993.75 3090.90 48.56 o 4 5 0 190.24 183.00 6.09 o 5 5 0 309.10 309.52 8.10 o 6 5 0 2306.76 2327.39 41.11 o 7 5 0 2239.20 2174.09 38.96 o 8 5 0 1015.79 958.58 19.85 o 9 5 0 69.30 65.28 7.13 o 10 5 0 579.75 579.85 19.35 o 11 5 0 1285.88 1317.94 56.21 o 12 5 0 455.29 435.76 28.07 o 13 5 0 4.50 -14.41 14.41 o 0 6 0 9180.26 9968.35 230.80 o 1 6 0 4228.37 4454.06 74.82 o 2 6 0 1.84 3.36 4.48 o 3 6 0 1555.03 1630.12 29.86 o 4 6 0 6635.40 6903.72 114.47 o 5 6 0 3015.85 3010.09 52.25 o 6 6 0 591.26 566.95 14.71 o 7 6 0 405.32 402.02 12.12 o 8 6 0 2254.64 2245.48 40.87 o 9 6 0 1674.41 1666.19 31.95 o 10 6 0 523.77 517.03 17.83 o 11 6 0 14.13 21.43 14.83 o 12 6 0 554.16 556.44 55.80 o 1 7 0 76.02 83.10 6.08 o 2 7 0 1.72 5.05 5.21 o 3 7 0 207.54 209.48 7.98 o 4 7 0 249.21 252.07 8.72 o 5 7 0 227.77 238.55 9.50 o 6 7 0 248.37 221.19 9.62 o 7 7 0 37.86 46.70 8.41 o 8 7 0 20.97 18.68 11.31 o 9 7 0 0.05 -0.42 11.38 o 10 7 0 51.96 40.65 17.29 o 11 7 0 0.15 -18.41 57.19 o 0 8 0 2614.55 2694.66 67.90 o 1 8 0 1066.91 1088.68 22.27 o 2 8 0 15.70 37.23 8.00 o 3 8 0 468.99 477.91 14.38 o 4 8 0 2306.76 2384.63 53.48 o 5 8 0 721.26 707.03 20.87 o 6 8 0 158.26 124.41 10.95 o 7 8 0 120.98 109.87 11.10 o 8 8 0 866.27 851.61 24.81 o 9 8 0 320.04 318.19 22.64 o 1 9 0 570.73 585.06 19.31 o 2 9 0 704.23 728.17 23.15 o 3 9 0 1127.56 1129.90 33.21 o 4 9 0 465.28 448.90 19.52 o 5 9 0 421.03 418.74 25.89 o 6 9 0 996.09 949.24 40.72 o 1 10 0 1.93 13.85 17.13 o -15 1 1 383.19 440.90 18.77 o -14 1 1 1098.58 1155.93 36.71 o -13 1 1 565.40 600.91 20.38 o -12 1 1 278.10 290.93 14.15 o -11 1 1 1756.46 1823.02 42.77 o -10 1 1 4235.97 4308.32 90.24 o -9 1 1 1350.76 1294.15 25.41 o -8 1 1 440.41 439.03 10.58 o -7 1 1 3677.84 3410.72 53.79 o -6 1 1 14670.70 13920.02 335.44 o -5 1 1 12167.46 11317.64 283.54 o -4 1 1 388.48 362.32 7.15 o -3 1 1 1600.17 1475.95 23.18 o -2 1 1 51356.40 50748.30 815.51 o -1 1 1 10236.66 10398.49 155.69 o 0 1 1 2066.37 2114.14 32.35 o 1 1 1 499.42 535.51 8.37 o 2 1 1 9739.34 9569.13 134.03 o 3 1 1 19984.64 19373.60 289.85 o 4 1 1 7651.26 7055.64 128.46 o 5 1 1 957.14 998.36 17.18 o 6 1 1 3692.36 3542.77 55.29 o 7 1 1 9201.36 8951.96 178.88 o 8 1 1 6848.76 6600.17 101.47 o 9 1 1 733.07 746.58 20.23 o 10 1 1 590.44 581.62 15.72 o 11 1 1 1892.60 1965.93 