#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/61/2016152.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2016152_Fobs loop_ _publ_author_name 'Gelmboldt, Vladimir O.' 'Ganin, Eduard V.' 'Domasevitch, Konstantin V.' _publ_section_title ; Hydrogen-bonded frameworks of bis(2-carboxypyridinium) hexafluorosilicate and bis(2-carboxyquinolinium) hexafluorosilicate dihydrate ; _journal_coeditor_code GG3102 _journal_issue 9 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first o530 _journal_page_last o534 _journal_volume 63 _journal_year 2007 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 91.943 _cell_angle_gamma 90.000 _cell_length_a 9.3571 _cell_length_b 7.8717 _cell_length_c 9.8053 _exptl_crystal_F_000 396.00 _reflns_d_resolution_high 0.7288 _[local]_cod_data_source_file gg3102Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' ip2_90 in P2(1)/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 78.32 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 1593.18 1568.43 78.22 o 6 0 0 2185.57 2097.92 92.64 o 8 0 0 679.05 669.11 29.80 o 10 0 0 159.24 153.09 3.65 o 12 0 0 70.49 64.56 3.44 o 3 1 0 452.25 413.55 12.55 o 4 1 0 1577.02 1594.84 53.13 o 5 1 0 827.88 902.23 18.29 o 6 1 0 1186.45 1228.46 26.33 o 7 1 0 730.02 706.35 17.20 o 8 1 0 72.16 79.21 2.04 o 9 1 0 472.62 464.27 7.66 o 10 1 0 40.95 39.35 1.20 o 11 1 0 6.23 4.92 1.32 o 12 1 0 3.89 5.08 1.47 o 0 2 0 1076.02 1098.64 8.89 o 1 2 0 1044.00 1074.15 34.11 o 2 2 0 5634.52 6041.50 124.83 o 3 2 0 943.18 1001.03 19.51 o 4 2 0 1660.79 1735.60 46.07 o 5 2 0 59.03 51.92 1.12 o 6 2 0 513.47 484.96 10.38 o 7 2 0 160.10 152.63 3.33 o 8 2 0 24.99 24.02 1.14 o 9 2 0 4.88 3.52 1.23 o 10 2 0 2.11 2.84 1.32 o 11 2 0 0.71 2.23 1.43 o 12 2 0 0.07 0.07 1.74 o 1 3 0 19.04 23.87 1.29 o 2 3 0 2254.45 2356.92 64.21 o 3 3 0 2065.28 2074.43 40.52 o 4 3 0 193.04 191.47 4.75 o 5 3 0 19.97 19.23 1.48 o 6 3 0 52.39 53.41 1.43 o 7 3 0 42.17 41.66 1.35 o 8 3 0 546.63 515.74 8.53 o 9 3 0 62.12 64.71 1.67 o 10 3 0 0.12 0.66 1.65 o 11 3 0 11.93 15.72 1.82 o 12 3 0 0.08 0.31 1.79 o 0 4 0 2222.82 2342.14 42.93 o 1 4 0 1031.19 1044.13 18.69 o 2 4 0 701.46 