#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/62/2016215.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2016215_Fobs loop_ _publ_author_name 'Sun, Wei' 'Li, Yan-Tuan' 'Wu, Zhi-Yong' 'Liu, Jin-Liang' _publ_section_title ; Aqua-2\kO-\m-{N,N'-bis[2-(dimethylamino)ethyl]oxamidato(2--)}-1\k^2^O,O':2\k^4^N,N',N'',N'''-bis(4,4'-dimethyl-2,2'-bipyridine-1\k^2^N,N')copper(II)nickel(II) bis(perchlorate) methanol hemisolvate ; _journal_coeditor_code SF3053 _journal_issue 10 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first m462 _journal_page_last m464 _journal_volume 63 _journal_year 2007 _space_group_IT_number 61 _symmetry_space_group_name_Hall '-P 2ac 2ab' _symmetry_space_group_name_H-M 'P b c a' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 21.3468 _cell_length_b 14.8520 _cell_length_c 25.0872 _exptl_crystal_F_000 3888.00 _reflns_d_resolution_high 0.8334 _[local]_cod_data_source_file sf3053Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' b25 in Pbca' _shelx_refln_list_code 4 _shelx_f_calc_maximum 634.25 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' '-x, -y, -z' 'x-1/2, y, -z-1/2' 'x, -y-1/2, z-1/2' '-x-1/2, y-1/2, z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 319330.25 347879.69 62265.37 o 6 0 0 26165.85 30644.57 5493.92 o 8 0 0 9552.99 9353.39 1683.44 o 10 0 0 9970.27 8192.58 1474.30 o 12 0 0 28286.12 29184.72 5230.26 o 14 0 0 7259.95 7413.44 1337.46 o 16 0 0 19279.13 18443.17 3312.81 o 18 0 0 19.76 -22.90 91.87 o 20 0 0 132.54 44.82 146.43 o 22 0 0 28.56 -110.93 142.88 o 24 0 0 2893.41 3784.90 1037.41 o 2 1 0 152207.13 163065.08 29202.47 o 4 1 0 367058.94 386366.91 46232.51 o 6 1 0 915.00 1251.47 163.65 o 8 1 0 93662.48 89889.52 11381.19 o 10 1 0 10193.99 8066.88 1025.39 o 12 1 0 1823.88 1493.21 199.50 o 14 1 0 5834.28 5550.85 710.81 o 16 1 0 9463.52 9051.63 1152.82 o 18 1 0 40.76 85.00 86.14 o 20 1 0 4246.05 4268.95 648.87 o 22 1 0 157.84 401.25 175.49 o 24 1 0 107.74 203.97 128.46 o 0 2 0 402269.63 443672.41 116143.76 o 2 2 0 278.65 129.09 34.43 o 4 2 0 103080.33 101643.72 12167.27 o 6 2 0 2542.42 2876.46 355.10 o 8 2 0 29577.61 29816.50 3776.67 o 10 2 0 7976.03 7701.63 979.13 o 12 2 0 8230.42 6512.90 831.40 o 14 2 0 2907.81 3311.53 429.08 o 16 2 0 7997.48 7390.14 943.80 o 18 2 0 1152.59 1094.67 193.22 o 20 2 0 152.22 -33.31 77.13 o 22 2 0 5.60 -94.57 144.87 o 24 2 0 2022.65 2245.65 646.50 o 2 3 0 3933.89 5189.11 771.79 o 4 3 0 399436.97 430032.19 51381.83 o 6 3 0 11939.50 12034.66 1460.00 o 8 3 0 81284.06 78588.99 9428.30 o 10 3 0 579.26 849.41 119.97 o 12 3 0 2894.46 2952.28 380.58 o 14 3 0 111.14 89.92 