#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/62/2016212.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2016212_Fobs loop_ _publ_author_name 'Clegg, William' 'Marder, Todd B.' 'Nlate, Sylvain' 'Scott, Andrew J.' _publ_section_title ; 2,3,5,6-Tetrakis[3,5-bis(trifluoromethyl)phenoxy]-2,5-bis(dimethylamino)2,3,5,6-tetrabora-1,4-dioxane diethyl ether 0.667-solvate ; _journal_coeditor_code SF3048 _journal_issue 10 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first o603 _journal_page_last o605 _journal_volume 63 _journal_year 2007 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 79.708 _cell_angle_beta 67.589 _cell_angle_gamma 71.879 _cell_length_a 14.8006 _cell_length_b 15.1969 _cell_length_c 18.1644 _exptl_crystal_F_000 1704.00 _reflns_d_resolution_high 0.8409 _[local]_cod_data_source_file sf3048Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' tbm100 in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 345.43 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 4910.96 6831.93 212.32 o 3 0 0 10951.92 10364.07 205.67 o 4 0 0 2237.91 2273.54 54.27 o 5 0 0 2359.61 2627.94 63.37 o 6 0 0 1969.12 2649.31 66.29 o 7 0 0 664.10 684.07 31.18 o 8 0 0 24.85 13.06 18.31 o 9 0 0 3106.72 3176.75 85.07 o 10 0 0 108.08 88.30 25.62 o 11 0 0 1413.79 1396.70 56.37 o 12 0 0 10.49 25.44 23.44 o 13 0 0 179.34 140.03 31.35 o 14 0 0 5.88 1.07 28.27 o 15 0 0 109.61 100.29 42.74 o -15 1 0 106.18 484.71 272.99 o -14 1 0 3.89 11.56 26.67 o -13 1 0 1.07 7.16 21.59 o -12 1 0 76.93 38.84 25.80 o -11 1 0 16.85 -4.54 21.14 o -10 1 0 0.02 -8.12 18.98 o -9 1 0 820.14 940.72 43.53 o -8 1 0 330.75 250.19 26.92 o -7 1 0 15.15 11.20 18.38 o -6 1 0 6654.73 6861.66 285.85 o -5 1 0 414.41 332.27 25.74 o -4 1 0 99.78 114.40 15.56 o -3 1 0 14994.80 14314.49 281.96 o -2 1 0 73.56 46.77 7.16 o -1 1 0 1965.49 1989.08 35.13 o 2 1 0 93.44 102.47 21.60 o 3 1 0 430.73 568.02 20.77 o 4 1 0 14.67 -6.91 10.71 o 5 1 0 1307.21 1596.32 46.88 o 6 1 0 131.07 195.64 21.18 o 7 1 0 2385.59 3115.42 78.32 o 8 1 0 2456.59 2904.22 86.86 o 9 1 0 15.15 26.35 20.40 o 10 1 0 425.74 547.41 47.34 o 11 1 0 17.86 10.03 22.98 o 12 1 0 41.27 54.89 24.27 o 13 1 0 14.83 34.34 28.24 o 14 1 0 510.28 530.39 49.38 o 15 1 0 0.03 -11.99 27.53 o -15 2 0 0.01 16.24 35.02 o -14 2 0 27.20 13.62 27.48 o -13 2 0 66.39 59.26 