750.36 17.42 o 3 4 0 579.99 606.03 19.56 o 4 4 0 1043.92 1071.20 22.01 o 5 4 0 51.78 47.30 1.82 o 6 4 0 446.68 433.95 13.04 o 7 4 0 51.81 42.72 1.81 o 8 4 0 159.34 137.69 2.44 o 9 4 0 75.52 69.98 1.44 o 10 4 0 104.69 93.61 1.87 o 11 4 0 0.12 0.00 1.89 o 1 5 0 190.11 170.58 2.64 o 2 5 0 0.14 1.47 0.96 o 3 5 0 711.24 691.27 17.58 o 4 5 0 338.02 341.10 7.59 o 5 5 0 0.34 1.77 1.07 o 6 5 0 0.46 2.17 1.09 o 7 5 0 70.67 65.77 1.95 o 8 5 0 52.42 43.97 1.26 o 9 5 0 117.47 104.58 2.51 o 10 5 0 81.48 81.83 3.44 o 11 5 0 29.29 24.77 1.55 o 0 6 0 574.15 568.77 15.64 o 1 6 0 247.18 240.58 6.10 o 2 6 0 97.20 91.41 2.38 o 3 6 0 4.05 3.76 1.07 o 4 6 0 5.59 5.05 1.10 o 5 6 0 111.56 117.02 2.48 o 6 6 0 53.44 45.78 1.82 o 7 6 0 81.52 76.31 1.48 o 8 6 0 5.07 5.43 1.35 o 9 6 0 6.43 8.95 1.36 o 10 6 0 108.53 116.83 6.33 o 1 7 0 104.93 103.04 2.23 o 2 7 0 28.32 29.84 1.15 o 3 7 0 109.25 112.55 2.55 o 4 7 0 30.86 29.88 2.16 o 5 7 0 60.82 58.09 2.36 o 6 7 0 29.50 23.48 1.18 o 7 7 0 90.65 85.50 2.89 o 8 7 0 2.53 2.44 1.37 o 9 7 0 7.28 9.92 1.59 o 0 8 0 7.64 7.23 1.61 o 1 8 0 6.04 7.74 1.25 o 2 8 0 0.28 0.33 1.03 o 3 8 0 4.66 4.11 1.11 o 4 8 0 266.90 271.65 5.80 o 5 8 0 23.56 26.72 1.57 o 6 8 0 107.94 96.34 1.59 o 7 8 0 23.83 17.11 1.53 o 8 8 0 4.25 0.46 1.31 o 1 9 0 0.71 1.55 1.25 o 2 9 0 2.66 2.21 1.28 o 3 9 0 15.19 19.08 1.43 o 4 9 0 2.22 1.83 1.34 o 5 9 0 35.49 35.63 1.49 o 6 9 0 6.84 8.62 1.59 o 7 9 0 5.07 5.54 1.69 o 0 10 0 35.14 33.59 2.21 o 1 10 0 11.84 10.69 1.27 o 2 10 0 39.44 37.85 1.60 o 3 10 0 67.34 64.91 1.69 o 4 10 0 94.76 92.35 2.47 o -11 0 1 45.26 47.59 1.82 o -9 0 1 80.75 76.01 2.03 o -7 0 1 1215.42 1100.66 23.67 o -5 0 1 561.74 530.96 21.40 o -3 0 1 1062.73 1041.74 14.98 o 3 0 1 370.12 394.25 19.97 o 5 0 1 1339.66 1294.24 5.07 o 7 0 1 239.77 233.23 2.10 o 9 0 1 40.57 40.97 1.81 o 11 0 1 9.07 8.12 2.01 o -12 1 1 5.05 5.31 1.57 o -11 1 1 31.84 31.63 1.35 o -10 1 1 51.93 51.39 1.21 o -9 1 1 8.26 10.02 1.07 o -8 1 1 914.91 863.88 22.60 o -7 1 1 13.05 15.05 1.01 o -6 1 1 7.65 13.17 1.22 o -5 1 1 120.06 126.80 2.99 o -4 1 1 321.81 288.67 9.61 o -3 1 1 62.57 53.15 1.65 o -2 1 1 4107.59 3934.74 213.57 o 2 1 1 