79.35 o 16 3 0 4980.15 4888.04 627.49 o 18 3 0 30.94 -12.37 77.16 o 20 3 0 7442.53 7429.92 1113.53 o 22 3 0 293.12 -83.47 124.06 o 24 3 0 1077.10 968.19 339.00 o 0 4 0 105192.98 110741.51 28980.92 o 2 4 0 798.28 515.16 73.49 o 4 4 0 55.36 51.17 33.85 o 6 4 0 11408.07 13339.18 1601.75 o 8 4 0 77901.05 78549.29 9412.48 o 10 4 0 856.37 1030.94 132.92 o 12 4 0 40928.32 40000.40 5069.66 o 14 4 0 171.27 173.45 54.79 o 16 4 0 2934.80 3150.92 480.82 o 18 4 0 38.91 -37.26 103.64 o 20 4 0 138.94 -80.32 225.19 o 22 4 0 2030.92 2355.35 514.05 o 24 4 0 1920.80 2273.16 657.14 o 2 5 0 13687.83 14292.36 1869.10 o 4 5 0 9418.13 9412.94 1299.48 o 6 5 0 35561.06 35108.43 4828.26 o 8 5 0 25042.57 27152.51 3250.28 o 10 5 0 38334.01 40420.73 4853.68 o 12 5 0 2252.68 2494.27 299.87 o 14 5 0 4073.22 4273.53 549.54 o 16 5 0 16051.63 15918.66 2361.69 o 18 5 0 683.29 778.96 190.39 o 20 5 0 11433.73 11739.43 2121.00 o 22 5 0 5.54 -114.31 126.92 o 24 5 0 2327.38 2361.14 464.59 o 0 6 0 15919.24 16977.94 4466.90 o 2 6 0 3247.67 2938.37 389.47 o 4 6 0 6695.43 7677.15 1058.50 o 6 6 0 53242.87 59933.56 8221.50 o 8 6 0 52178.47 51230.90 7043.28 o 10 6 0 1.93 -22.62 40.02 o 12 6 0 62421.96 65145.53 7812.96 o 14 6 0 7329.48 7917.46 1096.78 o 16 6 0 16270.68 16255.05 2915.01 o 18 6 0 18975.69 17650.87 3170.72 o 20 6 0 70.17 -111.15 111.15 o 22 6 0 1671.69 1877.20 383.16 o 24 6 0 1180.58 1376.70 469.90 o 2 7 0 2709.45 2969.55 393.49 o 4 7 0 34349.14 36800.71 5442.45 o 6 7 0 16027.26 16501.60 2276.43 o 8 7 0 20757.03 22314.34 3079.00 o 10 7 0 16480.30 16860.83 2316.76 o 12 7 0 1.70 -55.72 55.72 o 14 7 0 9188.76 9275.77 1675.69 o 16 7 0 13113.84 13728.16 2472.91 o 18 7 0 392.84 281.61 135.59 o 20 7 0 5456.17 5547.38 1018.12 o 22 7 0 421.49 238.47 205.00 o 0 8 0 2623.22 2846.44 759.20 o 2 8 0 3882.12 4830.03 634.48 o 4 8 0 402.88 527.14 98.32 o 6 8 0 7380.76 7049.89 973.04 o 8 8 0 6643.36 7232.28 997.43 o 10 8 0 4831.03 4508.16 742.14 o 12 8 0 17344.64 18916.48 3074.04 o 14 8 0 3325.50 3934.93 730.61 o 16 8 0 2348.23 2568.15 492.87 o 18 8 0 1636.02 2085.05 414.93 o 20 8 0 425.49 67.10 160.85 o 22 8 0 1299.22 1209.86 278.56 o 2 9 0 33463.80 37300.19 4865.57 o 4 9 0 761.10 666.22 116.53 o 6 9 0 426.26 203.29 61.53 o 8 9 0 19495.27 22648.34 3656.99 o 10 9 0 4556.01 4695.01 780.24 o 12 9 0 1054.86 1130.02 243.73 o 14 9 0 4031.45 4351.96 800.46 o 16 9 0 917.87 764.02 197.66 o 18 9 0 3193.88 3713.91 1022.77 o 20 9 0 2039.98 2131.26 427.33 o 22 9 0 58.29 -185.26 309.05 o 0 10 0 41505.60 44632.11 7984.60 o 2 10 0 1237.63 1399.50 194.81 o 4 10 0 24229.74 27389.52 4046.92 o 6 10 0 8666.61 8019.73 1304.56 o 