51.39 o 12 1 1 2517.09 2656.60 59.67 o 13 1 1 556.31 563.70 19.32 o 14 1 1 1.22 1.20 10.47 o 15 1 1 449.92 435.05 26.77 o -15 2 1 9.76 62.64 32.14 o -14 2 1 49.70 36.26 12.30 o -13 2 1 716.87 818.06 24.79 o -12 2 1 1412.59 1561.35 53.26 o -11 2 1 713.82 705.16 28.40 o -10 2 1 77.60 86.86 8.07 o -9 2 1 2331.78 2297.83 46.15 o -8 2 1 4007.09 3843.88 65.11 o -7 2 1 2976.57 2936.82 50.15 o -6 2 1 780.65 747.56 13.80 o -5 2 1 2994.65 2870.05 44.65 o -4 2 1 8774.52 8125.56 156.03 o -3 2 1 10907.50 10551.55 147.79 o -2 2 1 15402.46 16409.08 228.93 o -1 2 1 3119.96 3488.66 49.44 o 0 2 1 23988.37 26525.52 395.27 o 1 2 1 15746.70 17118.59 255.42 o 2 2 1 9606.80 9918.49 138.57 o 3 2 1 69.43 82.72 4.91 o 4 2 1 8647.68 8855.37 124.44 o 5 2 1 8284.50 7964.60 112.57 o 6 2 1 6805.81 6486.91 92.32 o 7 2 1 414.97 375.91 9.97 o 8 2 1 1031.33 980.72 18.99 o 9 2 1 4951.03 4929.99 91.56 o 10 2 1 3320.03 3324.82 72.99 o 11 2 1 92.71 91.75 9.75 o 12 2 1 139.12 130.13 12.86 o 13 2 1 527.34 563.57 25.36 o 14 2 1 901.54 1042.00 29.96 o -14 3 1 46.46 56.87 13.30 o -13 3 1 41.54 38.73 20.70 o -12 3 1 43.90 77.92 16.01 o -11 3 1 40.07 39.05 14.79 o -10 3 1 122.77 105.41 9.08 o -9 3 1 0.28 -0.15 6.05 o -8 3 1 42.39 53.98 5.13 o -7 3 1 176.56 165.42 6.22 o -6 3 1 74.26 79.73 5.36 o -5 3 1 357.26 335.99 6.90 o -4 3 1 126.92 133.14 3.95 o -3 3 1 38.78 44.33 2.72 o -2 3 1 3953.78 4344.58 61.63 o -1 3 1 9.23 21.24 1.91 o 0 3 1 256.88 264.64 5.55 o 1 3 1 166.92 175.64 4.39 o 2 3 1 294.29 317.55 6.49 o 3 3 1 144.85 137.56 4.52 o 4 3 1 31.32 52.58 3.05 o 5 3 1 475.04 520.23 13.91 o 6 3 1 0.23 6.98 2.99 o 7 3 1 323.85 297.17 7.43 o 8 3 1 229.50 205.12 7.17 o 9 3 1 28.35 31.19 9.51 o 10 3 1 7.31 12.69 7.71 o 11 3 1 61.88 71.47 8.85 o 12 3 1 111.02 101.45 10.74 o 13 3 1 10.17 11.51 10.25 o 14 3 1 8.14 3.58 12.79 o -14 4 1 59.65 63.10 23.25 o -13 4 1 792.99 788.32 134.04 o -12 4 1 1252.29 1153.44 75.55 o -11 4 1 571.11 560.90 20.27 o -10 4 1 63.56 64.13 7.71 o -9 4 1 1964.00 2001.75 36.69 o -8 4 1 3584.16 3561.32 57.28 o -7 4 1 2375.04 2311.78 37.69 o -6 4 1 857.93 856.83 15.85 o -5 4 1 2233.14 2188.19 35.07 o -4 4 1 8291.41 8318.51 125.65 o -3 4 1 8689.77 8958.85 134.94 o -2 4 1 7676.13 8515.16 119.74 o -1 4 1 1750.98 1867.75 29.71 o 0 4 1 14366.51 15930.81 238.33 o 1 4 