26.94 o -12 2 0 283.68 278.41 35.31 o -11 2 0 863.03 764.90 48.26 o -10 2 0 602.38 627.84 38.63 o -9 2 0 9.86 9.87 18.71 o -8 2 0 4.36 10.65 16.99 o -7 2 0 39.55 33.57 16.21 o -6 2 0 421.22 508.71 26.92 o -5 2 0 0.05 -5.51 15.63 o -4 2 0 2947.95 2802.14 55.03 o -3 2 0 15146.27 14836.51 392.43 o -2 2 0 28556.46 28128.73 468.07 o -1 2 0 2558.35 2049.50 37.05 o 0 2 0 405.41 439.49 37.68 o 1 2 0 505.68 550.89 17.41 o 2 2 0 74.85 44.92 6.10 o 3 2 0 1842.70 1820.28 44.54 o 4 2 0 3833.96 4539.89 97.46 o 5 2 0 77.20 126.96 16.78 o 6 2 0 2012.23 2943.46 72.79 o 7 2 0 139.72 108.94 20.47 o 8 2 0 2940.08 4139.85 133.28 o 9 2 0 2078.80 2269.50 68.57 o 10 2 0 5.01 -2.32 20.23 o 11 2 0 101.91 80.86 26.17 o 12 2 0 101.09 89.82 27.74 o 13 2 0 2.60 21.75 27.34 o 14 2 0 330.24 308.33 44.62 o 15 2 0 35.10 67.83 37.69 o 16 2 0 0.00 18.81 35.49 o -14 3 0 14.44 30.97 43.20 o -13 3 0 126.51 127.76 32.13 o -12 3 0 75.89 51.85 29.14 o -11 3 0 52.30 27.32 24.67 o -10 3 0 135.97 73.52 23.01 o -9 3 0 12.22 27.51 18.06 o -8 3 0 1668.74 1538.97 51.02 o -7 3 0 65.38 54.60 19.37 o -6 3 0 441.33 446.04 25.97 o -5 3 0 7491.77 7382.45 132.76 o -4 3 0 1830.95 1377.89 32.86 o -3 3 0 476.01 568.91 18.12 o -2 3 0 748.30 701.87 19.85 o -1 3 0 10277.12 9111.58 115.55 o 0 3 0 10242.67 8766.02 186.63 o 1 3 0 1373.28 1107.58 31.71 o 2 3 0 5180.61 4778.29 104.94 o 3 3 0 24554.74 28960.64 483.06 o 4 3 0 21265.50 28586.24 478.72 o 5 3 0 5049.41 6462.67 116.65 o 6 3 0 26.33 32.92 13.25 o 7 3 0 244.28 376.62 22.39 o 8 3 0 333.67 408.55 28.92 o 9 3 0 1.14 -4.63 18.16 o 10 3 0 421.09 427.31 35.31 o 11 3 0 11.42 -6.25 22.61 o 12 3 0 59.95 92.19 29.56 o 13 3 0 111.56 150.11 32.17 o 14 3 0 484.72 481.52 38.58 o 15 3 0 126.00 115.34 33.98 o 16 3 0 277.69 244.29 64.80 o -14 4 0 5.81 54.54 33.66 o -13 4 0 0.08 -27.57 31.25 o -12 4 0 51.75 52.17 30.22 o -11 4 0 9.61 26.25 25.52 o -10 4 0 21.50 35.83 23.44 o -9 4 0 14.34 3.72 22.98 o -8 4 0 44.39 23.44 19.47 o -7 4 0 10.28 -7.84 14.53 o -6 4 0 889.21 1058.99 58.52 o -5 4 0 1061.13 1316.40 38.74 o -4 4 0 1010.06 896.20 26.40 o -3 4 0 4969.99 4737.91 175.55 o -2 4 0 9646.38 8967.32 496.30 o -1 4 0 59.84 77.08 14.59 o 0 4 0 212.70 113.10 9.68 o 1 4 0 2246.64 1912.32 75.37 o 2 4 0 14123.08 13872.06 369.04 o 3 4 0 4344.87 4115.04 74.33 o 4 4 0 150.48 212.58 13.66 o 5 4 0 4999.34 