8 10 0 506.67 615.35 133.54 o 10 10 0 10075.41 10752.49 1758.23 o 12 10 0 1419.81 1535.74 308.87 o 14 10 0 107.67 66.23 237.83 o 16 10 0 4718.15 4904.34 904.73 o 18 10 0 2510.04 2623.80 511.21 o 20 10 0 134.99 56.10 235.17 o 2 11 0 47854.75 52279.50 7848.75 o 4 11 0 2149.39 2732.68 507.17 o 6 11 0 18580.56 20332.54 3305.74 o 8 11 0 24552.64 30342.29 4909.99 o 10 11 0 926.02 727.84 182.15 o 12 11 0 1868.26 2281.10 442.22 o 14 11 0 2302.04 2726.68 522.25 o 16 11 0 76.70 -122.16 326.13 o 18 11 0 184.82 51.99 132.68 o 20 11 0 122.92 -134.47 134.47 o 0 12 0 38555.06 45463.62 8346.46 o 2 12 0 4486.43 4703.06 692.22 o 4 12 0 9914.60 11833.50 2128.17 o 6 12 0 10208.96 10837.48 1758.73 o 8 12 0 4448.71 4124.76 695.85 o 10 12 0 5323.79 6281.06 1144.59 o 12 12 0 1210.34 1056.08 237.46 o 14 12 0 71.35 91.61 204.55 o 16 12 0 376.81 489.59 174.03 o 18 12 0 88.66 -194.41 319.48 o 2 13 0 8122.99 8621.13 1255.26 o 4 13 0 2705.44 3347.53 616.54 o 6 13 0 2257.21 2948.93 482.45 o 8 13 0 4337.36 5225.37 868.90 o 10 13 0 15.22 -47.12 110.67 o 12 13 0 3123.98 3150.70 593.47 o 14 13 0 1788.49 1319.69 319.03 o 16 13 0 178.56 72.20 128.51 o 0 14 0 35.53 57.24 153.08 o 2 14 0 24.56 -95.12 95.12 o 4 14 0 4195.68 4936.70 728.97 o 6 14 0 5790.32 6286.50 1032.15 o 8 14 0 13.40 -79.93 110.59 o 10 14 0 4595.45 4696.41 867.06 o 12 14 0 1049.80 1012.46 241.80 o 14 14 0 55.19 -150.11 173.94 o 2 15 0 2597.25 3140.91 573.12 o 4 15 0 1023.21 1257.55 307.99 o 6 15 0 0.33 -112.16 112.16 o 8 15 0 1743.09 1892.51 374.79 o 10 15 0 1818.96 1868.73 375.37 o 12 15 0 396.75 573.64 188.49 o 0 16 0 1910.25 2198.62 595.91 o 2 16 0 576.05 790.26 286.64 o 4 16 0 12.62 -149.53 149.53 o 6 16 0 1022.86 832.41 297.29 o 8 16 0 1380.86 2139.91 419.16 o 10 16 0 316.78 74.49 244.71 o 2 17 0 302.88 280.87 210.77 o 4 17 0 1922.91 1950.58 552.87 o 6 17 0 138.22 140.21 216.98 o 1 1 1 6878.70 6369.11 1564.10 o 2 1 1 28384.87 24353.25 2426.72 o 3 1 1 66.95 73.46 17.61 o 4 1 1 1774.75 1360.80 119.36 o 5 1 1 3590.98 3250.67 285.75 o 6 1 1 12390.94 10981.66 984.68 o 7 1 1 10.44 19.64 23.01 o 8 1 1 13899.01 13708.49 1228.26 o 9 1 1 9394.59 9808.66 879.19 o 10 1 1 2424.67 2394.04 218.39 o 11 1 1 1865.74 2205.85 203.47 o 12 1 1 1128.57 1019.76 101.66 o 13 1 1 1107.93 1331.25 128.71 o 14 1 1 1301.92 1471.41 141.88 o 15 1 1 4.66 7.35 38.72 o 16 1 1 399.07 361.80 57.43 o 17 1 1 1148.65 1129.03 115.37 o 18 1 1 3.25 -48.32 48.32 o 19 1 1 863.37 908.55 108.53 o 20 1 1 640.96 583.75 91.71 o 21 1 1 132.64 168.63 73.30 o 22 1 1 229.07 150.44 83.15 o 23 1 1 13.52 214.28 92.91 o 24 1 1 151.58 256.59 97.74 o 25 1 1 11.20 -102.98 139.82 o 