#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/62/2016217.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2016217_Fobs loop_ _publ_author_name 'Portilla, Jaime' 'Quiroga, Jairo' 'Cobo, Justo' 'Low, John N.' 'Glidewell, Christopher' _publ_section_title ; 8-tert-Butyl-7-(4-chlorophenyl)-10-phenyl-5,6-dihydro-10H-benzo[h]pyrazolo[3,4-b]quinoline ; _journal_coeditor_code SK3154 _journal_issue 10 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first o582 _journal_page_last o584 _journal_volume 63 _journal_year 2007 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 93.750 _cell_angle_beta 91.803 _cell_angle_gamma 101.155 _cell_length_a 13.1170 _cell_length_b 15.9480 _cell_length_c 17.7170 _exptl_crystal_F_000 1464.00 _reflns_d_resolution_high 0.7696 _[local]_cod_data_source_file sk3154Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' JPT3 New: P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 548.96 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ 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529.58 o 2 1 0 74.39 37.74 3.46 o 3 1 0 23593.06 23681.54 229.58 o 4 1 0 61442.25 65336.57 655.39 o 5 1 0 2493.59 2363.90 30.72 o 6 1 0 6.16 4.63 6.21 o 7 1 0 7617.58 8314.79 102.58 o 8 1 0 4744.28 5034.55 73.96 o 9 1 0 385.66 339.35 16.63 o 10 1 0 1123.24 1271.65 40.58 o 11 1 0 920.66 1095.68 48.51 o 12 1 0 0.04 -20.45 26.36 o 13 1 0 125.44 112.51 31.11 o 14 1 0 1.90 -33.48 33.48 o 15 1 0 8.38 -49.40 49.40 o 16 1 0 80.31 12.07 42.69 o -16 2 0 151.36 100.32 48.04 o -15 2 0 131.99 115.77 40.30 o -14 2 0 0.34 -19.77 34.56 o -13 2 0 554.04 596.97 35.51 o -12 2 0 199.72 274.73 26.24 o -11 2 0 235.41 252.75 26.62 o -10 2 0 29.81 35.95 12.22 o -9 2 0 96.41 125.60 11.91 o -8 2 0 890.44 878.15 18.73 o -7 2 0 6301.11 7050.44 90.91 o -6 2 0 4897.53 4811.64 61.27 o -5 2 0 232.54 305.74 14.37 o -4 2 0 60480.03 64642.48 867.38 o -3 2 0 18442.21 17901.55 189.16 o -2 2 0 817.99 758.23 9.44 o 1 2 0 1296.14 1146.03 15.79 o 2 2 0 21865.35 22017.26 234.13 o 3 2 0 1950.80 1839.91 24.08 o 4 2 0 18166.16 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56.54 o 6 3 0 11.96 12.10 8.06 o 7 3 0 1071.58 1040.40 21.50 o 8 3 0 1.74 5.31 14.88 o 9 3 0 137.38 175.00 20.48 o 10 3 0 5.44 -3.70 16.16 o 11 3 0 149.42 150.58 23.46 o 12 3 0 16.14 48.23 59.63 o 13 3 0 324.52 297.25 52.89 o 14 3 0 220.02 245.07 38.69 o 15 3 0 5.99 -42.01 42.01 o 