#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/61/2016199.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2016199_Fobs loop_ _publ_author_name 'de Silva, Fernando' 'Wardell, James L.' 'Wardell, Solange M. S. V.' 'Ferreira, Vitor F.' 'Low, John N.' 'Glidewell, Christopher' _publ_section_title ; \p-Stacked dimers in 6-methoxy-3,3-dimethyl-3H-benzo[f]chromene, and centrosymmetric dimers containing C---H···\p(arene) hydrogen bonds in racemic 3-bromo-2,2,6,6-tetramethyl-3,4-dihydro-2H,6H-1,5-dioxatriphenylene ; _journal_coeditor_code GG3118 _journal_issue 10 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first o568 _journal_page_last o571 _journal_volume 63 _journal_year 2007 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 106.343 _cell_angle_gamma 90.000 _cell_length_a 10.7350 _cell_length_b 13.7043 _cell_length_c 12.0692 _exptl_crystal_F_000 768.00 _reflns_d_resolution_high 0.7688 _[local]_cod_data_source_file gg3118IVsup3.hkl _[local]_cod_data_source_block IV #BEGIN Tags that were not found in dictionaries: _shelx_title ' 0297 New: P21/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 183.82 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 439.73 -1.19 1.19 o 2 0 0 15956.77 14625.01 290.35 o 3 0 0 680.28 657.06 14.07 o 4 0 0 8123.95 7906.13 92.23 o 5 0 0 10955.14 10819.32 109.57 o 6 0 0 6808.89 6909.46 85.87 o 7 0 0 87.01 125.52 12.27 o 8 0 0 5947.56 6098.95 115.88 o 9 0 0 661.07 682.98 23.60 o 10 0 0 1026.76 1136.96 36.24 o 11 0 0 2805.86 2863.78 83.75 o 12 0 0 11.10 -2.18 30.83 o 13 0 0 570.63 472.82 58.57 o 2 1 0 8875.06 8409.02 102.87 o 3 1 0 11432.68 10912.30 101.20 o 4 1 0 2333.72 2323.09 20.70 o 5 1 0 1.26 8.54 4.88 o 6 1 0 1803.84 1775.30 17.60 o 7 1 0 2280.12 2356.94 28.32 o 8 1 0 7617.39 7895.58 73.35 o 9 1 0 1072.57 1035.81 17.23 o 10 1 0 244.84 240.65 12.74 o 11 1 0 1040.81 985.92 24.74 o 12 1 0 1398.75 1351.51 48.34 o 13 1 0 1080.80 1112.73 47.19 o 1 2 0 9861.50 9229.00 125.95 o 2 2 0 591.66 614.71 8.01 o 3 2 0 431.87 465.66 8.15 o 4 2 0 441.18 430.18 6.63 o 5 2 0 3557.30 3606.57 29.10 o 6 2 0 3884.03 4016.92 33.40 o 7 2 0 3.89 0.68 6.41 o 8 2 0 1514.77 1539.62 21.66 o 9 2 0 84.36 89.11 9.19 o 10 2 0 686.84 703.54 15.88 o 11 2 0 602.82 552.81 17.72 o 12 2 0 41.78 39.29 16.78 o 13 2 0 13.04 -4.48 22.70 o 1 3 0 4961.01 4732.74 38.76 o 2 3 0 648.03 644.54 9.01 o 3 3 0 1087.08 1074.80 10.74 o 4 3 0 331.80 353.06 5.99 o 5 3 0 584.38 675.57 9.85 o 6 3 0 117.05 146.53 6.90 o 7 3 0 79.49 97.00 7.08 o 