0 2 1 121397.73 129602.58 23183.08 o 1 2 1 953.42 813.05 108.30 o 2 2 1 206.44 247.93 35.04 o 3 2 1 5317.18 5536.82 542.25 o 4 2 1 52641.77 50304.83 4261.92 o 5 2 1 36702.96 36643.53 3105.82 o 6 2 1 5488.07 5374.03 459.13 o 7 2 1 131.25 182.62 28.35 o 8 2 1 8762.60 9010.13 788.09 o 9 2 1 2259.27 2101.19 193.05 o 10 2 1 390.89 322.36 42.92 o 11 2 1 5795.32 5843.84 526.64 o 12 2 1 575.41 562.94 63.40 o 13 2 1 1358.20 1786.86 165.97 o 14 2 1 3483.72 3356.23 306.65 o 15 2 1 96.64 10.84 41.37 o 16 2 1 97.69 70.23 42.48 o 17 2 1 2867.40 2935.51 270.11 o 18 2 1 4890.99 5054.42 493.70 o 19 2 1 893.64 1028.30 129.56 o 20 2 1 166.05 117.27 64.81 o 21 2 1 149.14 125.90 65.78 o 22 2 1 449.75 575.96 129.56 o 23 2 1 645.66 689.04 151.24 o 24 2 1 21.29 -54.35 185.80 o 25 2 1 55.80 -121.58 121.58 o 1 3 1 19345.23 20873.52 2225.07 o 2 3 1 78.45 78.77 37.11 o 3 3 1 42139.43 47003.37 4247.29 o 4 3 1 54500.18 54992.77 4960.58 o 5 3 1 3961.06 3757.13 323.69 o 6 3 1 85035.21 88176.86 7457.28 o 7 3 1 6422.55 7115.72 607.84 o 8 3 1 29550.91 26981.91 2286.47 o 9 3 1 10977.89 10391.92 882.38 o 10 3 1 21687.34 20231.15 1764.01 o 11 3 1 29.61 36.86 29.52 o 12 3 1 269.55 130.18 35.70 o 13 3 1 679.84 589.98 67.30 o 14 3 1 8322.40 7586.26 684.61 o 15 3 1 74.36 60.80 54.76 o 16 3 1 3554.59 3547.07 346.03 o 17 3 1 1923.52 1916.11 196.93 o 18 3 1 148.71 275.48 67.57 o 19 3 1 1030.20 1238.64 148.00 o 20 3 1 108.63 166.67 83.99 o 21 3 1 4.49 -69.67 69.67 o 22 3 1 262.93 245.06 85.76 o 23 3 1 36.06 201.30 112.34 o 24 3 1 264.16 55.41 129.67 o 25 3 1 0.16 -110.33 110.33 o 0 4 1 63426.27 71039.52 13152.23 o 1 4 1 148.79 111.70 28.57 o 2 4 1 6773.92 6355.22 677.86 o 3 4 1 765.64 787.66 85.48 o 4 4 1 74444.98 75691.38 7341.43 o 5 4 1 10447.69 10799.97 974.54 o 6 4 1 2302.96 2412.95 211.76 o 7 4 1 11811.16 12431.46 1055.53 o 8 4 1 13775.68 14380.39 1223.20 o 9 4 1 2559.75 2464.70 208.73 o 10 4 1 663.41 594.33 58.73 o 11 4 1 691.01 589.36 73.84 o 12 4 1 986.28 916.73 89.09 o 13 4 1 865.26 825.67 85.79 o 14 4 1 4792.48 4710.23 427.40 o 15 4 1 4.55 -39.27 39.27 o 16 4 1 142.44 70.66 47.93 o 17 4 1 10967.90 9988.54 1051.39 o 18 4 1 3716.81 3939.61 421.69 o 19 4 1 584.10 559.02 100.47 o 20 4 1 46.81 -72.55 72.55 o 21 4 1 338.87 203.65 89.85 o 22 4 1 701.78 829.76 185.60 o 23 4 1 1.11 -84.97 84.97 o 24 4 1 0.89 2.98 139.49 o 1 5 1 556.15 635.61 74.96 o 2 5 1 396.71 373.08 44.24 o 3 5 1 7919.17 7889.67 794.39 o 4 5 1 6532.47 6511.62 636.76 o 5 5 1 3651.48 3800.79 372.43 o 6 5 1 1622.89 1890.38 185.31 o 7 5 1 7698.10 8562.89 777.45 o 8 5 1 14329.01 13222.20 1200.75 o 9 5 1 2912.26 2924.09 250.62 o 10 5 1 