1 12642.66 13304.54 199.32 o 2 4 1 6740.86 7208.66 109.02 o 3 4 1 8.95 15.35 2.73 o 4 4 1 6362.67 6703.92 101.85 o 5 4 1 7845.41 7793.57 118.33 o 6 4 1 7161.29 7282.68 103.58 o 7 4 1 151.65 146.11 6.80 o 8 4 1 885.12 835.06 21.94 o 9 4 1 4550.28 4248.66 89.59 o 10 4 1 3174.75 2993.32 65.98 o 11 4 1 62.57 71.80 10.59 o 12 4 1 132.21 115.44 12.90 o 13 4 1 413.62 449.90 21.36 o -13 5 1 71.59 51.80 18.14 o -12 5 1 7.39 2.21 26.90 o -11 5 1 487.36 488.28 20.68 o -10 5 1 1209.66 1227.26 31.26 o -9 5 1 832.92 833.54 24.95 o -8 5 1 5.82 12.82 5.68 o -7 5 1 595.77 569.03 13.36 o -6 5 1 5345.26 5318.90 88.82 o -5 5 1 2409.89 2456.12 42.74 o -4 5 1 46.69 48.60 4.29 o -3 5 1 1244.84 1286.48 23.72 o -2 5 1 3080.22 3245.82 50.69 o -1 5 1 5749.77 6052.51 92.23 o 0 5 1 497.47 491.08 9.83 o 1 5 1 4.01 3.02 2.89 o 2 5 1 2576.54 2611.22 41.32 o 3 5 1 5379.96 5635.67 86.38 o 4 5 1 3663.36 3786.67 59.12 o 5 5 1 26.80 34.52 4.79 o 6 5 1 1642.76 1700.60 28.74 o 7 5 1 1829.36 1871.33 34.14 o 8 5 1 1441.48 1423.61 29.96 o 9 5 1 243.56 234.91 12.22 o 10 5 1 170.35 175.95 12.26 o 11 5 1 513.11 493.20 18.97 o 12 5 1 557.79 583.92 34.96 o 13 5 1 569.52 569.95 56.54 o -12 6 1 30.29 49.42 29.62 o -11 6 1 6.35 8.90 17.31 o -10 6 1 3.79 11.03 10.30 o -9 6 1 70.11 73.36 9.65 o -8 6 1 115.67 101.48 9.88 o -7 6 1 24.96 20.98 7.32 o -6 6 1 325.78 317.17 13.24 o -5 6 1 48.34 39.96 5.64 o -4 6 1 837.90 851.18 17.53 o -3 6 1 314.59 308.46 8.87 o -2 6 1 333.53 379.89 9.82 o -1 6 1 73.59 85.20 5.43 o 0 6 1 672.98 735.13 15.36 o 1 6 1 498.95 514.42 11.88 o 2 6 1 225.31 233.99 7.71 o 3 6 1 30.40 40.05 4.97 o 4 6 1 256.55 259.80 8.49 o 5 6 1 369.47 362.42 11.24 o 6 6 1 818.38 821.88 16.22 o 7 6 1 11.68 10.61 5.68 o 8 6 1 20.63 19.02 7.05 o 9 6 1 276.07 257.85 20.56 o 10 6 1 202.65 184.17 13.39 o 11 6 1 0.38 5.66 13.25 o 12 6 1 10.03 1.66 13.83 o -10 7 1 1410.67 1326.16 69.16 o -9 7 1 758.13 738.83 22.58 o -8 7 1 0.07 4.70 10.19 o -7 7 1 643.37 621.35 19.20 o -6 7 1 4178.88 4180.34 88.88 o -5 7 1 2046.61 2139.85 48.41 o -4 7 1 100.49 113.92 8.79 o -3 7 1 795.38 787.73 18.86 o -2 7 1 3626.13 3795.12 71.79 o -1 7 1 3984.90 4238.39 79.48 o 0 7 1 714.85 744.35 17.93 o 1 7 1 27.09 33.66 5.92 o 2 7 1 2484.76 2653.59 48.28 o 3 7 1 3712.39 3859.45 66.20 o 4 7 1 2282.61 2372.92 46.49 