6229.77 136.44 o 6 4 0 7.99 10.87 12.31 o 7 4 0 654.22 783.70 29.55 o 8 4 0 3515.99 4648.67 94.13 o 9 4 0 274.12 224.95 23.11 o 10 4 0 1.44 -7.51 16.23 o 11 4 0 262.84 260.28 28.96 o 12 4 0 626.43 610.83 37.40 o 13 4 0 22.18 3.82 33.61 o 14 4 0 194.35 196.39 37.13 o 15 4 0 150.71 149.97 37.13 o 16 4 0 0.00 13.47 32.06 o -13 5 0 1.41 30.33 45.04 o -12 5 0 22.58 33.09 38.60 o -11 5 0 1.19 33.09 29.37 o -10 5 0 110.24 80.59 25.37 o -9 5 0 164.83 155.15 26.55 o -8 5 0 1009.31 842.99 39.78 o -7 5 0 46.70 50.82 16.32 o -6 5 0 2122.75 2140.08 50.39 o -5 5 0 1968.08 1980.11 82.82 o -4 5 0 1964.00 2086.43 45.86 o -3 5 0 639.84 803.35 35.53 o -2 5 0 532.39 424.37 15.57 o -1 5 0 1488.92 1330.40 33.03 o 0 5 0 1106.08 958.02 21.17 o 1 5 0 45.17 45.78 8.96 o 2 5 0 1983.68 1972.93 62.04 o 3 5 0 450.99 430.07 20.13 o 4 5 0 3162.74 3462.21 82.81 o 5 5 0 1595.14 1925.57 42.84 o 6 5 0 3.51 4.39 11.73 o 7 5 0 5204.07 6681.60 125.82 o 8 5 0 1060.40 1014.80 35.53 o 9 5 0 470.12 572.13 31.28 o 10 5 0 0.19 -1.68 17.24 o 11 5 0 9.11 32.32 22.05 o 12 5 0 478.07 540.35 39.65 o 13 5 0 433.55 449.53 38.89 o 14 5 0 28.74 32.54 30.46 o 15 5 0 209.15 188.37 36.77 o 16 5 0 51.85 60.61 36.91 o -13 6 0 0.21 7.35 43.20 o -12 6 0 9.92 15.63 39.52 o -11 6 0 38.98 12.06 25.99 o -10 6 0 4.43 -6.45 20.98 o -9 6 0 373.97 260.40 30.09 o -8 6 0 3.70 -16.12 13.03 o -7 6 0 12.84 -12.73 12.91 o -6 6 0 358.37 346.25 22.28 o -5 6 0 319.72 383.50 28.33 o -4 6 0 36.44 48.52 12.91 o -3 6 0 622.27 481.74 19.48 o -2 6 0 10.66 8.63 9.25 o -1 6 0 3425.80 3232.61 85.97 o 0 6 0 992.65 1011.11 17.42 o 1 6 0 280.61 410.02 19.30 o 2 6 0 2990.52 3521.59 96.97 o 3 6 0 2931.89 3096.28 243.57 o 4 6 0 20.39 18.35 9.99 o 5 6 0 1540.60 1747.23 40.17 o 6 6 0 94.66 141.64 17.08 o 7 6 0 546.85 610.92 25.90 o 8 6 0 67.12 73.90 18.66 o 9 6 0 1306.66 1555.11 46.87 o 10 6 0 882.48 1149.98 43.41 o 11 6 0 1444.30 1524.63 52.48 o 12 6 0 1320.78 1631.14 58.21 o 13 6 0 200.47 199.97 33.97 o 14 6 0 26.65 -1.32 25.73 o 15 6 0 38.54 49.65 34.03 o 16 6 0 57.25 58.05 35.47 o -12 7 0 0.00 5.51 44.12 o -11 7 0 23.23 0.00 39.52 o -10 7 0 27.68 -1.84 34.01 o -9 7 0 0.53 -12.97 17.86 o -8 7 0 101.34 92.21 21.31 o -7 7 0 539.48 521.79 26.80 o -6 7 0 533.49 525.08 32.34 o -5 7 0 123.62 130.33 17.25 o -4 7 0 0.02 8.94 12.27 o -3 7 0 248.77 220.85 16.76 o -2 