8 3 0 1027.17 1035.34 15.85 o 9 3 0 1022.40 1028.97 17.22 o 10 3 0 35.68 18.54 11.85 o 11 3 0 273.51 244.79 16.73 o 12 3 0 0.71 -16.10 16.10 o 13 3 0 99.24 103.70 21.44 o 0 4 0 3490.95 3450.91 39.23 o 1 4 0 861.15 845.88 7.74 o 2 4 0 439.87 446.66 5.71 o 3 4 0 61.14 65.37 4.74 o 4 4 0 2990.96 3099.72 27.16 o 5 4 0 434.52 431.48 7.42 o 6 4 0 249.21 218.60 6.81 o 7 4 0 550.76 565.46 15.26 o 8 4 0 2563.81 2588.78 33.48 o 9 4 0 4.63 10.37 9.06 o 10 4 0 54.81 54.15 10.54 o 11 4 0 9.16 21.63 11.87 o 12 4 0 1.03 29.71 18.62 o 13 4 0 217.95 225.72 38.21 o 1 5 0 252.10 270.06 3.85 o 2 5 0 5886.24 5697.86 46.28 o 3 5 0 494.68 416.27 6.17 o 4 5 0 3738.63 4165.84 37.01 o 5 5 0 994.77 1188.83 14.87 o 6 5 0 1874.17 2027.34 30.34 o 7 5 0 3616.62 3697.34 40.81 o 8 5 0 387.14 377.29 9.88 o 9 5 0 1357.74 1375.45 24.47 o 10 5 0 11.31 11.22 10.43 o 11 5 0 275.21 241.15 15.73 o 12 5 0 939.57 938.53 30.85 o 0 6 0 5025.19 4725.26 57.31 o 1 6 0 4626.50 4514.15 33.67 o 2 6 0 1621.22 1672.61 15.39 o 3 6 0 184.06 180.80 4.44 o 4 6 0 9565.40 9594.37 82.49 o 5 6 0 2075.76 2006.09 21.41 o 6 6 0 3134.77 3261.97 32.42 o 7 6 0 86.77 83.88 7.96 o 8 6 0 50.32 55.05 8.32 o 9 6 0 1365.19 1406.84 26.32 o 10 6 0 2824.87 2837.54 61.46 o 11 6 0 1296.39 1278.65 46.70 o 12 6 0 4.62 9.55 32.62 o 1 7 0 1564.15 1389.82 12.16 o 2 7 0 5951.78 5812.83 51.60 o 3 7 0 10314.53 10145.70 105.47 o 4 7 0 420.91 367.83 12.85 o 5 7 0 917.17 922.97 12.74 o 6 7 0 956.87 930.49 12.65 o 7 7 0 1198.27 1248.02 17.94 o 8 7 0 3449.30 3570.36 49.85 o 9 7 0 778.87 736.61 17.71 o 10 7 0 28.10 38.78 11.87 o 11 7 0 754.41 694.43 36.00 o 12 7 0 1414.14 1357.65 52.36 o 0 8 0 5744.36 5566.35 107.15 o 1 8 0 2293.35 2242.10 21.07 o 2 8 0 6.09 3.43 3.45 o 3 8 0 275.08 293.07 6.31 o 4 8 0 614.24 590.10 8.77 o 5 8 0 5818.23 5985.16 63.78 o 6 8 0 867.70 864.48 12.87 o 7 8 0 8.37 7.56 6.91 o 8 8 0 234.30 224.44 16.02 o 9 8 0 1468.13 1480.74 33.26 o 10 8 0 543.22 541.75 28.40 o 11 8 0 478.94 454.34 30.55 o 1 9 0 88.67 84.53 3.86 o 2 9 0 667.07 623.13 13.27 o 3 9 0 728.75 744.10 10.92 o 4 9 0 242.90 274.72 5.93 o 5 9 0 40.07 50.66 5.12 o 6 9 0 354.62 377.96 9.15 o 7 9 0 281.41 300.77 9.41 o 8 9 0 262.78 236.48 10.77 o 9 9 0 182.88 178.50 12.21 o 10 9 0 237.16 249.33 23.15 o 11 9 0 254.91 248.82 29.04 o 0 10 0 30.13 50.05 6.12 o 1 10 0 23.05 22.68 3.43 o 2 10 0 813.92 833.81 12.30 o 3 10 0 31.32 33.74 4.29 o 4 10 0 1647.78 1741.18 22.51 o 5 10 0 29.51 34.20 5.58 o 6 10 0 323.07 297.83 10.53 o 7 10 0 398.98 364.66 12.48 