o 5 7 1 26.06 32.81 5.93 o 6 7 1 1043.17 1033.37 23.48 o 7 7 1 1684.01 1703.42 35.54 o 8 7 1 1459.86 1364.37 33.34 o 9 7 1 298.55 275.19 15.97 o 10 7 1 119.63 137.82 16.76 o -9 8 1 224.26 194.10 14.63 o -8 8 1 468.13 456.92 17.58 o -7 8 1 459.30 444.75 17.48 o -6 8 1 25.80 23.25 8.98 o -5 8 1 275.30 259.83 16.49 o -4 8 1 257.66 232.72 12.40 o -3 8 1 884.48 885.07 21.40 o -2 8 1 327.09 335.36 18.88 o -1 8 1 83.25 92.06 8.30 o 0 8 1 766.00 781.85 19.38 o 1 8 1 1212.55 1239.83 27.43 o 2 8 1 780.23 822.55 20.23 o 3 8 1 89.79 82.82 8.15 o 4 8 1 565.56 581.94 16.26 o 5 8 1 778.02 802.81 24.05 o 6 8 1 208.78 195.60 13.37 o 7 8 1 72.00 71.04 13.81 o 8 8 1 174.87 163.30 19.25 o 9 8 1 263.90 255.15 30.86 o -6 9 1 293.95 301.10 16.76 o -5 9 1 105.36 104.14 13.15 o -4 9 1 22.62 8.47 9.60 o -3 9 1 51.29 57.97 9.40 o -2 9 1 315.27 312.75 12.48 o -1 9 1 232.86 241.88 11.28 o 0 9 1 96.70 114.36 9.43 o 1 9 1 4.20 15.69 7.80 o 2 9 1 302.71 318.28 14.50 o 3 9 1 112.33 102.38 11.13 o 4 9 1 111.70 129.07 12.19 o 5 9 1 34.17 6.04 11.47 o 6 9 1 36.93 32.35 20.06 o -15 0 2 517.88 572.55 43.00 o -14 0 2 2.38 -14.47 16.20 o -13 0 2 362.95 411.17 46.34 o -12 0 2 2239.24 2388.53 75.91 o -11 0 2 2068.93 2109.36 55.70 o -10 0 2 922.26 884.19 27.80 o -9 0 2 745.39 708.60 29.35 o -8 0 2 3941.92 3744.81 142.95 o -7 0 2 10973.21 10540.67 243.12 o -6 0 2 4205.51 4287.02 101.34 o -5 0 2 110.73 108.11 6.84 o -4 0 2 7342.40 7166.12 165.51 o -3 0 2 18672.57 17835.40 389.56 o -2 0 2 29382.46 28060.34 553.18 o -1 0 2 824.78 802.92 26.83 o 0 0 2 2599.30 2637.69 66.85 o 1 0 2 25547.60 25690.98 506.35 o 2 0 2 25777.85 26198.78 516.71 o 3 0 2 8638.79 8507.82 194.95 o 4 0 2 148.93 122.83 6.06 o 5 0 2 12458.66 11574.05 321.37 o 6 0 2 15888.39 15047.27 344.69 o 7 0 2 8007.73 7655.08 178.73 o 8 0 2 87.46 86.57 9.87 o 9 0 2 4585.35 4619.33 111.29 o 10 0 2 6219.66 6427.34 281.89 o 11 0 2 1522.58 1555.80 74.65 o 12 0 2 537.16 537.77 26.11 o 13 0 2 664.25 652.59 30.16 o 14 0 2 877.01 859.46 36.78 o -15 1 2 40.40 21.31 31.76 o -14 1 2 210.06 250.47 15.47 o -13 1 2 212.82 230.68 15.79 o -12 1 2 50.86 35.56 9.01 o -11 1 2 111.14 103.89 8.49 o -10 1 2 463.06 426.13 12.44 o -9 1 2 886.81 815.09 22.46 o -8 1 2 1194.66 1123.83 23.54 o -7 1 2 38.11 37.32 4.73 o -6 1 2 2281.42 2211.28 38.39 o -5 1 2 2976.19 2778.33 43.39 o -4 1 2 3589.88 3390.31 52.74 o -3 1 2 10.86 16.47 2.13 o -2 1 2 4190.73 4450.58 67.57 o -1 1 2 3592.75 3840.05 58.39 o 0 1 2 3597.64 3624.11 51.48 o 1 1 2 1104.16 1140.48 17.04 o 2 1 2 413.20 426.71 9.60 o 3 1 2 4018.78 3848.31 54.92 o 4 1 2 5728.18 5548.52 91.09 o 5 1 2 744.70 712.95 14.22 o 6 1 2 3.51 5.45 6.08 o 7 1 2 1394.08 1357.51 45.28 o 8 1 2 2032.10 2023.70 37.54 o 9 1 2 450.29 477.50 13.27 o 10 1 2 42.17 44.22 6.86 o 11 1 2 29.84 29.17 7.54 o 12 1 2 633.58 627.70 21.05 o 13 1 2 377.45 409.67 17.17 o 14 1 2 63.08 103.73 19.59 o -14 2 2 2.64 15.41 14.80 o -13 2 2 129.21 127.62 13.11 o -12 2 2 637.69 600.54 34.96 o -11 2 2 491.16 470.64 22.09 o -10 2 2 362.40 343.87 11.68 o -9 2 2 297.80 288.12 9.40 o -8 2 2 836.04 808.66 17.61 o -7 2 2 3313.89 3139.95 55.08 o -6 2 2 1479.76 1361.72 24.12 o -5 2 2 78.36 73.28 4.18 o -4 2 2 3681.43 3634.09 74.40 o -3 2 2 3702.13 3558.09 60.47 o -2 2 2 7243.69 7519.77 116.65 o -1 2 2 249.51 251.07 5.58 o 0 2 2 550.05 570.02 10.16 o 1 2 2 6371.82 6516.00 91.89 o 2 2 2 6171.03 6302.62 88.99 o 3 2 2 3657.00 3824.63 54.82 o 4 2 2 6.59 6.85 2.12 o 5 2 2 5056.04 5150.77 78.85 o 6 2 2 4949.59 4774.33 68.84 o 7 2 2 2192.11 2113.35 37.98 o 8 2 2 30.48 34.43 8.22 o 9 2 2 1387.73 1310.90 26.11 o 10 2 2 1990.72 2028.97 41.66 o 11 2 2 274.00 289.74 12.22 o 12 2 2 254.70 257.41 12.03 o 13 2 2 163.67 146.12 13.12 o 14 2 2 259.10 272.93 19.08 o -14 3 2 767.06 736.19 45.07 o -13 3 2 741.40 739.42 70.18 o -12 3 2 215.29 156.66 20.26 o -11 3 2 379.83 400.08 13.87 o -10 3 2 1724.28 1842.53 35.22 o -9 3 2 3066.76 3043.94 49.54 o -8 3 2 4550.69 4493.86 90.79 o -7 3 2 117.01 109.08 5.68 o -6 3 2 7656.75 7475.33 113.69 o -5 3 2 9895.21 9566.40 144.22 o -4 3 2 13107.88 13249.49 191.52 o -3 3 2 17.85 22.96 2.44 o -2 3 2 11859.99 12909.96 180.54 o -1 3 2 12005.63 12265.75 184.15 o 0 3 2 12205.15 12383.75 185.52 o 1 3 2 3145.25 3311.19 50.97 o 2 3 2 1974.62 2114.69 33.35 o 3 3 2 10677.66 10989.89 154.48 o 4 3 2 17708.61 18292.65 255.90 o 5 3 2 2846.92 2825.31 41.75 o 6 3 2 5.92 14.27 3.68 o 7 3 2 4528.13 4370.96 74.06 o 8 3 2 7055.57 7009.59 135.51 o 9 3 2 1752.76 1725.40 43.60 o 10 3 2 173.03 167.08 10.24 o 11 3 2 110.10 134.91 10.35 o 12 3 2 2319.79 2347.74 48.47 o 13 3 2 1319.55 1377.16 