5614.39 5892.38 17.52 o 3 1 1 455.46 434.88 9.62 o 4 1 1 68.38 67.87 2.03 o 5 1 1 105.23 88.84 2.41 o 6 1 1 1.16 2.26 1.11 o 7 1 1 17.57 20.43 1.30 o 8 1 1 322.59 303.96 3.81 o 9 1 1 1.08 0.60 1.01 o 10 1 1 36.98 35.23 1.26 o 11 1 1 10.78 11.70 1.33 o 12 1 1 13.36 13.27 1.49 o -12 2 1 12.91 15.66 1.62 o -11 2 1 17.14 17.45 1.44 o -10 2 1 29.67 25.37 1.36 o -9 2 1 218.81 210.90 2.81 o -8 2 1 77.45 76.29 1.41 o -7 2 1 743.76 688.69 11.41 o -6 2 1 0.38 0.25 0.96 o -5 2 1 0.04 1.76 1.09 o -4 2 1 268.26 298.39 13.59 o -3 2 1 2469.70 2550.04 87.06 o -2 2 1 2904.87 3091.00 88.23 o 0 2 1 357.75 359.49 6.88 o 1 2 1 6058.95 6015.82 16.52 o 2 2 1 4324.67 4427.13 95.03 o 3 2 1 346.24 399.65 12.89 o 4 2 1 801.07 777.33 22.97 o 5 2 1 161.40 143.13 3.61 o 6 2 1 24.03 24.50 1.14 o 7 2 1 68.17 63.86 2.66 o 8 2 1 2.98 2.63 1.30 o 9 2 1 178.39 168.81 2.17 o 10 2 1 13.19 11.30 1.47 o 11 2 1 88.10 89.25 1.72 o 12 2 1 29.38 27.58 2.02 o -12 3 1 0.16 0.99 1.43 o -11 3 1 1.49 0.70 1.37 o -10 3 1 55.59 55.02 1.17 o -9 3 1 5.60 6.53 1.16 o -8 3 1 451.14 458.98 13.13 o -7 3 1 4.97 4.13 1.07 o -6 3 1 0.93 2.34 0.97 o -5 3 1 78.59 84.24 3.28 o -4 3 1 618.51 698.76 24.00 o -3 3 1 280.46 276.89 8.83 o -2 3 1 338.55 376.43 13.49 o -1 3 1 1.77 8.69 1.37 o 0 3 1 6.77 11.89 1.50 o 1 3 1 1106.70 1108.65 13.89 o 2 3 1 1041.41 958.08 17.66 o 3 3 1 91.51 101.25 2.85 o 4 3 1 315.92 379.05 10.04 o 5 3 1 279.43 303.84 8.17 o 6 3 1 0.56 1.30 1.12 o 7 3 1 81.96 85.04 2.53 o 8 3 1 227.62 244.63 5.76 o 9 3 1 20.98 23.23 1.21 o 10 3 1 55.04 53.22 1.78 o 11 3 1 24.67 27.60 1.59 o 12 3 1 46.23 43.78 2.57 o -11 4 1 5.39 6.89 1.36 o -10 4 1 60.11 60.88 2.33 o -9 4 1 6.19 8.22 1.15 o -8 4 1 114.87 104.07 2.97 o -7 4 1 146.33 157.39 4.56 o -6 4 1 3.52 4.23 1.06 o -5 4 1 101.40 98.47 1.60 o -4 4 1 1055.21 1083.68 32.44 o -3 4 1 586.15 674.94 21.59 o -2 4 1 41.51 52.75 1.09 o -1 4 1 1290.13 1306.17 23.49 o 0 4 1 532.33 541.72 8.91 o 1 4 1 852.53 875.10 16.64 o 2 4 1 469.94 497.70 9.59 o 3 4 1 77.40 94.46 2.06 o 4 4 1 358.68 410.34 8.81 o 5 4 1 134.70 140.84 3.33 o 6 4 1 48.11 48.86 1.81 o 7 4 1 0.01 1.86 1.10 o 8 4 1 15.62 18.58 0.99 o 9 4 1 21.76 