7 0 1711.92 1767.12 39.08 o -1 7 0 588.57 608.93 19.80 o 0 7 0 4579.15 4361.92 59.36 o 1 7 0 794.35 870.84 67.10 o 2 7 0 3993.55 3914.86 93.29 o 3 7 0 461.69 457.43 64.80 o 4 7 0 24.64 14.06 16.54 o 5 7 0 1084.72 1160.26 49.90 o 6 7 0 419.86 409.31 21.94 o 7 7 0 1351.60 1368.37 43.60 o 8 7 0 756.24 869.30 32.89 o 9 7 0 175.66 170.75 22.92 o 10 7 0 45.42 41.91 21.02 o 11 7 0 330.03 291.45 30.85 o 12 7 0 58.74 94.19 27.86 o 13 7 0 1.12 -1.50 24.03 o 14 7 0 68.48 46.02 29.11 o 15 7 0 1.57 -15.70 29.26 o 16 7 0 89.47 105.60 39.07 o -12 8 0 18.26 214.16 54.23 o -11 8 0 0.01 -15.63 40.44 o -10 8 0 209.33 281.26 53.31 o -9 8 0 16.57 37.73 26.50 o -8 8 0 457.67 422.14 35.86 o -7 8 0 756.75 806.68 90.54 o -6 8 0 279.74 275.16 23.50 o -5 8 0 108.85 84.51 18.26 o -4 8 0 2.90 1.23 14.53 o -3 8 0 19.31 1.95 12.57 o -2 8 0 222.30 171.63 14.73 o -1 8 0 145.07 143.10 13.58 o 0 8 0 3035.40 3243.92 56.31 o 1 8 0 715.62 626.07 39.06 o 2 8 0 979.26 1038.85 58.83 o 3 8 0 545.01 461.65 20.19 o 4 8 0 0.73 -7.35 18.38 o 5 8 0 1722.90 2019.34 64.80 o 6 8 0 44.70 81.34 15.54 o 7 8 0 71.04 105.32 17.33 o 8 8 0 4.77 12.45 15.27 o 9 8 0 87.94 54.78 21.85 o 10 8 0 0.63 17.01 23.01 o 11 8 0 553.17 659.95 38.06 o 12 8 0 703.16 868.81 46.65 o 13 8 0 151.41 118.61 31.49 o 14 8 0 104.14 83.11 33.68 o 15 8 0 136.34 127.02 37.88 o -11 9 0 139.76 61.58 50.55 o -10 9 0 299.05 227.03 51.47 o -9 9 0 42.05 53.15 32.24 o -8 9 0 364.09 388.94 39.12 o -7 9 0 272.10 294.82 80.88 o -6 9 0 37.37 46.88 40.44 o -4 9 0 386.02 397.13 37.93 o -3 9 0 5.06 31.48 14.28 o -2 9 0 1156.16 1229.02 73.63 o -1 9 0 1470.63 1441.69 46.47 o 0 9 0 894.66 938.85 19.40 o 1 9 0 177.43 181.87 11.63 o 2 9 0 1896.75 1675.89 54.23 o 3 9 0 1.60 2.47 9.78 o 4 9 0 1037.00 1059.32 90.54 o 5 9 0 1302.09 1301.05 106.16 o 6 9 0 1399.16 1423.63 137.41 o 7 9 0 0.52 -4.30 13.17 o 8 9 0 119.16 88.24 19.29 o 9 9 0 125.59 79.41 21.19 o 10 9 0 255.83 244.93 28.97 o 11 9 0 2459.84 2529.57 90.11 o 12 9 0 642.54 678.99 53.90 o 13 9 0 425.25 504.89 54.58 o 14 9 0 166.67 114.78 41.17 o 15 9 0 20.76 2.66 35.72 o -10 10 0 3.24 5.51 36.77 o -9 10 0 0.78 30.25 33.99 o -8 10 0 14.71 0.53 38.60 o -7 10 0 1.03 8.17 24.46 o -6 10 0 16.76 17.13 24.65 o -5 10 0 19.28 4.98 20.76 o -4 10 0 1078.42 1091.74 51.93 o -3 10 0 329.31 398.53 31.71 o -2 10 0 48.61 63.72 14.64 