41.92 o 14 3 2 278.64 302.65 24.30 o -13 4 2 6.96 13.15 14.92 o -12 4 2 193.33 213.04 17.30 o -11 4 2 327.38 339.19 16.56 o -10 4 2 1.18 14.33 7.89 o -9 4 2 0.75 5.43 6.24 o -8 4 2 828.53 816.94 21.33 o -7 4 2 455.14 439.48 10.55 o -6 4 2 27.72 31.83 4.61 o -5 4 2 18.02 19.66 3.54 o -4 4 2 51.55 68.55 3.72 o -3 4 2 2515.08 2652.52 38.87 o -2 4 2 1097.71 1110.89 17.38 o -1 4 2 161.65 173.82 4.94 o 0 4 2 290.80 283.73 6.53 o 1 4 2 1835.76 2039.00 32.53 o 2 4 2 2116.28 2258.41 35.86 o 3 4 2 0.84 -0.14 3.05 o 4 4 2 376.85 394.48 8.70 o 5 4 2 90.53 76.95 5.68 o 6 4 2 662.90 669.64 13.52 o 7 4 2 511.16 500.76 13.01 o 8 4 2 3.36 -0.24 6.12 o 9 4 2 249.93 219.97 12.55 o 10 4 2 233.68 219.02 12.56 o 11 4 2 463.73 430.40 17.49 o 12 4 2 3.35 2.17 12.77 o 13 4 2 86.11 76.89 13.50 o -13 5 2 190.79 190.08 30.65 o -12 5 2 103.05 152.36 20.65 o -11 5 2 86.52 94.51 12.78 o -10 5 2 584.93 578.47 17.19 o -9 5 2 828.75 826.15 22.79 o -8 5 2 1658.71 1603.26 38.86 o -7 5 2 25.17 29.40 6.91 o -6 5 2 2271.34 2179.63 38.99 o -5 5 2 2530.31 2501.63 48.26 o -4 5 2 4488.04 4669.59 86.06 o -3 5 2 10.35 12.02 4.14 o -2 5 2 2726.40 2950.48 46.47 o -1 5 2 3270.18 3294.38 51.54 o 0 5 2 3541.89 3675.33 57.15 o 1 5 2 849.91 894.24 15.96 o 2 5 2 771.29 833.64 15.24 o 3 5 2 1851.51 1871.91 30.79 o 4 5 2 4895.41 5007.10 77.41 o 5 5 2 862.23 853.10 16.15 o 6 5 2 10.36 9.65 4.44 o 7 5 2 1269.22 1253.28 28.66 o 8 5 2 2015.16 1998.58 45.66 o 9 5 2 540.07 511.46 17.49 o 10 5 2 76.13 84.50 11.05 o 11 5 2 22.83 54.39 21.83 o 12 5 2 724.84 699.13 40.47 o -11 6 2 992.21 1045.24 29.95 o -10 6 2 85.44 97.57 13.12 o -9 6 2 84.07 67.79 10.08 o -8 6 2 1990.65 1955.29 45.45 o -7 6 2 2323.58 2334.52 52.56 o -6 6 2 638.84 633.36 18.63 o -5 6 2 0.28 3.81 6.29 o -4 6 2 508.90 496.29 18.29 o -3 6 2 6084.35 6039.29 110.91 o -2 6 2 4397.81 4575.69 85.03 o -1 6 2 589.80 625.28 15.51 o 0 6 2 800.71 842.95 19.23 o 1 6 2 6141.66 6424.20 117.57 o 2 6 2 6919.05 7241.20 110.65 o 3 6 2 897.43 880.38 16.58 o 4 6 2 271.23 274.87 7.99 o 5 6 2 2195.20 2221.84 36.85 o 6 6 2 3930.22 3936.56 62.56 o 7 6 2 2014.61 2009.11 40.63 o 8 6 2 39.84 35.89 8.63 o 9 6 2 1221.35 1176.54 31.18 o 10 6 2 1517.82 1552.95 39.38 o 11 6 2 1130.73 1144.74 32.46 o -10 7 2 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