24.54 1.25 o 10 4 1 10.66 11.08 1.32 o 11 4 1 37.03 39.30 1.68 o -11 5 1 0.44 0.00 1.99 o -10 5 1 14.88 15.91 1.41 o -9 5 1 15.86 18.29 2.04 o -8 5 1 23.68 26.49 1.22 o -7 5 1 2.02 3.80 1.12 o -6 5 1 449.35 436.53 14.91 o -5 5 1 281.11 287.30 8.81 o -4 5 1 1194.75 1210.01 30.79 o -3 5 1 140.00 152.98 3.11 o -2 5 1 898.76 936.42 14.41 o -1 5 1 162.76 170.51 1.75 o 0 5 1 746.64 768.05 11.16 o 1 5 1 880.18 903.19 12.47 o 2 5 1 2037.74 2047.00 41.15 o 3 5 1 19.24 15.07 1.08 o 4 5 1 243.72 254.56 6.08 o 5 5 1 337.61 341.31 5.87 o 6 5 1 165.46 162.48 4.35 o 7 5 1 131.38 125.70 3.82 o 8 5 1 29.86 33.17 1.25 o 9 5 1 51.52 49.19 1.39 o 10 5 1 4.70 5.91 1.54 o 11 5 1 8.25 11.32 1.63 o -10 6 1 13.75 18.35 2.13 o -9 6 1 43.88 35.77 1.41 o -8 6 1 41.46 45.77 1.58 o -7 6 1 118.55 106.97 2.91 o -6 6 1 0.07 1.33 1.08 o -5 6 1 814.76 759.24 23.92 o -4 6 1 0.71 4.15 1.09 o -3 6 1 361.22 369.77 7.98 o -2 6 1 68.75 68.83 1.71 o -1 6 1 65.00 64.90 1.40 o 0 6 1 0.76 2.12 1.04 o 1 6 1 10.58 10.85 1.06 o 2 6 1 192.60 190.02 5.46 o 3 6 1 522.28 507.94 15.46 o 4 6 1 412.08 402.78 11.38 o 5 6 1 722.01 703.16 13.76 o 6 6 1 77.63 83.76 2.02 o 7 6 1 19.81 20.15 1.32 o 8 6 1 0.66 0.82 1.25 o 9 6 1 68.49 67.70 1.78 o 10 6 1 18.52 24.30 1.60 o -9 7 1 10.03 13.03 1.92 o -8 7 1 2.98 10.21 3.31 o -7 7 1 57.11 52.90 1.15 o -6 7 1 2.89 1.87 1.22 o -5 7 1 6.93 7.11 1.03 o -4 7 1 31.29 33.62 1.10 o -3 7 1 1.97 3.94 1.18 o -2 7 1 23.54 23.66 1.13 o -1 7 1 0.27 0.41 1.09 o 0 7 1 193.44 196.40 3.98 o 1 7 1 55.94 54.20 1.19 o 2 7 1 94.33 82.62 2.47 o 3 7 1 125.54 115.50 5.14 o 4 7 1 7.90 10.20 1.23 o 5 7 1 115.25 101.19 2.36 o 6 7 1 0.77 0.77 1.24 o 7 7 1 30.29 30.84 1.41 o 8 7 1 10.81 11.31 1.37 o 9 7 1 7.77 6.92 1.49 o -8 8 1 1.91 4.79 1.77 o -7 8 1 36.97 33.35 1.77 o -6 8 1 80.35 81.06 2.20 o -5 8 1 7.72 6.15 1.06 o -4 8 1 0.67 0.11 1.44 o -3 8 1 29.96 35.64 1.43 o -2 8 1 130.95 132.61 2.24 o -1 8 1 6.41 6.98 1.09 o 0 8 1 3.19 4.68 1.16 o 1 8 1 2.87 4.16 1.17 o 2 8 1 16.94 19.25 1.18 o 3 8 1 116.79 113.69 2.86 o 4 8 1 2.08 2.26 1.44 o 5 8 1 0.43 0.63 1.27 o 6 8 1 42.55 43.19 1.43 o 7 8 1 72.59 64.25 1.75 o 8 8 1 31.89 32.08 1.30 o -7 9 1 