o 8 10 0 64.24 30.33 8.29 o 9 10 0 411.62 429.29 22.46 o 10 10 0 18.77 53.00 18.87 o 11 10 0 18.86 21.60 24.33 o 1 11 0 321.74 355.78 6.85 o 2 11 0 566.57 589.31 11.15 o 3 11 0 785.06 806.18 17.33 o 4 11 0 246.39 224.90 13.70 o 5 11 0 1.41 -1.96 3.86 o 6 11 0 357.53 341.37 9.05 o 7 11 0 349.34 323.51 10.88 o 8 11 0 281.16 275.80 24.18 o 9 11 0 318.15 322.98 27.62 o 10 11 0 65.07 25.16 25.00 o 0 12 0 906.37 921.65 18.90 o 1 12 0 2270.23 2379.56 31.12 o 2 12 0 262.40 247.68 8.96 o 3 12 0 637.70 667.02 16.88 o 4 12 0 1852.89 1861.61 31.79 o 5 12 0 925.72 1002.29 26.72 o 6 12 0 229.89 256.54 17.91 o 7 12 0 29.14 30.27 8.31 o 8 12 0 25.93 27.06 17.28 o 9 12 0 379.03 401.01 62.88 o 1 13 0 106.16 111.02 5.21 o 2 13 0 2199.63 2196.85 36.38 o 3 13 0 286.68 295.91 12.28 o 4 13 0 477.84 510.09 21.90 o 5 13 0 219.89 210.28 17.42 o 6 13 0 215.43 202.70 18.15 o 7 13 0 1279.69 1266.25 40.96 o 8 13 0 1083.27 1121.92 46.41 o 9 13 0 60.38 33.24 21.29 o 0 14 0 1053.35 1091.65 25.88 o 1 14 0 288.74 296.16 7.48 o 2 14 0 377.04 351.92 12.75 o 3 14 0 231.92 234.24 11.74 o 4 14 0 458.69 427.38 20.04 o 5 14 0 785.31 819.75 27.10 o 6 14 0 298.15 354.93 20.44 o 7 14 0 51.80 54.67 25.67 o 8 14 0 127.87 89.98 26.33 o 1 15 0 640.76 617.56 13.84 o 2 15 0 147.85 161.82 12.04 o 3 15 0 211.36 224.75 16.61 o 4 15 0 19.89 12.46 14.29 o 5 15 0 132.11 130.28 23.14 o 6 15 0 419.64 411.74 30.72 o 7 15 0 299.18 247.28 27.34 o 0 16 0 141.15 119.96 14.89 o 1 16 0 90.13 83.89 10.95 o 2 16 0 30.03 27.62 23.11 o 3 16 0 25.17 17.05 13.13 o 4 16 0 36.79 36.26 19.35 o 5 16 0 17.78 36.22 35.14 o 1 17 0 12.09 9.39 14.14 o 2 17 0 22.84 23.91 21.03 o 3 17 0 1.02 7.00 15.09 o -13 1 1 224.05 187.62 26.59 o -12 1 1 49.72 42.42 17.38 o -11 1 1 104.26 90.06 11.22 o -10 1 1 1000.60 1044.12 20.81 o -9 1 1 2975.95 2985.07 38.18 o -8 1 1 4893.24 4988.83 48.85 o -7 1 1 1709.38 1689.37 17.80 o -6 1 1 5.92 9.31 5.58 o -5 1 1 194.70 181.84 5.80 o -4 1 1 6471.07 6166.66 49.33 o -3 1 1 3209.49 3306.99 26.75 o -2 1 1 1684.76 1680.23 40.45 o 0 1 1 10499.94 -0.76 0.76 o 1 1 1 1859.81 1750.28 34.54 o 2 1 1 2347.19 2395.89 23.28 o 3 1 1 642.92 638.00 8.39 o 4 1 1 185.37 246.64 5.89 o 5 1 1 978.27 1079.62 12.33 o 6 1 1 1747.95 1794.99 20.85 o 7 1 1 2359.06 2388.84 23.70 o 8 1 1 92.15 100.93 8.30 o 9 1 1 566.76 555.20 14.59 o 10 1 1 136.13 146.99 11.15 o 11 1 1 381.28 418.72 16.81 o 12 1 1 9.05 -19.46 19.46 o 13 1 1 617.44 582.70 32.00 o -13 2 1 300.17 327.38 29.95 o -12 2 1 1259.88 1194.24 56.20 o -11 2 1 