o -1 10 0 32.31 -1.22 12.41 o 0 10 0 740.20 738.41 25.00 o 1 10 0 54.40 63.33 11.67 o 2 10 0 1228.35 1358.72 56.07 o 3 10 0 2.41 23.29 14.45 o 4 10 0 1022.23 1054.59 71.23 o 5 10 0 228.92 211.40 38.60 o 6 10 0 684.12 456.82 47.80 o 7 10 0 44.49 -6.43 23.90 o 8 10 0 99.23 139.27 27.82 o 9 10 0 725.09 828.40 46.37 o 10 10 0 1341.23 1398.45 68.02 o 11 10 0 6.50 3.67 26.32 o 12 10 0 30.63 62.93 31.28 o 13 10 0 14.16 20.97 34.28 o 14 10 0 20.36 51.47 42.19 o 15 10 0 21.53 17.81 41.74 o -9 11 0 8.44 13.81 37.09 o -8 11 0 202.82 212.65 39.04 o -7 11 0 83.71 126.17 32.46 o -6 11 0 14.92 20.13 26.03 o -5 11 0 995.36 1003.94 81.34 o -4 11 0 106.04 69.10 26.55 o -3 11 0 37.51 46.55 23.01 o -2 11 0 13.05 1.21 18.45 o -1 11 0 414.48 428.32 51.47 o 0 11 0 1430.33 1389.11 46.76 o 1 11 0 101.15 106.08 19.62 o 2 11 0 244.88 283.10 44.12 o 3 11 0 279.43 221.51 42.28 o 4 11 0 253.28 265.63 44.12 o 5 11 0 428.52 379.61 47.80 o 6 11 0 383.51 376.85 47.80 o 7 11 0 210.09 185.67 44.12 o 8 11 0 2071.84 1820.83 105.70 o 9 11 0 335.54 410.36 39.90 o 10 11 0 482.70 414.41 75.37 o 11 11 0 251.47 283.55 43.69 o 12 11 0 45.92 28.51 33.72 o 13 11 0 108.63 31.93 42.28 o 14 11 0 4.92 0.00 44.12 o 15 11 0 41.82 27.15 39.94 o -8 12 0 146.84 271.15 76.29 o -7 12 0 4.27 91.00 64.34 o -6 12 0 8.86 50.55 45.96 o -5 12 0 91.98 144.31 48.71 o -4 12 0 3.40 -0.92 36.77 o -3 12 0 29.00 39.52 45.04 o -2 12 0 919.23 948.56 74.45 o -1 12 0 172.79 211.40 44.12 o 0 12 0 1197.95 1011.06 75.37 o 1 12 0 547.99 539.54 60.66 o 2 12 0 72.15 5.51 33.09 o 3 12 0 367.83 363.06 49.63 o 4 12 0 57.04 31.25 34.93 o 5 12 0 101.78 135.11 44.12 o 6 12 0 204.80 214.16 45.96 o 7 12 0 880.54 654.43 63.42 o 8 12 0 175.94 150.74 42.28 o 9 12 0 1307.43 1469.71 102.03 o 10 12 0 52.39 54.23 43.20 o 11 12 0 53.71 51.93 32.50 o 12 12 0 5.78 -9.11 30.87 o 13 12 0 36.08 28.51 36.33 o 14 12 0 156.29 139.36 52.85 o -7 13 0 21.33 16.54 56.99 o -6 13 0 0.01 -5.51 43.20 o -5 13 0 0.28 34.93 47.80 o -4 13 0 11.54 35.85 48.71 o -3 13 0 97.08 131.44 52.39 o -2 13 0 56.59 45.96 41.36 o -1 13 0 131.32 214.16 55.15 o 0 13 0 959.93 1030.36 78.13 o 1 13 0 122.16 102.03 45.96 o 2 13 0 364.16 303.32 56.07 o 3 13 0 13.77 27.57 31.25 o 4 13 0 88.49 111.22 45.04 o 5 13 0 301.75 196.70 47.80 o 6 13 0 0.27 0.92 30.33 o 7 13 0 41.15 17.46 32.17 o 9 13 0 0.08 7.35 