0.14 0.00 2.97 o -6 9 1 60.55 57.09 1.82 o -5 9 1 1.05 0.27 1.53 o -4 9 1 67.36 73.07 1.45 o -3 9 1 0.00 0.00 1.15 o -2 9 1 122.00 129.51 1.87 o -1 9 1 16.85 16.40 1.14 o 0 9 1 70.23 72.69 2.24 o 1 9 1 0.26 0.60 1.27 o 2 9 1 261.18 253.26 4.42 o 3 9 1 0.75 0.41 1.40 o 4 9 1 41.87 46.64 1.66 o 5 9 1 18.65 20.72 1.28 o 6 9 1 23.62 24.60 1.65 o -4 10 1 6.51 4.73 1.41 o -3 10 1 105.74 110.23 2.97 o -2 10 1 0.02 0.63 1.57 o -1 10 1 71.30 72.70 1.69 o 0 10 1 7.70 7.37 1.55 o 1 10 1 37.10 36.29 1.40 o 2 10 1 0.09 0.00 1.27 o 3 10 1 73.13 71.43 1.71 o 4 10 1 17.75 16.01 1.68 o -12 0 2 8.58 6.30 1.92 o -10 0 2 67.59 63.05 1.93 o -8 0 2 358.35 344.03 12.12 o -6 0 2 1504.43 1439.84 69.23 o -4 0 2 1.93 3.08 1.84 o -2 0 2 908.93 906.97 7.17 o 2 0 2 380.58 384.36 7.70 o 4 0 2 677.94 668.06 28.12 o 6 0 2 78.09 81.41 2.28 o 8 0 2 12.01 14.18 2.12 o 10 0 2 1.39 0.79 1.44 o 12 0 2 65.86 68.35 6.18 o -12 1 2 6.94 4.67 1.59 o -11 1 2 3.83 4.81 1.16 o -10 1 2 0.01 0.00 1.30 o -9 1 2 224.95 212.85 4.19 o -8 1 2 4.44 3.85 1.02 o -7 1 2 771.68 716.79 17.59 o -6 1 2 79.96 81.76 2.00 o -5 1 2 70.82 56.75 2.64 o -4 1 2 33.15 46.61 1.69 o -3 1 2 417.10 353.80 10.86 o -2 1 2 298.93 292.56 7.84 o -1 1 2 72.05 95.41 3.16 o 1 1 2 1491.45 1517.83 76.59 o 2 1 2 484.89 441.20 4.90 o 3 1 2 539.04 499.04 7.45 o 4 1 2 1331.26 1364.54 32.65 o 5 1 2 382.67 404.66 8.02 o 6 1 2 131.60 137.16 2.80 o 7 1 2 249.55 250.72 3.98 o 8 1 2 32.13 31.40 1.37 o 9 1 2 31.01 32.12 1.30 o 10 1 2 10.11 9.86 1.36 o 11 1 2 101.75 97.78 2.13 o 12 1 2 20.55 22.09 1.82 o -12 2 2 2.94 3.98 1.60 o -11 2 2 0.04 0.73 1.25 o -10 2 2 13.07 14.26 1.35 o -9 2 2 38.84 38.97 1.20 o -8 2 2 120.39 113.79 2.02 o -7 2 2 80.14 83.62 2.47 o -6 2 2 273.58 243.42 5.79 o -5 2 2 64.44 62.00 1.93 o -4 2 2 242.16 260.78 12.36 o -3 2 2 825.10 857.54 33.03 o -2 2 2 153.39 182.82 6.63 o -1 2 2 0.04 5.47 1.33 o 0 2 2 369.78 297.46 6.75 o 1 2 2 700.10 752.92 9.65 o 2 2 2 87.79 112.21 1.50 o 3 2 2 570.57 551.49 11.20 o 4 2 2 777.39 782.60 18.56 o 5 2 2 474.82 457.67 10.57 o 6 2 2 129.09 129.07 2.59 o 7 2 2 46.27 44.64 1.06 o 8 2 2 84.76 86.18 1.59 o 9 2 2 2.37 3.32 1.25 o 10 2 2 100.59 