2210.97 2000.55 171.77 o 11 5 1 173.76 139.14 31.20 o 12 5 1 632.09 471.19 52.99 o 13 5 1 1554.56 1763.60 159.64 o 14 5 1 1347.48 1712.31 174.52 o 15 5 1 27.13 61.21 61.85 o 16 5 1 106.05 147.62 95.39 o 17 5 1 0.71 -40.38 62.12 o 18 5 1 0.77 -57.98 66.59 o 19 5 1 203.61 59.81 86.84 o 20 5 1 36.73 -25.53 149.55 o 21 5 1 250.82 124.21 94.99 o 22 5 1 164.45 69.97 95.97 o 23 5 1 115.53 -123.21 123.21 o 24 5 1 26.34 -110.93 110.93 o 0 6 1 795.49 874.71 178.35 o 1 6 1 2275.07 2260.33 245.17 o 2 6 1 8207.63 9689.49 959.39 o 3 6 1 5513.43 5826.05 611.00 o 4 6 1 45.34 195.50 36.42 o 5 6 1 3167.43 3668.99 361.89 o 6 6 1 3020.30 2504.10 247.56 o 7 6 1 44.43 18.40 30.39 o 8 6 1 14177.31 15877.50 1548.59 o 9 6 1 226.99 228.49 39.01 o 10 6 1 1726.81 1487.61 140.34 o 11 6 1 53.49 24.82 29.66 o 12 6 1 2406.80 2405.76 209.84 o 13 6 1 114.46 92.30 38.07 o 14 6 1 0.76 -7.99 52.18 o 15 6 1 1427.60 1455.45 184.52 o 16 6 1 58.59 21.16 74.28 o 17 6 1 1321.63 1407.09 203.56 o 18 6 1 45.13 -23.95 77.53 o 19 6 1 259.55 198.31 90.03 o 20 6 1 58.56 -75.65 75.65 o 21 6 1 167.09 -82.63 82.63 o 22 6 1 24.71 -88.26 88.26 o 23 6 1 0.10 -130.46 130.46 o 24 6 1 308.26 54.28 135.31 o 1 7 1 1716.36 1874.02 204.60 o 2 7 1 12504.36 13804.74 1373.01 o 3 7 1 1371.91 1408.39 154.97 o 4 7 1 35.73 33.77 30.22 o 5 7 1 4465.68 4950.30 487.03 o 6 7 1 11680.19 12326.96 1202.78 o 7 7 1 750.78 975.51 103.35 o 8 7 1 330.71 367.47 53.23 o 9 7 1 315.86 215.13 43.64 o 10 7 1 29.33 -8.51 36.77 o 11 7 1 1754.87 1861.80 186.93 o 12 7 1 1407.21 1361.04 139.28 o 13 7 1 837.02 797.46 108.73 o 14 7 1 301.32 231.16 71.97 o 15 7 1 1851.47 1882.61 262.05 o 16 7 1 2899.37 3083.15 408.28 o 17 7 1 80.02 -4.69 80.67 o 18 7 1 105.45 96.07 86.85 o 19 7 1 254.72 157.57 86.20 o 20 7 1 1071.92 845.62 152.53 o 21 7 1 122.82 -12.85 93.30 o 22 7 1 2.96 -98.55 98.55 o 23 7 1 1.07 -159.41 159.41 o 0 8 1 31427.52 30649.71 4535.52 o 1 8 1 2118.57 2210.90 241.44 o 2 8 1 20.02 -3.33 38.93 o 3 8 1 875.23 794.64 94.18 o 4 8 1 7393.71 8151.34 820.44 o 5 8 1 735.38 928.95 97.55 o 6 8 1 553.49 489.68 61.25 o 7 8 1 2627.93 2650.95 257.64 o 8 8 1 8724.71 9507.74 930.06 o 9 8 1 240.37 120.97 44.16 o 10 8 1 6325.87 6588.01 699.61 o 11 8 1 29.73 -2.49 45.91 o 12 8 1 3564.66 3797.78 469.53 o 13 8 1 24.42 53.19 77.25 o 14 8 1 1039.58 961.27 152.57 o 15 8 1 105.61 92.07 76.90 o 16 8 1 234.12 118.29 115.08 o 17 8 1 1265.36 1307.32 194.83 o 18 8 1 279.57 104.06 92.34 o 19 8 1 697.00 649.92 143.40 o 20 8 1 215.88 48.55 89.77 o 21 8 1 129.18 6.31 99.68 o 22 8 1 235.61 141.38 196.75 o 1 9 1 1784.68 2145.76 214.45 o 2 9 1 20327.95 20713.86 1910.88 o 3 9 1 