40.44 o 10 13 0 289.25 276.66 56.07 o 11 13 0 31.45 25.74 43.20 o 12 13 0 4.62 8.27 44.12 o 13 13 0 73.64 102.21 43.58 o -6 14 0 24.76 52.39 58.83 o -5 14 0 7.30 22.06 56.07 o -4 14 0 7.65 11.03 46.88 o -3 14 0 162.12 151.66 49.63 o -2 14 0 56.21 89.16 47.80 o -1 14 0 137.15 121.33 47.80 o 0 14 0 214.49 256.44 55.15 o 1 14 0 298.23 346.52 56.99 o 2 14 0 130.82 143.39 50.55 o 3 14 0 211.79 240.82 52.39 o 4 14 0 14.68 16.54 34.01 o 5 14 0 5.66 16.54 35.85 o 6 14 0 130.57 136.03 45.96 o 7 14 0 323.98 244.49 52.39 o 8 14 0 388.41 320.78 56.07 o 9 14 0 91.61 62.50 42.28 o 10 14 0 1.07 5.51 46.88 o 11 14 0 64.50 56.99 47.80 o 12 14 0 4.64 -6.43 52.39 o 13 14 0 122.46 166.37 64.34 o -4 15 0 20.13 56.99 57.91 o -3 15 0 0.40 56.07 57.91 o -2 15 0 56.36 65.26 48.71 o -1 15 0 2.28 13.79 38.60 o 0 15 0 147.47 207.73 60.66 o 1 15 0 250.80 303.32 62.50 o 2 15 0 121.93 168.20 51.47 o 3 15 0 6.26 7.35 41.36 o 4 15 0 7.29 13.79 34.93 o 5 15 0 78.45 43.20 36.77 o 6 15 0 151.59 156.25 46.88 o 7 15 0 51.54 30.33 40.44 o 8 15 0 84.95 95.59 50.55 o 9 15 0 18.73 17.46 48.71 o 10 15 0 0.27 -30.33 36.77 o 11 15 0 53.62 -5.51 45.96 o 12 15 0 10.92 48.71 53.31 o -2 16 0 0.11 13.79 52.39 o -1 16 0 6.60 -24.82 34.93 o 0 16 0 108.87 137.87 57.91 o 1 16 0 1.80 -8.27 33.09 o 2 16 0 29.03 28.49 36.77 o 4 16 0 416.59 463.25 68.02 o 5 16 0 47.47 48.71 44.12 o 6 16 0 34.24 -3.68 32.17 o 7 16 0 18.16 34.93 40.44 o 8 16 0 8.83 -12.87 41.36 o 9 16 0 20.84 7.35 45.04 o 10 16 0 86.82 51.47 48.71 o 0 17 0 6.61 -12.87 45.04 o 1 17 0 12.40 48.71 50.55 o 2 17 0 54.56 121.33 57.91 o 3 17 0 16.52 4.60 38.60 o 4 17 0 120.56 164.53 57.91 o 5 17 0 32.43 79.05 55.15 o 6 17 0 41.76 59.74 51.47 o 8 17 0 19.97 22.98 42.28 o -7 -17 1 18.18 51.47 44.12 o -6 -17 1 3.15 -13.79 35.85 o -5 -17 1 12.55 11.95 42.28 o -4 -17 1 142.82 116.73 54.23 o -3 -17 1 0.37 -22.98 30.33 o -2 -17 1 274.60 275.74 60.66 o -1 -17 1 1.59 73.53 53.31 o 0 -17 1 57.22 136.03 60.66 o -10 -16 1 0.39 -5.51 45.96 o -9 -16 1 5.87 17.46 40.44 o -8 -16 1 13.99 5.51 44.12 o -7 -16 1 6.71 -10.11 36.77 o -6 -16 1 44.62 56.07 40.44 o -5 -16 1 19.26 42.28 43.20 o -3 -16 1 288.82 226.11 52.39 o -2 -16 1 138.73 142.47 50.55 o -1 -16 1 318.19 344.68 56.07 o 0 -16 1 0.16 -27.57 35.85 o 1 -16 1 35.90 39.52 53.31 o 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