2204.62 2255.33 42.98 o -10 2 1 964.10 995.67 18.11 o -9 2 1 4.00 4.92 8.71 o -8 2 1 340.70 354.44 10.15 o -7 2 1 2270.44 2384.19 21.59 o -6 2 1 5738.73 5796.33 54.34 o -5 2 1 2229.48 2211.41 25.19 o -4 2 1 60.85 105.74 4.93 o -3 2 1 296.56 291.58 4.84 o -2 2 1 4764.94 4703.63 39.27 o -1 2 1 172.15 213.02 3.88 o 0 2 1 18400.26 16462.46 211.77 o 1 2 1 3703.78 3661.22 52.08 o 2 2 1 1981.91 1972.96 23.24 o 3 2 1 1673.93 1599.62 18.33 o 4 2 1 2675.12 2430.42 22.54 o 5 2 1 10633.80 11011.33 83.67 o 6 2 1 425.65 435.46 8.56 o 7 2 1 311.47 330.30 9.94 o 8 2 1 7110.48 7319.77 86.10 o 9 2 1 2104.61 2161.32 30.37 o 10 2 1 670.94 666.77 16.76 o 11 2 1 28.05 29.14 14.54 o 12 2 1 305.34 285.45 24.00 o 13 2 1 1394.25 1298.21 52.05 o -13 3 1 609.00 629.61 35.03 o -12 3 1 1265.41 1371.92 57.58 o -11 3 1 1.84 11.76 13.01 o -10 3 1 702.14 746.05 19.93 o -9 3 1 4019.05 4158.05 57.06 o -8 3 1 4192.41 4276.21 47.08 o -7 3 1 1610.27 1728.46 30.48 o -6 3 1 48.09 75.01 6.68 o -5 3 1 3357.83 3451.34 29.25 o -4 3 1 18405.72 18064.14 140.71 o -3 3 1 6230.79 6088.24 56.20 o -2 3 1 538.36 481.48 6.08 o -1 3 1 11892.19 11559.52 92.44 o 0 3 1 21145.42 18975.27 227.35 o 1 3 1 30217.84 27647.04 282.87 o 2 3 1 13629.14 12856.44 121.20 o 3 3 1 789.55 718.40 8.38 o 4 3 1 7995.41 8631.64 78.37 o 5 3 1 111.61 83.56 7.83 o 6 3 1 5831.14 5834.75 57.69 o 7 3 1 7025.29 7087.99 66.78 o 8 3 1 355.53 395.55 10.66 o 9 3 1 2.76 6.08 9.58 o 10 3 1 664.35 655.66 16.71 o 11 3 1 1490.53 1534.33 34.81 o 12 3 1 990.62 972.83 41.73 o -13 4 1 6.72 21.58 21.02 o -12 4 1 1185.68 1176.31 38.86 o -11 4 1 1667.06 1714.32 37.82 o -10 4 1 3491.26 3534.15 58.35 o -9 4 1 352.50 386.17 11.28 o -8 4 1 2239.61 2293.31 30.58 o -7 4 1 2892.58 2947.57 32.31 o -6 4 1 6456.86 6598.95 65.73 o -5 4 1 2593.30 2610.23 23.53 o -4 4 1 132.83 137.65 5.47 o -3 4 1 1083.83 1063.27 9.51 o -2 4 1 6999.10 6502.36 45.67 o -1 4 1 27601.44 25775.83 204.36 o 0 4 1 279.72 229.40 3.49 o 1 4 1 91.64 98.20 4.55 o 2 4 1 1328.68 1286.27 14.73 o 3 4 1 6412.26 6172.84 53.56 o 4 4 1 9814.69 10182.33 95.99 o 5 4 1 600.26 516.20 8.94 o 6 4 1 25.63 11.99 7.02 o 7 4 1 650.02 656.03 11.22 o 8 4 1 379.93 377.27 11.76 o 9 4 1 3930.39 4135.78 56.97 o 10 4 1 1512.13 1483.11 30.05 o 11 4 1 24.87 19.66 12.27 o 12 4 1 833.37 821.56 29.63 o -13 5 1 371.71 394.99 30.93 o -12 5 1 350.08 329.53 19.89 o -11 5 1 29.16 46.20 16.12 o -10 5 1 660.43 662.89 18.31 o -9 5 1 2319.60 2389.58 34.99 o -8 5 1 737.13 765.34 14.80 o -7 5 1 516.72 520.04 11.02 o -6 