81.88 26.74 35.48 o 4 9 1 98.38 125.83 38.82 o 5 9 1 14.15 -2.21 36.60 o 6 9 1 6785.06 6634.98 652.37 o 7 9 1 190.24 162.05 46.97 o 8 9 1 980.23 908.14 110.08 o 9 9 1 232.51 340.34 69.91 o 10 9 1 709.48 525.03 85.89 o 11 9 1 203.51 209.99 70.20 o 12 9 1 3070.97 3282.91 404.88 o 13 9 1 1050.95 837.46 138.34 o 14 9 1 325.41 260.20 86.26 o 15 9 1 446.35 479.44 127.51 o 16 9 1 2198.43 2902.66 390.72 o 17 9 1 1751.65 1687.96 239.71 o 18 9 1 21.42 -88.19 88.19 o 19 9 1 129.95 -90.53 90.53 o 20 9 1 803.71 820.39 164.60 o 21 9 1 24.94 -89.17 89.17 o 22 9 1 10.22 -173.37 173.37 o 0 10 1 1211.38 1190.01 187.92 o 1 10 1 450.58 479.20 67.77 o 2 10 1 905.84 1274.27 125.47 o 3 10 1 1667.17 1675.48 185.45 o 4 10 1 497.87 585.20 77.93 o 5 10 1 1846.22 2327.02 261.24 o 6 10 1 4818.09 5148.48 545.18 o 7 10 1 245.64 132.82 54.28 o 8 10 1 1880.61 1920.82 228.66 o 9 10 1 720.65 662.49 98.80 o 10 10 1 3567.13 4156.18 512.54 o 11 10 1 282.43 146.26 105.23 o 12 10 1 2505.05 2895.77 384.90 o 13 10 1 0.03 -72.51 72.51 o 14 10 1 727.96 760.84 138.59 o 15 10 1 473.71 416.98 106.97 o 16 10 1 805.09 825.71 148.43 o 17 10 1 250.88 305.78 108.97 o 18 10 1 44.43 -91.43 91.43 o 19 10 1 102.57 -113.62 113.62 o 20 10 1 10.29 -175.23 175.23 o 21 10 1 34.00 -100.06 100.06 o 1 11 1 42.36 -38.04 38.04 o 2 11 1 11.88 3.04 35.01 o 3 11 1 164.15 4.25 48.94 o 4 11 1 27.34 -49.37 49.37 o 5 11 1 101.16 -22.58 56.51 o 6 11 1 451.07 446.48 81.61 o 7 11 1 701.99 720.19 106.80 o 8 11 1 147.77 212.91 62.77 o 9 11 1 101.12 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583.10 86.69 o 13 7 10 7575.65 8361.87 843.20 o 14 7 10 606.04 513.10 83.36 o 15 7 10 215.69 107.32 64.19 o 16 7 10 18.78 57.38 60.32 o 17 7 10 6111.35 7135.05 718.24 o 18 7 10 765.35 796.51 112.37 o 19 7 10 1798.68 1799.64 234.06 o 20 7 10 1063.07 1588.18 213.03 o 21 7 10 1685.10 2131.20 308.48 o 0 8 10 6006.31 5801.16 807.66 o 1 8 10 3150.03 3213.11 319.68 o 2 8 10 59.85 16.14 39.85 o 3 8 10 9056.77 9138.71 931.31 o 4 8 10 1521.89 2057.47 264.62 o 5 8 10 1336.41 1656.50 210.50 o 6 8 10 2694.14 3069.82 379.53 o 7 8 10 406.96 471.92 86.70 o 8 8 10 57.72 -54.78 54.78 o 9 8 10 3146.88 3480.52 387.92 o 10 8 10 2372.82 2273.92 239.80 o 11 8 10 2924.68 3275.96 335.86 o 12 8 10 2942.39 3606.73 366.59 o 13 8 10 1558.16 1498.46 164.60 o 14 8 10 52.14 39.75 67.40 o 15 8 10 7447.62 7444.41 751.16 o 16 8 10 514.24 516.39 112.69 o 17 8 10 17.75 -62.70 62.70 o 18 8 10 326.72 240.10 113.53 o 19 8 10 1905.46 2011.01 232.77 o 20 8 10 3.83 -54.90 124.47 o 21 8 10 537.34 769.31 155.47 o 1 9 10 6023.38 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