100.71 2.14 o 11 2 2 77.43 78.38 1.59 o 12 2 2 22.49 22.64 1.83 o -12 3 2 7.40 8.11 1.55 o -11 3 2 1.80 3.53 1.15 o -10 3 2 6.67 4.66 1.22 o -9 3 2 17.29 19.11 1.28 o -8 3 2 3.91 2.56 1.11 o -7 3 2 25.99 23.60 1.80 o -6 3 2 0.92 0.88 1.23 o -5 3 2 25.41 27.75 1.14 o -4 3 2 168.93 164.21 6.71 o -3 3 2 187.09 205.67 5.48 o -2 3 2 120.55 128.06 4.62 o -1 3 2 19.07 28.60 1.28 o 0 3 2 1321.13 1382.30 21.24 o 1 3 2 477.45 450.93 4.95 o 2 3 2 736.35 770.58 12.98 o 3 3 2 299.01 280.73 4.15 o 4 3 2 265.43 287.29 7.38 o 5 3 2 0.99 5.29 1.36 o 6 3 2 0.42 1.69 0.99 o 7 3 2 53.84 48.43 1.15 o 8 3 2 264.53 265.35 4.76 o 9 3 2 25.89 27.14 1.24 o 10 3 2 0.22 1.18 1.38 o 11 3 2 154.76 161.66 7.48 o 12 3 2 21.04 23.23 1.77 o -11 4 2 53.29 58.52 2.79 o -10 4 2 39.10 41.27 1.57 o -9 4 2 0.30 0.45 1.21 o -8 4 2 207.67 194.87 6.32 o -7 4 2 79.71 85.79 3.29 o -6 4 2 296.34 287.05 9.16 o -5 4 2 96.18 107.48 2.30 o -4 4 2 198.67 209.69 6.40 o -3 4 2 93.80 88.72 2.69 o -2 4 2 288.25 305.51 6.08 o -1 4 2 1064.13 1068.71 24.73 o 0 4 2 189.89 183.25 3.27 o 1 4 2 974.54 940.04 11.78 o 2 4 2 265.35 266.40 5.13 o 3 4 2 190.86 209.33 6.25 o 4 4 2 1125.36 1115.71 23.64 o 5 4 2 33.34 31.94 1.11 o 6 4 2 15.96 16.09 1.19 o 7 4 2 244.06 235.96 5.58 o 8 4 2 20.12 20.02 1.20 o 9 4 2 63.11 65.26 2.21 o 10 4 2 124.48 127.82 4.28 o 11 4 2 0.06 0.00 1.60 o -11 5 2 8.68 9.92 1.53 o -10 5 2 5.49 5.28 1.49 o -9 5 2 81.54 77.06 3.59 o -8 5 2 26.69 31.43 1.50 o -7 5 2 412.34 394.41 14.19 o -6 5 2 11.98 10.85 1.02 o -5 5 2 447.52 426.75 11.65 o -4 5 2 254.17 261.65 3.39 o -3 5 2 405.20 415.40 10.70 o -2 5 2 9.63 9.99 1.04 o -1 5 2 0.01 7.92 1.25 o 0 5 2 536.66 554.29 11.33 o 1 5 2 953.08 934.66 13.24 o 2 5 2 11.78 14.93 1.10 o 3 5 2 906.93 906.61 22.32 o 4 5 2 123.91 122.65 2.46 o 5 5 2 29.03 33.68 1.17 o 6 5 2 8.82 8.80 1.14 o 7 5 2 77.62 85.56 1.72 o 8 5 2 3.12 3.73 1.21 o 9 5 2 8.33 8.43 1.17 o 10 5 2 0.30 1.29 1.44 o 11 5 2 19.91 18.88 1.64 o -10 6 2 26.98 29.46 2.48 o -9 6 2 28.62 30.43 1.60 o -8 6 2 27.78 24.24 1.53 o -7 6 2 113.78 122.16 3.48 o -6 6 2 80.31 77.96 3.18 o -5 6 2 78.94 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