5 1 0.65 1.87 6.75 o -5 5 1 193.17 178.55 5.57 o -4 5 1 9862.20 10304.36 95.10 o -3 5 1 1826.12 1725.64 17.12 o -2 5 1 326.27 331.30 4.69 o -1 5 1 1148.84 1245.36 10.52 o 0 5 1 34.06 29.10 3.54 o 1 5 1 7341.73 7199.86 66.83 o 2 5 1 2294.80 2292.90 19.16 o 3 5 1 412.33 426.26 6.77 o 4 5 1 140.01 175.45 5.47 o 5 5 1 2057.29 2133.78 29.17 o 6 5 1 1745.12 1793.81 20.36 o 7 5 1 2353.48 2468.90 28.04 o 8 5 1 699.37 744.74 16.93 o 9 5 1 959.40 950.09 19.21 o 10 5 1 353.06 315.53 15.11 o 11 5 1 621.97 602.29 24.87 o 12 5 1 588.86 542.76 29.36 o -12 6 1 179.77 199.52 22.57 o -11 6 1 194.08 187.72 19.14 o -10 6 1 161.62 148.77 14.03 o -9 6 1 11.89 15.31 9.20 o -8 6 1 1.41 7.08 8.70 o -7 6 1 59.41 59.92 7.20 o -6 6 1 157.88 204.73 7.01 o -5 6 1 2300.53 2493.76 29.76 o -4 6 1 2007.56 2229.93 20.07 o -3 6 1 1741.34 1826.29 17.93 o -2 6 1 2016.93 2080.17 22.34 o -1 6 1 52.37 80.09 3.06 o 0 6 1 346.10 293.32 5.20 o 1 6 1 81.20 86.59 5.19 o 2 6 1 17.11 12.57 4.60 o 3 6 1 79.51 87.78 4.99 o 4 6 1 1676.67 1741.56 18.34 o 5 6 1 479.88 473.75 8.06 o 6 6 1 174.49 186.56 7.20 o 7 6 1 276.27 286.66 9.03 o 8 6 1 6.77 8.70 7.76 o 9 6 1 113.68 110.21 9.60 o 10 6 1 196.87 215.49 15.60 o 11 6 1 6.81 -10.20 13.82 o 12 6 1 69.00 57.70 25.82 o -12 7 1 80.76 105.20 23.98 o -11 7 1 3.41 31.50 17.17 o -10 7 1 11.22 8.19 12.09 o -9 7 1 203.57 207.14 10.50 o -8 7 1 632.39 663.63 12.92 o -7 7 1 15.63 4.95 7.73 o -6 7 1 134.45 130.18 6.75 o -5 7 1 553.64 640.63 9.64 o -4 7 1 3531.13 3909.05 36.30 o -3 7 1 114.40 89.42 4.38 o -2 7 1 193.38 208.96 5.24 o -1 7 1 216.24 224.77 5.28 o 0 7 1 2223.93 2220.19 18.07 o 1 7 1 204.96 225.48 8.35 o 2 7 1 155.37 166.26 6.38 o 3 7 1 885.82 903.93 12.13 o 4 7 1 933.51 951.20 11.12 o 5 7 1 367.10 369.73 9.19 o 6 7 1 218.78 231.62 7.87 o 7 7 1 248.14 277.10 13.67 o 8 7 1 52.50 51.13 8.11 o 9 7 1 0.92 -4.33 10.86 o 10 7 1 179.50 148.78 14.36 o 11 7 1 76.25 92.73 26.57 o 12 7 1 101.28 66.75 21.52 o -12 8 1 432.61 393.76 30.94 o -11 8 1 538.57 508.49 27.88 o -10 8 1 191.78 181.47 19.05 o -9 8 1 128.91 138.76 9.52 o -8 8 1 57.59 65.23 7.37 o -7 8 1 1295.78 1291.75 18.36 o -6 8 1 1168.66 1159.93 15.14 o -5 8 1 1268.92 1363.39 16.07 o -4 8 1 154.14 178.03 7.11 o -3 8 1 709.86 755.56 10.49 o -2 8 1 2096.85 2143.47 23.46 o -1 8 1 2351.40 2395.17 23.28 o 0 8 1 968.97 963.28 10.25 o 1 8 1 89.18 101.66 2.74 o 2 8 1 916.87 940.57 12.63 o 3 8 1 17.97 15.33 5.47 o 4 8 1 3266.41 3291.17 33.79 o 5 8 1 1165.82 1192.59 20.87 o 6 8 1 7.76 2.65 4.81 o 7 8 1 248.56 