16 3 0 0.77 -35.08 44.26 o -17 4 0 72.87 40.67 107.88 o -16 4 0 4.95 -53.75 74.15 o -15 4 0 53.19 60.28 43.45 o -14 4 0 186.95 139.18 56.48 o -13 4 0 162.33 81.21 28.87 o -12 4 0 106.53 55.09 22.57 o -11 4 0 785.28 928.23 28.53 o -10 4 0 373.55 389.13 17.30 o -9 4 0 106.27 153.90 14.77 o -8 4 0 1710.77 1799.26 29.34 o -7 4 0 460.04 512.72 13.37 o -6 4 0 114.93 72.54 6.79 o -5 4 0 2197.84 2220.87 27.85 o -4 4 0 2573.35 2354.57 29.96 o -3 4 0 1365.56 1262.35 16.45 o -2 4 0 655.48 692.56 9.58 o -1 4 0 23.93 23.04 2.78 o 0 4 0 47.09 48.52 4.19 o 1 4 0 0.99 14.08 5.33 o 2 4 0 36.89 44.80 6.02 o 3 4 0 166.37 153.85 8.15 o 4 4 0 261.05 211.01 9.34 o 5 4 0 749.49 754.57 17.14 o 6 4 0 32.98 4.15 9.32 o 7 4 0 1.70 15.47 12.26 o 8 4 0 16.60 2.23 12.94 o 9 4 0 1.72 3.69 13.44 o 10 4 0 233.11 260.06 19.83 o 11 4 0 1.06 13.14 26.58 o 12 4 0 118.31 93.43 52.13 o 13 4 0 14.91 -13.99 34.57 o 14 4 0 0.08 40.74 38.19 o 15 4 0 16.77 0.94 42.96 o -17 5 0 0.22 44.06 88.96 o -16 5 0 83.62 187.57 58.34 o -15 5 0 13.82 -1.74 41.40 o -14 5 0 110.59 60.50 36.57 o -13 5 0 5.84 7.26 22.87 o -12 5 0 18.72 4.33 18.08 o -11 5 0 3.30 17.29 12.95 o -10 5 0 166.23 164.09 15.61 o -9 5 0 313.91 296.26 15.99 o -8 5 0 605.41 623.51 20.17 o -7 5 0 698.04 769.81 15.43 o -6 5 0 60.28 26.45 9.37 o -5 5 0 375.58 378.30 10.08 o -4 5 0 218.09 213.11 7.33 o -3 5 0 39.94 37.83 3.33 o -2 5 0 0.12 -1.87 2.70 o -1 5 0 219.17 188.14 4.93 o 0 5 0 292.92 279.93 7.09 o 1 5 0 222.64 244.08 9.26 o 2 5 0 5.65 0.10 5.79 o 3 5 0 18.35 17.73 6.88 o 4 5 0 11.33 22.22 7.96 o 5 5 0 501.48 509.80 14.39 o 6 5 0 818.11 760.07 20.66 o 7 5 0 78.76 92.19 15.82 o 8 5 0 127.68 120.53 14.74 o 9 5 0 6.58 -10.40 15.93 o 10 5 0 1.63 0.61 17.91 o 11 5 0 354.91 418.90 32.32 o 12 5 0 105.01 55.45 50.61 o 13 5 0 174.47 159.96 39.42 o 14 5 0 78.71 152.37 50.51 o 15 5 0 3.46 -36.88 44.92 o -16 6 0 2.55 94.19 43.66 o -15 6 0 14.58 51.33 49.61 o -14 6 0 18.23 -13.55 40.67 o -13 6 0 54.72 85.15 31.69 o -12 6 0 1.15 0.42 16.42 o -11 6 0 29.27 17.80 13.11 o -10 6 0 733.40 767.32 22.64 o -9 6 0 0.07 6.77 9.69 o -8 6 0 25.25 16.89 7.00 o -7 6 0 2391.30 2566.14 37.75 o -6 6 0 28.12 16.56 6.22 o -5 6 0 224.58 168.67 7.51 o -4 6 0 62.43 62.08 5.29 o -3 6 0 285.10 211.20 6.83 o -2 6 0 81.92 67.44 4.00 o -1 6 0 382.20 363.69 8.87 o 0 6 0 6244.32 6144.65 62.85 o 1 6 0 486.82 411.49 10.92 o 2 6 0 736.33 612.21 13.81 o 3 6 0 2531.17 