253.12 8.35 o 8 8 1 226.37 257.63 11.72 o 9 8 1 907.38 894.11 25.02 o 10 8 1 385.32 354.94 22.53 o 11 8 1 85.56 100.69 25.59 o -11 9 1 37.79 58.84 24.82 o -10 9 1 515.56 494.02 28.49 o -9 9 1 1648.29 1631.73 33.58 o -8 9 1 1474.39 1493.49 29.54 o -7 9 1 132.15 144.09 8.42 o -6 9 1 91.06 98.87 5.93 o -5 9 1 39.14 49.50 5.31 o -4 9 1 2051.27 2042.30 25.10 o -3 9 1 7962.49 8050.99 104.07 o -2 9 1 489.14 484.41 8.26 o -1 9 1 740.76 801.29 10.10 o 0 9 1 298.08 273.38 5.62 o 1 9 1 2649.55 2663.26 31.04 o 2 9 1 3419.08 3360.71 49.25 o 3 9 1 5927.83 6216.92 89.73 o 4 9 1 479.77 520.40 14.15 o 5 9 1 4367.94 4542.17 57.30 o 6 9 1 2002.62 2011.58 29.19 o 7 9 1 526.05 551.67 13.55 o 8 9 1 557.70 588.97 20.84 o 9 9 1 6.76 -1.00 10.01 o 10 9 1 631.89 613.52 40.65 o 11 9 1 1528.22 1559.66 61.20 o -11 10 1 1200.02 1135.16 49.26 o -10 10 1 508.88 460.95 29.06 o -9 10 1 26.76 30.33 13.47 o -8 10 1 85.12 95.80 10.18 o -7 10 1 1085.41 1118.12 20.81 o -6 10 1 3368.47 3473.57 53.01 o -5 10 1 783.61 809.09 14.91 o -4 10 1 2.38 4.07 5.52 o -3 10 1 11.87 10.22 5.49 o -2 10 1 2404.06 2353.36 25.75 o -1 10 1 4092.47 4033.19 45.15 o 0 10 1 761.87 713.85 10.24 o 1 10 1 735.94 765.45 11.71 o 2 10 1 225.73 213.89 10.56 o 3 10 1 3790.40 3970.80 55.47 o 4 10 1 1497.97 1527.37 27.26 o 5 10 1 2406.33 2520.42 50.41 o 6 10 1 56.49 63.74 6.60 o 7 10 1 698.71 755.69 20.34 o 8 10 1 1113.22 1151.24 31.50 o 9 10 1 1259.90 1164.93 38.47 o 10 10 1 384.29 383.88 25.79 o -10 11 1 24.21 22.20 21.32 o -9 11 1 1043.10 1079.61 36.47 o -8 11 1 663.65 660.95 22.67 o -7 11 1 602.66 570.33 19.16 o -6 11 1 22.04 32.58 7.38 o -5 11 1 1239.67 1285.52 19.86 o -4 11 1 992.30 1015.43 16.18 o -3 11 1 2376.37 2453.23 30.58 o -2 11 1 1091.87 1085.69 15.90 o -1 11 1 529.03 525.58 12.15 o 0 11 1 1485.33 1477.97 17.68 o 1 11 1 828.34 846.51 18.53 o 2 11 1 3080.24 3103.26 55.69 o 3 11 1 9.63 10.25 7.99 o 4 11 1 73.08 52.89 11.98 o 5 11 1 400.72 389.26 14.89 o 6 11 1 920.84 916.81 25.07 o 7 11 1 578.50 564.20 15.87 o 8 11 1 219.54 207.18 16.01 o 9 11 1 2.53 -0.45 17.49 o 10 11 1 668.61 568.83 75.81 o -10 12 1 122.03 91.36 24.91 o -9 12 1 34.21 51.57 24.14 o -8 12 1 3.10 -8.34 10.33 o -7 12 1 178.42 179.83 8.85 o -6 12 1 1333.08 1415.76 30.78 o -5 12 1 105.50 110.27 10.55 o -4 12 1 147.29 152.35 7.05 o -3 12 1 37.89 44.68 5.45 o -2 12 1 22.75 24.69 4.64 o -1 12 1 524.57 520.34 10.03 o 0 12 1 1754.25 1772.42 22.44 o 1 12 1 137.95 139.24 8.32 o 2 12 1 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