2781.88 37.25 o 4 6 0 0.14 0.94 9.24 o 5 6 0 538.06 666.61 19.57 o 6 6 0 1758.78 1976.31 44.10 o 7 6 0 277.99 298.24 19.53 o 8 6 0 16.06 26.85 18.26 o 9 6 0 20.98 -5.96 17.27 o 10 6 0 35.10 40.41 23.76 o 11 6 0 5.74 24.84 26.18 o 12 6 0 47.98 41.99 43.76 o 13 6 0 206.36 201.64 55.99 o 14 6 0 11.37 -9.19 47.81 o 15 6 0 11.18 -3.29 60.72 o -16 7 0 18.90 17.11 46.68 o -15 7 0 0.08 -29.00 40.53 o -14 7 0 99.70 98.26 40.68 o -13 7 0 24.64 32.15 25.70 o -12 7 0 23.18 18.16 32.16 o -11 7 0 48.99 35.98 17.95 o -10 7 0 31.08 18.50 11.61 o -9 7 0 244.64 232.38 11.96 o -8 7 0 17.46 -5.75 10.99 o -7 7 0 2279.45 2309.30 34.19 o -6 7 0 93.25 103.50 7.92 o -5 7 0 245.10 248.77 11.98 o -4 7 0 2400.23 2510.29 31.68 o -3 7 0 416.98 435.67 9.04 o -2 7 0 376.72 253.75 6.56 o -1 7 0 280.42 216.81 7.68 o 0 7 0 1120.70 1074.97 16.60 o 1 7 0 420.22 450.64 15.50 o 2 7 0 41.94 44.56 9.10 o 3 7 0 2284.37 2445.34 35.33 o 4 7 0 170.60 195.64 13.30 o 5 7 0 407.19 412.75 19.43 o 6 7 0 156.14 143.73 16.51 o 7 7 0 124.30 177.70 18.75 o 8 7 0 169.36 149.63 22.29 o 9 7 0 19.03 23.36 22.18 o 10 7 0 116.74 56.34 27.78 o 11 7 0 8.66 9.52 27.15 o 12 7 0 264.31 290.75 48.50 o 13 7 0 27.69 12.91 40.50 o 14 7 0 0.45 -8.37 63.17 o -16 8 0 4.00 11.84 53.35 o -15 8 0 0.07 -16.75 42.41 o -14 8 0 196.22 194.49 50.43 o -13 8 0 1.83 1.72 31.61 o -12 8 0 280.50 162.54 32.80 o -11 8 0 98.68 106.43 28.28 o -10 8 0 32.19 22.30 16.51 o -9 8 0 465.94 444.67 24.39 o -8 8 0 375.35 329.87 20.89 o -7 8 0 125.06 112.96 9.85 o -6 8 0 4941.45 5753.37 71.14 o -5 8 0 195.78 209.04 9.06 o -4 8 0 62.13 52.24 6.44 o -3 8 0 8470.66 9443.96 85.18 o -2 8 0 738.76 690.27 11.34 o -1 8 0 23.06 36.80 7.03 o 0 8 0 1153.87 1123.80 17.99 o 1 8 0 53.85 39.10 10.00 o 2 8 0 436.49 405.46 13.33 o 3 8 0 732.95 710.03 18.21 o 4 8 0 212.50 157.72 13.56 o 5 8 0 2883.14 3096.76 66.37 o 6 8 0 105.82 87.27 18.93 o 7 8 0 296.27 292.88 23.84 o 8 8 0 0.36 10.23 21.09 o 9 8 0 256.23 336.26 44.33 o 10 8 0 1.31 29.47 26.94 o 11 8 0 44.87 57.21 38.06 o 12 8 0 673.80 666.26 50.69 o 13 8 0 13.91 10.16 41.84 o 14 8 0 37.20 12.54 70.50 o -16 9 0 4.68 18.94 136.13 o -15 9 0 21.08 -5.61 45.09 o -14 9 0 355.92 451.99 56.32 o -13 9 0 0.10 -41.48 53.66 o -12 9 0 165.02 52.97 41.38 o -11 9 0 289.26 271.32 31.08 o -10 9 0 85.83 62.13 21.04 o -9 9 0 39.88 20.24 12.00 o -8 9 0 518.29 521.44 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